wyświetlamy 1000 najlepszych wyników Pomoc
Wyniki wyszukiwania dla: FRUITS AND VEGETABLES SAMPLES
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Co-microprecipitation/flotation of trace amounts of cadmium from environmental samples through its complexation with iodide and neutralization with cetyltrimethylammonium bromide in the presence of perchlorate ions
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Fabrication of a Molecularly Imprinted Polymer Adsorbent for Pipette Tip Micro Solid-phase Extraction of Levofloxacin from Aqueous Samples Prior to its Spectrophotometric Determination
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Solid phase microextraction–comprehensive twodimensional gas chromatography–time-of-flight mass spectrometry: a new tool for determining PAHs in airport runoff water samples
Publikacjafundamental aspect of airport operations is the pollution caused by airport runoff waters. Polycyclic aromatic hydrocarbons (PAHs) are one of the most important groups of xenobiotics which are commonly found in runoff water originating from airports. Only very limited data on the analysis of airport runoff water have been published until now. Therefore, a reliable and accurate analytical method based on headspace solid-phase microextraction...
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Izolacja lotnych związków organicznych z próbek wody. Metody i aparatura. Analysis of volatile organic compounds (VOCs) in water samples. Methods and apparatus.
PublikacjaOmówiono techniki wykorzystywane do przygotowania próbek wody do oznaczeń analitów z grupy lotnych związków organicznych (VOCs) za pomocą chromatografii gazowej. Opisano wady i zalety takich technik jak: bezpośrednie dozowanie próbki wody do kolumny chromatograficznej, ekstrakcja rozpuszczalnikiem, ekstrakcja do fazy stałej lub stacjonarnej, ekstrakcja membranowa oraz analiza fazy nadpowierzchniowej. Omówiono także nowe rozwiązania...
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Rapid assessment of the authenticity of limequat fruit using the electronic nose and gas chromatography coupled with mass spectrometry
PublikacjaCitrus fruits are very popular food products. There are many species and varieties of them. There are also documented cases of some citrus fruits causing a severe allergic reaction. Some species of the citrus fruits, especially hybrid ones show a reduced allergenic effect due to the lack of seeds. There is a need for rapid methods for evaluation of citrus’ botanical origin. During research, the headspace of three citrus fruits...
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Determination of parent and methylated polycyclic aromatic hydrocarbons in water samples by dispersive liquid–liquid microextraction–two dimensional gas chromatography–time-of-flight mass spectrometry
PublikacjaPolycyclic aromatic hydrocarbons (PAHs) are contaminants frequently found in environmental waters. Owing to their toxic effects, it is important to develop analytical methodologies that allow their fast and reliable determination. Dispersive liquid–liquid microextraction (DLLME) allows a quick extraction of analytes with little organic solvent consumption. The best results regarding sample preparation are obtained when 40 mL of...
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Determination of profenofos in seawater and foodstuff samples after its molecularly imprinted polymer pipette-tip micro solid phase extraction optimized by response surface methodology
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Comparison of Air-Assisted, Vortex-Assisted and Ultrasound-Assisted Dispersive Liquid–Liquid Microextraction for the Determination of BTEX Compounds in Water Samples Prior to GC-FID Analysis
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Przegląd metod oznaczania pozostałości pestycydów i polichlorowanych bifenyli w próbkach żywności = Methods of determination of residues of pesticides and polychlorinated biphenyls in food samples - a review
PublikacjaOznaczanie pozostałości pestycydów i analitów z grupy polichlorowanych bifenyli w próbkach żywności wymaga zastosowania specyficznych technik w zakresie przygotowania próbki do analizy, jak i samych technik analizy instrumentalnej, pozwalających na uzyskanie bardzo niskiej granicy oznaczalności. Problemem związanym ze stosowaniem związków z grupy pestycydów i polichlorowanych bifenyli jest konieczność kontroli ich pozostałości...
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Sample preparation procedure using extraction and derivatization of carboxylic acids from aqueous samples by means of deep eutectic solvents for gas chromatographic-mass spectrometric analysis
PublikacjaThe paper presents a new procedure for the determination of organic acids in a complex aqueous matrixusing ultrasound-assisted dispersive liquid–liquid microextraction followed by injection port derivati-zation and GC–MS analysis. A deep eutectic solvent (choline chloride: 4-methylphenol in a 1:2 mol ratio)was used both as an extracting solvent and as a derivatizing agent to yield ion pairs which were next con-verted to methyl...
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Dariusz Witt prof. dr hab. inż.
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Solid-phase extraction using octadecyl-bonded silica modified with photosynthetic pigments from Spinacia oleracea L. for the preconcentration of lead(II) ions from aqueous samples
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Correction to: Chromium‑based metal organic framework for pipette tip micro‑solid phase extraction: an effective approach for determination of methyl and propyl parabens in wastewater and shampoo samples
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Próbki wód spływnych - sposób pobierania z różnych powierzchni i ich skład chemiczny = Samples of runoff water - sampling procedures for different surfaces and chemical composition
PublikacjaPrzedstawiono dane dotyczące chemizmu wód spływnych dostających się do środowiska w wyniku zmywania przez opady atmosferyczne zanieczyszczeń z takich powierzchni jak: arterie komunikacyjne, dachy budynków, obszary rolnicze i leśne oraz hałdy odpadów. Wyniki uzyskane w trakcie badań własnych zestawiono z danymi literaturowymi. Informacje o metodyce pobierania próbek i położeniu stanowiska obserwacyjnego warunkują prawidłowy wynik...
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Enzymatic cleavage of specific dipeptide conjugated with ferrocene as a flexible ultra-sensitive and fast voltammetric assay of matrix metalloproteinase-9 considered a prognostic cancer biomarker in plasma samples
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Green, simple analytical method for biogenic amines determination in fruit juice samples using salting-out assisted liquid-liquid microextraction and gas chromatography-mass spectrometry
PublikacjaSalting-out assisted liquid-liquid microextraction (SALLME) was integrated with the derivatization procedure to establish a one-step sample pre-treatment approach for rapid analysis of 14 biogenic amines (BAs) in fruit juices. The methodology consists of salting-out of analytes, derivatization with ethyl chloroformate (ECF), extraction with ethyl acetate (EtAc), and the analysis of the derivatized BAs using gas chromatography-mass...
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Simultaneous analysis of non-steroidal anti-inflammatory drugs and estrogenic hormones in water and wastewater samples using gas chromatography–mass spectrometry and gas chromatography with electron capture detection
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Application of gas flow headspace liquid phase micro extraction coupled with gas chromatography-mass spectrometry for determination of 4-methylimidazole in food samples employing experimental design optimization
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The Mesoporous Porphyrinic Zirconium Metal-Organic Framework for Pipette-Tip Solid-Phase Extraction of Mercury from Fish Samples Followed by Cold Vapor Atomic Absorption Spectrometric Determination
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Determination of Heavy Metals Concentration in Water and Soil at Various Locations in Lahore and their Harmful Impacts on Human and Plants life
PublikacjaHeavy metals poisoning of soil and water has resulted from industrial expansion in Lahore, Pakistan, creating a significant environmental hazard. As a result, monitoring the contamination of soil and water around industrial sites is critical. The fact that higher concentrations of heavy metals have a negative influence on both plants and human life and this cannot be ignored. Higher heavy metal concentrations have a direct impact...
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Marek Tobiszewski dr hab. inż.
OsobyUrodzony 07.04.1984 roku w Gdańsku. W 2012 roku obronił z wyróżnieniem doktorat, w 2017 roku uzyskał habilitację na podstawie osiągnięcia naukowego „Opracowanie służących do oceny uciążliwości środowiskowej procedur analitycznych i rozpuszczalników”. Pracuje w Katedrze Chemii Analitycznej od 2012 roku. Jego zainteresowania naukowe łączą analitykę chemiczną, zwłaszcza analityka związków organicznych w próbkach środowiskowych, z...
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Application of Box-Behnken design in response surface methodology for the molecularly imprinted polymer pipette-tip solid phase extraction of methyl red from seawater samples and its determination by spectrophotometery
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Separation and determination of ciprofloxacin in seawater, human blood plasma and tablet samples using molecularly imprinted polymer pipette‐tip solid phase extraction and its optimization by response surface methodology
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Skład zanieczyszczeń wprowadzanych do środowiska wzdłuż dróg o różnym natężeniu ruchu pojazdów mechanicznych = Composition of pollutants in the water samples collected along the highways with different traffic intensity
PublikacjaProwadzono monitoring poziomu stężeń wybranych zanieczyszczeń w próbkach wód opadowych, spływnych, gruntowych i rzecznych, pobieranych wzdłuż dróg o różnym natężeniu ruchu pojazdów. Zlokalizowano pięć stałych punktów pobierania próbek wzdłuż dwóch szlaków komunikacyjnych; drogi o małym natężeniu ruchu nr 501 w miejscowości Sztutowo oraz wzdłuż drogi krajowej nr A7 na odcinku Nowy Dwór Gdański - Elbląg. Próbki pobierano przez okres...
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Oznaczanie stężeń jonów fluorkowych w próbkach wody pitnej z terenu miasta Malborka = Determination of fluoride ions in drinking water samples collected from the area of the town of Malbork
PublikacjaW pracy przedstawiono badania próbek wody pitnej z terenu miasta Malborka. Próbki wody pobierano sześciokrotnie (w miesięcznych odstępach - październik 2008, listopad 2008, grudzień 2008, styczeń 2009, luty 2009 oraz marzec 2009) w siedmiu punktach leżących w głównych dzielnicach miasta Malborka. Pobrane próbki podano analizie w celu oznaczenia następujących parametrów: zawartość anionów: F-, Cl-, Br-, 2NO , 3NO , 34 PO , 24 SO...
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The flavour of fruit spirits and fruit liqueurs: a review
PublikacjaFruit spirits and liqueurs are among the most popular spirit-based beverages made from fruits such as plums, cherries, melon, apple, citrus and pear. The types of fruits and production methods have a great significance for the quality of the final product. The production process of spirits consists of the following stages: fermentation, distillation and maturation. For this reason scientists started to investigate the composition...
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Comparative Analysis of Phytochemical Profiles and Selected Biological Activities of Various Morphological Parts of Ligustrum vulgare
PublikacjaLigustrum vulgare (LV), widely cultivated in Europe and often used in hedges, has been histori-cally recognized in folk medicine for its potential health benefits. This study focused on exploring the untargeted identification of secondary metabolites in ethanol extracts (70% v/v) from differ-ent morphological parts (young shoots, leaves, flowers and fruits) of LV at various stages of plant development, using ultra-high-performance...
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Justyna Płotka-Wasylka dr hab. inż.
OsobyUrodziła się w Słupsku (24.03.1986).W 2005 roku ukończyła I Liceum Ogólnokształcące im. Jana II Sobieskiego w Wejherowie i rozpoczęła studia na Wydziale Chemicznym Politechniki Gdańskiej. Po ich ukończeniu w 2010 rozpoczęła pracę naukową na tej uczelni, uzyskując w 2014 roku stopień doktora nauk chemicznych. Tematem jej rozprawy doktorskiej, wykonywanej pod kierunkiem prof. Marka Biziuka oraz dr Caluma Morrisona (Uniwersytet w...
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Box-Behnken design optimization of pipette tip solid phase extraction for methyl orange and acid red determination by spectrophotometry in seawater samples using graphite based magnetic NiFe2O4 decorated exfoliated as sorbent
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FLAME ATOMIC ABSORPTION SPECTROMETRIC DETERMINATION OF TRACE AMOUNTS OF SILVER IN RADIOLOGICAL WASTE SAMPLES AFTER SOLID PHASE EXTRACTION USING MULTI-WALLED CARBON NANO-TUBES MODIFIED BY SODIUM DODECYL SULFATE
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Detecting Apples in the Wild: Potential for Harvest Quantity Estimation
PublikacjaKnowing the exact number of fruits and trees helps farmers to make better decisions in their orchard production management. The current practice of crop estimation practice often involves manual counting of fruits (before harvesting), which is an extremely time-consuming and costly process. Additionally, this is not practicable for large orchards. Thanks to the changes that have taken place in recent years in the field of image...
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Development of a solventless stir bar sorptive extraction/thermal desorption large volume injection capillary gas chromatographic-mass spectrometric method for ultra-trace determination of pyrethroids pesticides in river and tap water samples
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Application of Box–Behnken design in the optimization of a simple graphene oxide/zinc oxide nanocomposite-based pipette tip micro-solid phase extraction for the determination of Rhodamine B and Malachite green in seawater samples by spectrophotometry
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Identification attempts of toluene sources in post-flood sediment samples from the Odra river (flood 1997). Identyfikacja źródeł toluenu w próbkach osadów popowodziowych pobranych z rzeki Odry (powódź 1997).
PublikacjaPrzedstawiono badania mające na celu oznaczanie zawartości toluenu w próbkach osadów dennych i w próbkach mikrobiologicznych. W badaniach wykorzystano zestaw do jednoczesnego wymywania i wychwytywania analitów na stałym sorbencie (Purge and Trap). Oznaczenia końcowe wykonano z wykorzystaniem techniki chromatografii gazowej połączonej ze spektrometrem mas.
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Bioactive Ingredients with Health-Promoting Properties of Strawberry Fruit (Fragaria x ananassa Duchesne)
PublikacjaStrawberries (Fragaria x ananassa Duchesne) belong to the berry group and are characterized primarily by delightful sensory properties. Due to their chemical composition, these fruits are a rich source of bioactive compounds that can modify the metabolic and physiological functions of the body. The aim of this work is to present the current state of research on bioactive ingredients found in these fruits in the context of their...
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Nowoczesne techniki przygotowania próbki do oznaczania analitów organicznych z zastosowaniem chromatografii gazowej. Część II. Aparatura. Modern techniques of preparation of samples for determining organic analytes by gas chromatography. Part II. Instrumentation.
PublikacjaW pracy dokonano przeglądu szerokiego spektrum technik przygotowania próbki ze szczególnym uwzględnieniem technik o charakterze prośrodowiskowym. Opisu technik dokonano pod kątem wykorzystywanych mechanizmów izolacji analitów oraz stosowanych rozwiązań aparaturowych.
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The Influence of Different Hydrothermal Processes Used in the Preparation of Brussels Sprouts on the Availability of Glucosinolates to Humans
PublikacjaCruciferous vegetables represent a valuable source of bioactive compounds. However, there is currently a deficiency of information regarding the extent to which these compounds remain bioaccessible to the body following thermal treatment and digestion processes within the digestive tract. Accordingly, the aim of this study was to evaluate the impact of heat treatment and in vitro digestion on the level of selected bioactive compounds...
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Bioactivities of Phenolic Compounds from Kiwifruit and Persimmon
PublikacjaFruit used in the common human diet in general, and kiwifruit and persimmon particularly, displays health properties in the prevention of heart disease. This study describes a combination of bioactivity, multivariate data analyses and fluorescence measurements for the differentiating of kiwifruit and persimmon, their quenching and antioxidant properties. The metabolic differences are shown, as well in the results of bioactivities...
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Characterization of metabolites in different kiwifruit varieties by NMR and fluorescence spectroscopy
PublikacjaIt is known from our previous studies that kiwifruits, which are used in common human diet, have preventive properties of coronary artery disease. This study describes a combination of 1H NMR spectroscopy, multivariate data analyses and fluorescence measurements in differentiating of some kiwifruit varieties, their quenching and antioxidant properties. A total of 41 metabolites were identified by comparing with literature data...
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Application of polyethylene glycol-coated iron oxide nanoparticles for magnetic solid phase extraction of copper from seawater samples and its determination by graphite furnace atomic absorption spectrometry using response surface methodology for optimization of extraction
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Bioactive compounds and the antioxidant capacity in new kiwi fruit cultivars
PublikacjaThe aim of this investigation was to find the best among seven different kiwi fruit cultivars (‘Hayward’, ‘Daheung’, ‘Haenam’, ‘Bidan’, ‘Hort16A’, ‘Hwamei’ and ‘SKK12’) for human consumption and to classify them as groups. Therefore, the contents of bioactive compounds and the level of antioxidant capacities of these cultivars were determined in four different extracts and compared. It was found that the contents of the bioactive...
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Detection of Bioactive Compounds in Organically and Conventionally Grown Asparagus Spears
PublikacjaIn the recent reports, there are contradictory conclusions about the nutritional and health properties of organic and conventionally growing vegetables. We hypothesized that organic cultivation system results in higher quality of asparagus (Asparagus officinalis L.) because of organic manure and effective organisms. Therefore, new analytical methods were applied in order to find the differences in bioactive compounds between the...
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Characterization of home-made and regional fruit wines by evaluation of correlation between selected chemical parameters
PublikacjaSince the last decade of the 20th century, there has been rising interest in the production of fruit wines, as evidenced by the high number of published papers and books covering this matter. When aiming to produce quality fruit wines, it is essential to evaluate the analytical parameters of the beverage. In this context, there are a large number of analyses for the evaluation of wines and fruit wines. This article characterizes...
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Young shoots of red cabbage are a better source of selected nutrients and glucosinolates in comparison to the vegetable at full maturity
PublikacjaCruciferous vegetables are a valuable source of ingredients with health benefits. The most characteristic compounds of cruciferous vegetables with identified anticancer properties are glucosinolates. Young shoots and sprouts of red cabbage are becoming a popular fresh food rich in nutrients and bioactive compounds. The objective of this research was to determine, for the first time in a comprehensive approach, whether young shoots...
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Nowoczesne techniki przygotowania próbki do oznaczania analitów organicznych z zastosowaniem chromatografii gazowej. Część I. Podstawy teoretyczne ekstrakcji. Modern techniques of preparation of samples for determining organic analytes by gas chromatography. Part I. Theoretical principles of extraction.
PublikacjaPrzedstawiono podstawy teoretyczne technik izolacji i wzbogacania analitów organicznych z próbek gazowych oraz ciekłych. Już pobieżna analiza literatury dotyczącej omawianych zagadnień, pokazuje jak różnorodne i bogate spektrum technik jest stosowane na etapie przygotowania próbki. Z drugiej strony, z punktu widzenia podstaw fizykochemicznych, większość technik opiera się na dwóch zjawiskach: adsorpcji analitów na medium zatrzymującym...
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The Influence of Co-Fermentation of Agri-Food Waste with Primary Sludge on Biogas Production and Composition of the Liquid Fraction of Digestate
PublikacjaEnergy self-sufficiency is a current trend in wastewater treatment plants. This effect can be achieved by increasing the production of electricity from biogas and by reducing energy consumption for technological processes. One idea, in line with the circular economy concept, is the use of waste rich in organic matter as co-substrates for the fermentation process. The aim of this study was to determine the effect of waste co-fermentation...
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A novel analytical approach in the assessment of unprocessed Kaffir lime peel and pulp as potential raw materials for cosmetic applications
PublikacjaVolatile fraction of fruits is a rich source of bioactive and aroma compounds, which can be used in the cosmetics industry after meeting relevant criteria. This is particularly evident in citrus fruits, especially in Citrus hystrix, in which the headspace consists mainly of terpenes. Due to the insufficient sensitivity of analytical methods, essential oils are used in investigations in contrast to fresh fruits. Therefore, a novel...
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Evaluation of candidate reference material obtained from selenium - enriched sprouts for the purpose of selenium speciation analysis
PublikacjaSelenium is an essential element in animals and humans. Diet supplementation with selenium-rich vegetables has better chemoprotective effect than Se (IV) and SeMet. The production of selenium-enriched vegetables requires a preliminary stage in soil preparation, which may subsequently pose a risk of soil contamination. It seems that the sprouting of seeds under controlled conditions would be a good solution for delivering SeMetSeCys...
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In-tube extraction for the determination of the main volatile compounds in Physalis peruviana L
PublikacjaAn analytical procedure based on in-tube extraction followed by gas chromatography with mass spectrometry has been developed for the analysis of 24 main volatile components in cape gooseberry (Physalis peruviana L.) samples. According to their chemical structure, the compounds were organized into different groups: one hydrocarbon, one aldehyde, four alcohols, four esters, and 14 monoterpenes. By single-factor experiments, incubation...
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Zastosowanie połączenia mikroekstrakcji do fazy stacjonarnej i chromatografii gazowej do oznaczania lotnych kwasów tłuszczowych w próbkach środowiskowych i pokrewnych=Application of combination of solid phase microextraction and gas chromatography for determination of volatile fatty acids in environmental and related samples
PublikacjaOznaczanie lotnych kwasów tłuszczowych (LKT) w próbkach środowiskowych wymaga najczęściej izolacji i wzbogacania analitów na etapie przygotowania próbek oraz zastosowania techniki o dużym potencjale separacyjnym i identyfikacyjnym na etapie oznaczeń końcowych. W pracy dokonano krytycznego przeglądu zastosowań wygodnej i często stosowanej techniki mikroekstrakcji do fazy stacjonarnej (SPME) w połączeniu z wysokosprawną techniką...