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Synthesis and Spectroscopic Characterization of Selected Phenothiazines and Phenazines Rationalized Based on DFT Calculation
PublikacjaTwo unique structures were isolated from the phosphorylation reaction of 10H-phenothiazine.The 5,5-dimethyl-2-(10H-phenothiazin-10-yl)-1,3,2-dioxaphosphinane 2-oxide (2a) illustrates theproduct of N-phosphorylation of phenothiazine. Moreover, a potential product of 2a instability,a thiophosphoric acid 2b, was successfully isolated and structurally characterized. Molecule 2a,similarly to sulfoxide derivative...
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DAWKOWANIE ODPADÓW Z PRODUKCJI ALKOHOLU DLA POPRAWY EFEKTYWNOŚCI DENITRYFIKACJI I BILANSU ENERGETYCZNEGO W OCZYSZCZALNI ŚCIEKÓW „RUPTAWA” W JASTRZĘBIU-ZDRÓJ
PublikacjaWielofazowe układy osadu czynnego, umożliwiające efektywny przebieg procesów biologicznego usuwania związków organicznych, azotu i fosforu, są powszechnie stosowane w dużych i średnich komunalnych oczyszczalniach ścieków w Polsce. Doświadczenia eksploatacyjne jednoznacznie wskazują, że uzyskanie niskich stężeń związków biogennych w ściekach oczyszczonych jest możliwe, ale wymaga zapewnienia optymalnych warunków dla przebiegu biochemicznych...
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Jak wiele wiedzy warto zdobyć na studiach? Strategie studiowania na przykładzie studentów zarządzania Politechniki Gdańskiej
PublikacjaDane statystyczne dotyczące obiektywnej sytuacji osób kończących studia na uczelni wyższej (np. łatwość znalezienia pracy, początkowe zarobki) wskazują na racjonalność podjęcia decyzji o studiowaniu. Jednocześnie w obliczu głosów krytykujących system kształcenia wyższego, dla studentów najistotniejszym profitem osiąganym w wyniku studiów może stawać się dyplom ich ukończenia. W artykule opisane są przeprowadzone przez autorów badania...
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The electronic excited states of dichloromethane in the 5.8-10.8 eV energy range investigated by experimental and theoretical methods
PublikacjaWe present a comprehensive experimental high-resolution vacuum ultraviolet (VUV) photoabsorption spectrum of dichloromethane, CH 2 Cl 2 , with absolute cross sections determined for the full 5.8–10.8 eV energy-range. The calculations on the vertical excitation energies and oscillator strengths were performed using the equation-of-motion coupled cluster method, restricted to the single and double excitations level (EOM-CCSD), and...
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A comparison of structural and luminescence properties of lead(II) coordination polymers with isomeric thiophenecarboxylate ligands
PublikacjaTwo new lead(II) coordination polymers with isomeric thiophenecarboxylates, namely [Pb(2tpCOO)2]n (1) and [Pb(3tpCOO)2(H2O)]n (2) (2tpCOO− = thiophene-2-carboxylate, 3tpCOO− = thiophene-3-carboxylate), were synthesized and characterized. Single crystal X-ray crystallography revealed a distorted pentagonal pyramidal geometry {PbO6} around Pb in 1 and a distorted dodecahedral geometry {PbO8} in 2. The distortion derived from the...
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Taurine as a water structure breaker and protein stabilizer
PublikacjaThe enhancing effect on the water structure has been confirmed for most of the osmolytes exhibiting both stabilizing and destabilizing properties in regard to proteins. The presented work concerns osmolytes, which should be classified as “structure breaking” solutes: taurine and N,N,N-trimethyltaurine (TMT). Here, we combine FTIR spectroscopy, DSC calorimetry and DFT calculations to gain an insight into the interactions between...
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Microbial diversity of inflamed and noninflamed gut biopsy tissues in inflammatory bowel disease.
PublikacjaBACKGROUND: Inflammatory bowel disease (IBD) is a chronic gastrointestinal condition without any known cause or cure. An imbalance in normal gut biota has been identified as an important factor in the inflammatory process. METHODS: Fifty-eight biopsies from Crohn's disease (CD, n = 10), ulcerative colitis (UC, n = 15), and healthy controls (n = 16) were taken from a population-based case-control study. Automated ribosomal intergenic...
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Characteristics and fate of organic nitrogen in municipal biological nutrient removal wastewater treatment plants
PublikacjaThe aim of this study was to investigate the occurrence and fate of colloidal and dissolved organic nitrogen (CON and DON) across biological nutrient removal (BNR) activated sludge bioreactors. Primary and secondary effluent total nitrogen (TN) measurements and component fractionation, CON and DON concentration profiles across BNR bioreactors, and laboratory batch experiments with the process mixed liquor were carried out at several...
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Positron Scattering and Annihilation in Organic Molecules
PublikacjaIn this paper, we address the problem of connecting positron lifetimes in liquids with collision cross sections in gases. We present the analyses of annihilation lifetime spectra of positrons in the liquid benzene, c-hexane, n-hexane, methanol and ethanol and calculations of scattering cross sections of positrons with benzene and c-hexane in the gas phase.
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Volunteerism in the last year as a moderator between empathy and altruistic social value orientation: An exploratory study
PublikacjaVolunteerism is a sustained prosocial activity, and young adults are one of the most important targets for organizations recruiting volunteers. Empathy and altruistic social value orientation measured by a decomposed game are dispositional traits that might foster engagement in volunteerism. Using a self-report online-based questionnaire study on two groups of young adults (aged 18-35, N = 224 non-volunteers and N = 178 volunteers...
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Graph security testing
PublikacjaSet S ⊂ V is called secure set iff ∀ X ⊂ S | N [ X ] ∩ S | ≥ | N ( X ) \ S | [3]. That means that every subset of a secure set has at least as many friends (neighbour vertices in S) as enemies (neighbour vertices outside S) and will be defended in case of attack. Problem of determining if given set is secure is co −NP -complete, there is no efficient algorithm solving it [3]. Property testers are algorithms that distinguish inputs...
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Electromodulation and magnetomodulation of exciton dissociation in electron donor (starburst amine) : electron acceptor (bathocuproine) system
PublikacjaElectric field dependencies of electromodulated photoluminescence and photocurrents as well as the magnetic field effects on photocurrents, photovoltaic characteristics, electromodulated photoluminescence and photoluminescence have been investigated in vacuum evaporated films of m-MTDATA:BCP (4,4',4''-tris(N-(3-methylphenyl)-N-phenylamino)triphenylamine and bathocuproine) system. The electromodulation processes do remain in accordance...
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Optical emission spectroscopy of plasma generated by a waveguide-supplied microwave plasma source operated at 915MHz
PublikacjaIn this paper we present the results of an optical emission spectroscopic study of an atmospheric pressure microwave (915 MHz) nitrogen and nitrogen with carbon dioxide (1%) plasma at high working gas flow rate. This study was aimed at determining rotational Trot and vibrational Tvib temperatures of N+2 ions and N2, CN molecules. The plasma was generated in a waveguide-supplied cavity-resonant type microwave plasma source. All...
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The interference between electrode and poly(ethylene oxide) electrolytes
PublikacjaSpektroskopia impedancyjna zastosowana została do scharakteryzowania granicy faz elektroda-elektrolit poli(oksyetylenowy) zawierający sole litu. Udział rozpuszczalnika w pojemności wewnętrznej warstwy, Cs(σ), dla CH3(OCH2CH2 )nOCH3 DLA N=4,8,10 oraz dla PMEO [(CH2CH2O)mCH2O]m m=5-10 został wyznaczony z wartości pojemności warstwy sztywnej pomniejszonej o udział metalu CM. Wyznaczono wartość pojemności dipolowej Ci(dip) dla PEO...
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Butyrylcholinesterase signal sequence self-aggregates and enhances amyloid fibril formation in vitro
PublikacjaAlzheimer’s disease (AD) pathogenesis has been attributed to extracellular aggregates of amyloid β (Aβ) plaques and neurofibrillary tangles in the human brain. It has been reported that butyrylcholinesterase (BChE) also accumulates in the brain Aβ plaques in AD. We have previously found that the BChE substitution in 5′UTR caused an in-frame N-terminal extension of 41 amino acids of the BChE signal peptide. The resultant variant...
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Social Capital, Human Capital, Tacit Knowledge, and Innovations: A Polish-US Cross-Country Study
PublikacjaThis study measures the relationship between human and social capital (internal and external) and tacit knowledge sharing's influence on innovativeness among knowledge workers employed in Polish (n=1050) and US (n=1118) organizations. The structural equation modeling method revealed that internal social capital matters more for organizational innovativeness in the US. In Poland, both external and internal were important. Specifically,...
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Efektywność działania środków przeciwstarzeniowych w procesie przyśpieszonego starzenia cieplnego
PublikacjaPrzedmiotem przedstawionych badań są wulkanizaty kauczuku naturalnego i butadienowo-styrenowego. Celem pracy było zbadanie efektywności działania środków przeciwstarzeniowych w procesie przyspieszonego starzenia cieplnego (w czasie 7 i 14 dni w temperaturze 70°C). Do badań wykorzystano dwie substancje przeciwstarzeniowe: komercyjnie dostępny przeciwutleniacz IPPD (N–fenylo-N′-izopropylo-p-fenylenodiamina) oraz ekologiczny przeciwutleniacz...
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Searching by Heterogeneous Agents
PublikacjaIn this work we introduce and study a pursuit-evasion game in which the search is performed by heterogeneous entities. We incorporate heterogeneity into the classical edge search problem by considering edge-labeled graphs. In such setting a searcher, once a search strategy initially decides on the label of the searcher, can be present on an edge only if the label of the searcher and the label of the edge are the same. We prove...
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Cholesky factorization of matrices in parallel and ranking of graphs.
PublikacjaUporządkowane kolorowanie znajduje zastosowanie przy równoległej faktoryzacji macierzy metodą Cholesky'ego. Praca zawiera opis tego zastosowania. Podano także algorytmy optymalnego uporządkowanego kolorowania krawędzi pewnych klas grafów: grafów pełnych dwudzielnych oraz powstałych z pełnych dwudzielnych przez usunięcie O(log n) krawędzi.
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Efficiency and kinetices of coupled transport of copper Ions Through Liquid Membranes Containing Technical Hydroxyoxime Carries
PublikacjaBadano wpływ różnych parametrów (składu faz wodnych, stężenia przenosnika, rozpuszczalnika organicznego na kinektykę i wydajność transportu jonów miedzi. Dużą wydajność procesu mozna otrzymać uzywając około 10 x mniejszego stężenia przenosanika w n-oktanie niż w przypadku innych rozpuszczalników technicznych.
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Dicyclohexylammonium benzenethiolate. Acta Cryst. Sect. E Struct. Rep. [on-line]**2003 vol. 59 s. o765-o766, 2 rys. 2 tab. bibliogr. 11 poz. tiofenolan dicykloheksyloamoniowy.
PublikacjaZwiązek o wzorze C12H24N+ x C6H5S- został otrzymany poprzez reakcję tiofeno-lu z dicykloheksyloaminą. Oba fragmenty jonowe powiązane są w długie łańcu-chy poprzez wiązania N-H...S. Strukturę cząsteczkową i krystaliczną wyzna-czono posługując się rentgenowską analizą strukturalną.
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One-Step Synthesis of b-Lactams with Retro-Amide Side Chain
PublikacjaAbstract: A one pot synthesis for preparation of 1,4-disubstituted-2-oxo-azetidine-3-carboxylic acid amides was developed. 5-(α-N-substituted-amino-α'-hydroxy)methylene Meldrum's acids act as a source of ketenes that react with aldimines in boiling toluene to give b-lactams with retro-amid side chain.
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Bromidotetrakis(1H-2-ethyl-5-methylimidazole-κN3)copper(II) bromide
PublikacjaAtom Cu(II) w tytułowym kompleksie jest skoordynowany przez cztery atomy N obojętnych cząsteczek imidazolu oraz jon bromkowy. Jon kompleksowy ma geometrię piramidy kwadratowej. Kationy kompleksowe w krysztale tworzą układ dipoli ułożonych ''głowa do ogona'' równolegle do osi c.
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Recognition of two-phase flow patterns with the use of dynamic image analysis
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Effect of Hybrid Modulation on Performance of Wireless Battery Charger Operating in CC/CV Mode
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Energy shifts of K- and L-lines as spectroscopic diagnostic of Z-pinch plasmas
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Modeling of the M X-ray line structures for tungsten and L X-ray line structures for molybdenum
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Effect of exercise training on insulin sensitivity, mitochondria and computed tomography muscle attenuation in overweight women with and without polycystic ovary syndrome
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Chinifur, a Selective Inhibitor and "Subversive Substrate" for Trypanosoma congolense Trypanothione Reductase
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Classification of Covid-19 using Differential Evolution Chaotic Whale Optimization based Convolutional Neural Network
PublikacjaCOVID-19, also known as the Coronavirus disease-2019, is an transferrable disease that spreads rapidly, affecting countless individuals and leading to fatalities in this worldwide pandemic. The precise and swift detection of COVID-19 plays a crucial role in managing the pandemic's dissemination. Additionally, it is necessary to recognize COVID-19 quickly and accurately by investigating chest x-ray images. This paper proposed a...
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Cascade Object Detection and Remote Sensing Object Detection Method Based on Trainable Activation Function
PublikacjaObject detection is an important process in surveillance system to locate objects and it is considered as major application in computer vision. The Convolution Neural Network (CNN) based models have been developed by many researchers for object detection to achieve higher performance. However, existing models have some limitations such as overfitting problem and lower efficiency in small object detection. Object detection in remote...
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Synthesis of new conjugates of MDP and nor-MDP with retro-tuftsin derivatives as potential immunomodulators
PublikacjaZsyntetyzowano nowe analogi muramylodipeptydu (MDP) i nor-muramylo-dipeptydu (nor-MDP) z pochodnymi retro-tuftsyny jako potencjalne immunomodulatory. Przedstawiono także syntezę odpowiednich pochodnych retro-tuftsyny. Do syntezy wykorzystano metodę mieszanych bezwodników z chloromrówczanem izobutylu i N-metylomorfoliną w bezwodnym DMF.
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The effect of temperature difference on heat transport in solar cells
PublikacjaW pracy omówiono wpływ wzrostu temperatury i mechanizm transportu ciepła na drodze przewodzenia w układach hybrydowych PV/T. Wyznaczono współczynniki przewodzenia krystalicznego krzemu typu n i p oraz gęstość strumienia ciepła w zakresie temperatur od 0 do 100 st. C.
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Exploring of electronic structure of nitrogen-modified TiO2 photocatalysts through photocurrent and surface photovoltage studies
PublikacjaPrzeprowadzono pomiary fotonapięcia powierzchniowego i fotoprądu w obecności różnych reduktorów celem otrzymania eksperymentalnego potwierdzenia położenia pasma walencyjnego w strukturze elektronowej tlenku tytanu(IV) modyfikowanego azotem. Zaobserwowano silne sprzężenie poziomów N 2p i O 2p, którego konsekwencją jest powstanie nowego pasma walencyjnego
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Multi-agent graph searching and exploration algorithms
PublikacjaA team of mobile entities, which we refer to as agents or searchers interchangeably, starting from homebases needs to complete a given task in a graph.The goal is to build a strategy, which allows agents to accomplish their task. We analyze strategies for their effectiveness (e.g., the number of used agents, the total number of performed moves by the agents or the completion time).Currently, the fields of on-line (i.e., agents...
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Denitrification Process Enhancement and Diversity of the Denitrifying Community in the Full Scale Activated Sludge System after Adaptation to Fusel Oil
PublikacjaImplementation of anaerobic digestion of primary sludge in modern wastewater treatment plants (WWTPs) limits the availability of organic carbon for denitrification in conventional nitrification-denitrification (N/DN) systems. In order to ensure efficient denitrification, dosage of the external carbon source is commonly undertaken. However, application of commercial products, such us ethanol or acetate, greatly increases operational...
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Expression profiles and genomic organisation of group A protein phosphatase 2C genes inBrassica oleracea
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The detection of capsaicin and dihydrocapsaicin in horse serum following long-term local administration
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Przydatność białka rybiego w postaci kolagenu lub żelatyny oraz polisacharydu - kapa-karagenu do wytwarzania aktywnych opakowań biodegradowalnych = Usefulness of fish collagen, gelatin and carrageenan for preparation of active biodegradable packages
PublikacjaSummary - The possibility of use of protein films made of fish collagen or gelatin as well as polysaccharide carrageenan films as carriers of enzymes (lysozyme or lysostaphyne), for preparation of microbiologically active packages, was investigated. It was found that crosslinking of such systems with N-[3(dimethylamino)propyl]-N'-ethylcarboimide (EDC) does not influence the activity of lysozyme immobilized in the films (Table 1)....
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pH-tunable equilibria in azocrown ethers with histidine moieties
PublikacjaEtery koronowe posiadające elektro- i fotoaktywne reszty azowe oraz ugrupowania z ruchliwymi protonami jak w grupie COOH histydyny charakteryzują się unikalnym, zależnym od pH, efektem stymulowania pozornej obecności/nieobecności ugrupowania azowego. Obserwowane różnice właściwości elektrochemicznych eterów azokoronowych z resztą N-acetylohistydyny lub resztami imidazolu uwidaczniają się przebiegiem chemicznej redukcji w silnie...
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Direct-Ultrasonic Assisted Microextraction Coupled with RTL-GC-FID/GC-MS as a Future Standard Procedure for Monitoring 26 potentially Allergenic Fragrances in Water Samples
PublikacjaThis research topic grew up as a result of awareness of constant anthropogenic and natural input to the environment constituents of personal care products (PCPs) residues. This group of emerging pollutants encompasses a wide range of chemicals, including potentially allergenic fragrance compounds. The aim of the present study was to investigate presence of 26 fragrance allergens in water samples. Simple and rapid methodology based...
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Fragmentation of Tetrahydrofuran Molecules by H+, C+, and O+ Collisions at the Incident Energy Range of 25–1000 eV
PublikacjaWe have studied fragmentation processes of the gas-phase tetrahydrofuran (THF) molecules in collisions with the H+, C+, and O+ cations. The collision energies have been varied between 25 and 1000 eV and thus covered a velocity range from 10 to 440 km/s. The following excited neutral fragments of THF have been observed: the atomic hydrogen H(n), n = 4–9, carbon atoms in the 2p3s 1P1, 2p4p 1D2, and 2p4p 3P states and vibrationally...
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A facile method for Tauc exponent and corresponding electronic transitions determination in semiconductors directly from UV–Vis spectroscopy data
PublikacjaIn this work, a facile method allowing for estimation of the exponent in the Tauc equation directly from the UV–vis spectra is presented. It is based on the Taylor expansion of the logarithmic version of the Tauc equation. The Tauc exponent is calculated from the tangent slope of the absorption data. Knowledge of this coefficient provides information about the optical transition types and is used as an input for the calculations...
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Deodorization of model biogas by means of novel non-ionic deep eutectic solvent
PublikacjaThe paper presents new non-ionic deep eutectic solvent (DES) composed of natural and non-toxic components i.e. guaiacol, camphor and levulinic acid in 1:1:3 molar ratio as a promising absorbent for removal of selected volatile organic compounds (VOCs) including dichloromethane, toluene, hexamethyldisiloxane and propionaldehyde from model biogas. The affi nity of DES for VOCs was determined as vapour-liquid coeffi cients and the...
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Hydration of Simple Model Peptides in Aqueous Osmolyte Solutions
PublikacjaThe biology and chemistry of proteins and peptides are inextricably linked with water as the solvent. The reason for the high stability of some proteins or uncontrolled aggregation of others may be hidden in the properties of their hydration water. In this study, we investigated the effect of stabilizing osmolyte–TMAO (trimethylamine N-oxide) and destabilizing osmolyte–urea on hydration shells of two short peptides, NAGMA (N-acetyl-glycine-methylamide)...
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Modelization of Nutrient Removal Processes at a Large WWTP Using a Modified ASM2d Model
PublikacjaThe biodegradation of particulate substrates starts by a hydrolytic stage. Hydrolysis is a slow reaction and usually becomes the rate limiting step of the organic substrates biodegradation. The objective of this work was to evaluate a novel hydrolysis concept based on a modification of the activated sludge model (ASM2d) and to compare it with the original ASM2d model. The hydrolysis concept was developed in order to accurately...
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A universal method for the identification of genes encoding amatoxins and phallotoxins in poisonous mushrooms
PublikacjaABSTRACT Background. As the currently known diagnostic DNA targets amplified in the PCR assays for detection of poisonous mushrooms have their counterparts in edible species, there is a need to design PCR primers specific to the genes encoding amanitins and phallotoxins, which occur only in poisonous mushrooms. Objective. The aim of the study was testing of PCR-based method for detection of all genes encoding hepatotoxic cyclic...
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Essential Oils, Silver Nanoparticles and Propolis as Alternative Agents Against Fluconazole Resistant Candida albicans, Candida glabrata and Candida krusei Clinical Isolates
PublikacjaDevelopment of effective and safe therapeutic treatment of fungal infections remains one of the major challenge for modern medicine. The aim of presented investigation was to analyze the in vitro antifungal activity of selected essential oils, ethanolic extracts of propolis and silver nanoparticles dropped on TiO2 against azole-resistant C. albicans (n = 20), C. glabrata (n = 14) and C. krusei (n = 10) clinical isolates. Among...
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Combined partial denitrification/anammox process for nitrogen removal in wastewater treatment
PublikacjaRecently, the combined partial denitrification and anammox (PD/anammox) has received special attention as a viable alternative for N removal using organic matter present in municipal wastewater. In comparison with conventional nitrification-denitrification, PD/anammox provides enormous opportunities to achieve sustainable wastewater treatment due to the lack of dissolved oxygen (DO) demand, a smaller amount of organic carbon (C)...
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Tensile and Fatigue Behavior of Additive Manufactured Polylactide
PublikacjaThis article presents the results of monotonic tensile and fatigue tests conducted on commercial polylactide or polylactic acid (PLA). The results of fatigue tests for this material present in the literature are limited, especially for additive manufactured elements. The specimens were manufactured using the injection molding and the fused filament fabrication (FFF) method. The FFF specimens were divided into five subgroups, depending...