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Spectroscopic and magnetic studies of highly dispersible superparamagnetic silica coated magnetite nanoparticles
PublikacjaSuperparamagnetic behavior in aqueously well dispersible magnetite core-shell Fe3O4@SiO2 nanoparticles is presented. The magnetic properties of core-shell nanoparticles were measured with use of the DC, AC magnetometry and EPR spectroscopy. Particles were characterized by HR-TEM and Raman spectroscopy, showing a crystalline magnetic core of 11.5 ± 0.12 nm and an amorphous silica shell of 22 ± 1.5 nm in thickness. The DC, AC magnetic...
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Fiber optic displacement sensor with signal analysis in spectral domain
PublikacjaIn this paper, a study of a low-coherence fiber optic displacement sensor is presented. The sensor consisted of a broadband source whose central wavelength was either at 1310 nm or 1550 nm, a sensing Fabry-Pérot interferometer operating in reflective mode and an optical spectrum analyzer acting as the detection setup. All these components were connected by a single-mode fiber coupler. Metrological parameters of the sensor were...
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Polarimetric studies of L-arginine-doped potassium dihydrogen phosphate single crystals
PublikacjaConoscopic interference patterns, channelled spectra and polarimetric techniques have been used for the characterization of pure and doped (with L-arginine amino acid) potassium dihydrogen phosphate (KDP) single crystals. Experimental polarimetric data have been obtained for the frequently used wavelength of 633 nm and for two close wavelengths of 532 and 543 nm in a high-accuracy dual-wavelength polarimeter. The measurement of...
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ZnO ALD-Coated Microsphere-Based Sensors for Temperature Measurements
PublikacjaIn this paper, the application of a microsphere-based fiber-optic sensor with a 200 nm zinc oxide (ZnO) coating, deposited by the Atomic Layer Deposition (ALD) method, for temperature measurements between 100 and 300°C, is presented. The main advantage of integrating a fiber-optic microsphere with a sensing device is the possibility of monitoring the integrity of the sensor head in real-time, which allows for higher accuracy during...
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A method of predicting the best conditions for large-size workpiece clamping to reduce vibration in the face milling process
PublikacjaThe paper presents an innovative method of solving the problem of vibration suppression during milling of large-size details. It consists in searching for the best conditions for clamping the workpiece based on a rapid modal identification of the dominant natural frequencies only and requires repetitive changes in the tightening torque of the clamping screws. Then, by estimating the minimum work of the cutting forces acting in...
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Nanodiamonds Doped with Manganese for Applications in Magnetic Resonance Imaging
PublikacjaNanodiamonds (NDs) are emerging with great potential in biomedical applications like biomarking through fluorescence and magnetic resonance imaging (MRI), targeted drug delivery, and cancer therapy. The magnetic and optical properties of NDs could be tuned by selective doping. Therefore, we report multifunctional manganese-incorporated NDs (Mn-NDs) fabricated by Mn ion implantation. The fluorescent properties of Mn-NDs were tuned...
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The effect of nanoparticles size on photocatalytic and antimicrobial properties of Ag-Pt/TiO2 photocatalysts
PublikacjaAg-Pt-modified TiO2 nanocomposites were synthesized using the sol–gel method. Bimetallic modified TiO2 nanoparticles exhibited improved photocatalytic activity under visible-light irradiation, better than monometallic Ag/TiO2 and Pt/TiO2 nanoparticles (NPs). All modified powders showed localized surface plasmon resonance (LSPR) in visible region. The photocatalysts’ characteristics by X-ray diffractometry (XRD), scanning transmission...
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Thermal and physical properties of ZrO2–AlO(OH) nanopowders synthesised by microwave hydrothermal method
PublikacjaIndustrially relevant nanopowder was synthesised by microwave hydrothermal synthesis to obtain well-controlled composition (ZrO2–AlO(OH) system) which was found to determine a number of physical and thermal characteristics. This study reports variation of particle size, density, specific surface area (SSABET), as well as thermal behaviour of nanopowder mixtures of ZrO2–AlO(OH) in the whole range of compositions. It was found that...
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N-doped carbon nanospheres as selective fluorescent probes for mercury detection in contaminated aqueous media: chemistry, fluorescence probing, cell line patterning, and liver tissue interaction
PublikacjaA precise nano-scale biosensor was developed here to detect Hg2+ in aqueous media. Nitrogen-doped carbon nanospheres (NCS) created from the pyrolysis of melamine–formaldehyde resin were characterized by FESEM, XRD, Raman spectra, EDS, PL, UV–vis spectra, and N2 adsorption–desorption, and were used as a highly selective and sensitive probe for detecting Hg2+ in aqueous media. The sensitivity of NCS to Hg2+ was evaluated by photoluminescence...
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STUDY ON THE RELATIONSHIP BETWEEN VEHICLE MAINTENANCE AND FUEL CONSUMPTION
PublikacjaA contemporary road vehicle (RV) is a rather complex system, consisting of a large number of subsystems, assemblies, units, and elements (parts). While operating, an RV interacts with the environment, and its elements interact with each other. Consequently, the properties (parameters) of these elements change in the process - hardness, roughness, size, relative position, gapping, etc. A partial solution to the presented problems...
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Analiza użytkowa systemów telekomunikacji satelitarnej
PublikacjaOpisano kierunki rozwoju osobistej telekomunikacji satelitarnej. Omówiono zapotrzebowanie na usługi świadczone przy użyciu techniki satelitarnej. Przeanalizowano doświadczenia wynikające z eksploatacji systemów typu LEO i GEO, z punktu widzenia ich możliwości użytkowych i aktualnego zapotrzebowania rynku na usługi telekomunikacyjne dostarczane poprzez satelitę. Scharakteryzowano przydatność quasi-globalnego podsystemu Inmarsat-GAN...
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What defines excellent lighting design for humans and animals?
PublikacjaWhat defines excellent lighting design for humans and animals? The answer to the above question is more than complex. It is not enough nowadays to design a project to make it aesthetically pleasing. Nor is it sufficient to create nicely lit environments, or simply to achieve the light levels required by the lighting norms or standards. With the new scientific research of the last few decades that relates directly or indirectly...
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Fuzzy Multi-Regional Fractional PID controller for Pressurized Water nuclear Reactor
PublikacjaThe paper presents the methodology for the synthesis of a Fuzzy Multi-Regional Fractional Order PID controller (FMR-FOPID) used to control the average thermal power of a PWR nuclear reactor in the load following mode. The controller utilizes a set of FOPID controllers and the fuzzy logic Takagi-Sugeno reasoning system. The proposed methodology is based on two optimization parts. The first part is devoted to finding the optimal...
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Determination of pitting corrosion stage of stainless steel by galvanodynamic impedance spectroscopy
PublikacjaThis paper investigates the methodology for differentiation of multistep process of pitting corrosion of AISI 304 stainless steel in the environment of iron (III) chloride. Measurements were performed using Galvanodynamic Electrochemical Impedance Spectroscopy (GDEIS). Application of this methodology allowed monitoring of natural corrosion process without external current (IDC = 0A) nor potential perturbation of the system. Applied...
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Ellipticity in couple-stress elasticity
PublikacjaWe discuss ellipticity property within the linear couple-stress elasticity. In this theory, there exists a deformation energy density introduced as a function of strains and gradient of macrorotations, where the latter are expressed through displacements. So the couple-stress theory could be treated as a particular class of strain gradient elasticity. Within the micropolar elasticity, the model is called Cosserat pseudocontinuum...
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Cyfrowy akcelerator wybranych modułów standardu kompresji wideo H.264
PublikacjaW artykule przedstawiono konfigurowalny cyfrowy akcelerator estymacji ruchu przeznaczony dla enkodera wideo standardu H.264. Akcelerator został zaimplementowany w technologii FPGA oraz w układzie ASIC w technologii UMC 90 nm. Obie implementacje zostały zweryfikowane, a szczegółowe wyniki pomiarów akceleratora ASIC zostały porównane z innymi dostępnymi w literaturze propozycjami. System został zoptymalizowany do współpracy z oprogramowaniem...
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Ekspertyza dla Rady Dzielnicy Gdańsk Osowa - w sprawie wniosku do Studium uwarunkowań i kierunków zagospodarowania przestrzennego Miasta Gdańska
PublikacjaEkspertyza posłużyła jako podstawa do sporządzenia Uchwały Rad Dzielnic do Studium nr XI/24/2015 z dnia 9 grudnia 2015 w sprawie wniosków do Studium uwarunkowań i kierunków zagospodarowania przestrzennego Miasta Gdańska
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Pial artery and subarachnoid width response to apnoea in normal humans
PublikacjaBackground: Little is known about intracranial pressure (ICP)-cerebral haemodynamic interplay during repetitive apnoea. A recently developed method based on near-infrared transillumination/backscattering sounding (NIR-T/BSS) noninvasively measures changes in pial artery pulsation (cc-TQ) as well as subarachnoid width (sas-TQ) in humans. Method: We tested the complex response of the pial artery and subarachnoid width to apnoea...
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Anti-cancer effect of Rumex obtusifolius in combination with arginase/nitric oxide synthase inhibitors via downregulation of oxidative stress, inflammation, and polyamine synthesis
PublikacjaCancer continues to be a leading cause of death worldwide, making the development of new treatment methods crucial in the fight against it. With cancer incidence rates increasing worldwide, ongoing research must focus on identifying new and effective ways to prevent and treat the disease. The combination of herbal extracts with chemotherapeutic agents has gained much interest as a novel strategy to combat cancer. Rumex obtusifolius...
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Wrzenie nanocieczy na poziomych gładkich i chropowatych rurkach
PublikacjaPrzedstawiono wyniki pomiarów współczynnika przejmowania ciepła podczas wrzenia nanocieczy Al2O3 na rurce ze stali nierdzewnej przy ciśnieniu atmosferycznym, pod- i nadciśnieniu. Koncentracja nanocząstek o średnim wymiarze 47 nm wynosiła 0.01%, 0.1% oraz 1%.
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Rewitalizacja posadzek betonowych typu lastrico w obiektach zabytkowych. Część 2
PublikacjaW artykule przedstawiono zagadnienia materiałowe i technologiczne dotyczące posadzek typu lastrico w aspekcie oceny ich stanu technicznego oraz sposobów naprawy i rewitalizacji. Tekst stanowi kontynuacje artykułu zamieszczonego w Builder Science3 nr 9/2021
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Ag/Pt-modified TiO2 nanoparticles for toluene photooxidation in the gas phase
PublikacjaAg/Pt-modified TiO2nanocomposites were synthesized using the sol–gel method. The effect of metal typeand amount as well as synthesis route on the photocatalytic activity in reaction of toluene removal, usedas a model volatile organic compound, was investigated. Toluene, at the concentration of about 200 ppm,was irradiated over modified TiO2using light-emitting diodes (LEDs, max= 415 nm). The results showedthat toluene could be...
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Measurements of fundamental properties of homogeneous tissue phantoms
PublikacjaWe present the optical measurement techniques used in human skin phantom studies. Their accuracy and the sources of errors in microscopic parameters’ estimation of the produced phantoms are described. We have produced optical phantoms for the purpose of simulating human skin tissue at the wavelength of 930 nm. Optical coherence tomography was used to measure the thickness and surface roughness and to detect the internal inhomogeneities....
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Portable Raman spectrometer - design rules and applications
PublikacjaRaman spectroscopy has become more popular due to its new prospective field applications in forensic sciences, war against terrorism, environment protection and other field chemical analysis. Raman spectrometers can be miniaturised to portable devices and their price is decreasing due to development of optoelectronics components. Unfortunately, this technology has still numerous limitations that influence their design and limit...
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Singlet Exciton Diffusion in Vacuum-Evaporated Films of Amine-Based Materials as Studied by Photocurrent and Photoluminescence Quenching Methods
PublikacjaThe singlet exciton diffusion lengths are determined by the photoconductivity as well as the luminescence surface quenching technique, in vacuum‐evaporated layers of (4,4′,4″‐tris(N‐(3‐methylphenyl)‐N‐phenylylamino) triphenylamine) (m‐MTDATA), 4,4′,4″‐tris[2‐naphthyl(phenyl)amino] triphenylamine (2TNATA), and N,N′‐diphenyl‐N,N′‐bis(3‐methylphenyl)‐[1,1′‐biphenyl]‐4,4′‐diamine (TPD) which are frequently used for fabrication of electroluminescent...
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Enhancement of fiber-optic low-coherence Fabry-Pérot interferometer with ZnO ALD films
PublikacjaIn this paper investigation of the enhanced fiber-optic low coherence Fabry-Pérot interferometer with zinc oxide (ZnO) film deposited by atomic layer deposition (ALD) was presented. Model of the interferometer, which was constructed of single-mode optical fiber with applied ZnO ALD films, was built. The interferometer was also examined by means of experiment. Measurements were performed for both reflective and transmission modes,...
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The low coherence Fabry-Pérot interferometer with diamond and ZnO layers
PublikacjaThe authors present a fiber-optic Fabry-Pérot interferometer built with the application of diamond and zinc oxide (ZnO) thin layers. Thin ZnO films were deposited on the tip of a standard telecommunication single-mode optical fiber (SMF- 28) while the diamond layer was grown on the plate of silicon substrate. Investigated ZnO layers were fabricated by atomic layer deposition (ALD) and the diamond films were deposited using Microwave...
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FIBRE-OPTIC SENSOR FOR SIMULTANEOUS MEASUREMENT OF THICKNESSAND REFRACTIVE INDEX OF LIQUID LAYERS
PublikacjaIn this paper, we present a fibre-optic sensor for simultaneous measurement of refractive index and thickness of liquid layers. We designed an experimental low-coherence setup with two broadband light sources and an extrinsic fibre-optic Fabry–Pérot interferometer acting as the sensing head. We examined how the refractive index of a liquid film and its thickness affect spectrum at the output of a fibre-optic interferometer. We...
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Implementation of SiN thin film in fiber-optic sensor working in telecommunication range of wavelengths
PublikacjaMirrors are used in optical sensors and measurement setups. This creates a demand for mirrors made of new materials and having various properties tailored to specific applications. In this work, we propose silicon covered with a thin silicon nitride layer as a mirror for near-infrared measurements. SiN layer was deposited on a standard silicon wafer with a Low-Pressure Chemical Vapor Deposition furnace. Then, the created layer...
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Design, Synthesis, and Enzymatic Evaluation of Novel ZnO Quantum Dot-Based Assay for Detection of Proteinase 3 Activity
PublikacjaHerein, the synthesis and application of functionalized quantum dot-based protease probes is described. Such probes are composed of nontoxic ZnO nanocrystals decorated by amino groups followed by linker and labeled peptide attachment. Spherical NH2-terminated ZnO quantum dots (QDs) with the average size ranging from 4 to 8 nm and strong emission centered at 530 nm were prepared using the sol−gel method. The fluorescence of ZnO...
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Identyfikacja wad powierzchni tocznej szyn za pomocą sygnału wibroakustycznego
PublikacjaW artykule przedstawiono koncepcję metody identyfikacji najczęściej występujących wad powierzchni tocznej szyn za pomocą sygnałów wibroakustycznych. Opisano badane wady szyn take, jak: squat, head checking oraz wybuksowanie. Przedstawiono metodykę prowadzonych badań oraz wyniki analiz zarejestrowanych sygnałów dla warunków techniczno-eksploatacyjnych panujących na liniach kolejowych nr 213 Reda – Hel oraz nr 131 Chorzów Batory...
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Ekspertyza dla Rady Dzielnicy Gdańsk Orunia -Św. Wojciech-Lipce - w sprawie wniosku do sporządzanego Studium Uwarunkowań i Kierunków Zagospodarowania Przestrzennego Miasta Gdańska
PublikacjaEkspertyza posłużyła jako podstawa do sporządzenia Uchwały Nr IX/25/2015 z dnia 09.12.2015 Rady Dzielnicy Gdańsk Orunia -Św. Wojciech-Lipce - w sprawie wniosku do sporządzanego Studium Uwarunkowań i Kierunków Zagospodarowania Przestrzennego Miasta Gdańska
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Studies on the influence of β-cyclodextrin derivatives on the physical stability of famotidine
PublikacjaThe usage of Fourier transform infrared spectroscopy, near infrared spectroscopy, differential scanning calorimetry and microscopy is presented in this work focused on the exploration of the effect of CD on the physical stability of famotidine (FAM). The most significant information was achieved by analysis of the second derivatives ofnear infrared (NIR) spectra recorded. Changes in the shape of spectra derivatives allow...
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Landfill leachate treatment at a pilot plant using hydrophyte systems
PublikacjaConstructed wetlands can provide an effective and economical solution to landfill leachate treatment. In the article the performance of a CW for leachate treatment, consisting of two horizontal flow constructed wetlands (HF-CW) beds, working at the municipal landfill in Gdansk-Szadolki in the period 2004-2005 is being discussed. The plant has been operating since 2001. Clogging problems and surface flow occurred in the system...
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Stability of free floating ship. Part II
PublikacjaJest to część II artykułu, którego I część ukazała się w PMR 2/2005. Ramiona prostujące są niejednoznaczne dla statku swobodnego, bowiem zależą od sposobu działania momentu przechylającego. Omówiono dwa przypadki, gdy moment przechylający jest równoległy do płaszczyzny symetrii statku oraz gdy wykonuje najmniejszą pracę, czyli gdy jest równoległy do głównej osi bezwładności wodnicy pływania. Pokazano, że przemieszczenia kątowe...
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Technika satelitarna w telekomunikacji
PublikacjaScharakteryzowano różne rozwiązania satelitarnych systemów telekomunikacyjnych, głównie pod względem rodzaju zastosowanej orbity, co ma zasadnicze znaczenie użytkowe. Dokonano przeglądu dotychczasowych reprezentatywnych projektów takich systemów, analizując kolejne fazy ich rozwoju oraz występujące bariery technologiczno-ekonomiczne. Przedstawiono stan prac ETSI w zakresie specyfikacji GMR, której praktycznym przykładem są pierwsze...
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Sposoby i skutki fałszowania paliw silnikowych oraz metody wykrywania.Cz. 2
PublikacjaPrzedstawiono dwie grupy metod kontroli jakości paliwa - metody konwencjonalne i wybrane ''metody przesiewowe'' - w tym zastosowanie spektrofotometrii w bliskiej podczerwieni (NIR), które umożliwiają identyfikację sfałszowanego paliwa. Opisano także metodykę badań prowadzącą do oznaczenia nieznanego parametru użytkowego badanego paliwa, począwszy od utworzenia optymalnych postaci równań korelacyjnych poprzez kontrolę ich poprawności...
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The effect of a belt position in the spindle driving system on critical rotational speeds
PublikacjaThe aim of this paper was to examine how the belt pulley position affects critical rotational speeds of the modernized spindle of the sliding table saw Fx3. Methodology of determination of critical rotational speeds of the spindle in a function of the spindle design features and its driving system is presented. Spindles in these kind of machine tools are mainly driven with V-belts, and the pulleys on the spindles might be positioned:...
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Evidence for solid state electrochemical degradation within a small molecule OLED
PublikacjaAcridone derivative have been synthesised and used as OLED (Organic Light Emitting Diode) emitters which were found to be electroactive. Electrochemical investigations showed a side reaction takes place inside an active layer which diminished the overall device efficiency. By using a dopant and host active layer architecture, the formation of the by product was removed. The by-product was identified as a σ-dimer formed inside an...
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Distillery Wastes as External Carbon Sources for Denitrification in Municipal Wastewater Treatment Plants
PublikacjaW pracy przedstawiono wyniki badań nad zastosowaniem półproduktów oraz produktów odpadowych z gorzelni i destylarni, jako potencjalne źródło zewnętrznego węgla organicznego w celu poprawy denitryfikacji w systemach z biologicznym usuwaniem związków biogennych. W celu porównania efektywności trzech badanych substancji (oleje fuzlowe, odcieki i syrop) wykonano testy na szybkość redukcji azotanów (z ang. NUR) oraz szybkość zużycia...
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Distillery Wastes as External Carbon Sources for Denitrification in Municipal Wastewater Treatment Plants
PublikacjaW pracy przedstawiono wyniki badań nad zastosowaniem półproduktów oraz produktów odpadowych z gorzelni i destylarni, jako potencjalne źródło zewnętrznego węgla organicznego w celu poprawy denitryfikacji w systemach z biologicznym usuwaniem związków biogennych. W celu porównania efektywności trzech badanych substancji (oleje fuzlowe, odcieki i syrop) wykonano testy na szybkość redukcji azotanów (z ang. NUR) oraz szybkość zużycia...
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Krajowy Program Bezpieczeństwa Ruchu Drogowego 2005-2007-2013. GAMBIT 2005
PublikacjaW artykule przedstawiono syntezę Krajowego Programu Bezpieczeństwa Ruchu Drogowego GAMBIT 2005. Jest to dokument opracowany na zamówienie Krajowej Rady BRD, przyjęty przez Radę Ministrów w dniu 19 kwietnia 2005 jako program dla Polski na lata 2005-2007-2013. Polska wchodząc do Unii Europejskiej w maju 2004 przyjęła cel ustalony w Polityce Transportowej UE ''w ciągu dekady zmniejszyć o połoweę liczbę śmiertelnych ofiar wypadków...
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Sensitivity of the Baltic Sea level prediction to spatial model resolution
Publikacjahe three-dimensional hydrodynamic model of the Baltic Sea (M3D) and...
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Simultaneous Determination of Indolic Compounds in Plant Extracts by Solid-Phase Extraction and High-Performance Liquid Chromatography with UV and Fluorescence Detection
PublikacjaA high-performance liquid chromatographic method with UV and fluorescence detection (HPLC-DAD-FLD) was developed for simultaneous determination of indolic compounds in plant material. Indole-3-carbinol (I3C), indole-3-acetic acid (I3AA), indole-3-acetonitrile (I3ACN), and 3,3′-diindolylmethane (DIM) were used as representative compounds that cover a wide spectrum of indole structures occurring in nature. For concentration and purification...
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Segmentation Quality Refinement in Large-Scale Medical Image Dataset with Crowd-Sourced Annotations
PublikacjaDeployment of different techniques of deep learning including Convolutional Neural Networks (CNN) in image classification systems has accomplished outstanding results. However, the advantages and potential impact of such a system can be completely negated if it does not reach a target accuracy. To achieve high classification accuracy with low variance in medical image classification system, there is needed the large size of the...
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Amberlyst-15 catalysed synthesis of novel indole derivatives under ultrasound irradiation: Their evaluation as serotonin 5‑HT2C receptor agonists
PublikacjaA series of indole based novel Schiff bases was designed as potential agonists of 5‑HT2C receptor that was supported by docking studies in silico. These compounds were synthesized via Amberlyst-15 catalysed condensation of an appropriate pyrazole based primary amine with the corresponding indole-3-aldehyde under ultrasound irradiation at ambient temperature. A number of target Schiff bases were obtained...
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Assessment of Emotional Expressions after Full-Face Transplantation
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Chemoselektywność w reakcjach wybranych związków fosforu z pochodnymi hydroksyloaminy
PublikacjaZaprezentowane reakcje wielofunkcyjnych pochodnych hydroksyloaminy składają w większości przypadków z ciągów równoległych i następczych procesów, które prowadzą do powstawania mieszanin produktów. Uzyskane i przeanalizowane rezultaty badań pogłębiają wiedzę na temat ważnej biologicznie i mającej znaczenie praktyczne reakcji przeniesienia fosforylu z udziałem pochodnych hydroksyloaminy. I tak, zbadano wpływ budowy reagentów i mechanizmy...
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Anticancer Study on IrIII and RhIII Half-Sandwich Complexes with the Bipyridylsulfonamide Ligand
PublikacjaTwo non-platinum compounds, organometallic half-sandwich complexes [(η 5 -Cp)IrCl(L)]PF 6 (1) and [(η 5 -Cp)RhCl(L)]PF 6 (2) were prepared by treating pentamethylcyclopentadienyl chloride dimers of iridium(III) or rhodium(III) with the obtained 4-amino-N-(2,2'-bipyridin-5- yl)benzenesulfonamide ligand (L) and ammonium hexafluorophosphate. The crystal structures of ligand (L) and complexes 1 and 2 were obtained and then analyzed. Coordination...
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Chemiluminogenic acridinium salts: A comparison study. Detection of intermediate entities appearing upon light generation
PublikacjaThe nine derivatives of acridine-9-carboxylic acid (CMADs) capable for chemiluminescence (CL), representing various classes of compounds were isolated in a chemically pure state (assessed by RP-HPLC) and identified using high resolution mass spectrometry (ESI-QTOF) and magnetic resonance (1H NMR) techniques. Among them are aryl acridinium esters, containing certainly selected and located substituents in both aromatic systems, an...