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Wyniki wyszukiwania dla: GC-FID
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Determination the method of free alcohol fermented beverage production based on roasted raw materials.
Dane BadawczeData set presents the results of monosaccharides and ethyl alcohol determination in samples of fermented cereal drink with increased health value based on barley malt and roasting of rye, chicory and beetroot, and with the addition of hops. The HPLC method with RID detector was used for determinations
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Evaluation of Professional Demands and Financial Reward Through the Perception of Police Managers
PublikacjaThe aim of the study was to examine the relationship between job demands and salary in the subjective perception of mid-level police managers. An occupational stress model in which effort spent on job demands are not balanced by the received reward, was adopted. The study comprised 51 police officers (4 women). The partial least squares method was used for the analysis, and the SmartPLS 2.0 program was applied. The income and...
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Efficient FPGA Implementation of an RFIR Filter Using the APC–OMS Technique with WTM for High-Throughput Signal Processing
PublikacjaNowadays, Finite Impulse Response (FIR) filters are used to change the attributes of a signal in the time or frequency domain. Among FIR filters, a reconfigurable filter has the advantage of changing the coefficient in real-time, while performing the operation. In this paper, the Anti-Symmetric Product Coding (APC) and Odd Multiple Storage (OMS) modules are utilized to implement the reconfigurable FIR filter (RFIR–APC–OMS). Herein,...
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Badanie wpływu częstotliwości zasilania cewki i stopnia dyskretyzacji układu cewka - dysk na wyniki obliczeń.
PublikacjaW artykule przedstawione są rezultaty badań teoretycznych wpływu częstotliwości prądów cewki i stopnia układu cewki sprzężonej z nieruchomym przewodzącym dyskiem (NID) na wyniki obliczeń. Badania dotyczą NID o wybranych parametrach. Autorzy zastosowali hybrydowy model anlityczno-numeryczny wykorzystujący związki analityczne określające zarówno indukcyjności własne pierścieni o przekroju kołowym jak i indukcyjności wzajemne.
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Can we really solve an arch stability problem?
PublikacjaWe bring attention to the problem of solving nonlinear boundary-value problems for elastic structures such as arches and shells. Here we discuss a classical problem of a shear-deformable arch postbuckling. Considering a postbuckling behaviour of a circular arch we discuss the possibility to find numerically a solution for highly nonlinear regimes. The main attention is paid to the problem of determination of all solutions. The...
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Strategie zarządzania obszarami śródmiejskimi - kwestia przestrzeni handlu
PublikacjaArtykuł opisuje strategie zarządzania śródmiejskimi przestrzeniami handlu, m. in. Town Centre Management (TCM) jak i Business Improvement Districts (BID). Artykuł zawiera opis genezy strategii oraz głównych zadań przez nie realizowanych (zarządzanie, marketing, estetyzacja, ochrona). Artykuł kończy spojrzenie na alternatywy dla komercyjnych aspektów BID związanych z zarządzeniem śródmieściem jako strategią aktywizacji społecznej.
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Calculations of material factors for a set of 20 thermistors
Dane BadawczeThe presented data set is part of the research aimed at determining the actual characteristics of each thermistor in a package of twenty NTC10k type sensors.
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Calculations of the resistance values of 10 ratio resistors
Dane BadawczeThe presented data set is part of the research aimed at determining the actual characteristics of each thermistor in a package of twenty NTC10k type sensors.
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'22/'23 Badanie żywności techniką PCR - KID
Kursy OnlineCEL: Student identyfikuje i klasyfikuje patogeny oraz grzyby toksynotwórcze w żywności i ocenia ich szkodliwość. Przedstawia podstawowe systemy diagnostyczne, stosowane do wykrywania zafałszowań w żywności. Wyjaśnia zasady działania techniki PCR.
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Inter Applied Chemistry Programme 9 Mid-Monitoring
Kursy OnlineKurs przeznaczony do Monitorowania losu absolwentów IACP
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Experimental and theoretical studies on the photodegradation of 2-ethylhexyl 4-methoxycinnamate in the presence of reactive oxygen and chlorine species
Publikacja2-Ethylhexyl 4-methoxycinnamate (EHMC) is one of the most commonly used sunscreen ingredient. In this study we investigated photodegradation of EHMC in the presence of such common oxidizing and chlorinating systems as H2O2, H2O2/HCl, H2O2/UV, and H2O2/HCl/UV. Reaction products were detected by gas chromatography with a mass spectrometric detector (GC-MS). As a result of experimental studies chloro-substituted 4-methoxycinnamic...
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Evaluation of headspace solid-phase microextraction for the analysis of volatile carbonyl compounds in spirits and alcoholic beverages
PublikacjaOpracowano metodę oznaczania C1-C6 związków karbonylowych w układzie GC-ECD w roztworach alkoholowych poprzez derywatyzację pentafluorobenzylohydroksy-aminą i mikroekstrakcję w fazie stacjonarnej z fazy nadpowierzchniowej. Zoptymalizowano warunki eksperymantalne: zawartość alkoholu, czas ekspozycji, temperaturę i sposób mieszania próbki. W metodzie tej najpierw przeprowadza się rozcieńczenie spirytusu lub napojów alkoholowych do...
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Comparison of different techniques for extracting Polychlorinated Biphenyls from bottom sediment samples using Isotope Dilution Mass Spectrometry
PublikacjaIn this work, problems that may occur during determination of trace levels of polychlorinated biphenyls in sediment samples are described. The main error sources are connected with extraction of analytes prior to final determination. During model studies, polychlorinated biphenyls have been extracted from sediment reference material (METRANAL 2) with the use of different solvents (dichloromethane, hexane, and toluene); the process...
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Studies on applicability of new solid-phase microextraction fibers for the selective extraction and determination of short - chain monocarboksylic acids
PublikacjaShort-chain monocarobxylic acids, sometimes referred to as volatile fatty acids (VFA), are a group of low molecular weight alkyl monocarboxylic acids that are widely distributed within the environment. These molecules contain any from 2 to 8 carbon atoms and originate from the anaerobic biodegradation of organic matter such as carbohydrates, proteins, and fats. These compounds are commonly found in the effluents from animal farming,...
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Novel analytical method for detection of orange juice adulteration based on ultra-fast gas chromatography
PublikacjaThe food authenticity assessment is an increasingly important issue in food quality and safety. The application of an electronic nose based on ultra-fast gas chromatography technique enables rapid analysis of the volatile compounds from food samples. Due to the fact that this technique provides chemical profiling of natural products, it can be a powerful tool for authentication in combination with chemometrics. In this article,...
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Preparation, characterization and anti-colitis activity of curcumin-asafoetida complex encapsulated in turmeric nanofiber
PublikacjaUlcerative colitis (UC) is a main form of inflammatory bowel disease (IBD). Asafoetida (ASF) and turmeric have traditionally been used for the treatment of various inflammatory diseases, including UC, because ASF is rich in sulfur compounds and turmeric contains curcumin (CUR). Turmeric nanofiber (TNF), the modified cell wall component of turmeric is considered to play important role in the human diet, health and can be used as...
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Transportable, Portable and Micro Gas Chromatographs
PublikacjaSignificant benefits can be obtained by miniaturization of conventional benchtop gas chromatographs. The attractive features arising from miniaturization include low-power requirements, low heat capacity of separation columns, low consumption of mobile phase, enhanced performance, higher portability, and easily coupling to detectors and secondary chromatographic systems. In separation sciences, including gas phase separations,...
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Genotoxic properties of glucosinolates and isothiocyanates present in Brassica vegetables
PublikacjaThe bioactive phytochemicals found in Brassica vegetables, in this number glucosinolates (GLS), as well as products of their degradation such as isothiocyanates (ITC) and indoles, are regarded as the most promising chemopreventive compounds. These secondary metabolites display stron antibiological activity and constitute defence system preventing the development of agrophages attacking Brassica plants. Such properties suggest...
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DMSO hydration redefined: Unraveling the hydrophobic hydration of solutes with a mixed hydrophilic–hydrophobic characteristic
PublikacjaHydrophobic hydration of solutes with a mixed hydrophilic--hydrophobic characteristics is still poorly understood. This is because both experimental and theoretical methods find it difficult to see the ice-like water structure around the nonpolar solute groups, unlike hydrogen bonds with the hydrophilic groups. In order to unravel this problem, we have investigated DMSO hydration by means of infrared spectroscopy and theoretical...
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Nontoxic Goiter (NTG) and Radioiodine: What Do Patients Think About It? Quality of Life in Patients with NTG Before and After 131-I Therapy
PublikacjaObjective Despite numerous publications regarding nontoxic goiter (NTG) treatment and an increasing interest in patients’ quality of life, few studies present the outcome of 131-I treatment from the patients’ perspective. Our study’s main aim was to verify whether there is any improvement in life quality following 131-I treatment. Materials and methods Thirty-five patients with NTG qualified to participate in the study. All patients...
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Comparison of protein precipitation methods for various rat brain structures prior to proteomic analysis
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Thermal and solutal performance of Cu/CuO nanoparticles on a non-linear radially stretching surface with heat source/sink and varying chemical reaction effects
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Mieszkanie w drzewostanie. Habitat Trzeciej Fali EXPO 2010 Wrocław. Habitat 2002.
Publikacja''Mieszkanie w drzewostanie'' to próba odpowiedzi na potrzeby miasta Wrocławia w zakresie zaplecza mieszkaniowego dla planowanej w 2010 roku wystawy EXPO.Jest to propozycja stworzenia najbardziej naturalnego i przyjaznego środowiska łączącego w jednym miejscu funkcje: mieszkania, pracy i rekreacje.
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Determinants of the surface quality, density and dimensional correctness in selective laser melting of the Ti-13Zr-13Nb alloy
PublikacjaSelective laser melting is widely used for custom-designed elements. Successful manufacturing depends on laser treatment parameters and material features. This research aimed to determine the effects of laser power, scan time and hatch distance on surface quality, relative density and dimensional precision for cuboids made of the Ti-13Zr-13Nb alloy. The influence of energy density, energy flux and pre-heating was seen to be decisive...
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Discriminatory expressions, the young and social networks: The effect of gender
PublikacjaIn the framework of the «Project I: CUD» (Internet: Creatively Unveiling Discrimination), carried out in the United Kingdom, Italy, Belgium, Romania and Spain, we conducted a study into the expressions of discrimination used by young people on social network sites. To do so we designed a methodological strategy for detecting discriminatory content in 493 Facebook profiles and used this strategy to collect 363 examples for further...
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ZASTOSOWANIE APLIKACJI INTERNETOWEJ W OCENIE JAKOŚCI DOPASOWANIA APARATÓW SŁUCHOWYCH
PublikacjaW pracy opisano zastosowanie aplikacji internetowej do oceny jakości dopasowania aparatów słuchowych. Metoda oceny polega na badaniu ankietowym, uzupełnionym testem rozumienia słów jednosylabowych w polu swobodnym. Opisywana aplikacja internetowa pozwala na przeprowadzenie badania z dowolnego komputera z dostępem do sieci. Dzięki implementacji metody w postaci aplikacji internetowej, można w systematyczny i uporządkowany sposób...
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Application of gas chromatography to the analysis of spirit-based alcoholic beverages
PublikacjaSpirit-based beverages are alcoholic drinks, which production processes are dependent on the type and origin of raw materials. The composition of this complex matrix is difficult to analyze and scientists commonly choose a gas chromatography techniques for this reason. With a wide selection of extraction methods and detectors it is possible to provide qualitative and quantitative analysis for many chemical compounds with a various...
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Krzysztof Jan Kaliński prof. dr hab. inż.
OsobyUkończył studia magisterskie na Wydziale Mechanicznym Technologicznym (MT) PG (1980, dyplom z wyróżnieniem). Stopień doktora otrzymał na Wydziale Budowy Maszyn PG (1988, praca wyróżniona), stopień doktora habilitowanego na Wydziale Mechanicznym (WM) PG (2002, praca wyróżniona), a tytuł profesora nauk technicznych – w 2013 r. Od 2015 r. jest profesorem zwyczajnym, a od 2019 r. - profesorem. Obszar jego badań naukowych obejmuje:...
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Krzysztof Druet dr inż.
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Separation and determination of the group-type composition of modern base and lubricating oils with a wide range of polarity, especially emitted to the environment
PublikacjaLubricating oils are composed of base oils (>85% v/v) and enriching additives (<15% v/v). Three types of base oils may be distinguished: 1) traditional bases (obtained by low-volatile fractions from crude oil distillation refining), 2) synthetic bases (mainly poly-alpha-olefins, sometimes esters, especially succinic acid esters), 3) bases of natural origin (especially obtained from refined plant oils). The bases of natural origin...
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Dataset of phase portraits of the fractional prey-predator model with Holling type-II interaction (without predator harvesting)
Dane BadawczeThe need for a fractional generalization of a given classical model is often due to new behaviors which cannot be taken into account by the model. In this situation, it can be useful to look for a fractional deformation of the initial system, trying to fit the fractional exponent of differentiation in order to catch properly the data.
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Areas of Updraft Air Motion in an Idealised Weather Research and Forecasting Model Simulation of Atmospheric Boundary Layer Response to Different Floe Size Distributions
PublikacjaPresented dataset is part of a numerical modelling study focusing on the analysis of the influence of sea ice floe size distribution (FSD) on the horizontal and vertical structure of convection in the atmosphere. The total area and spatial arrangement of the up-drafts indicates that the FSD affects the total moisture content and the values of area averaged turbulent fluxes in the model domain. In fact, while convective updrafts...
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ProSIL Software for functional saferty management in life cycle = Aplikacja ProSIL do zarządzania bezpieczeństwem funkcjonalnym w cyklu życia
PublikacjaIn the paper the ProSIL software to aid the functional safety management is presented. The software consists of three modules to aid: determination of the required SIL level (ProSILen), veryfication of the SIL level (ProSILver). In the aplication the method of the calibrated risk graph to determine the required safety integrity level SIL for defined safety instrumented functions is applied. The methods concerning functional safety...
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Ship Evolutionary Trajectory Planning Method with Application of Polynomial Interpolation
PublikacjaPaper presents the application of evolutionary algorithms and polynomial interpolation in ship evolutionary trajectory planning method. Evolutionary algorithms allows to find a coIlision free trajectory in real time, while polynomial interpolation allows to model smooth trajectory which keeps continuity of velocity and acceleration values along path. Combination of this two methods allows to find trajectory, which under some assumptions,...
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Algorytmy sterowania dla poprawy jakości regulacji położenia w serwonapędach
PublikacjaW serwonapędach o kaskadowej strukturze regulacji momentu, prędkości i położenia, opartej na algorytmach PID, w stanach dynamicznych występują uchyby, które trudno zmniejszyć tylko przez dobór nastaw regulatorów. W referacie zaproponowano metody ich redukcji, oparte na zastosowaniu sprzężenia do przodu. Przedstawiono także modyfikacje algorytmu PID, polegające na dynamicznej adaptacji nastaw do aktualnych wartości uchybu. Omówiono...
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Sprawozdanie z badań laboratoryjnych gruntu w aparacie trójosiowego ściskania
PublikacjaOpis badania gruntu niespoistego w aparacie trójosiowego ściskania metodą CID. Przedstawienie wyników badań wraz z analizą.
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X-ray diffractometry results of the Sr0.86Ti0.65Fe0.35O3 powder
Dane BadawczeThis dataset contains results of X-ray diffractometry mesurement (XRD) of the Sr0.86Ti0.65Fe0.35O3-d (STF35) powder. The phase composition of the investigated STF35 powder was analyzed by XRD at room temperature. It confirms the formation of the cubic perovskite oxide phase. Calculated average lattice constant is a 3.90882(1) Å, with Goodness of Fit...
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Electrical characterization of diamond/boron doped diamond nanostructures for use in harsh environment applications
PublikacjaThe polycrystalline boron doped diamond (BDD) shows stable electrical properties and high tolerance for harsh environments (e.g. high temperature or aggressive chemical compounds) comparing to other materials used in semiconductor devices. In this study authors have designed electronic devices fabricated from non-intentionally (NiD) films and highly boron doped diamond structures. Presented semiconductor devices consist of highly...
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Accelerated solvent extraction-gas chromatographic determination of acidic herbicides in soil
PublikacjaPrzyspieszona ekstrakcja rozpuszczalnikiem z wykorzystaniem wody jako ekstraktanta okazała się skutecznym sposobem izolacji herbicydów kwasowych (MCPP, MCPA, 2,4-D, 2,4,5-T, PCP, dinoseb, dinoterb) z próbek gleby. Wysoka zawartość substancji iłowych powodowała problemy techniczne, które udało się pokonać poprzez zwiększenie stosunku piasku do gleby w celce ekstrakcyjnej. Anality przenoszono z ekstraktu wodnego do rozpuszczalnika...
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The Sonocatalytic Activation of Persulfates on Iron Nanoparticle Decorated Zeolite for the Degradation of 1,4-Dioxane in Aquatic Environments
PublikacjaIn the chemical industry, 1,4-diethylene dioxide, commonly called dioxane, is widely used as a solvent as well as a stabilizing agent for chlorinated solvents. Due to its high miscibility, dioxane is a ubiquitous water contaminant. This study investigates the effectiveness of catalyst- and ultrasound (US)-assisted persulfate (PS) activation with regard to degrading dioxane. As a first step, a composite catalyst was prepared using...
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Contamination of Runoff Water at Gdańsk Airport (Poland) by Polycyclic Aromatic Hydrocarbons (PAHs) and Polychlorinated Biphenyls (PCBs)
PublikacjaAirport runoff can contain high concentrations of various pollutants, in particular polycyclic aromatic hydrocarbons (PAHs) and polychlorinated biphenyls (PCBs), the environmental levels of which have to be monitored. Airport runoff water samples, collected at the Gdańsk-Rębiechowo Airport from 2008 to 2009, were analysed for PAHs and PCBs by gas chromatography. The aromatic fractions were separated by liquid-liquid extraction...
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Characterization of home-made and regional fruit wines by evaluation of correlation between selected chemical parameters
PublikacjaSince the last decade of the 20th century, there has been rising interest in the production of fruit wines, as evidenced by the high number of published papers and books covering this matter. When aiming to produce quality fruit wines, it is essential to evaluate the analytical parameters of the beverage. In this context, there are a large number of analyses for the evaluation of wines and fruit wines. This article characterizes...
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Interaction of human serum albumin with volatiles and polyphenols from some berries
PublikacjaHeadspace solid-phase microextraction coupled with comprehensive two-dimensional gas chromatography with time-of-flight mass spectrometry (HS-SPME/GC GCeTOFMS) identified 19 and quantified 6 monoterpenes in gooseberries, blueberries and cranberries. As a protein model human serum albumin (HSA) was used in interaction with terpenes. Specific binding of terpenes to HSA under the physiological conditions was a result of the formation...
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Chemical Composition of Atmospheric Air in Nemoral Scots Pine Forests and Submountainous Beech Forests: The Potential Region for the Introduction of Forest Therapy
PublikacjaStudies show that forests are one of the main recreational destinations. This can be explained by their beneficial effects on the health of their visitors, which can be attributed to compounds from the terpene group. The aim of this research was to determine the chemical composition of air in the interiors of Nemoral Scots pine forests and submountainous beech forests, with the determination of compounds of the terpene group. Samples...
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An Approach to Mean Path Loss Model Estimation for Off-Body Channels
PublikacjaThis paper presents an approach to estimation of the mean path loss model parameters in off-body Body Area Networks channels. In this approach, the path loss exponent is constrained to a value obtained for the line-of-sight (LoS) propagation in the co-polarised channel, considering a generalised static scenario. The comparison of the goodness of fit between the proposed approach and other approaches, for a set of measurements obtained...
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Multiscalar Model Based Control Systems for AC Machines
PublikacjaContents of the Chapter: Nonlinear transformations and feedback linearization. Models of the squirrel cage induction machine: Vector model of the squirrel cage induction machine. Multiscalar models of the squirrel cage induction machine.Feedback linearization of multiscalar models of the induction motor.Models of the double fed induction machine: Vector model of the double fed induction machine. Multiscalar model of the...
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Pomoszcz Ministerstwa Inostrannych del Polszy Armenji, Azerbejdzżany i Gruzji = Polish Development Assistance for Armenia, Azerbaijan and Georgia
PublikacjaGeorgia has been one of the priority areas of development assistance of Polish Ministry of Foreign Affairs from 2004, because it plays a important role in Polish forsign policy in the framework of the Eastern Partnership. The largest amounts of development aid supporting the transformation were allocated for this country. Since founding the Eastern Partnership initiative in 2009 also Azerbaijan and Armenia have been included to...
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Chinese Foreign Direct Investments in Europe. The Polish Case
PublikacjaThe first aim of this paper is to analyze the features that have motivated Chinese outbound investments in the European Union. The paper outlines also the policies adopted by the European institutions and its member states to encourage the increase of the Chinese FDI without harming the internal European market, and consequently phase out all concerns that are afflicting the European public opinion. The second purpose is more focused...
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Poland – Iran trade turnover annually in 2009-2014 (millions of USD)
Dane BadawczeIn 2014, Polish exports to Iran was worth of 34.9 million EUR and imports 22.4 million (the trade turnover exceeded 57 million EUR). Year 2015 did not bring recovery in economic relations - the value of trade exchange exceeded only EUR 60 million. In comparison to 2011 when the total value of bilateral trade reached EUR 167 million.
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Analiza stanu nawierzchni i klas pojazdów na podstawie parametrów ekstrahowanych z sygnału fonicznego
PublikacjaCelem badań jest poszukiwanie parametrów wektora cech ekstrahowanego z sygnału fonicznego w kontekście automatycznego rozpoznawania stanu nawierzchni jezdni oraz typu pojazdów. W pierwszej kolejności przedstawiono wpływ warunków pogodowych na charakterystykę widmową sygnału fonicznego rejestrowanego przy przejeżdżających pojazdach. Następnie, dokonano parametryzacji sygnału fonicznego oraz przeprowadzano analizę korelacyjną w celu...