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Reactions of R<sub>2</sub>P-P(SiMe<sub>3</sub>)Li with [(R'<sub>3</sub>P)<sub>2</sub>PtCl<sub>2</sub>]. A General and Efficient Entrance to Phosphanylphosphinidene Complexes of Platinum. Syntheses and Structures of [(η<sub>2</sub>-P=P<sup>i</sup>Pr<sub>2</sub>)Pt(p-Tol<sub>3</sub>P)<sub>2</sub>], [(η<sub>2</sub>-P=P<sup>t</sup>Bu<sub>2</sub>)Pt(p-Tol<sub>3</sub>P)<sub>2</sub>], [{η<sub>2</sub>-P=P(N<sup>i</sup>Pr<sub>2</sub>)2}Pt(p-Tol<sub>3</sub>P)<sub>2</sub>] and [{(Et<sub>2</sub>PhP)<sub>2</sub>Pt}<sub>2</sub>P<sub>2</sub>].
PublikacjaReakcje pochodnych litowych difosfanów R2P-P(SiMe3)Li z (R'3P)2PtCl2 zachodzą łatwo i prowadzą do wytworzenia bocznie (side-on) związanych fosfanofosfinidenowych kompleksów platyny [(η2-P=PR2)Pt(PR'3)2] (dla R=tBu, iPr, Et2N, iPr2N). Reakcja Ph2P-P(SiMe3)Li...
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Paweł Szymon Dąbrowski dr inż.
OsobyDr inż. Paweł Szymon Dąbrowski w latach 2004-2009 studiował na kierunku geodezja i kartografia na Uniwersytecie Warmińsko-Mazurskim w Olsztynie, gdzie uzyskał tytuł zawodowy magistra inżyniera. W latach 2009-2016 pracował w wykonawstwie geodezyjnym w Iławie i Gdańsku. Doświadczenie zawodowe zdobył on podczas realizacji inwestycji Pomorskiej Kolei Metropolitalnej, co pomogło mu w zdobyciu w 2015 r. geodezyjnych uprawnień zawodowych...
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Primary degradation of antidiabetic drugs
PublikacjaType 2 diabetes is a chronic disease affecting a large portion of the world population and is treated by orally administered drugs. Since these drugs are often taken in high doses and are excreted unchanged or partially metabolised many of them are nowadays detected in surface waters or wastewater treatment plants effluents. Unmetabolised antidiabetics or some of their transformation products retain their pharmacological activity,...
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Pilot installation for thermal utilization of meat-and-bone meal using the rotary kiln pyrolyzer and the fluidised bed boiler
PublikacjaThe technology of thermal utilization of meat-and-bone meal (MBM) is still at the research state. However, there are already a number of existing pilot-scale installations that provide the complete, effective and environmentally safe process conducting. The universal technology was developed that allows to combust various types of waste, including animal waste, municipal waste and sludge, mixed at any ratio with different types...
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A memory efficient and fast sparse matrix vector product on a Gpu
PublikacjaThis paper proposes a new sparse matrix storage format which allows an efficient implementation of a sparse matrix vector product on a Fermi Graphics Processing Unit (GPU). Unlike previous formats it has both low memory footprint and good throughput. The new format, which we call Sliced ELLR-T has been designed specifically for accelerating the iterative solution of a large sparse and complex-valued system of linear equations arising...
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Kompleksowa analiza symulacyjna układu napędowego zespołu trakcyjnego
PublikacjaThe paper describes an approach to comprehensive analysis of traction electric drive. The drivetrain of ED-74 electric unit equipped with four inverter-fed induction motors was modeled in Matlab/Simulink. The model consists of functional blocks as: motors, inverters, drive controllers, filters. Structure and operation of the model was described. Chosen simulation results were presented and discussed. Two methods of modeling the...
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New empirical correlations for the viscosity of selected organic phase change materials
PublikacjaAlthough there are many methods and instruments for measuring viscosity, it is still difficult to determine a reliable value of the dynamic viscosity of complex chemicals such as paraffins and fatty acids. This is due to the complex and heterogeneous structure of these compounds in the case of commercial products. On the other hand, the measuring instrument should be selected very carefully, including its measuring principle and...
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Topological modifications for performance improvement and size reduction of wideband antenna structures
PublikacjaCompact antennas belong to the key components of modern communication systems. Their miniaturization is often achieved by introducing appropriate topological changes such as simple ground plane slots or tapered feeds. More sophisticated modifications are rarely considered in the literature because they normally lead to significant increase of the number of tunable parameters, which makes the antenna design process more challenging....
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Comparative Greenness Evaluation
PublikacjaGreenness of analytical procedure is multivariable aspect as many greenness criteria should be taken into consideration. On the other hand, modern analytical chemistry offers dozens of analytical procedures, based on different sample preparation and final determination techniques that are used for the determination of a given analyte in a given matrix. For such complex decision-making processes, multi-criteria decision analysis...
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Result of the 6-min walk test is an independent prognostic factor of surgically treated non-small-cell lung cancer
PublikacjaPathological tumour, node and metastasis (TNM) stage remains the most significant prognostic factor of non-small-cell lung cancer (NSCLC). Meanwhile, age, gender, pulmonary function tests, the extent of surgical resection and the presence of concomitant diseases are commonly used to complete the prognostic profile of the patient with early stage of NSCLC. The aim of this study is to assess how the result of a 6-min walk test (6MWT)...
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Equitable coloring of hypergraphs
PublikacjaA hypergraph is equitablyk-colorable if its vertices can be partitioned into k sets/colorclasses in such a way that monochromatic edges are avoided and the number of verticesin any two color classes differs by at most one. We prove that the problem of equitable 2-coloring of hypergraphs is NP-complete even for 3-uniform hyperstars. Finally, we apply the method of dynamic programming for designing a polynomial-time algorithm to...
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The estrogenicity of wastewater samples.
Dane BadawczeThe principle of operation of the kit is based on the fact that the tested sample with endocrine activity (containing compounds capable of binding to the human estrogen receptor α, hERα) releases the fluorescently labeled ligand (FluormoneTM ES2) from the receptor-ligand complex, which results in a reduction of the polarization value fluorescence. The...
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Janusz Smulko prof. dr hab. inż.
OsobyUrodził się 25 kwietnia 1964 r. w Kolnie. Ukończył w 1989 r. z wyróżnieniem Wydział Elektroniki Politechniki Gdańskiej, specjalność aparatura pomiarowa. Zajął II miejsce w konkursie Czerwonej Róży na najlepszego studenta Wybrzeża w 1989 r. Od początku kariery związany z Politechniką Gdańską: asystent (1989–1996), adiunkt (1996–2012), profesor nadzwyczajny PG (od 2012). Odbył staże naukowe w Texas A&M University (2003, NATO...
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Interference aware bluetooth scatternet (re)configuration algorithm IBLUERA
PublikacjaThis paper presents a new algorithm IBLUEREA, which enables reconfiguration of Bluetooth scatternet to reduce interference. IBLUEREA makes use of the complex model comparing ISM environment efficiency. The mechanism envisages the use of the assessment of the probability of successful (unsuccessful) frame transmission in order to take a decision concerning co-existence of technologies which make use of the same ISM band (here Bluetooth...
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Compact antenna array comprising fractal-shaped microstripradiators
PublikacjaA design method of antenna array consisting of eight microstrip patches modified with Sierpinski fractal curves has been presented andexperimentally validated in this paper. Method proposed has enabled the achievement of considerable miniaturization of array length (26%),together with multi-band behavior of the antenna, which proves the attractiveness of presented design methodology and its ability to be implemented in more complex...
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Free-surface elevation in open vortex flow controls
PublikacjaRotational form of fluid motion is complex, but very important in science and technology. The paper is devoted to the hydraulic mechanism of flow in open vortex flow controls, or regulators. The velocity field was described by the kinematic model, and intensity of rotation - by means of the energy balance between the input and dissipation. In consequence some algebraic expresions were obtained, which can be useful in approximated...
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Stanisław Galla dr inż.
OsobyUrodził się w 1970 w Gdańsku. Jest absolwentem Technikum Mechaniczno Elektrycznego w Gdańsku (1990). Studiował na Wydziale Elektrotechniki Politechniki Gdańskiej (studia ukończył w 1996). Rozprawę doktorską pt. „Metodyka zwiększania dokładności pomiarów małoczęstotliwościowych wskaźników zaburzeń okresowych występujących w sieciach niskiego napięcia” obronił w 2009 r na Wydziale Elektrotechniki i Automatyki Politechniki Gdańskiej....
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Quality of service in optical burst switched networks
PublikacjaIn the paper analytical models of two service differentiation schemes for optical burst switched network: extended offset time based and PPS (Preemptive Priority Scheme) are revised. Also accordance of analytical models for those schemes is studied when complete class isolation is assumed. Furthermore authors introduce an analytical model which describes an effective degree of isolation when burst switched network employs both...
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Quality of service in optical burst switched networks
PublikacjaIn the paper analytical models of two service differentiation schemes for optical burst switched network: extended offset time based and PPS (Preemptive Priority Scheme) are revised. Also accordance of analytical models for those schemes is studied when complete class isolation is assumed. Furthermore authors introduce an analytical model which describes an effective degree of isolation when burst switched network employs both...
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Analysis of the image force effects on the recombination at the donor-acceptor interface in organic bulk heterojunction solar cells
PublikacjaWe consider the influence of image force effects on the recombination at the donor-acceptor interface in organic bulk heterojunction solar cells. The conclusion is that the charge carriers of one sign located in the material with lower permittivity recombine at the boundary between donor and acceptor phases. This process competes with the recombination of opposite sign charge carriers, leading to the reduction of the Langevin-type...
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Multi-headed chimera states in coupled pendula
PublikacjaWe discuss the occurrence of the chimera states in the network of coupled, excited by the clock’s mechanisms pendula. We find the patterns of multi-headed chimera states in which pendula clustered in different heads behave differently (oscillate with different frequencies) and create different types of synchronous states (complete or phase synchronization). The mathematical model of the network shows that the observed chimera states...
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Nongeminate recombination in organic bulk heterojunction solar cells: Contribution of exciton–polaron interaction
PublikacjaA new model to explain nongeminate recombination in organic bulk heterojunction solar cells is presented. We suggest that the annihilation of excitons on charge carriers at the interface between donor and acceptor phases competes with the bimolecular recombination of Coulombically bound electron–hole pairs. The exciton–polaron interaction gives visible contribution to the reduction of Langevin recombination. An analytical formula,...
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Consolidating logs in varying formats into a structured repository = konsolidacja logów w zmiennych formatach do strukturalnego repozytorium
PublikacjaDuring multi-agent systems development, testing and re- search, possibly voluminous logs are created at distributed agent loca-tions. These logs describe individual agents behavior and state changes. To get the complete picture of the multi-agent system working, it is necessary to consolidate these logs and to store them in a format appropriate for diverse analyzes. Specic issues arise during consolidation if the log formats are...
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Integrable zero-range potentials in a plane
PublikacjaWe examine general statements in the Wronskian representation of Darboux transformations for plane zero-range potentials. Such expressions naturally contain scattering problem solution. We also apply Abel theorem to Wronskians for differential equations and link it to chain equations for Darboux transforms to fix conditions for further development of the underlying distribution concept. Moutard transformations give a convenient...
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Weighted difference schemes for systems of quasilinear first order partial functional differential equations
PublikacjaThe paper deals with initial boundary value problems of the Dirichlet type for system of quasilinear functional differential equations. We investigate weighted difference methods for these problems. A complete convergence analysis of the considered difference methods is given. Nonlinear estimates of the Perron type with respect to functional variables for given functions are assumed. The proof of the stability of difference problems...
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Analysis of economical lighting of highways in the environment of SMOL language
PublikacjaThe paper puts forward and implements a method of designing and creating a modelling simulation environment for eztensive and complete analysis of economical lighting on highways. From a general design viewpoint, the proposed solution explores the concept of a network description language (SMOL), which has been designed to describe the necessary network functions, mechanisms, and devices; for the purpose of their computer simulation...
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Infinite chromatic games
PublikacjaIn the paper we introduce a new variant of the graph coloring game and a new graph parameter being the result of the new game. We study their properties and get some lower and upper bounds, exact values for complete multipartite graphs and optimal, often polynomial-time strategies for both players provided that the game is played on a graph with an odd number of vertices. At the end we show that both games, the new and the classic...
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The Concept of Geodetic Analyses of the Measurement Results Obtained by Hydrostatic Leveling
PublikacjaThe article discusses the issue of hydrostatic leveling. Its application is presented in structural health monitoring systems in order to determine vertical displacements of controlled points. Moreover, the article includes a complete computation scheme that utilizes the estimation from observation differences, allowing the elimination of the influence of individual sensors’ systematic errors. The authors suggest two concepts of...
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Zarządzanie terminowością w projektach. Wskaźniki i narzędzia
PublikacjaCzas jest istotnym elementem tzw. trójkąta projektu, dlatego też terminowość, rozu-miana, jako realizacja przedsięwzięcia w zadanym czasie, to parametr, który powinien podle-gać szczególnemu nadzorowi, a ryzyko nieterminowej realizacji powinno być wykrywane niezwłocznie. Istniejące już metody, takie jak np. wartość wypracowana (j.ang Earned Value - EV) pozwalają zaadresować te wyzwania, jednak ze względu na swoją złożoność mogą...
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Fatigue behaviour of SLM maraging steel under variable-amplitude loading
PublikacjaOne of the most challenging issues for additive manufactured materials is fatigue endurance. Engineering components often operate under complex, variable amplitude loadings, in which existing technological imperfections promote fatigue cracks growth and damage of elements eventually. In this study the effects of different variable-amplitude strain levels on fatigue life, 18Ni300 steel was tested. The work presents various behaviours...
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Rational method of grit chamber efficiency determination
PublikacjaAlthough grot chambers are designed with utmost care, they still remain difficuly to control. As concentration of grit is non-uniform, representative measurements of the sand concentration is a very complex issue. In the paper the results of measure,ents performed at WTP in Gdańsk and Gdynia were analyzed. The proposed method to determine grit chambers efficiency is based on comparison of suspension flow in the inlet and flux of...
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Applying Generative Modelling Tools to Explore Architectural Forms
PublikacjaThe digital generative methods open up new areas for exploration of formal and tectonic features, accentuate form’s ability to emerge and perform. They allow for automatic generation of variations of solutions, and digital production of “difficult” components of architectural forms using CNC technology.The paper deals with contemporary architectural explorations of complex , curvilinear surfaces in the context of generative...
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Modal parameters identification with Particle Swarm Optimization
PublikacjaThe paper presents method of the modal parameters identification based on the Particle Swarm Optimization (PSO) algorithm [1]. The basic PSO algorithm is modified in order to achieve fast convergence and low estimation error of identified parameters values. The procedure of identification as well as algorithm modifications are presented and some simple examples for the SISO systems are provided. Results are compared with the results...
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Engineering Analysis with ANSYS Software Second Edition
PublikacjaThe best way to learn complex systems is by means of hands-on experience. With an innovative and clear tutorial based approach, this powerful book provides a comprehensive introduction to the fundamental areas of engineering analysis needed on research or commercial engineering projects. With its detailed step-by-step explanations and sample problems, this book will develop the reader's understanding of FEA and their ability to...
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DBpedia and YAGO as Knowledge Base for Natural Language Based Question Answering—The Evaluation
PublikacjaThe idea of automatic question answering system has a very long history. Despite constant improvement of the systems asking questions in the natural language requires very complex solutions. In this paper the DBpedia and YAGO are evaluated as a knowledge bases for simple class 1 and 2 question answering system. For this purpose a question answering system was designed and implemented. The proposed solution and the knowledge bases...
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Does system of local government subsidisation fulfil revenue equalisation function? Evidence from Poland
PublikacjaThe article will discuss functions that should pursue general grants. One of them is revenue equalization. To achieve it after applying the mechanism of subsidising revenues should be reduced. In addition, to be completed, the size of the support should be inversely proportional to achieved own revenues. Besides the theoretical analysis, which will present the general grants structure and the ability of fulfilling revenue equalisation...
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Optical properties of daylight curable resin doped with nanodiamond powder
PublikacjaIn this paper a new material for 3D printing was elaborated on. Since diamond has very good optical properties, an idea occurred to us to apply it in 3D printing process. A mixture of nanodiamond powder and a standard 3D printing resin was created and several printouts have been completed. They have been tested for their abilities to transmit and absorb light in a wide spectrum of wavelengths. It turned out that the nanopowder...
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Comprehensive Comparison of a Few Variants of Cluster Analysis as Data Mining Tool in Supporting Environmental Management
PublikacjaA few variants of hierarchical cluster analysis (CA) as tool of assessment of multidimensional similarity in environmental dataset are compared. The dataset consisted of analytical results of determination of metals (Na, K, Ca, Sc, Fe, Co, Zn, As, Br, Rb, Mo, Sb, Cs, Ba, La, Ce, Sm, Hf and Th) in ambient air dried and kept alive, by the means of hydroponics, moss baskets collected in 12 locations on the area of Tricity (Poland)....
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Rendezvous of Heterogeneous Mobile Agents in Edge-Weighted Networks
PublikacjaWe introduce a variant of the deterministic rendezvous problem for a pair of heterogeneous agents operating in an undirected graph, which differ in the time they require to traverse particular edges of the graph. Each agent knows the complete topology of the graph and the initial positions of both agents. The agent also knows its own traversal times for all of the edges of the graph, but is unaware of the corresponding traversal...
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Rendezvous of heterogeneous mobile agents in edge-weighted networks
PublikacjaWe introduce a variant of the deterministic rendezvous problem for a pair of heterogeneous agents operating in an undirected graph, which differ in the time they require to traverse particular edges of the graph. Each agent knows the complete topology of the graph and the initial positions of both agents. The agent also knows its own traversal times for all of the edges of the graph, but is unaware of the corresponding traversal...
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Self-competence and histrionic self-presentation style
Dane BadawczeThe database contains the results from N = 2642 respondents who answered demographic questions and completed two questionnaires measuring the general self-competence and the histrionic self-presentation style. The concept of self-competence is considered as a person’s perception of their own ability to behave such that tasks are successfully completed....
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KONCEPCJA WSPÓŁPRACY SYSTEMU STRUMIENIOWEJ TRANSMISJI DANYCH CZASU RZECZYWISTEGO STRADAR Z EUROPEJSKIM SYSTEMEM EUROSUR
PublikacjaPrzedstawiono koncepcję współpracy systemów STRADAR i EUROSUR, w celu wymiany informacji związanych z ochroną granic UE. Opisano cechy zrealizowanego demonstratora STRADAR i zasady komunikacji oraz bezpieczeństwa wymiany informacji w systemie EUROSUR. Opisano warianty wymiany infor-macji pomiędzy systemami STRADAR i EUROSUR, od najprostszych, możliwych do zastosowania w obecnej wersji STRADAR, do zautomatyzowanych, wymagających...
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Applicability of phenolic acids as effective enhancers of cocrystals solubility of methylxanthines
PublikacjaApplicability of phenolic acids as potential cocrystal formers for methylxanthine derivatives was analyzed both in terms of cocrystallization probabilities and solubility advantage. The cocrystal formation abilities were evaluated using mixing enthalpy estimated within the conductor like screening model for real solvents (COSMO-RS) framework. The solubility improvement of potential cocrystals was estimated by formulation of the...
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Synthesis of 5-Substituted 1H-Tetrazoles from Nitriles in the Presence of Heterogeneous Catalyst
PublikacjaTetrazoles are five-membered heterocyclic compounds containing in their rings four nitrogen atoms. They have wide applications as corrosion inhibitors, analytical reagents, high-energy materials and gas generating compositions. Tetrazoles also play important role in coordination chemistry as ligands and in medicinal chemistry as metabolically stable surrogates for carboxylic acids. In recent years, investigation of new method of...
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Local Structure and Stability of SEI in Graphite and ZFO Electrodes Probed by As K-edge Absorption Spectroscopy
PublikacjaThe evolution of the solid electrolyte interphase (SEI) during the first Li uptake in advanced Li-ion electrodes is studied by X-ray absorption spectroscopy (XAS). The As atoms present in the electrolyte solution were used as a local probe for monitoring the SEI growth on different electrodes. High-quality As K-edge spectra were collected in fluorescence mode for a set of graphite and carbon-coated ZnFe2O4 electrodes. XAS measurements...
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Interplay between Aryl···Perfluoroaryl and Hydrogen Bonding Interactions in Cocrystals of Pentafluorophenol with Molecules of Trigonal Symmetry
PublikacjaCocrystals of seven star-shaped triaryl compounds with pentafluorophenol (pfp) were prepared and structurally characterized by the single-crystal X-ray diffraction method. Cocrystallization of pfp with planar (or almost planar) compounds gave six 3:1 molecular complexes with well-defined layered structures. The layers are composed of alternating pfp3 trimers, linked by hydrogen bonding, and triaryl molecules held together in planes...
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Tailoring optical constants of few-layer black phosphorus coatings: Spectroscopic ellipsometry approach supported by ab-initio simulation
Publikacja2D black phosphorus (BP) has attracted extensive attention as an anisotropic platform for novel optoelectronic and polarizing optics applications. Insight into the factors that tune the optical and polarizing properties of 2D BP reveals their essential influence on BP-based photonic and optoelectronic devices. In this work, studies of the optical constants of few-layer black phosphorus coatings are studied and discussed, with particular...
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New bis(azobenzocrown)s with dodecylmethylmalonyl linkers as ionophores for sodium selective potentiometric sensors
PublikacjaNovel biscrowns 1 and 2 were synthesized from 13-membered azobenzocrown ethers containing bromoalkylenoxy chains in para position relative to the azo group. The synthesized diester molecules are dodecylmethylmalonic acid derivatives differing by the linker length. The synthesized compounds have the potential of being used as sodium ionophores in ion-selective electrodes. They were characterized and used as ionophores in classic...
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Testing Situation Awareness Network for the Electrical Power Infrastructure
PublikacjaThe contemporary electrical power infrastructure is exposed to new types of threats. The cause of such threats is related to the large number of new vulnerabilities and architectural weaknesses introduced by the extensive use of Information and Communication Technologies (ICT) in such complex critical systems. The power grid interconnection with the Internet exposes the grid to new types of attacks, such as Advanced Persistent...
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A new approach to determination of the two-mass model parameters of railway current collector
PublikacjaThe paper presents two mathematical models of railway current collectors both with two degrees of freedom. The first one, hereinafter Pantograph Articulated Model (PAM), has one degree of freedom in rotational motion and the second degree of freedom in translational motion. The second model, called henceforth as Pantograph Reference Model (PRM), has both degrees of freedom in translational motion. Differential equations of the...