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Search results for: DIRECT DIGITAL SYNTHESIS
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Analysis and synthesis of structural system dimensional deviations
PublicationBłedne zasady określania dopuszczalnych odchyłek wymiarowych stalowych elementów konstrukcyjnych lub wręcz ich brak często powodują trudności w czasie montażu konstrukcji. W każdym układzie konstrukcyjnym można wyróżnić tzw. Koordynacyjne Wymiary Montażowe (KWM). Odchyłki wymiarowe (tolerancje) KWM decydują o zachowaniu poprawnej geometrii ustroju budowlanego po jego zamontowaniu na placu budowy. KWM tworzą zamknięte ciągi wymiarowe,...
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Synthesis of parametric images in the medical active thermography
PublicationArtykuł przedstawia zastosowanie nowej metody syntezy obrazów w termografii dla potrzeb opisu ilościowego właściwości termicznych tkanek. opis taki umożliwia różnicowanie przypadków medycznych. Metodę zastosowania dla licznych pomiarów fantomowych oraz in vitro. Przedstawiono i omówiono rezultaty prac.
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New chromogenic azothiacrown ethers - synthesis and properties
PublicationOtrzymano nowe chromogeniczne chromojonofory z atomami siarki i dwiema grupami azowymi w makrocyklu. Związki te zastosowano w membranowych elektrodach jonoselektywnych i badano właściwości elektrod w stosunku do jonów metali alkalicznych i przejściowych. Kompleksowanie azotiakoron z jonami metali badano też w układzie dioksan-woda (1:1) metodami spektroskopowymi. Oznaczono stałe trwałości kompleksów miedzi i srebra. W przeciwieństwie...
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Chromogenic Macrocyclic Derivatives of Azoles - Synthesis and Properties
PublicationOpisano syntezę makrocyklicznych azokoron zawierających resztę pirolu i imi-dazolu w makropierścieniu. Zbadano zdolność kompleksowania kationów metaliprzez otrzymane związki makrocykliczne przy pomocy spektrofotometrii UV-Visw acetonitrylu. Zbadano także właściwości jonoforowe związków w membranowychelektrodach jonoselektywnych. Ustalono strukturę krystalograficzną 18-czło-nowej pochodnej pirolu.
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Acylic congener of cucurbituril: synthesis and recognition properties.
PublicationZaprezentowano syntezę analogów acyklicznych cucurbiturilu oraz ich zdolności do kompleksowania wybranych 16 amin, dioli, kwasów dikarboksylowych, pochodnych guanidyny oraz pirydyny. Obserwowane tworzenie kompleksów przebiegało około 180 razy słabiej niż dla cucurbiturilu. Wyniki te świadczą o potencjalnych możliwościach zbliżonych do analogów cyklicznych pod względem tworzenia kompleksów i rozpoznawania wyżej wymienionych...
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New approach for the synthesis of Ag3PO4-graphene photocatalysts
PublicationA facile and effective plasma sputtering method for the preparation of a visible light active photocatalyst - rhombic dodecahedral silver phosphate Ag3PO4 covered with nanographene (Ag3PO4-GR) with improved stability has been developed. Proposed method allows for the usage of readily available materials for nanographene sputtering and for easy scaling-up. The stability improvement, confirmed by visible light-induced phenol degradation...
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Electrochemically Induced Synthesis of Triphenylamine-based Polyhydrazones
PublicationTriphenylamine-based hydrazones were subjected to electropolymerization process that gave well conductive hydrazone based polymers. The first example of polyhydrazone formation during the electrochemical process was shown. The estimation of polymer structure was demonstrated using IR spectroelectrochemistry. The EPR spectroelectrochemistry allowed to explain why in some cases dimer couldn’t be formed. The results of electrochemical,...
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Ag modified ZnO microsphere synthesis for efficient sonophotocatalytic degradation of organic pollutants and CO2 conversion
PublicationThe synthesis and design of non-precious and efficient sonophotocatalyts by an environment friendly technique are requisites for solar energy conversion and environmental remediation. This work reports the preparation of Ag/ZnO microspheres with different Ag contents through deposition–precipitation method for pollutant degradation and CO2 conversion. Detail structural investigation reveals that ZnO microspheres and Ag-ZnO microspheres...
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Ribes nigrum L. Extract-Mediated Green Synthesis and Antibacterial Action Mechanisms of Silver Nanoparticles
PublicationSilver nanoparticles (Ag NPs) represent one of the most widely employed metal-based engineered nanomaterials with a broad range of applications in different areas of science. Plant extracts (PEs) serve as green reducing and coating agents and can be exploited for the generation of Ag NPs. In this study, the phytochemical composition of ethanolic extract of black currant (Ribes nigrum) leaves was determined. The main components...
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A Canonical Switched Capacitor DC-DC Converter. A look at how the historical SC synthesis problem is getting solved
PublicationWe reconsider a solution to the historical problem in switched capacitor (SC) DC-DC converter synthesis. Specifically, we retackle the problem of constructing an SC twophase network realizing arbitrary voltage conversion ratio within rational bounds defined. Theoretical foundations are available in our earlier research [3] where a nonconstructive proof of existence was given. We briefly review and comment on known circuit solutions...
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Synthesis and properties of porous Sr 0.96 Y 0.04 Ti 1−x Nb x O 3
PublicationA series of porous, single phase Sr0.96Y0.04Ti1-xNbxO3 samples was obtained using a wet synthesis method (modified citrate sol-gel) method. Temperature-programmed reduction (TPR) and temperature-programmed oxidation (TPO) measurements have shown high stability of the obtained material in variable (oxidizing/reducing) atmospheres. All samples exhibit high conductivity in hydrogen atmosphere with the highest value (around 1S/cm)...
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Direct conversion of secondary phosphine oxides and H-phosphinates with [di(acyloxy)iodo]benzenes to phosphinic and phosphonic amides
PublicationW publikacji przedstawiono metodę pozwalająca na bezpośrednie otrzymywanie amidów kwasu fosfinowego i fosfonowego w reakcji drugorzędowych tlenków fosfin lub H-fosfinianów z [di(acyloksy)iodo]benzenami w obecności amin pierwszo lub drugorzędowych. Wykorzytując silne acylujące właściwości układu [di(acyloksy)iodo]benzen/R2P(O)H.
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Prediction of pile shaft capacity in tension based on some direct CPT methods – Vistula Marshland test site
PublicationThis paper presents different CPT methodologies for the prediction of the pile shaft resistance in tension on the example of three reference screw piles of the Jazowa test site in Poland. The shaft capacity was estimated based on the cone resistance, sleeve friction and CPT excess pore water pressure. Three piles with a diameter of 0.4 m and the length...
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Direct Current Atmospheric Pressure Microdischarge Generated between a Miniature Flow Helium Microjet and a Flowing Liquid Cathode
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A comparison of McGrath MAC® and standard direct laryngoscopy in simulated immobilized cervical spine pediatric intubation: a manikin study
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Determination of EC50 toxicity data of selected heavy metals toward heterocypris incongruens and their comparison to "direct-contact" and microbiotests
PublicationW artykule omówiono czułość organizmu Heterocypris incongruens wobec metali ciężkich. Pomimo iż test Ostracodtoxkit F jest dostępny hadlowo na rynku od wielu lat to brak jest danych na temat czułości i selektywności tego organizmu, a dane na ten temat są niezbędne podczas interpretowania wyników oznaczeń toksyczności chronicznej próbek gleb i osadów. Wyniki LC50 oraz EC50 zostały też porównane z danymi innych handlowo dostępnych...
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A pilot study to assess an in-process inspection method for small diameter holes produced by Direct Metal Laser Sintering
PublicationPurpose The purpose of this research is to evaluate the geometric quality of small diameter holes in parts printed by DMLS technology. An in-process optical inspection method is proposed and assessed during a pilot study. The influence of the theoretical hole diameter assumed in a CAD system and the sample thickness (hole length) on the hole clearance was analysed. Design/methodology/approach The samples made of two different...
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Poly(3,4-ethynenedioxythiophene)-Prussian Blue hybrid material evidence of direct chemical interaction betwenn PB andpEDOT
PublicationPrzedstawiono syntezę materiału złożonego z poli(3,4-etylenodioksytiofenu) oraz analogu błękitu pruskiego. Sieć struktury BP utworzona została wewnątrz matrycy polimerowej pEDOT-u za pomocą metody polaryzacji multicyklicznej. Chemiczne oddziaływania Fe z BP oraz siarki z pEDOT zostały potwierdzone metodą XPS. Obecność BP potwierdzono FTiR - stwierdzono obecność drgań rozciągających Fe-C oraz Fe-N. Metoda cyklowoltamperometryczna...
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Prediction of Pile Shaft Capacity in Tension Based on Some Direct CPT Methods—Vistula Marshland Test Site
PublicationThis paper presents different CPT methodologies for the prediction of the pile shaft resistance in tension on the example of three reference screw piles of the Jazowa test site in Poland. The shaft capacity was estimated based on the cone resistance, sleeve friction and CPT excess pore water pressure. Three piles with diameter 0.4 m and the length varied from 8 m to 14.6 m were subjected to static load tests in tension. Their...
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One-Step Synthesis of W/O and O/W Emulsifiers in the Presence of Surface Active Agents
PublicationThe main goal of this study was to describe the method of the synthesis of the dodecyl-, tetradecyl-, hexadecyl- and octadecyl-propylene glycol emulsifiers in the presence of selected anionic and nonionic surfactants. Acyl propylene glycol emulsifiers were produced by esterification of propane-1,2-diol (propylene glycol, PG) with C12:0-C18:0 fatty acids in the presence of anionic sodium dodecyl sulfate (SDS) and nonionic-poly(ethylene...
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Synthesis, Characterization and Biological Investigations of Half-Sandwich Ruthenium(II) Complexes Containing Benzimidazole Moiety
PublicationHalf-sandwich Ru(II) complexes belong to group of biologically active metallo-compounds with promising antimicrobial and anticancer activity. Herein, we report the synthesis and characteri- zation of arene ruthenium complexes containing benzimidazole moiety, namely, [(η6-p-cymene)RuC l(bimCOO)] (1) and [(η6-p-cymene)RuCl2(bim)] (2) (where bimCOO = benzimidazole-2-carboxylate and bim = 1-H-benzimidazole). The compounds were characterized...
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In silico assessment and sonochemical synthesis of 2-alkynyl 3-chloropyrazines as prospective ligands for SARS-CoV-2
PublicationThe recent global pandemic caused by COVID-19 has triggered an intense effort worldwide towards the development of an effective cure for this disease. In our effort we have explored the 2-alkynyl substituted 3-chloropyrazine framework as a potential template for the design of molecules for this purpose. Our strategy was supported by the in silico studies of representative compounds to assess their binding affinities via docking...
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Synthesis and biological evaluation of N-acylated tyramine sulfamates containing C-F bonds as steroid sulfatase inhibitors
PublicationSteroid sulfatase (STS) is responsible for the hydrolysis of biologically inactive sulfated steroids into their active un-sulfated forms and promotes the growth of various hormone-dependent cancers (e.g., breast cancer). Therefore, the STS enzyme is a promising therapeutic target for the treatment of steroid-sensitive cancers. Herein, we report the synthesis and biological evaluation of sulfamate analogs as potential STS inhibitors...
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Design, Synthesis, and Enzymatic Evaluation of Novel ZnO Quantum Dot-Based Assay for Detection of Proteinase 3 Activity
PublicationHerein, the synthesis and application of functionalized quantum dot-based protease probes is described. Such probes are composed of nontoxic ZnO nanocrystals decorated by amino groups followed by linker and labeled peptide attachment. Spherical NH2-terminated ZnO quantum dots (QDs) with the average size ranging from 4 to 8 nm and strong emission centered at 530 nm were prepared using the sol−gel method. The fluorescence of ZnO...
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A new and convenient method for the preparation of functionalized phosphorothioates
PublicationA new and efficient method for the synthesis of alkyl and aryl phosphorothioates in high yields via the reaction of (5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorin-2-yl)disulfanyl derivatives with trimethyl phosphite was developed.
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An Eye Tracking Based Examination of Visual Attention During Pairwise Comparisons of a Digital Product’s Package
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Applying Hidden Markov Models to Visual Activity Analysis for Simple Digital Control Panel Operations
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Non-destructive testing of industrial structures with the use of multi-camera Digital Image Correlation method
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Assessment of Citizens’ Actions against Light Pollution with Guidelines for Future Initiatives
PublicationDue to the wide reach of media reports about scientific research and technological tools such as the world wide web (WWW), the Internet, and web browsers, citizens today have access to factual information about the negative impact of artificial light at night (ALAN) on their dark skies, and their health and well-being. This means they can now make educated decisions and take the necessary steps to help protect themselves and their...
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A Novel Method for the Deblurring of Photogrammetric Images Using Conditional Generative Adversarial Networks
PublicationThe visual data acquisition from small unmanned aerial vehicles (UAVs) may encounter a situation in which blur appears on the images. Image blurring caused by camera motion during exposure significantly impacts the images interpretation quality and consequently the quality of photogrammetric products. On blurred images, it is difficult to visually locate ground control points, and the number of identified feature points decreases...
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The method of analysis of damage reinforced concrete beams using terrestial laser scanning
PublicationThe authors present an analysis of the possibility to assess deformations and mechanisms of destructing bent reinforced concrete beams using the terrestrial laser scanning. As part of the experiments carried out at the Regional Laboratory of Construction of the Concrete Structures Division of the Civil and Environmental Engineering Faculty at Gdansk University of Technology, the reinforced concrete beams were subjected to destruction...
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REALIZACJA ELEMENTÓW SKŁADOWYCH ŁĄCZA RADIOWEGO Z UŻYCIEM URZĄDZEŃ RADIA PROGRAMOWALNEGO TYPU USRP
PublicationPrzez ostatnią dekadę projektowanie systemów radiowych zaczęło w coraz większym stopniu polegać na cyfrowym przetwarzaniu sygnałów. Możliwość i moc obliczeniowa procesorów ogólnego przeznaczenia GPP (General Purpose Processor), procesorów sygnałowych DSP (Digital Signal Processor) oraz układów programowalnych FPGA (Field Programmable Gate Array) znacząco wzrosła zgodnie z prawem Moor’a. Naturalnym następstwem tego trendu było większe...
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I love to write and create. Can I earn money doing it? Entrepreneurial process of bloggers
PublicationNew technologies and a new way of looking at the life of future generations, open up new perspectives of entrepreneurial activities. One of them is to run a blog. Although the first blogs appeared many years ago and earning money from running them is also known to bloggers, little research is devoted to this form of entrepreneurship. The analysis of this phenomenon was carried out using the netnography method, which is not common...
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Novel Cast Polyurethanes Obtained by Using Reactive Phosphorus-Containing Polyol: Synthesis, Thermal Analysis and Combustion Behaviors
PublicationPhosphorus-containing polyol applications in polyurethane synthesis can prevent volatilization of flame retardants and their migration on the surface of a material. In this work, novel cast polyurethanes were prepared by a one-step method with the use of different amounts of phosphorus-containing polyol, 4,4′–diphenylmethane diisocyanate and 1,4-butanediol. The chemical structure, thermal, physicochemical and mechanical properties...
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Two-step synthesis of niobium doped Na–Ca–(Mg)–P–Si–O glasses
PublicationNiobium doped biosolubility glasses in the Na–Ca–(Mg)–P–Si–O system were prepared by using an untypical two-step synthesis route. The parent glass was melted in air atmosphere at 1350 °C followed by re-melting the glass in Nb crucible with the addition of metallic Mg/Ca powder in the nitrogen atmosphere. The second melting step was carried out at 1450–1650 °C, using an induction furnace. The topography and structure of the obtained...
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The pulsed laser ablation synthesis of colloidal iron oxide nanoparticles for the enhancement of TiO2 nanotubes photo-activity
PublicationThe rapid, only a few minutes long synthesis of FeO, Fe3O4, and Fe2O3nanoparticles mixture utilizing the pulsedlaser ablation using simply pure iron target and water was demonstrated. The size and crystal phase of Fe-basedNPs were characterized using DLS and HR-TEM techniques, respectively. The metastable suspension of FeO,Fe3O4, and Fe2O3nanoparticles was used to the decoration of anodized TiO2nanotubes (TiO2-NTs) by means ofthe...
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Synthesis and steroid sulfatase inhibitory activities of N-phosphorylated 3-(4-aminophenyl)-coumarin-7-O-sulfamates
PublicationIn the present work, we report convenient methods for the synthesis and biological evaluation of N-phosphorylated derivatives of 3-(4-aminophenyl)-coumarin-7-O-sulfamate as potential steroid sulfatase (STS) inhibitors. Their binding modes were modeled using docking techniques. The inhibitory effects of the synthesized compounds were tested on STS isolated from human placenta. All of the newly synthesised coumarin derivatives were...
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Novel 1,2,3-Triazole Derivatives as Mimics of Steroidal System—Synthesis, Crystal Structures Determination, Hirshfeld Surfaces Analysis and Molecular Docking
PublicationHerein, we present the synthesis and crystal structures determination of five 4-(1-phenyl-1H-1,2,3-triazol-4-yl)phenol derivatives containing halogen atoms, 6a–e, which may be used as an excellent mimic of steroids in the drug development process. Good quality crystals obtained for all of the synthesized compounds allowed the analysis of their molecular structures. Subsequently, the determined crystal structures were used to calculate...
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Structural, electrical, and magnetic study of La-, Eu-, and Er- doped bismuth ferrite nanomaterials obtained by solution combustion synthesis
PublicationIn this work, the multiferroic bismuth ferrite materials Bi0.9RE0.1FeO3 doped by rare-earth (RE = La, Eu, and Er) elements were obtained by the solution combustion synthesis. Structure, electrical, and magnetic properties of prepared samples were investigated by X-ray photoelectron spectroscopy, Mössbauer spectroscopy, electrical hysteresis measurement, broadband dielectric spectroscopy, and SQUID magnetometry. All obtained nanomaterials...
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Evaluation of Nanoporous Carbon Synthesized from Direct Carbonization of a Metal–Organic Complex as a Highly Effective Dye Adsorbent and Supercapacitor
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Comparison of sono-direct and sono-alternate current electro-coagulation processes for removal of color and turbidity from domestic wastewater
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Particulate Emissions from European Vehicles Featuring Direct Injection Spark Ignition Engines Tested Under Laboratory Conditions
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Neutrocyte-to-lymphocyte ratio predicts the presence of a replicative hepatitis C virus strand after therapy with direct-acting antivirals
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Direct measurements of odorous volatile organic compounds present in biosolids cakes by Proton Transfer Reaction – Mass Spectrometry Technique
PublicationThis paper show the results of investigation of concentration of odorous chemical compounds emitted upon ageing of anaerobically stabilised biosolids that could contribute to the overall odour character of nuisance emissions. Biosolids samples from wastewater treatment plant were collected in spring time. Concentrations of volatile organic compounds using a US EPA flux hood and Proton Transfer Reaction-Time of Flight-Mass Spectrometry...
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Design and Synthesis of NTU-9/C3N4 Photocatalysts: Effects of NTU-9 Content and Composite Preparation Method
PublicationHybrid materials based on graphitic carbon nitride (g-C3N4) and NTU-9 metal–organic frameworks (MOF) were designed and prepared via solvothermal synthesis and calcination in air. The as-prepared photocatalysts were subsequently characterized using Brunauer–Emmett–Teller (BET) analysis, UV-Vis diffuse reflectance spectroscopy (DRS), photoluminescence (PL) emission spectroscopy, X-ray diffraction (XRD), X-ray photoelectron spectroscopy...
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Synthesis of some optically active terpenoid-derived thioamides
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Heterogeneity of ingot of the fused iron catalyst for ammonia synthesis
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Investigation of manganese-doped iron ammonia synthesis catalysts
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Wustite based iron-cobalt catalyst for ammonia synthesis
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CdS Nanocrystallines: Synthesis, Structure and Nonlinear Optical Properties
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