Search results for: MILLING PROCESS
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Comparative X-ray diffraction and Mössbauer spectroscopy studies of BiFeO3 ceramics prepared by conventional solid-state reaction and mechanical activation
PublicationThe aim of this work was to prepare BiFeO3 by modified solid-state sintering and mechanical activation processes and to investigate the structure and hyperfine interactions of the material. X-ray diffraction and Mössbauer spectroscopy were applied as complementary methods. In the case of sintering, BiFeO3 phase was obtained from the mixture of precursors with 3 and 5 % excess of Bi2O3 during heating at 1023 K. Small amounts of...
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Mg2+ Doping Effects on the Structural and Dielectric Properties of CaCu3Ti4O12 Ceramics Obtained by Mechanochemical Synthesis
PublicationIn this study, ceramic CaCu3Ti4O12 (CCTO) and CaCu3−xMgxTi4O12 solid solutions in which 0.1 ≤ x ≤ 0.5 were prepared by the mechanochemical method, realized by a high‐energy ball milling technique. The effects of the Mg2+ ion concentration and sintering time on the dielectric response in the prepared ceramics were investigated and discussed. It was demonstrated that, by the use of a sufficiently high energy of mechanochemical treatment,...
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A Surveillance Of Dynamic Processes in Selected Mechatronic Systems
PublicationThe paper concerns development of original method of optimal control at energy performance index and its application to dynamic processes surveillance of some mechatronic systems. The latter concerns chatter vibration surveillance during highspeed slender milling of rigid details, as well as motion control of two-wheeled mobile platform. Results of on-line computer simulations and real performance on the target objects reflect...
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Nanotechnologies in Development of Structural Materials and Biomaterials
PublicationThe nanometric materials and technologies resulted in nanostructures are reviewed. The examples of nanomaterials are shown. The typical nanotechnologies, including plastic deformation, mechanical attrition, controlled detonation, hot plasma jet synthesis, laser vaporisation, CVD and PVD, mechanical milling, annealing, ultrasonic irradiation, nanolithography, electrocrystallisation, electrospinning, sol-gel method, cryogenic laser-enhanced...
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Fourier-transform infrared spectroscopy (FTIR) spectra of bulk boron and borophene flakes
Open Research DataThese data contain Fourier-transform infrared spectroscopy (FTIR) spectra of bulk boron and borophene flakes obtained during ball milling (450 rpm, 6 h, 1 g). Spectra were acquired to investigate the chemical bonds and functional groups on the surface of the pristine boron and borophene flakes.
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Chemical properties of bismuth telluride – carbon composites.
Open Research DataCarbon nanotubes and amorphous carbon have been introduced into bismuth telluride matrix (in 0.15 and 0.30 wt % ratio) in order to investigate influence of carbon on composite’s thermoelectric properties. Composites with well-dispersed additives have been obtained by sonication and ball-milling. Chemical composition of materials was confirmed by XPS...
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X-ray diffractometry results of the SrTi0.50Fe0.50O3-d powder
Open Research DataThis dataset contains results of X-ray diffractometry mesurement (XRD) of the SrTi0.50Fe0.50O3-d (STF50) powder after ball milling. The phase composition of the investigated STF50 powder was analyzed by XRD at room temperature. The X-ray diffractometry (XRD) technique was used to determine the phase composition of the fabricated powder. Measurements...
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X-ray diffractometry results of the SrTi0.35Fe0.65O3-d powder
Open Research DataThis dataset contains results of X-ray diffractometry mesurement (XRD) of the SrTi0.35Fe0.65O3-d (STF35) powder after ball milling. The phase composition of the investigated STF35 powder was analyzed by XRD at room temperature. The X-ray diffractometry (XRD) technique was used to determine the phase composition of the fabricated powder. Measurements...
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X-ray diffractometry results of the SrTi0.30Fe0.70O3-d powder
Open Research DataThis dataset contains results of X-ray diffractometry mesurement (XRD) of the SrTi0.30Fe0.70O3-d (STF70) powder after ball milling. The phase composition of the investigated STF70 powder was analyzed by XRD at room temperature. The X-ray diffractometry (XRD) technique was used to determine the phase composition of the fabricated powder. Measurements...
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A modified method of vibration surveillance by using the optimal control at energy performance index
PublicationA method of vibration surveillance by using the optimal control at energy performance index has been creatively modified. The suggested original modification depends on consideration of direct relationship between the measured acceleration signal and the optimal control command. The paper presents the results of experiments and Hardware- in-the-loop simulations of a new active vibration reduction algorithm based on the energy...
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Structure and thermoelectric properties of Cs-Bi-Te alloys fabricated by different routes of reduction of oxide reagents
PublicationCesium-bismuth-telluride polycrystalline materials were fabricated using a cost-effective method based on a reduction of oxide reagents, leading to a production of a material with good thermoelectric properties. Several samples with various initial stoichiometry were prepared by melting of oxide powders at 1050 °C, quenching, milling to powders and then reducing in pure hydrogen at 400 °C. Another concept was to obtain the CsBi4Te6...
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The effect of thermal modification on the quality of the milled surface of beech and pine wood
PublicationThe article deals with the effect of thermal modification on the quality of the created surface during milling on CNC milling cutters. The quality of the created surface is evaluated based on surface roughness, specifically its roughness parameter Ra. The observed surface is created by a shank cutter with a diameter of 20 mm and three cutting edges in a spiral at a standard speed of 18,000. min-1. The article compares thermally...
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Tetrahedrally modified MnMe0.1Co1.9O4 (Me = Zn, Mg, Li) spinels for non-enzymatic glucose sensing
PublicationIn this work, tetrahedrally modified MnMe0.1Co1.9O4 (Me = Zn, Mg, Li) spinels were prepared via the sol–gel synthesis method with subsequent ball-milling fragmentation. The prepared samples were evaluated as glucose–sensing catalyst. The reference MnCo2O4 spinel exhibited a sensitivity of 49 µA mM−1 cm−2 and a nonlinearity error of 5.2% in the response range from 0.02 to 1 mM. The partial substitution of cobalt in the reference...
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Structure and thermoelectric properties of bismuth telluride—Carbon composites
PublicationCarbon nanotubes and amorphous carbon have been introduced into a bismuth telluride matrix (0.15 and 0.30 wt.% ratio) to investigate the influence of the carbon on the composite’s thermoelectric properties. Composites with well-dispersed additives have been obtained by sonication and ball-milling methodology. Carbon nanotubes and an amorphous carbon addition led to a decrease in electric conductivity from 1120 S/cm to 77 S/cm....
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Solvent-Free Synthesis of Phosphonic Graphene Derivative and Its Application in Mercury Ions Adsorption
PublicationFunctionalized graphene was efficiently prepared through ball-milling of graphite in the presence of dry ice. In this way, oxygen functional groups were introduced into material. The material was further chemically functionalized to produce graphene derivative with phosphonic groups. The obtained materials were characterized by spectroscopic and microscopic methods, along with thermogravimetric analysis. The newly developed material...
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Robotics in architectural education
PublicationRobotics rapidly is becoming an important part of architectural design at all stages, from early conceptual work to construction. In this article is presented the present state of the art in the field related to architectural education, from computer numerical control (CNC) milling tools, through drones to multi-axis robotic arms. Professionals involved in modern design techniques often use them to create precise, complex forms...
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Fatigue life improvement using low transformation temperature weld material with measurement of residual stress
PublicationWelding processes often produce high levels of tensile residual stress. Low transformation temperature (LTT) welding wires utilise phase transformation strains to overcome the thermal contraction of a cooling weld. In this paper, the residual stress within each weld was quantified using the milling/strain gauge method, being the strain change measured as the weldment was milled away. The fatigue tests were conducted under uniaxial...
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Corrigendum to “Fatigue life improvement using low transformation temperature weld material with measurement of residual stress” [Int. J. Fatigue 164 (2022) 107137]
PublicationWelding processes often produce high levels of tensile residual stress. Low transformation temperature (LTT) welding wires utilise phase transformation strains to overcome the thermal contraction of a cooling weld. In this paper, the residual stress within each weld was quantified using the milling/strain gauge method, being the strain change measured as the weldment was milled away. The fatigue tests were conducted under uniaxial...
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Effect of sintering temperature on electrochemical performance of porous SrTi1-xFexO3-δ (x = 0.35, 0.5, 0.7) oxygen electrodes for solid oxide cells
PublicationThis work evaluates the effects of the sintering temperature (800 °C, 900 °C, 1000 °C) of SrTi1-xFexO3-δ (x = 0.35, 0.5, 0.7) porous electrodes on their electrochemical performance as potential oxygen electrode materials of solid oxide cells. The materials were prepared by a solid-state reaction method and revealed the expected cubic perovskite structure. After milling, the powders were characterised by a sub-micrometre particle...
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Styrene-Butadiene Rubber/Modified Ground Tire Rubber Blends Co-Vulcanization: Effect of Accelerator Type
PublicationGround tire rubber was thermo-mechanically modified with using a co-rotating twin screw extruder. Modification of GTR was conducted in autothermal conditions. Styrene-butadiene rubber and modified ground tire rubber blends were prepared via two-roll milling. Obtained compounds were cured with conventional system (sulfur/vulcanization accelerator ratio was 2:1). During this research three commonly vulcanization accelerators (MBT,...
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The Use of Direct Shear Test for Optimization of Interlayer Bonding Under a Poroelastic Layer
PublicationPoroelastic Road Surfaces (PERS) are characterised by porous structure with air void content of 20% or higher and stiffness almost 10 times lower than that of a standard asphalt course. Such properties enable noise reduction by up to 12 dB in comparison to SMA 11 mixture. However, the disadvantage of a poroelastic pavement is its low durability, which partially results from delamination from the lower layer. The paper aims to investigate...
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Porosity and shape of airborne wear microparticles generated by sliding contact between a low-metallic friction material and a cast iron
PublicationThe wear of brakes in transport vehicles is one of the main anthropogenic sources of airborne particulate matter in urban environments. The present study deals with the characterisation of airborne wear microparticles from a low-metallic friction material / cast iron pair used in car brakes. Particles were generated by a pin-on-disc machine in a sealed chamber at sliding velocity of 1.3 m/s and contact pressure of 1.5 MPa. They...
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D.C. electrical measurements of Bi2VO5.5 ceramic measured at high temperature region
Open Research DataD.C. electrical properties of Bi2VO5.5 ceramic was measured.
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Thermo-oxidative exfoliation of carbon black from ground tire rubber as potential reinforcement in green tires
PublicationConsidering the balance between rapidly growing global tire demand and scarcity of natural resources, recycling and reclaiming techniques of tire rubber have become the state of the art. Herein, we set out to implement a self-designed thermo-oxidative reactor for the exfoliation of carbon black (CB) from ground tire rubber, which is efficiently functioned under a thermo-oxidative reclaiming condition without any additive. The exfoliation...
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Linear impedance of Bi2VO5.5 ceramic of thickness 2.88 mm measured with impedance spectroscopy method at low temperature region
Open Research DataThe linear electrical properties of Bi2VO5.5 ceramic of thickness 2.88 mm was measured by impedance spectroscopy method.
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Linear impedance of Bi2VO5.5 ceramic of thickness 2.52 mm measured with impedance spectroscopy method at low temperature region
Open Research DataThe linear electrical properties of Bi2VO5.5 ceramic of thickness 2.52 mm was measured by impedance spectroscopy method.
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Selected Aspects of 3D Printing for Emergency Replacement of Structural Elements
PublicationThe paper presents a synthetic characterization of modern methods of manufacturing or regenerating machine elements. Considered methods are machining and additive methods, in particular 3D printing in the FDM/FFF technique. For the study, the authors made samples of the holder bracket using selected methods. Samples made by machining operations, 3D printing with various filling were tested. The paper contains a technical and economic...
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Numerical and experimental investigation of guided ultrasonic wave propagation in non-uniform plates with structural phase variations
PublicationThe article presents the results of numerical and experimental investigations of guided wave propagation in aluminum plates with variable thickness. The shapes of plate surfaces have been specially designed and manufactured using a CNC milling machine. The shapes of the plates were defined by sinusoidal functions varying in phase shift, which forced the changes in thickness variability alongside the propagation path. The main aim...
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The Effect of Surface Treatment with Isocyanate and Aromatic Carbodiimide of Thermally Expanded Vermiculite Used as a Functional Filler for Polylactide-Based Composites
PublicationIn this work, thermally expanded vermiculite (TE-VMT) was surface modified and used as a filler for composites with a polylactide (PLA) matrix. Modification of vermiculite was realized by simultaneous ball milling with the presence of two PLA chain extenders, aromatic carbodiimide (KI), and 4,4’-methylenebis(phenyl isocyanate) (MDI). In addition to analyzing the particle size of the filler subjected to processing, the efficiency...
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The topography of Bi2VO5.5 ceramic measured with SEM and confocal microscope
Open Research DataThe topography of Bi2VO5.5 ceramics was measured by SEM and confocal microscope.
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Linear impedance of as-quenched 40Bi2VO5.5-60SrB4O7 glass measured with impedance spectroscopy method at low temperature region
Open Research DataThe linear electrcial properties of 40Bi2VO5.5-60SrB4O7 glass was measured by impedance spectroscopy method.
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Linear impedance of Bi2VO5.5 ceramic prepared by traditional melt quenching technique measured with impedance spectroscopy method at low temperature region
Open Research DataThe linear electrical properties of Bi2VO5.5 ceramic prepared by traditional melt quenching technique was measured by impedance spectroscopy method.
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Linear impedance of 50Bi2VO5.5-50SrB4O7 glass measured with impedance spectroscopy method at low temperature region
Open Research DataThe linear electrcial properties of 50Bi2VO5.5-50SrB4O7 glass was measured by impedance spectroscopy method.
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A newly-developed model for predicting cutting power during wood sawing with circular saw blades
PublicationIn the classical approach, cutting forces and cutting power in sawing processes of orthotropic materials such as wood are generally calculated on the basis of the specific cutting resistance kc (cutting force per unit area of cut). For every type of sawing kinematics (frame saws, band saws and circular sawing machines) different empirical values of specific cutting resistance kc have to be applied. It should be emphasised that...
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The topography of as-quenched and heat treated 50(2Bi2O3-V2O5)-50SrB4O7 and 50Bi2VO5.5-50SrB4O7 glasses measured with confocal microscope
Open Research DataThe topography of as-quenched and heat treated 50(2Bi2O3-V2O5)-50SrB4O7 and 50Bi2VO5.5-50SrB4O7 glasses measured with confocal microscope.
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The topography of as-quenched and heat treated 50(2Bi2O3-V2O5)-50SrB4O7 and 50Bi2VO5.5-50SrB4O7 glasses measured with AFM
Open Research DataThe topography of as-quenched and heat treated 50(2Bi2O3-V2O5)-50SrB4O7 and 50Bi2VO5.5-50SrB4O7 glasses measured with AFM.
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The structure of strontium–borate glasses and glass-ceramics containing nanocrystallites of Bi2VO5.5. measured with X-ray diffraction method
Open Research DataThe structure of strontium–borate glasses and glass-ceramics containing Bi2VO5.5 nanocrystallites was measured by XRD.
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Thermal properties of strontium–borate glasses and glass-ceramics containing nanocrystallites of Bi2VO5.5. measured with DSC method
Open Research DataThermal properties of strontium–borate glasses and glass-ceramics containing nanocrystallites of Bi2VO5.5. was measured by DSC.
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The structure of Bi2VO5.5 ceramic prepared by 3 different ways measured with X-ray diffraction
Open Research DataThe structure of Bi2VO5.5 ceramics was measured by XRD.
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Thermal properties of ceramic Bi2VO5.5 and strontium–borate glass-ceramics containing crystalites of Bi2VO5.5. measured with DSC
Open Research DataThermal properties of ceramic Bi2VO5.5 and strontium–borate glass-ceramics containing Bi2VO5.5 crystallites was measured by DSC.
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The dependence of linear viscoelasticity limits of cold-recycled mixtures on time of curing and compaction method
PublicationCold-recycled mixtures are currently among the most widely used and investigated methods that enable recycling of old pavement structures in an environmentally friendly manner. Upon milling, the old pavement structure – whose gradation can be improved with addition of virgin aggregate – is mixed and compacted at ambient temperature. The main binding agents are bituminous emulsion and cement. Due to their dual binding behaviour,...
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The topography of strontium–borate glasses and glass-ceramics containing nanocrystallites of Bi2VO5.5. measured with SEM method
Open Research DataThe topography of strontium–borate glasses and glass-ceramics containing nanocrystallites of Bi2VO5.5. was measured by SEM.
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The structure of strontium–borate glass-ceramics containing crystalites of Bi2VO5.5. measured with X-ray diffraction and SEM methods
Open Research DataThe structure of strontium–borate glass-ceramics containing Bi2VO5.5 crystallites was measured by XRD and SEM.
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Nonlinear impedance as a function of A.C. voltage of Bi2VO5.5 ceramic of thickness 2.88 mm was measured at 693 K with impedance spectroscopy method
Open Research DataThe nonlinear electrical properties of Bi2VO5.5 ceramic of thickness 2.88 mm was measured by impedance spectroscopy method.
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Nonlinear impedance as a function of temperature and frequency for Bi2VO5.5 ceramic of thickness 2.52 mm was measured at different A.C. voltage with impedance spectroscopy method
Open Research DataThe nonlinear electrical properties of Bi2VO5.5 ceramic of thickness 2.52 mm was measured by impedance spectroscopy method.
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Nonlinear impedance as a function of A.C. voltage of Bi2VO5.5 ceramic of thickness 1.63 mm was measured with impedance spectroscopy method at high temperature region
Open Research DataThe nonlinear electrical properties of Bi2VO5.5 ceramic of thickness 1.63 mm was measured by impedance spectroscopy method.
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Nonlinear impedance as a function of A.C. voltage of Bi2VO5.5 ceramic of thickness 4.03 mm was measured with impedance spectroscopy method at high temperature region
Open Research DataThe nonlinear electrical properties of Bi2VO5.5 ceramic of thickness 4.03 mm was measured by impedance spectroscopy method.
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Nonlinear impedance as a function of A.C. voltage of Bi2VO5.5 ceramic of thickness 2.91 mm was measured with impedance spectroscopy method at high temperature region
Open Research DataThe nonlinear electrical properties of Bi2VO5.5 ceramic of thickness 2.91 mm was measured by impedance spectroscopy method.
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Nonlinear impedance as a function of frequency for Bi2VO5.5 ceramic of thickness 2.88 mm was measured at high temperature range with impedance spectroscopy method
Open Research DataThe nonlinear electrical properties of Bi2VO5.5 ceramic of thickness 2.88 mm was measured by impedance spectroscopy method.
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Nonlinear impedance as a function of A.C. voltage and temperature for Bi2VO5.5 ceramic of thickness 2.52 mm (after first heat-treatment at 913 K) was measured at different frequencies with impedance spectroscopy method
Open Research DataThe nonlinear electrical properties of Bi2VO5.5 ceramic of thickness 2.52 mm was measured by impedance spectroscopy method.