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Search results for: gas chromaography
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Determination of robenidine in animal feeds by liquid chromatography coupled with diode-array detection and mass spectrometry after accelerated solvent extraction
PublicationRobenidyna (chlorowodorek 1,3-bis[(4-chlorobenzylideno)amino]guanidyny) jest stosowana w celu zapobiegania i leczenia kokcydiozy - pasożytniczej choroby układu pokarmowego wielu zwierząt hodowlanych (kozy, owce, króliki, drób) wywoływanej przez pierwotniaki należące do rzędu Eimeria tenella, E. Necatrix, E. Acervulina, E. Maxima, E. Brunetti, and E. Mivati. Robenidyna wykazuje stosunkowo wysoką skuteczność terapeutyczną, przy niewielkiej...
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Application of ion chromatography for the determination of inorganic ions, especially thiocyanates in human saliva samples as biomarkers of environmental tobacco smoke exposure
PublicationŚrodowiskowy dym tytoniowy jest jednym z czynników decydujących o jakości powietrza wewnętrznego różnego typu pomieszczeń zamkniętych. Toksyczne składniki wydzielające się wraz z głównym i bocznym strumieniem dymu tytoniowego mają istotny wpływ na skład chemiczny płynów biologicznych. Jednym z biomarkerów narażenia na szkodliwe składniki środowiskowego dymu tytoniowego są jony rodankowe. Celem badań było znalezienie korelacji pomiędzy...
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Identification and characterization of the Indian Yellow dyestuff and its degradation products in historical oil paint tube by liquid chromatography mass spectrometry
PublicationAn analytical protocol for identification of dyes using reversed phase liquid chromatography-mass spectrometry with atmospheric pressure electrospray ionization (LC-ESI/MS) is presented. The developed method has been successfully applied in identification of euxanthic acid and euxanthone, the main components of the Indian Yellow dye in a historical oil paint tube produced by Richard Ain`es, a recognizable French company supplying...
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Procedure for and results of simultaneous determination of aromatic hydrocarbons and fatty acids methyl esters in diesel fuels by high performance liquid chromatography
PublicationW pracy przedstawiono taki sposób modyfikacji metody EN-12916 /ASTM D-6591, który zapewnia jednoczesne oznaczenie poszczególnych grup węglowodorów aromatycznych, całkowitej zawartości węglowodorów poliaromatycznych oraz zawartości FAME w oleju napędowym. Stosuje się nadal detektor refraktometryczny i elucję n-heptanem, jednak przepływ zwrotny eluentu jest wykonywany po elucji policyklicznych węglowodorów aromatycznych. Dodatkowo...
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Determination of trace levels of eleven bisphenol A analogues in human blood serum by high performance liquid chromatography–tandem mass spectrometry
PublicationChemicals showing structural or functional similarity to bisphenol A (BPA), commonly called BPA analogues, have recently drawn scientific attention due to their common industrial and commercial application as a substitute for BPA. In the European Union, the use of BPA has been severely restricted by law due to its endocrine disrupting properties. Unfortunately, it seems that all BPA analogues show comparable biological activity,...
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Rapid Characterization of the Human Breast Milk Lipidome Using a Solid-Phase Microextraction and Liquid Chromatography-Mass Spectrometry-Based Approach.
PublicationHuman breast milk (HBM) is a biofluid consisting of various biomolecules such as proteins, lipids, carbohydrates, minerals and bioactive substances. Due to its unique and complex composition, HBM provides not only nutritional components required for the growth of the infant, but also additional protection against infections. Global insight into the composition of HBM is crucial to understanding the health benefits infants receive...
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Application of Ion Chromatography for the Determination of Inorganic Ions, Especially Thiocyanates, in Human Semen Samples as Biomarkers of Environmental Tobacco Smoke Exposure.
PublicationPalenie tytoniu stanowi istotne źródło zanieczyszczenia powietrza wewnętrznego. Szkodliwość palenia tytoniu potwierdzają zarówno badania doświadczalne, jak i opracowania epidemiologiczne. Celem przeprowadzonych prac badawczych było uzyskanie informacji o poziomie zawartości jonów nieorganicznych, a zwłaszcza jonów rodankowych (jako biomarkerów narażenia na szkodliwe składniki obecne w środowiskowym dymie tytoniowym) w próbkach...
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Fingerprint comparison of low-volatile petroleum products by means of Thin Layer Chromatography (TLC) for identification of process leakages and environmental pollution
PublicationW pracy zbadano możliwość zastosowania stosunkowo prostej i szybkiej procedury przygotowania próbki, rozdzielania grup składników techniką cienkowarstwowej chromatografii cieczowej (TLC), wizualizacji w świetle UV 254 oraz 360 nm i analizy porównawczej cech plamek na płytkach TLC do określenia rodzaju niskolotnego materiału ropopochodnego stanowiącego zanieczyszczenie wód procesowych, lub wyciek z instalacji w rafinerii ropy naftowej....
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Comparison of classical and modern approach of determination of highly polar compounds by High Performance Liquid Chromatography coupled with Tandem Mass Spectrometry
PublicationAbstract: Sugars and sugar alcohols are known as highly polar compounds. Four analytes were taken into consideration for comparison of classical and modern approach of separation of highly polar substances. Mannitol was chosen as an example of simple sugar alcohol, sucrose and lactulose as examples of disaccharides and structural isomers, raffinose as an example of complex trisaccharide. Raffinose was also used as internal standard...
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Simultaneous Determination of Indolic Compounds in Plant Extracts by Solid-Phase Extraction and High-Performance Liquid Chromatography with UV and Fluorescence Detection
PublicationA high-performance liquid chromatographic method with UV and fluorescence detection (HPLC-DAD-FLD) was developed for simultaneous determination of indolic compounds in plant material. Indole-3-carbinol (I3C), indole-3-acetic acid (I3AA), indole-3-acetonitrile (I3ACN), and 3,3′-diindolylmethane (DIM) were used as representative compounds that cover a wide spectrum of indole structures occurring in nature. For concentration and purification...
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Sensitive simultaneous determination of 19 fluorobenzoic acids in saline waters by solid-phase extraction and liquid chromatography–tandem mass spectrometry
PublicationA solid-phase extraction (SPE) procedure using C18 stationary phase was optimized for the preconcentration of 19 fluorinated derivatives of benzoic acid (FBA): mono-, di-, tri-, and tetrafluorosubstituted in the ring, trifluoromethylbenzoic acid and 3,5-bistrifluoromethyl benzoic acid from undiluted salt-rich (>20%) reservoir waters. Quantitative (>90%) retention/elution of 16 out of 19 analyte compounds was achieved allowing a...
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Discrepancies in determination of biogenic amines in beer samples by reversed phase and hydrophilic interaction liquid chromatography coupled with tandem mass spectrometry
PublicationBiogenic amines (BAs) are nitrogenous organic bases occurring mainly in fermented food and beverages as a result of free amino acids bacterial decarboxylation. The reversed phase liquid chromatography (RPLC) and hydrophilic interaction liquid chromatography (HILIC) based methods were compared in terms of usefulness for determination of BAs in beer samples. Analysis of BAs with the use of RPLC method were carried out after their...
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Analysis of chiral pharmaceutical residues in influent and effluent samples at racemic and enantiomeric level using liquid chromatography-tandem mass spectrometry
PublicationIn this work, two different chromatographic methods for seasonal monitoring of pharmaceutical residue in wastewater samples were developed. In the case of enantiomeric separation of selected compounds, LC-MS technique combining with vancomycin based chiral stationary phase was used. The performance of chiral analysis enabled to monitor the pharmaceutical contamination at the enantiomeric level. The d-SPE procedure was developed...
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Pin-on-Substrate Gap Waveguide: An Extremely Low-Cost Realization of High-Performance Gap Waveguide Components
PublicationConsidering the limitations of currently available technologies for the realization of microwave components and antennas, a trade-off between different factors including the efficiency and fabrication cost is required. The main objective of this letter is to propose a novel method for the realization of gap waveguides (GWGs) that take advantage of conventional PCB fabrication technology, thus are low cost and light weight. Moreover,...
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Real-Time Monnitoring of Vegetable Oils' Thermal Degradation Using Proton Transfer Reaction Mass Spectrometry
PublicationThe volatile aldehydes, which are generated during frying, can be harmful to human health, therefore the concentration of these compounds in frying fumes should be monitored. In addition, aldehydes are markers of oils’ quality, and so it is possible to determine shelf-life or suitability for frying of these oils. Commonly, in order to determine aldehydes concentration gas chromatography is performed, however it does not allow for...
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Performance of a fuel cell optimized for in situ X-ray absorption experiments
PublicationKomercyjna komórka ogniwa paliwowego typu PEM została zmodyfikowana w celu realizacji pomiaru XAS w warunkach pracy ogniwa. Modyfikacja komórki miała na celu optymalizację jej parametrów pod kątem eksperymentu XAS realizowanego w modzie transmisyjnym i fluorescencyjnym, poprzez minimalizację absorpcji komórki, przy zachowaniu jej parametrów elektrochemicznych. W pracy zostały zaprezentowane szczegóły techniczne komórki a jej efektywność...
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CFD ship squat determination method validation by GPS-RTK measurements
PublicationArtykuł zawiera porównanie numerycznych obliczeń osiadania statku z wynikami badań rzeczywistych z wykorzystaniem metody GPS-RTK.
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GIS Integrated Modelling of a Himalayan Landscape
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Dmuchając na bardzo zimny gaz
PublicationZ punktu widzenia energetycznego bezpieczeństwa kraju, podstawową rolę odgrywają źródła surowca. Jednak, niezależnie od położenia terminalu eksportującego, wszystkie trasy wiodą przez Cieśniny Duńskie.
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The Symmetry of GPS Orbit Ascending Nodes
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Investigation on Tidal Components in GPS Coordinates
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GaAs-Si interfacial energy determination
PublicationBazując na półempirycznym modelu wiązań kowalencyjnych w krzemie wyznaczono energie międzypowierzchni GaAs-Si. Obliczona energia międzypowierzchni GaAs-Si zależna jest od orientacji podłoża Si. Minimalna energia międzypowierzchniowa wyznacza odpowiednią konfigurację atomów w pobliżu powierzchni, która określa optymalne warunki heteroepitaksji GaAs na podłożach Si.
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Multidimensional GIS for satellite imagery analysis
PublicationMultidimensional Geographical Information System allows storing, querying and processing of multidimensional query data. It is able to process satellite imagery and provide tools for its analysis. In the article authors present the developed system that analyzes a time series of SENTINEL - 1 mission satellite imagery acquired over the coast of Poland. The algorithm used finds and detects changes in the shape...
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MESOSCALE FUNCTIONS OF GPS SLANT DELAY
PublicationThe paper presents a computer module for GPS slant delay determination using data from COAMPS (Coupled Ocean/Atmosphere Mesoscale Prediction System) mesoscale non-hydrostatic model of the atmosphere which is run on IA64 Feniks computer cluster in the Department of Civil Engineering and Geodesy of the Military University of Technology. The slant delay is the result of integrating the ray (eikonal) equation for the spatial function...
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Handel targowy jako faux pas
PublicationWspółcześnie występujący handel targowy w przestrzeni publicznej posiada dwoisty charakter, polegający na niejednoznacznej odpowiedzi na pytanie czy powinno się ingerować współczesną architekturę w organizację targowisk czy jarmarków. Może tego rodzaju wydarzenia stanowią pewnego rodzaju nostalgię za tą pierwotną żywiołową formą handlu, której już się nie odnajdzie w galeriach handlowych, hipermarketach, gdzie rzesze ludzi pracują...
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41 Konferencja EGAS w Gdańsku
PublicationW artykule przedstawiono najważniejsze informacje dotyczące cyklicznej konferencji zorganizowanej pod patronatem Europejskiego Towarzystwa Fizycznego przez Wydział Fizyki Technicznej i Matematyki Stosowanej Politechniki Gdańskiej oraz Instytut Fizyki Doświadczalnej Uniwersytetu Gdańskiego.
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Numerical Modeling of Hydrogen-Rich Gas Production From Gasoline Autothermal Reforming in a Plug Flow Reactor for Electric Vehicles
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The role of fluids in high-pressure polymorphism of drugs: different behaviour of β-chlorpropamide in different inert gas and liquid media
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Occurrence and gas chromatographic determination of volatile fatty acids in landfill leachate. The case of two landfills in Gdansk Pomerania, Poland
PublicationWażnymi związkami pośrednimi degradacji materii organicznej na składowisku odpadów komunalnych są lotne kwasy tłuszczowe (LKT) i ich oznaczanie w wodach odciekowych pozwala monitorować procesy zachodzące na składowisku odpadów. Opracowano metodykę oznaczania LKT w próbkach wodnych polegającą na ekstrakcji LKT rozpuszczalnikiem organicznym i oznaczeniu w otrzymanym ekstrakcie za pomocą sprzężonego układu chromatograf gazowy-spektrometr...
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Influence of gas turbine controller adjustment on propulsion system behaviour in high sea conditions. Part 2. The simulation investigations.
PublicationDo badań przyjęto układ napędowy okrętowy z turbinami gazowymi napędzającymi poprzez przekładnię mechaniczną zębatą śrubę okrętową o zmiennym skoku.Przy użyciu programu komputerowego Matlab i jego nakładki Simulink wykonano symulację dynamiki układu napędowego statku pracującego na wzburzonym morzu.Zbadano wpływ nastaw i typu regulatora na pracę układu. Porównano nastawy układu regulacyjnego układu napędowego dla pracy...
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Specificity of automatic control of micro-turbines (steam or gas -driven and expanders) in dispersed generation system of heat and electric power
PublicationThis paper presents specific problems of automatic control of steam micro-turbines and expanders intended for the dispersed, combined generating of heat and electric power. The investigations concern ensurance of certainty of energy supply and its required quality.
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Membrane-SPME the best 'green' sample preparation technique for the gas chromatographic determination polar organic pollutants in polar media
PublicationOne of the most popular technique for sample preparation, which fulfill requirements of green analytical chemistry, is solid phase microextraction (SPME). Because of the undoubted advantages of SPME technique, solvent-free character of the extraction process and the enormous potential in analytical practice, a series of studies has been undertaken to develop new technical solutions, where improving the sensitivity and the extraction...
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Microstructural evolution and mechanical behavior of activated tungsten inert gas welded joint between P91 steel and Incoloy 800HT
PublicationThis study examines the welded joint between P91 steel and Incoloy 800HT using the Activated Tungsten Inert Gas (A-TIG) welding process. The focus is on analyzing the microstructure and evaluating the mechanical properties of joints made with different compositions of activating flux. Owing to the reversal of the Marangoni effect in which the conventional direction of molten metal flow in the weld pool is reversed due to the application...
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Assessment, optimisation and working fluid comparison of organic rankine cycle combined with negative CO2 gas power plant system
PublicationThis study aims to investigate the application of the Organic Rankine Cycle (ORC) as an alternative to low-pressure expansion in the negative CO2 power plant (nCO2PP). The reason for this study is that a detailed analysis of nCO2PP indicates a certain amount of waste heat present in the exhaust gas from the high-to-intermediate pressure gas turbine. Some of this energy can be used by the application of the expansion in a low-pressure...
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Monitoring the gas turbine start-up phase on the platform using a hierarchical model based on Multi-Layer Perceptron networks
PublicationVery often, the operation of diagnostic systems is related to the evaluation of process functionality, where the diagnostics is carried out using reference models prepared on the basis of the process description in the nominal state. The main goal of the work is to develop a hierarchical gas turbine reference model for the estimation of start-up parameters based on multi-layer perceptron neural networks. A functional decomposition...
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Experimental investigation of performance and emission characteristics of a miniature gas turbine supplied by blends of kerosene and waste tyre pyrolysis oil
PublicationFossil fuels are non-renewable sources of energy that could be depleted in the near future, giving rise to amajor energy crisis. Scientists from all over the world are working on new technologies to produce fuelnot only from renewable sources but also from waste. This article is concerned with: (i) waste tyremanagement by means of the pyrolysis process, (ii) investigation of physico-chemical parameters ofwaste tyre pyrolysis oil...
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Reversed-phase and normal-phase thin-layer chromatography and their application to the lipophilicity prediction of synthetic pyrethroids based on quantitative structure–retention relationships
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Application of high performance liquid chromatography with ultraviolet diode array detection and refractive index detection to the determination of class composition and the analysis of gasoline.
PublicationZaprezentowano nową metodę HPLC oznaczania składu grupowego benzyn i komponentów benzyn tj. oznaczania zawartości olefin, węglowodorów aromatycznych i parafinowo-naftenowych.
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Profiling and Qualitative Assessment of Enzymatically and Thermally Oxidized Egg Yolk Phospholipids using a Two‐Step High‐Performance Liquid Chromatography Protocol
PublicationA two‐step high‐performance liquid chromatography (HPLC) method for the profiling and qualitative assessment of oxidized phospholipids (oxPL) present in foods was developed. The applicability of the investigated two‐step HPLC protocol was verified for separation of enzymatically and thermally oxidized hen egg yolk phospholipids (PL) as a relevant food model. In the first step, seven individual PL classes were separated using hydrophilic...
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Comprehensive determination of flavouring additives and nicotine in e-cigarette refill solutions. Part I: Liquid chromatography-tandem mass spectrometry analysis
PublicationLiquid chromatography-tandem mass spectrometry with electrospray ionization (HPLC-ESI–MS/MS) methods were developed for the simultaneous determination of 42 flavouring compounds and nicotine in liquids for e-cigarettes. The chromatographic separation was performed using an Ace® Ultracore™ SuperC18™ (100 × 2.1 mm, 2.5 μm) column in both acidic and alkaline pH conditions to separate all the compounds. A simple “dilute & shoot” approach...
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Determination of amikacin and ciprofloxacin by liquid chromatography with pre-column derivatization to evaluate sustained delivery of antibiotics from Drug-Eluting Biopsy Needle
PublicationDetermination of chosen antibacterial antibiotics: amikacin and ciprofloxacin was carried out by HPLC-UV after derivatization with 9-fluorenylmethyl chloroformate and in their native form by HPLC-MS/MS. Developed methods have been applied to control the kinetics of antibiotic release from polymer-based controlled drug delivery system.
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Improvement of derivatized amino acid detection sensitivity in micellar electrokinetic capillary chromatography by means of acid-induced pH-mediated stacking technique
PublicationDerivatization is a frequently used sample prepara-tion procedure applicable to the enhancement of analyte de-tection sensitivity. Amino acids mostly require derivatization prior to electrophoretic or chromatographic analysis, especial-ly if spectrophotometric detection is used. This study presents an on-line preconcentration technique for derivatized amino acids. The sensitivity of the method was improved by the utilization of...
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Studies of the separation performance of silanized silica gel for simulated distillation
PublicationWe present the results of investigations of the chromatographic (sorptive) properties of silanized silica gel as a stationary phase for gas chromatography used for simulated distillation. Commercially available silanized sorbent (particle diameter range 63–200 m, average pore size 60 Å) was sieved to obtain the 80–100 mesh fraction (180–150 m). The obtained results revealed that silanized silica gel allows the complete separation...
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Evaluation of the Impact of Storage Conditions on the Biogenic Amines Profile in Opened Wine Bottles
PublicationA survey of biogenic amine (BA) profiles in opened wine bottles has been established to monitor the level of biogenic amines (BAs) in opened bottles against time and other conditions. Bottles of red and white wine were submitted to different temperatures, stopper type (screw cap, cork), and use of vacuum devices. A total of six wines made from a variety of grapes were obtained from vineyards from regions across Poland. Dispersive...
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Process control of air stream deodorization from vapors of VOCs using a gas sensor matrix conducted in the biotrickling filter (BTF)
PublicationThis article presents the validity, advisability and purposefulness of using a gas sensor matrix to monitor air deodorization processes carried out in a peat-perlite-polyurethane foam-packed biotrickling filter. The aim of the conducted research was to control the effectiveness of air stream purification from vapors of hydrophobic compounds, i.e., n-hexane and cyclohexane. The effectiveness of hydrophobic n-hexane and cyclohexane...
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The potential of LC–MS technique in direct analysis of perfume content
PublicationPerfumes are products that consist of a wide range of natural and synthetic compounds. Due to complex composition, the determination of their ingredients is a difficult task. Most of the perfume components are either volatile or semi-volatile; however, most of the attention has been paid to volatile ones, and thus, gas chromatography or electronic noses are generally used. Nevertheless, in this study, liquid chromatography coupled...
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Activation of the Normal Human Skin Cells by a Portable Dielectric Barrier Discharge-Based Reaction-Discharge System of a Defined Gas Temperature
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Technical and economical analysis of combined cycles of gas turbine -steam turbine on pipeline compressor stations. Part II - Economic analysis
PublicationW pracy przedstawiono zagadnienie nadbudowy zespołów turbosprężarkowych, znajdujących się na tłoczni gazu ziemnego, odzyskowymi blokami parowymi. W analizie tego przedsięwzięcia wzięto pod uwagę kilka wariantów konfiguracji układu parowego oraz kilka wariantów uwzględniających zmienność obciążenia turbin gazowych napędzających kompresory. Dla układu parowego dobrano wszystkie podstawowe parametry, a następnie wykonano obliczenia...
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Technical and economical analysis of combined cycles of gas turbine - steam turbine on pipeline compressor stations. Part I - Technical analysis
PublicationW pracy przedstawiono zagadnienie nadbudowy zespołów turbosprężarkowych, znajdujących się na tłoczni gazu ziemnego, odzyskowymi blokami parowymi. W analizie tego przedsięwzięcia wzięto pod uwagę kilka wariantów konfiguracji układu parowego oraz kilka wariantów uwzględniających zmienność obciążenia turbin gazowych napędzających kompresory. Dla układu parowego dobrano wszystkie podstawowe parametry, a następnie wykonano obliczenia...
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Technical and economical analysis of combined cycles of gas turbine - steam turbine on pipeline compressor stations. Part II - Economic analysis
PublicationW pracy przedstawiono zagadnienie nadbudowy zespołów turbosprężarkowych, znajdujących się na tłoczni gazu ziemnego, odzyskowymi blokami parowymi. W analizie tego przedsięwzięcia wzięto pod uwagę kilka wariantów konfiguracji układu parowego oraz kilka wariantów uwzględniających zmienność obciążenia turbin gazowych napędzających kompresory. Dla układu parowego dobrano wszystkie podstawowe parametry, a następnie wykonano obliczenia...