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Search results for: IMPEDANCE SPECTROMETER
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Direct measurements of odorous volatile organic compounds present in biosolids cakes by Proton Transfer Reaction – Mass Spectrometry Technique
PublicationThis paper show the results of investigation of concentration of odorous chemical compounds emitted upon ageing of anaerobically stabilised biosolids that could contribute to the overall odour character of nuisance emissions. Biosolids samples from wastewater treatment plant were collected in spring time. Concentrations of volatile organic compounds using a US EPA flux hood and Proton Transfer Reaction-Time of Flight-Mass Spectrometry...
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On-line assessment of oil quality during deep frying using an electronic nose and proton transfer reaction mass spectrometry
PublicationWe describe a novel method for the quality assessment of oil utilized for deep frying. The method is based on the analysis of frying fumes using a custom electronic nose. The quality score could be obtained after less than 3 min of analysis and without interrupting the frying process or sampling the oil directly. The obtained results were correlated with the peroxide value using a multivariate linear regression model. The most...
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Estimation of platinum in environmental water samples with solid phase extraction technique using inductively coupled plasma mass spectrometry
PublicationZoptymalizowano metodykę oznaczania śladowych poziomów stężeń platyny (IV) w oparciu o technikę ekstrakcji do fazy stałej w połączeniu ze spektrometrią mas z plazmą wzbudzoną indukcyjnie. Na etapie wzbogacania platyny wykorzystano żel krzemionkowy modyfikowany grupami aminopropylowymi. Ilościowy odzysk platyny uzyskano poprzez wykorzystanie 1.0 mol L-1 roztworu tiomocznika jako eluenta. Odchylenie standardowe wyników (RSD) było...
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Determination of nonsteroidal antiinflammatory drugs in water samples using liquid chromatography coupled with diode-array detector and mass spectrometry
PublicationOpracowano i zwalidowano metodykę do oznaczania śladowych ilości sześciu różnych związków z grupy niesteroidowych leków przeciwzapalnych w próbkach wodnych. Anality zostały wybrane spośród najczęsciej sprzedawanych leków w Polsce. Sprawdzono kilka różnych kolumienek ekstrakcyjnych i wybrano RP-18 jako najlepsze wypełnienie do wzbogacania oznaczanych związków. Opracowaną metodykę z powodzeniem zastosowano do analizy próbek rzeczywistych.
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Monolithic capsule phase microextraction prior to gas chromatography-mass spectrometry for the determination of organochlorine pesticides in environmental water samples
PublicationIn this study, a capsule phase microextraction (CPME) protocol followed by gas chromatography-mass spectrometry is proposed for the accurate and sensitive monitoring of organochlorine pesticides (OCPs) in environmental water samples. Different monolithic sol–gel encapsulated sorbents were compared and monolithic sol–gel poly(ethylene glycol)-based sorbent incorporated into porous microextraction capsules resulted in the highest...
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The Mechanism of a Retro-Diels–Alder Fragmentation of Luteolin: Theoretical Studies Supported by Electrospray Ionization Tandem Mass Spectrometry Results
PublicationThe mechanisms of retro-Diels–Alder fragmentation of luteolin are studied theoretically using the Density Functional Theory method (B3LYP hybrid functional) together with the 6-311++G(d,p) basis set and supported by electrospray ionization tandem mass spectrometry (ESI-MS) results. The reaction paths leading to the formation of 1,3A and 1,3B fragment ions observed as the main spectral features in the ESI-MS spectrum are described...
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Online Volatile Compound Emissions Analysis Using a Microchamber/Thermal Extractor Coupled to Proton Transfer Reaction-Mass Spectrometry
PublicationIndoor air is a complex and dynamic mixture comprising manifold volatile organic compounds (VOCs) that may cause physiological and/or psychological discomfort, depending on the nature of exposure. This technical note presents a novel approach to analyze VOC emissions by coupling a microchamber/thermal extractor (μ-CTE) system to a proton transfer reaction-mass spectrometer (PTR-MS). This configuration provides an alternative to...
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Direct injection liquid chromatography-mass spectrometry (DI-LC-MS) analysis for rapid lipidomic profiling of extracellular vesicles
PublicationExtracellular vesicles (EVs) are small, spherical particles produced by eukaryotic and prokaryotic cells, surrounded by a bilayer membrane and carrying various bioactive molecules, such as proteins, surface receptors, membrane and soluble proteins, lipids, and nucleic acids. EVs are of substantial interest because of their important roles in cell communication, epigenetic regulation and possible application in disease diagnosis...
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Jacek Ryl dr hab. inż.
PeopleI have obtained my PhD in chemical technology in 2010. In the same year, I was employed at the Department of Electrochemistry, Corrosion and Materials Engineering at the Faculty of Chemistry. In 2018 I received habilitation at the Faculty of Chemistry GUT in technical sciences in the discipline of chemical technology. From 2021, he was employed at the Institute of Nanotechnology and Materials Science at the Faculty of Technical...
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Simultaneous measurements of ECG, body Impedance and temperature
Open Research DataThe data are complementary part of the experiment designed to demonstrate how to use the network protocols to transmit medical data. The dataset contains biomedical signals of ECG, Impedanc and temperature acquired simultaneously. The data allow students to become familiar with data acquisition methods (simulate data transmission by medical device over...
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Jerzy Wtorek prof. dr hab. inż.
PeopleJerzy Wtorek received the M.Sc., the Ph.D. and the D.Sc. degrees in electronics from Gdańsk University of Technology, Gdańsk, Poland, in 1976, 1986, and 2004, respectively. He has been with Electronics, Telecommunication and Informatics Faculty, Gdańsk University of Technology since 1977. He is currently an Associate Professor at Biomedical Engineering Department. His research interests include the developing of noninvasive methods...
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Multifrequency Nanoscale Impedance Microscopy (m-NIM): A novel approach towards detection of selective and subtle modifications on the surface of polycrystalline boron-doped diamond electrodes
PublicationIn this paper, we describe the modification of Nanoscale Impedance Microscopy (NIM), namely, a combination of contact-mode atomic force microscopy with local impedance measurements. The postulated approach is based on the application of multifrequency voltage perturbation instead of standard frequency-by-frequency analysis, which among others offers more time-efficient and accurate determination of the resultant impedance spectra...
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High gain/bandwidth off‑chip antenna loaded with metamaterial unit‑cell impedance matching circuit for sub‑terahertz near‑field electronic systems
PublicationAn innovative off-chip antenna (OCA) is presented that exhibits high gain and efficiency performance at the terahertz (THz) band and has a wide operational bandwidth. The proposed OCA is implemented on stacked silicon layers and consists of an open circuit meandering line. It is shown that by loading the antenna with an array of subwavelength circular dielectric slots and terminating it with a metamaterial unit cell, its impedance...
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Linear impedance of Bi2VO5.5 glass-ceramic annealed at 423 K measured with impedance spectroscopy method at low temperature region
Open Research DataThe linear electrical properties of Bi2VO5.5 glass-ceramic annealed at 423 K prepared by traditional melt quenching technique was measured by impedance spectroscopy method.
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Analysis of electromagnetic disturbances in DC network of grid connected building-integrated photovoltaic system
PublicationThis paper focuses on conducted electromagnetic interference (EMI) emissions and propagation in the DC network of grid connected building integrated photovoltaic (PV) system. The investigated PV system, consists of ten solar panels, cabling and the grid-connected one phase inverter. The EMI simulation model of the real PV system has been developed with the aid of impedance analyzer measurements of solar panels and the DC network...
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Nonlinear impedance of 45Bi2VO5.5-55SrB4O7 fully crystallized glass measured with impedance spectroscopy method at high temperature region
Open Research DataThe nonlinear electrcial properties of 45Bi2VO5.5-55SrB4O7 fully crystallized glass was measured by impedance spectroscopy method.
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Linear impedance of Bi2VO5.5 ceramic of thickness 2.88 mm measured with impedance spectroscopy method at low temperature region
Open Research DataThe linear electrical properties of Bi2VO5.5 ceramic of thickness 2.88 mm was measured by impedance spectroscopy method.
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Linear impedance of 5(2Bi2O3-V2O5)-95SrB4O7 glass measured with impedance spectroscopy method at high temperature region
Open Research DataThe linear electrcial properties of 5(2Bi2O3-V2O5)-95SrB4O7 glass was measured by impedance spectroscopy method.
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Nonlinear impedance of 35Bi2VO5.5-65SrB4O7 fully crystallized glass measured with impedance spectroscopy method at high temperature region
Open Research DataThe nonlinear electrcial properties of 35Bi2VO5.5-65SrB4O7 fully crystallized glass was measured by impedance spectroscopy method.
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Linear impedance of 25Na2O–20CaO–5P2O5–50SiO2 glass measured with impedance spectroscopy method at low temperature region
Open Research DataThe linear electrical properties of 25Na2O–20CaO–5P2O5–50SiO2 glass was measured by impedance spectroscopy method.
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Linear impedance of 58(2Bi2O3-V2O5)-42SrB4O7 glass measured with impedance spectroscopy method at low temperature region
Open Research DataThe linear electrcial properties of 58(2Bi2O3-V2O5)-42SrB4O7 glass was measured by impedance spectroscopy method.
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Linear impedance of 50(2Bi2O3-V2O5)-50SrB4O7 glass measured with impedance spectroscopy method at high temperature region
Open Research DataThe linear electrcial properties of 50(2Bi2O3-V2O5)-50SrB4O7 glass was measured by impedance spectroscopy method.
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Linear impedance of 5(2Bi2O3-V2O5)-95SrB4O7 glass measured with impedance spectroscopy method at low temperature region
Open Research DataThe linear electrcial properties of 5(2Bi2O3-V2O5)-95SrB4O7 glass was measured by impedance spectroscopy method.
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Nonlinear impedance of 5(2Bi2O3-V2O5)-95SrB4O7 glass measured with impedance spectroscopy method at high temperature region
Open Research DataThe nonlinear electrcial properties of 5(2Bi2O3-V2O5)-95SrB4O7 glass was measured by impedance spectroscopy method.
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Linear impedance of Bi2VO5.5 ceramic of thickness 2.52 mm measured with impedance spectroscopy method at low temperature region
Open Research DataThe linear electrical properties of Bi2VO5.5 ceramic of thickness 2.52 mm was measured by impedance spectroscopy method.
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Linear impedance of 50(2Bi2O3-V2O5)-50SrB4O7 glass measured with impedance spectroscopy method at low temperature region
Open Research DataThe linear electrcial properties of 50(2Bi2O3-V2O5)-50SrB4O7 glass was measured by impedance spectroscopy method.
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Nonlinear impedance of 58(2Bi2O3-V2O5)-42SrB4O7 glass measured with impedance spectroscopy method at low temperature region
Open Research DataThe nonlinear electrcial properties of 58(2Bi2O3-V2O5)-42SrB4O7 glass was measured by impedance spectroscopy method.
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Nonlinear impedance of 30Bi2VO5.5-70SrB4O7 fully crystallized glass measured with impedance spectroscopy method at high temperature region
Open Research DataThe nonlinear electrcial properties of 30Bi2VO5.5-70SrB4O7 fully crystallized glass was measured by impedance spectroscopy method.
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Linear impedance as a function of A.C. voltage for 50(2Bi2O3-V2O5)-50SrB4O7 glass measured with impedance spectroscopy method
Open Research DataThe linear electrcial properties as a function of A.C. voltage for 50(2Bi2O3-V2O5)-50SrB4O7 glass was measured by impedance spectroscopy method.
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Dariusz Świsulski dr hab. inż.
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Badanie metody pomiaru impedancji pętli zwarciowej wykorzystującej składowe fazora napięcia. - A. Golijanek-Jędrzejczyk.
PublicationMonografia podejmuje ważną tematykę pomiarów impedancji pętli zwarciowej w układach elektroenergetycznych niskiego napięcia związaną z bezpieczeństwem użytkowania urządzeń elektrycznych. W siedmiu rozdziałach pracy zaprezentowano m.in. przegląd znanych metod i mierników do pomiaru impedancji pętli zwarciowej, podstawy teoretyczne oraz analizę metrologiczną dwóch metod impedancji pętli wykorzystujących składowe ortogonalne napięcia...
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Ograniczenie wpływu odkształcenia napięcia sieci na dokładność pomiaru impedancji uziemień urządzeń elektroenergetycznych
PublicationW pracy przedstawiono propozycję nowej metody pomiaru impedancji rozległych uziemień urządzeń elektroenergetycznych. Metoda ta pozwala ograniczyć wpływ odkształcenia napięcia sieci na błędy pomiaru impedancji. Badania i obliczenia błędów przeprowadzone zostały dla wybranych typów odkształceń krzywej napięcia i różnych parametrów obwodu badanego.
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Metody przewidywania temperaturowych zmian impedancji układu grzejnego na podstawie jego charakterystyki częstotliwościowej
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Wpływ błędów pomiaru wartości skutecznych napięć na dokładność wyznaczenia impedancji pętli zwarciowej
PublicationWartość impedancji pętli zwarciowej otrzymuje się na podstawie pomiaru dwóch wartości napięć dla obwodu nieobciążonego oraz obciążonego, najczęściej rezystancją, która stanowi sztuczne zwarcie. Obecnie krzywa napięcia sieci w miejscu pomiaru może być wyraźnie odkształcona. W referacie przedstawiono analizę wpływu błędu pomiaru okresu napięcia sieci na dokładność wyznaczenia impedancji pętli zwarciowej, z uwzględnieniem odkształcenia...
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Pomiar impedancji pętli zwarciowej w instalacjach fotowoltaicznych dużych mocy z magazynowaniem energii
PublicationW artykule przedstawiono różne konfiguracje przepływu energii w instalacjach fotowoltaicznych z zastosowaniem przekształtników energoelektronicznych o mocy od 10 do 1000 kVA. W pomiarach impedancji pętli zwarciowej (IPZ) w obwodach zasilanych z przekształtników przyrządami różnych producentów zaobserwowano wyniki pomiaru zależne od trybu pracy przekształtnika oraz od wartości wymuszanego prądu probierczego przyrządu. W artykule...
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Molecular Heterogeneity of Papillary Thyroid Cancer: Comparison of Primary Tumors and Synchronous Metastases in Regional Lymph Nodes by Mass Spectrometry Imaging
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Radiation-related Changes in Serum Proteome Profiles Detected by Mass Spectrometry in Blood of Patients Treated with Radiotherapy Due to Larynx Cancer
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Radiation-related Changes in Serum Proteome Profiles Detected by Mass Spectrometry in Blood of Patients Treated with Radiotherapy Due to Larynx Cancer
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Solid phase extraction and sequential elution for pre-concentration of traces of Mn and Zn in analysis of honey by flame atomic absorption spectrometry
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Element analysis of bee-collected pollen and bee bread by atomic and mass spectrometry – Methodological development in addition to environmental and nutritional aspects
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Determination of β-blockers and β-agonists using gas chromatography and gas chromatography–mass spectrometry – A comparative study of the derivatization step
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Quantification of DNA Modifications Using Two-Dimensional Ultraperformance Liquid Chromatography Tandem Mass Spectrometry (2D-UPLC-MS/MS)
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Sensitive simultaneous determination of 19 fluorobenzoic acids in saline waters by solid-phase extraction and liquid chromatography–tandem mass spectrometry
PublicationA solid-phase extraction (SPE) procedure using C18 stationary phase was optimized for the preconcentration of 19 fluorinated derivatives of benzoic acid (FBA): mono-, di-, tri-, and tetrafluorosubstituted in the ring, trifluoromethylbenzoic acid and 3,5-bistrifluoromethyl benzoic acid from undiluted salt-rich (>20%) reservoir waters. Quantitative (>90%) retention/elution of 16 out of 19 analyte compounds was achieved allowing a...
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Comparison of classical and modern approach of determination of highly polar compounds by High Performance Liquid Chromatography coupled with Tandem Mass Spectrometry
PublicationAbstract: Sugars and sugar alcohols are known as highly polar compounds. Four analytes were taken into consideration for comparison of classical and modern approach of separation of highly polar substances. Mannitol was chosen as an example of simple sugar alcohol, sucrose and lactulose as examples of disaccharides and structural isomers, raffinose as an example of complex trisaccharide. Raffinose was also used as internal standard...
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Steroid profiles as potential biomarkers in patients with urogenital tract cancer for diagnostic investigations analyzed by liquid chromatography coupled to mass spectrometry
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Molecularly imprinted stir bar sorptive extraction coupled with atomic absorption spectrometry for trace analysis of copper in drinking water samples
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Salt saturated single drop microextraction of gold from water samples and its determination by graphite furnace atomic absorption spectrometry
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Determination of selenium by X-ray fluorescence spectrometry using dispersive solid-phase microextraction with multiwalled carbon nanotubes as solid sorbent
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Comparison of mass spectrometry data and bioinformatics predictions to assess the bona fide localization of proteins identified in cell wall proteomics studies
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Determination of Butyltin Species in Sea Water Samples Using Solid Phase Extraction Followed by Liquid Chromatography - Tandem Mass Spectrometry
PublicationReverse phase liquid chromatography (RP-HPLC)-electrospray ionization-tandem mass spectrometry (ESI-MS-MS) was evaluated for the analysis of TBT using solid phase extraction as sample preparation method. TBT was extracted from acidified water samples (spiked with tripropyltin as internal standard) using reversed phase polymeric Strata-X cartridges. Analytes were eluted from cartridges using acetonitrile-water mixture and the volume...