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Divergent Synthesis of Functionalized Indenopyridin-2-ones and 2-Pyridones via Benzyl Group Transfer: Two Cases of Aza-semipinacol-Type Rearrangement
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TspGWI, a thermophilic class-IIS restriction endonuclease from Thermus sp.,recognizes novel asymmetric sequence 5´-ACGGA(N11/9)-3
PublikacjaA novel prototype class-IIS restriction endonuclease, TspGWI, was isolated from the thermophilic bacterium Thermus sp. GW. The recognition sequence and cleavage positions have been established: TspGWI recognizes the non-palindromic 5-bp sequence 5′-ACGGA-3′ and cleaves the DNA 11 and 9 nt downstream in the top and bottom strand, respectively. In addition, an accompanying endonuclease, TspGWII, an isoschizomer of Pst I, was found...
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Solvent influence on the crystal structures of new cadmium tri-tert -butoxysilanethiolate complexes with 1,4-bis(3-aminopropyl)piperazine: luminescence and antifungal activity
PublikacjaMonocrystals of dinuclear 1,4-bis(3-aminopropyl)piperazine-�4N1,N10:N4,N40-bis[bis(tri-tert-butoxysilanethiolato-�S)cadmium(II)], [Cd2(C12H27O3SSi)4(C10-H24N4)] or [Cd2{SSi(OtBu)3}4(�-BAPP)], 1, and polynuclear catena-poly[[bis- (tri-tert-butoxysilanethiolato-�S)cadmium(II)]-�-1,4-bis(3-aminopropyl)piperazine-�2N10:N40], [Cd(C12H27O3SSi)2(C10H24N4)]n or [Cd{SSi(OtBu)3}2(�-BAPP)]n, 2, with 1,4-bis(3-aminopropyl)piperazine (BAPP)...
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Anti-cancer effect of Rumex obtusifolius in combination with arginase/nitric oxide synthase inhibitors via downregulation of oxidative stress, inflammation, and polyamine synthesis
PublikacjaCancer continues to be a leading cause of death worldwide, making the development of new treatment methods crucial in the fight against it. With cancer incidence rates increasing worldwide, ongoing research must focus on identifying new and effective ways to prevent and treat the disease. The combination of herbal extracts with chemotherapeutic agents has gained much interest as a novel strategy to combat cancer. Rumex obtusifolius...
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Enhancement of PUR/PIR foam thermal stability after addition of Zostera marina biomass component investigated via thermal analysis and isoconversional kinetics
PublikacjaIn the present work, a thorough thermogravimetric (TG) analysis of bio-based polyurethane–polyisocyanurate (PUR–PIR) foams in both nitrogen and oxygen atmosphere is performed. A sustainable element of the foam is a biopolyol obtained via acid-catalyzed liquefaction of Zostera marina and Enteromorpha Algae biomass. Based on isoconversional analysis and apparent activation energies, several conclusions are obtained. In contradiction...
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Bio‑derived polyurethanes obtained by non‑isocyanate route using polyol‑based bis(cyclic carbonate)s—studies on thermal decomposition behavior
PublikacjaNon-isocyanate polyurethanes (NIPUs) constitute one of the most prospective groups of eco-friendly materials based on their phosgene-free synthesis pathway. Moreover, one of the steps of their obtaining includes the use of carbon dioxide (CO 2 ), which allows for the promotion of the development of carbon dioxide capture and storage technologies. In this work, non- isocyanate polyurethanes were obtained via three-step synthesis...
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Composite Sandwich Footbridge – Numerical ESL FEM Calculations vs. In Situ Measurements
PublikacjaSelected results of the static analysis of composite sandwich footbridge with the corresponding in situ measured values are compared in the paper. The analysed bridge is a research object, which was built in 2015 and is currently located at the Gdańsk University of Technology campus. Since it is a novel structure, a proper definition of the bridge numerical model, allowing its safe design, is very important. Therefore, instead...
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BDNF and Cortisol integrative system – Plasticity vs. degeneration: Implications of the Val66Met polymorphism
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State security and patriotism vs the implementation of obligations and prohibitions related to covid-19
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Physical Activity vs. Redox Balance in the Brain: Brain Health, Aging and Diseases
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Conditional Value-at-Risk Vs. Value-at-Risk to Multi-Objective Portfolio Optimization
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iGEL vs laryngeal tube for airway management during a normal airway scenario
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Urban Regeneration vs. Urban Sprawl - Problems and Prospects in Post-Socialist Cities
PublikacjaArtykuł dotyczy relacji pomiędzy procesami suburbanizacji a odnowy miasta na przykładzie miast post-socjalistycznych. W szczególnosci zaprezentowano w nim moziwości rozwoju koncepcji miasta kompaktowego oraz problemów wiążacych się z tym konceptem.
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“Shadow” vs. “Phase 3D” method within endoscopic examinations of marine engines
PublikacjaA visual investigation of surfaces creating internal, working spaces of marine combustion engines by means of specialized view-finders so called endoscopes is at present almost a basic method of technical diag-nostics. The surface structure of constructional material is visible during investigations like through the magnifying glass (usually with a precisely determined magnification), which makes possible a detection, recognition...
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Struktury fotowoltaiczne z planarnym heterozłączem półprzewodnik II-VI / półprzewodnik molekularny
PublikacjaArtykuł przedstawia wybrane wyniki badań własnych nad układami hybrydowymi zbudowanymi na bazie złącza półprzewodnik nieorganiczny II-VI/półprzewodnik organiczny. Na podstawie analizy położenia pasm energetycznych warstw wchodzących w skład wytworzonych ogniw oraz charakterystyk spektralnych prądu zwarcia tych urządzeń określone zostały procesy prowadzące do fotogeneracji nośników ładunku w badanych układach. W ogniwach zbudowanych...
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New dioxomolybdenum(VI) complexes of tetradentate Schiff base as catalysts for epoxidation of olefins
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Nanomateriały w tematyce VI Programu Ramowego Unii Europejskiej: analiza trendów
PublikacjaScharakteryzowano cele i zadania projektów badawczych VI Programu Ramowego UE poświęcone nanomateriałom.
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VI Krajowa Konferencja Naukowo - Techniczna Diagnostyka Procesów Przemysłowych DPP´2003.
PublikacjaW dniach 15-17 września 2003 roku odbyła się we Władysławowie Konferencja Naukowo Techniczna DPP´2003. Ma ona już 10 letnią tradycję. Konferencja jest organizowana cyklicznie począwszy od 1996 roku przez trzy ośrodki akademickie Politechnikę Gdańską, Politechnikę Warszawską oaz Uniwersytet Zielonogórski. Patronat nad Konferencją objęła PAN, Komitet Automatyki i Robotyki oraz Towarzystwo Konsultantów Polskich. Tegoroczna edycja...
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Spontaneous electron emission vs dissociation in internally hot silver dimer anions
PublikacjaReferring to a recent experiment, we theoretically study the process of a two-channel decay of the diatomic silver anion (Ag2-), namely the spontaneous electron ejection giving Ag2 + e- and the dissociation leading to Ag- + Ag. The ground state potential energy curves of the silver molecules of diatomic neutral and negative ion were calculated using proper pseudo-potentials and atomic basis sets. We also estimated the non-adiabatic...
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Experimental Studies of Concrete-Filled Composite Tubes under Axial Short- and Long-Term Loads
PublikacjaThe paper presents experimental studies on axially compressed columns made of concrete-filled glass fiber reinforced polymer (GFRP) tubes. The infill concrete was C30/37 according to Eurocode 2. The investigated composite pipes were characterized by different angles of fiber winding in relation to the longitudinal axis of the element: 20, 55 and 85 degrees. Columns of two lengths, 0.4 m and 2.0 m, were studied. The internal diameter...
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Miniaturized Metal-Mountable U-shaped Inductive-Coupling-Fed UHF RFID Tag Antenna with Defected Microstrip Surface
PublikacjaThis study presents a novel miniature ultra-high frequency (UHF) radio frequency identification (RFID) tag for metallic objects. Its arrangement includes a U-shaped feeder, which is inductively coupled to two E-type connected patches. Size reduction is achieved by means of utilizing the U-shaped feeder, and introducing a defection in the connection between the two E-type patches. The defection in the connection area between the...
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Micro-Raman spectroscopy in the studies of multiphase separated polyurethanes. [online] W: [Proc.] UTECH Europe 2003 . The International Polyurethane Industry Conference and Exhibition. 25/26/27 March 2003, The Hague, Netherlands. London: Crain Communications Ltd. Dostępny w World Wide Web: http://UTECH-2003.com + wydruk.**2003 [s. 123-130 bibliogr. 41 poz.]Mikro-Ramanowska spektroskopia w badaniach poliuretanów wykazujących separację wielofazową.
PublikacjaPrzedmiotem badań były trzy próbki poliuretanowe o zawartości 30% segmentówsztywnych otrzymanych z politlenku propylenu, diizocyjanianu difenylometanui butanodiolu. Próbki te wykazują morfologię wielofazową, w której można wy-różnić globule i sferolity rozproszone w matrycy polimerowej.Za pomocą spek-troskopii mikro-Ramana przeprowadzono mikroanalizę chemiczną wszystkich ele-mentów morfologicznych. Stwierdzono odmienny skład...
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Synergy between AgInS2 quantum dots and ZnO nanopyramids for photocatalytic hydrogen evolution and phenol degradation
PublikacjaDespite the unique properties of single semiconductor nanomaterials and quantum dots, poor photocatalytic activity has characterized them and the fabrication of nanocomposites has become necessary to enhance their photocatalytic performance. Thus, AgInS2 quantum dots (AIS QDs, 4.0±1.6 nm), have been successfully prepared and loaded onto ZnO nanopyramids (ZnO NPy). The effect of the nominal amount of AIS QDs decorating ZnO NPy on...
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Hybrid P3HT: PCBM/GaN nanowire/Si cascade heterojunction for photovoltaic application
PublikacjaPoly(3-hexylthiophene) (P3HT) and phenyl-C61-butyric acid methyl ester (PCBM) are commonly used for the fabrication of organic photovoltaics (OPV). Efficiency limitations of OPVs could be circumvented by incorporation of inorganic nanostructures into organic blends. Again, integration of organic solar cells with well-developed silicon photovoltaic technology is ultimately desirable. In present work, GaN nanowires with diameters...
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Do Phenyl Substituents Affect the Properties of Azobenzocrown Derivatives?
PublikacjaNew products of photo- and thermal rearrangements of 19-membered azoxybenzocrown with phenyl substituents in benzene rings in the para positions to oligooxyethylene fragments are characterized. The yields of photochemical transformations depend on the solvent. Para-hydroxyazocrown is formed with yields over 50% in propan-2-ol. Ortho-hydroxyazobenzocrown is obtained with yields up to 70% in toluene/acetic acid mixture. Macrocyclic...
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Tuning of photocatalytic activity by creating a tridentate coordination sphere for palladium
PublikacjaThe synthesis and characterisation of an asymmetric potential bridging ligand bmptpphz (bmptpphz = 2,17-bis(4-methoxyphenyl)tetrapyrido[3,2-a:2’,3’-c:3’’,2’’-h:2’’’,3’’’-j] phenazine) is presented. This ligand contains a 1,10-phenanthroline (phen) and a 2,9-disubstituted phen sphere and possesses a strong absorbance in the visible. Facile coordination of the phen sphere to a Ru(tbbpy)2 core leads to Ru(bmptpphz) ([(tbbpy)2Ru(bmptpphz)](PF6)2;...
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Effect of Particle Size of Fly Ash Microspheres (FAMs) on the Selected Properties of Concrete
PublikacjaThis paper presents the investigations of selected properties of concrete containing two fractions of fly ash microspheres (FAMs) with grain size up to 200 μm and up to 500 μm. Concrete mixtures with ordinary Portland cement and three substitution rates of cement by FAMs, 1.3%, 2.0%, and 2.6%, were investigated. For all concrete mixes, the constant water–binder ratio (w/b) equal to 0.50 was used. The research program included the...
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The importance of anchoring ligands of binuclear sensitizers on electron transfer processes and photovoltaic action in dye-sensitized solar cells
PublikacjaThe relatively low photon-to-current conversion efficiency of dye-sensitized solar cells is their major drawback limiting widespread application. Light harvesting, followed by a series of electron transfer processes, is the critical step in photocurrent generation. An in-depth understanding and fine optimization of those processes are crucial to enhance cell performance. In this work, we synthesize two new bi-ruthenium sensitizers...
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Improving osteoblasts cells proliferation via femtosecond laser surface modification of 3D-printed poly-ε-caprolactone scaffolds for bone tissue engineering applications
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$^{93m}$Mo Isomer Depletion via Nuclear Excitation by Electron Capture: Energy Released for Different Atomic Subshells as Benchmarks for a Beam-based Scenario Approach
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N,N’-Bis(salicylidene)ethylenediamine (Salen) as an Active Compound for the Recovery of Ni(II), Cu(II), and Zn(II) Ions from Aqueous Solutions
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Metabolic transformation of antitumor acridinone C-1305 but not C-1311 via selective cellular expression of UGT1A10 increases cytotoxic response: implications for clinical use.
PublikacjaThe acridinone derivates C-1305 and C-1311 are promising antitumor agents with high activity against several experimental cellular and tumor models and which are under evaluation in pre-clinical and early phase clinical trials. Recent evidence from our laboratories has indicated that both compounds were conjugated by several UGT isoforms with the most active being extrahepatic UGT1A10. The present studies were designed to test...
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Scope and limitations of the synthesis of functionalized quinolizidinones and related compounds by a simple precursor approach via addition of lithium allylmagnesates to 2-pyridones and RCM as key steps
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Multi-Analytical Techniques for the Study of Burial Clothes of Polish King Sigismund III Vasa (1566–1633) and His Wife Constance Habsburg (1588–1631)
PublikacjaThe subjects of this research are the burial clothes of Polish King Sigismund III Vasa and his wife Constance, which were woven and embroidered with silk and metal threads. Fragments of the textiles underwent spectroscopic, spectrometric, and thermogravimetric analyses. The hydrofluoric acid extraction method was improved to isolate various classes of dyes from the textile samples that had direct contact with human remains. High-performance...
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1,3-Alternate 25,27-dibenzoiloxy-26,28-bis-[3-propyloxy]-calix[4]arene-bonded silica gel as a new type of HPLC stationary phase
PublikacjaZsyntezowano nową fazę stacjonarną na bazie 25,27-dibenzoiloksy-26,28-bis[3-propyloksy]-kaliks[4]arenu w konformacji 1,3-naprzemianległej, chemicznie związaną z żelem krzemionkowym. Przeprowadzono badanie selektywności i sprawności tej fazy w rozdzielaniu: izomerów pozycyjnych benzenu, zasad purynowych i pirymidynowych oraz niesterydowych leków przeciwzapalnych. Zaprezentowano wyniki badania wpływu warunków chromatograficznych...
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TiO2-C nanocomposite synthesized via facile surfactant-assisted method as a part of less energy-consuming LED-based photocatalytic system for environmental applications
PublikacjaA novel facile method was used to incorporate carbon into the titania structure. An alternative synthesis method of carbon-doped TiO2 has been proposed by using a widely used and cheap surfactant. During the process, cetyltrimethylammonium bromide plays a dual role, as a morphology modifier and as a carbon source. The presented approach allows obtained TiO2-C nanostructures to be anatase nanocrystals with carbon being deposited...
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A novel (Ti/Ce)UiO-X MOFs@TiO2 heterojunction for enhanced photocatalytic performance: Boosting via Ce4+/Ce3+ and Ti4+/Ti3+ redox mediators
PublikacjaTitanium-substituted cerium-oxo-based UiO MOFs with terephthalate linkers modified by various groups (–Br, –NH2, –NO2) or their derivatives (N-heterocyclic or biphenyl groups) were combined with titanium dioxide in a multistep route to obtain a core-shell-like architecture. DFT simulations showed that Ce- and bimetallic Ti/Ce- MOFs exhibited different charge compensation. Extended characterization revealed the formation of heterojunctions between...
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TiO 2 Co x O y composite nanotube arrays via one step electrochemical anodization for visible light–induced photocatalytic reaction
PublikacjaTiO2CoxOy (x = 1, y = 1 or x = 3, y = 4) composite photocatalysts have been synthesized via one step anodic anodization of TiCo alloys. The effects of the cobalt content in the alloy (5, 10 and 15 wt%), water content (2, 5 and 10%) in the electrolyte solution, and applied voltage (30, 40 and 50 V) during the anodization process on the morphology and surface properties. Additionally, the dependence of cobalt content in the nanotubes...
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Analysis of server-side and client-side Web-GIS data processing methods on the example of JTS and JSTS using open data from OSM and geoportal
PublikacjaThe last decade has seen a rapid evolution of processing, analysis and visualization of freely available geographic data using Open Source Web-GIS. In the beginning, Web-based Geographic Information Systems employed a thick-client approach which required installation of platform-specific browser plugins. Later on, research focus shifted to platform-independent thin client solutions in which data processing and analysis was performed...
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A brief note on monotonic and fatigue fracture events investigation of thin-walled tubular austenitic steel specimens via fracture surface topography analysis (FRASTA)
PublikacjaThe main objective of this short communication is to show the fracture progression in each loading case and complement knowledge about fracture mechanisms underpinning the tensile and fatigue performance of thin-walled tubes. For this purpose, the fracture surface topography analysis (FRASTA) method was used in the thin-walled tubular austenitic stainless-steel specimens. Two cases were analyzed: monotonic tension, and uniaxial...
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Synthesis, physicochemical and theoretical studies on new rhodium and ruthenium dimers. Relationship between structure and cytotoxic activity
PublikacjaTwo dimeric compounds of the general formulae (Et3NH)2[Rh2(μ2-L)4Cl2] (1) (where L = thiophene-2-carboxylate) and [((η6-p-cymene)Ru)2(μ-Cl)3]PF6 (2) have been synthesized using a new method. The unique anionic complex 1 (space group P bca) has octahedral coordination in which the equatorial positions are occupied by the oxygen atoms of four thiophene-2-carboxylates in a paddle wheel fashion. In complex 2 (space group ), each Ru(II)...
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Optical Investigation of Hematocrit Level in Human Blood
PublikacjaW artykule przedstawiono możliwości wykorzystania metod optoelektronicznych, takich jak: spektroskopia Ramana i interferometria niskokoherencyjna do pomiaru poziomu hematokrytu ludzkiej krwi.
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Architekturführer Danzig: Gdansk Sopot Gdynia
PublikacjaIm Zweiten Weltkrieg bis auf die Grundmauern zerstört, wurde der historische Stadtkern der Hansestadt Danzig als polnisches Gdańsk wiederaufgebaut – ein Paradebeispiel für kritische Rekonstruktion in Polen und zugleich eine bis heute stark umstrittene Entscheidung. Zusammen mit dem mondänen Seebad Sopot und der modernen Hafenstadt Gdynia bildet die Bernsteinstadt eine Metropolregion an der polnischen Ostseeküste: die Dreistadt...
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Insight into Potassium Vanadates as Visible-Light-Driven Photocatalysts: Synthesis of V(IV)-Rich Nano/Microstructures for the Photodegradation of Methylene Blue
PublikacjaPhotocatalysis is regarded as a promising tool for wastewater remediation. In recent years, many studies have focused on investigating novel photocatalysts driven by visible light. In this study, K2V6O16·nH2O nanobelts and KV3O8 microplatelets were synthesized and investigated as photocatalysts. Samples were obtained via the facile method based on liquid-phase exfoliation with ion exchange. By changing the synthesis temperature...
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Avariâ stal'nogo rezervuara s dvojnoj stenkoj dlâ hraneniâ gorâčih produktov
PublikacjaPodano analizę przyczyn awaryjnych deformacji dwupłaszczowego zbiornika na asfalt magazynowany w temp. +200 C
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Labellum and gynostemium micromorphology in Polystachya (Orchidaceae)
PublikacjaPolystachya is a large, pantropical orchid genus of 200 species, most of which occur as epiphytes in sub-saharan Africa. The three-lobed labellum of most Polystachya species possesses a fleshy callus and various types of trichomes and papillae. In this paper, we present the results of micromorphological studies on the labellum of 20 species, representing eight of the 13 sections in the genus, using scanning electron microscopy...
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Low-Power Receivers for Wireless Capacitive Coupling Transmission in 3-D-Integrated Massively Parallel CMOS Imager
PublikacjaThe paper presents pixel receivers for massively parallel transmission of video signal between capacitive coupled integrated circuits (ICs). The receivers meet the key requirements for massively parallel transmission, namely low-power consumption below a single μW, small area of less than 205 μm2, high sensitivity better than 160 mV, and good immunity to crosstalk. The receivers were implemented and measured in a 3-D IC (two face-to-face...
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Throughput vs. Resilience in Multi-hop Wireless Sensor Networks with Periodic Packet Traffic
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Sensory Characteristics of Tonic Waters with Various Sweetening Substances vs Young Consumers' Opinion
PublikacjaThe attitude of young consumers towards food products containing low calorie sweeteners was analyzed as well as consumers’ awareness to the medical recommendations regarding artificial sweeteners. The questionnaire was carried out within the group of 97 respondents at the age of 21 – 30. Strongly negative attitude towards consumption of food products containing low calorie sweeteners was declared by almost half of respondents....
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Reduction of measurement data before Digital Terrain Model generation vs. DTM generalisation
PublikacjaModern data acquisition technologies provide large datasets that are not always necessary in its entirety to properly accomplish the goal of the study. In addition, such datasets are often cumbersome for rational processing, and their processing is time and labour consuming. Therefore, methods that enable to reduce the size of the measurement dataset, such as the generalization of the Digital Terrain Model (DTM) or the reduction...