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Wyniki wyszukiwania dla: STEAM EJECTOR CONDENSER DIRECT-CONTACT CONDENSATION CFD GAS-LIQUID SEPARATION EHD
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Micellar liquid chromatography for lipophilicity determination of new biologically active 1,3‐purinodiones
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Characteristic of Morpholinium Ionic Liquids as Gas Chromatography Stationary Phases with McReynolds Constants and Activity Coefficients at Infinite Dilution
PublikacjaIn this work, four ionic liquids based on N-alkyl-N-methylmorpholinium cation ([Mor1,R] where R= 2, 4, 8, 10) and bis(trifluoromethanesulfonyl)imide anion [TFSI] were synthesized. Using gas-liquid chromatography a number of parameters describing the sorption properties of the investigated ionic liquids were determined. The values of Kovats indices, McReynolds constants, and activity coefficients at infinite dilution were the basis...
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Towards Cancer Patients Classification Using Liquid Biopsy
PublikacjaLiquid biopsy is a useful, minimally invasive diagnostic and monitoring tool for cancer disease. Yet, developing accurate methods, given the potentially large number of input features, and usually small datasets size remains very challenging. Recently, a novel feature parameterization based on the RNA-sequenced platelet data which uses the biological knowledge from the Kyoto Encyclopedia of Genes and Genomes, combined with a classifier...
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Force-deformation spectroscopy in contact mode
Dane BadawczeThe deformation-distance spectroscopic curve is obtained by registering the value of the probe cantilever deflection as a function of the elongation of the piezoelectric scanner. It assumes a simple relationship in the form of Hooke’s law, linking the deformation of the lever with the amount of its deflection caused by the proximity of the probe and...
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Hold-Up Problems in International Gas Trade: A Case Study
PublikacjaThe infrastructure required for international natural gas trade is considerable, which often leads to hold-up problems and supply disruptions. This study discusses disruptions of gas supply from Algeria, Indonesia, Russia, and Turkmenistan since the early 1980s. The novelty of this study is its focus on the issues related to transit countries, which are rarely considered in the literature. The results of the study classify supply...
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Method of selecting the LS-SVM algorithm parameters in gas detection process
PublikacjaIn this paper we showed the method of resistive gas sensors data processing. The UV irradiation and temperature modulation was applied to improve gas sensors’ selectivity and sensitivity. Noise voltage across the sensor’s terminals (proportional to its resistance fluctuations) was recorded to estimate power spectral density. This function was an input data vector for LS-SVM (least squares – support vector machine) algorithm, which...
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Comparison of target strength (TS) distributions obtained by means of the use of direct and indirect techniques in sea cages
PublikacjaThe aim of this study is to verify the reliability of a processing application developed for the indirect measurement of target strength (TS), with a view to the integration into a single-beam system for its utilization in fish farms. Dorsal and ventral measurements are carried out for gilt-head sea-bream (Spams Aurata) for 5 size classes using a split-beam EK60 echosounder and single-beam data obtained from one of the channels...
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APPLICATION OF ULTRAFAST GAS CHROMATOGRAPHY TO RECOGNIZE ODOR NUISANCE
PublikacjaPotentialities of ultrafast gas chromatography applied to periodical monitoring of odor nuisance originating from a municipal landfill have been examined. The results of investigation on classification of the atmospheric air samples collected in a vicinity of the landfill during winter and summer season have been presented. The investigation was performed using ultrafast gas chromatography of Fast/Flash GC type HERACLES II by Alpha...
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A simplified model of 3-D pipe system conveying flowing liquid
PublikacjaThe paper presents a model reduction technique of a 3-D pipe system with flowing liquid. In the analysis and design of control (mechatronic) systems it is useful to work with simple, low order models. A hybrid reduced order model is proposed. The system model consists of two parts, the modal model and the finite element model.
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Optimisation of pressurised liquid extraction for elimination of sulphur interferences during determination of organotin compounds in sulphur-rich sediments by gas chromatography with flame photometric detection
PublikacjaOpracowano metodę analizy osadów dennych na zawartość związków cynoorganicznych (MBT, DBT, TBT, MPhT, DPhT, TPhT) przy użyciu przyspieszonej ekstrakcji rozpuszczalnikiem i chromatografii gazowej z detektorem płomieniowo-fotometrycznym. Detektor ten pozwala selektywnie wykrywać niewielkie ilości pochodnych cynoorganicznych. Niestety, bardzo często spotykana w osadach siarka oraz jej pochodne zakłócają sygnał detektora. Z tego względu...
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Room temperature ionic liquid-based dispersive liquid–liquid microextraction of uranium in water samples before spectrophotometric determination
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In-Syringe Dispersive Liquid-Liquid Microextraction Coupled with High- Performance Liquid Chromatography for Trace Analysis of Naphthalene Sulfonates in Seawater
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Thermal self-action effects of acoustic beam in a vibrationally relaxing gas
PublikacjaThermal self-action of acoustic beam in a molecular gas with excited internal degrees of molecules’ freedom, is studied. This kind of thermal self-action differs from that in a Newtonian fluid. Heating or cooling of a medium takes place due to transfer of internal vibrational energy. Equilibrium and non-equilibrium gases, which may be acoustically active, are considered. A beam in an acoustically active gas is self-focusing unlike...
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Polypyrrole based gas sensor for ammonia detection
PublikacjaThe nature of polypyrrole response to toxic gases does not allow using the sensor in a conventional way. The main aim of this study is to acquire the information about the concentration using different approaches: a linear approximation, a non-linear approximation and a tangent method. In this paper a two-steps procedure for sensor response measurements has been utilized. Polypyrrole films were electrochemically synthesized on...
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Roadmap on dynamics of molecules and clusters in the gas phase
PublikacjaThis roadmap article highlights recent advances, challenges and future prospects in studies of the dynamics of molecules and clusters in the gas phase. It comprises nineteen contributions by scientists with leading expertise in complementary experimental and theoretical techniques to probe the dynamics on timescales spanning twenty orders of magnitudes, from attoseconds to minutes and beyond, and for systems ranging in complexity...
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Problems of gas detection by resistance fluctuations in gas sensors
PublikacjaPrzedstawiono problemy budowy dystrybutora gazów oraz próbek zapachowych do badań sensorów gazu. Podano układ elektroniczny wykorzystywany do rejestracji fluktuacji rezystancji obserwowany w czujnikach gazu. Załączono przykładowe wyniki obserwacji sygnałów losowych.
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Enantioselective comprehensive two-dimensional gas chromatography of lavender essential oil
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Wavelet Transform Analysis of Temperature Modulated Gas Sensor Response
PublikacjaThe aim of the study was to evaluate whether it is possible to extract the information about the gas concentration despite the influence of humidity. Commercial semiconductor sensor response was examined under the application of a periodic temperature change. The data was collected using measurement protocol for different concentrations of ammonia at specified levels of relative humidity. In this work we focused on the evaluation...
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Modelling of optical components made of liquid crystals and liquid crystalline polymers
PublikacjaW artykule przedstawiono koncepcję wykorzystania ciekłych kryształów i polimerów ciekłokrystalicznych do budowy dwójłomnych elementów optycznych - płytek opóźniających, pryzmatów Wollastona i Nomarskiego. Przedstawiono wyniki modelowania pryzmatów Nomarskiego wykonanych z polimerów ciekłokrystalicznych i dokonano porównania ich właściwości z właściwościami pryzmatów wykonanych z typowych materiałów dwójłomnych.
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Fabrication of the cross-linked PVA/TiO2/C nanocomposite membrane for alkaline direct methanol fuel cells
PublikacjaA crosslinked Poly(vinyl alcohol) based composite membrane was developed through a phase inversion process for use in alkaline direct methanol fuel cells (ADMFCs). The titanium dioxide (TiO2) and carbon nanoparticles (NPs) have been incorporated into the PVA polymer matrix to improve the mechanical and thermal properties. The membrane samples were further modified with maleic acid, a carboxylic acid acting as the cross-linker,...
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Application of Infrared Thermography to Non-Contact Testing of Varistors
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Equilibration Time of Solid Contact Ion-Selective Electrodes
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The reactions occuring on the implant as a result of contact with human tissue
PublikacjaObecnosc implantu w ciele czlowieka powoduje liczne, czesto nieprzewidywalne skutki. Powodem takiej sytuacji jest duza roznorodnosc interakcji materialu medycznego z kontaktujaca sie z nim tkanka. Stwierdzenie to dotyczy glownie oddzialywan i skutkow zachodzacych na poziomie molekularnym w poszczegolnych komorkach kontaktujacej sie tkanki.
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The Rolling Contact Fatigue of PVD Coated Spur Gears
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Probable allergic contact dermatitis mimicking erythema muliforme
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The surface contact characteristics after sliding and rolling burnishing.
PublikacjaW pracy przedstawiono zastosowanie nowej metody SCGC i odpowiedniego programu komputerowego JKC do oceny pomierzonej mikrostereometrii powierzchni części maszyn, głównie na potrzeby kontroli jakości. Na przykładzie powierzchni nagniatanych wykazano cechy nowej metody: wizualizację ułatwiającą wyobrażenie pomierzonej sfery chropowatości, położenie w niej najważniejszych parametrów oceny (rozkład geometrycznej powierzchni kontaktu,...
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Verification of multiband system for non-contact emissivity measurements
PublikacjaW pracy przeprowadzono weryfikację wielopasmowej pasywnej metody pomiaru emisyjności obiektu na drodze eksperymentalnej. W oparciu o zrealizowane stanowisko pomiarowe dokonano pomiarów emisyjności wybranych obiektów. Uzyskano dobrą zgodność wyników pomiarów z wynikami wcześniejszej komputerowej analizy systemu. Potwierdziło to przydatność wielopasmowej metody do pomiaru emisyjności w warunkach roboczych.
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Highly Active TiO2 Microspheres Formation in the Presence of Ethylammonium Nitrate Ionic Liquid
PublikacjaSpherical microparticles of TiO2 were synthesized by the ionic liquid-assisted solvothermal method at different reaction times (3, 6, 12, and 24 h). The properties of the prepared photocatalysts were investigated by means of UV-VIS diffuse-reflectance spectroscopy (DRS), Brunauer–Emmett–Teller (BET) surface area measurements, scanning electron microscopy (SEM), X-ray diffraction analysis (XRD), and X-ray photoelectron spectroscopy...
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An electronic nose based on the semiconducting and electrochemical gas sensors
PublikacjaThe practical application of human nose for fragrance recognition is severely limited by the fact that our sense of smell is subjective and gets tired easily. Consequently, there is a significant need for an instrument that can be a substitution of the human sense of smell. Development of an electronic nose devices is an active area of research starting from pioneering research of Dodd and Persuad in the mid-1980s. Such systems...
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The adaptive spatio-temporal clustering method in classifying direct labor costs for the manufacturing industry
PublikacjaEmployee productivity is critical to the profitability of not only the manufacturing industry. By capturing employee locations using recent advanced tracking devices, one can analyze and evaluate the time spent during a workday of each individual. However, over time, the quantity of the collected data becomes a burden, and decreases the capabilities of efficient classification of direct labor costs. However, the results obtained...
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Experimental determination of dynamic properties of cylindrical steel tank model filled with liquid
PublikacjaIn technical branches, such as chemical or petroleum industries, cylindrical steel tanks are essential structures used for storage of liquid products. Any failure might have disastrous consequences, therefore their safety and reliability is essential. The aim of the present paper is to show the results of the experimental study which has been conducted on a scaled model of a real tank used in Poland. The investigation was carried...
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New Simple and Robust Method for Determination of Polarity of Deep Eutectic Solvents (DESs) by Means of Contact Angle Measurement
PublikacjaThe paper presents a new method for evaluating the polarity and hydrophobicity of deep eutectic solvents (DESs) based on the measurement of the DES contact angle on glass. DESs consisting of benzoic acid derivatives and quaternary ammonium chlorides–tetrabutylammonium chloride (TBAC) and benzyldimethylhexadecylammonium chloride (16-BAC)—in selected molar ratios were chosen for the study. To investigate the DESs polarity, an optical...
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Influence of separation gap on the response of colliding models of steel structures under seismic and paraseismic excitations
PublikacjaAs a result of high urbanization, the need to erect closely-spaced buildings forces designers to consider collisions between structures taking place during ground motions. Experimental and numerical studies have confirmed that such collisions (often referred to as structural pounding) may cause serious damage to the structural elements and even lead to total collapse of colliding structures. The main reason of earthquake-induced...
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Application of ultrasound-assisted solvent extraction of porous membrane packed liquid samples for polyphenols determination in wine samples
PublikacjaPolyphenols play a crucial role in a proper human health maintenance as well as their presence very often correspond to the quality assessment of producs like wine. Thus, their monitoring is of high interest. However, as they occur in a complex matrices their extraction is very often necessary prior the analysis. Herein, a new ultrasound-assisted solvent extraction of porous membrane packed liquid sample technique has been optimized...
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Fluctuation-enhanced scent sensing using a single gas sensor
PublikacjaScent or aroma sensing during aromatherapy can be carried out by applying only a single resistance gas sensor (TGS - Taguchi Gas Sensors). This paper considers the efficiency of detection of essential oils by DC resistance and its fluctuations observed in TGS sensors. A detailed study has been conducted for scents emitted by five popular essential oils using three sensor types (TGS 2600, TGS 2602, TGS 823). The research was focused...
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The application of ultrafiltration for separation of glycerol solution fermented by bacteria
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Separation of CO2 from biogas using absorption columns
PublikacjaBiogaz zawiera ok. 50-70% metanu, 30-40% di tlenku węgla oraz niewielkie ilości innych związków jak siarkowodór czy amoniaku. Dla uzyskania wysokokalorycznego gazu konieczne jest usunięcie ze strumienia di tlenku węgla. Praca opisuje potencjał użycia do tego celu kolumn absorpcyjnych oraz cieczy jonowych jako absorbenta
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The recovery and the separation of metal ions from galvanic wastewaters
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The application of membrane extraction in the separation of zinc and cadmium ions
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Techniques of preparing plant material for chromatographic separation and analysis
PublikacjaArtykuł przedstawia dyskusję na temat technik wykorzystywanych podczas przygotowywania próbek materiału roślinnego do rozdzielania chromatograficznego i analizy. Opisane techniki to: suszenie, homogenizacja, ługowanie, ekstrakcja. Przedstawiono także techniki ekstrakcyjne tj. ekstrakcja z wykorzystaniem ultradźwięków, przyśpieszona ekstrakcja rozpuszczalnikiem, ekstrakcja z wykorzystaniem mikrofal, ekstrakcja z wykorzystaniem rozpuszczalnika...
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Sensitive method for determination of benzoic acid in beverages and food samples using air–assisted hydrophobic deep eutectic solvent-based dispersive liquid-liquid microextraction
PublikacjaA simple, reliable and rapid air–assisted hydrophobic deep eutectic solvent-based dispersive liquid–liquid microextraction (AA-HDES-DLLME) was developed for analysis of benzoic acid in various beverages and food samples. The final determination stage was performed via UV–visible spectrophotometry. The key parameters (extraction time, HDES type and volume, dispersant volume, pH and sample volume) of the AA-HDES-DLLME method were...
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EXPERIMENTAL VERIFICATION OF THE METHOD OF FLOW BOILING AND FLOW CONDENSATION HEAT TRANSFER PREDICTION FOR SELECTED FLUIDS
PublikacjaIn the paper presented are the results of calculations using authors own model to predict heat transfer coefficient during flow boiling of different refrigerants. The experimental data from various research studies from literature were collected. Calculations were conducted for a full range of quality variation and a wide range of mass velocity. The aim of the study was to test the sensitivity of the in- house developed model....
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Early stages of condensation from the gaseous phase in a H2O-N2 system: a molecular dynamics study.
PublikacjaW pracy przedstawiono wyniki symulacji wczesnych etapów kondensacji z fazy gazowej w układzie xH2O (1-x)N2. Przeanalizowano całkowitą liczbę klastrów, średni rozmiar klastra i rozmiar klastra maksymalnego w funkcji czasu.
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Assessment of evaporator tubes corrosion in low-emission steam boilers
PublikacjaW artykule przedstawiono wyniki badań rur ekranowych(16Mo3) kotła niskoemisyjnego po jednym roku i dwóch latach eksploatacji. Powierzchnie rur pokryte zostały warstwami natryskiwanymi cieplne - pojedynczą ze stopu 70%Ni 30%Cr i podwójną Ni-30Cr /Al2O3. Rury bez powłok natryskiwanych wykazywały pocienienie ze względu na działanie korozji siarkowej oraz korozyjnego oddziaływania warstwy stopionych soli. Pojedyncza warstwa 70%Ni 30%Cr...
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Application of Artificial Neural Networks in Investigations of Steam Turbine Cascades
PublikacjaZaprezentowano wyniki badań numerycznych zastosowania sieci neuronowych przy obliczeniach przepływów w palisadach turbin parowych. Na podstawie uzyskanych wyników wykazano, że sieci neuronowe mogą być używane do szacowania przestrzennego rozkładu parametrów przepływu, takich jak entalpia, entropia, ciśnienie czy prędkość czynnika w kanale przepływowym. Omówiono również zastosowania tego typu metod przy projektowaniu palisad, stopni...
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Control of mass concentration of reagents by sound in a gas with nonequilibrium chemical reactions
PublikacjaThe weakly nonlinear dynamics of a chemically reacting gas is studied. Nonlinear interaction of acoustic and nonacoustic types of motion are considered. We decompose the base equations using the relationships of the gas-dynamic perturbations specific for every type of motion. The governing equation for the mass fraction of a reagent influenced by dominating sound is derived and discussed. The conclusions concern the equilibrium...
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Comparison of an Electronic Nose Based on Ultrafast Gas Chromatography, Comprehensive Two-Dimensional Gas Chromatography, and Sensory Evaluation for an Analysis of Type of Whisky
PublikacjaWhisky is one of the most popular alcoholic beverages. There are many types of whisky, for example, Scotch, Irish, and American whisky (called bourbon). The whisky market is highly diversified, and, because of this, it is important to have a method which would enable rapid quality evaluation and authentication of the type of whisky. The aim of this work was to compare 3 methods: an electronic nose based on the technology of ultrafast...
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Application of gas chromatography–tandem mass spectrometry for the determination of amphetamine-type stimulants in blood and urine
PublikacjaAmphetamine, methamphetamine, phentermine, 3,4-methylenedioxyamphetamine (MDA), 3,4-methylenedioxymethamphetamine (MDMA), and 3,4-methylenedioxy-N-ethylamphetamine (MDEA) are the most popular amphetamine-type stimulants. The use of these substances is a serious societal problem worldwide. In this study, a method based on gas chromatography-tandem mass spectrometry (GC-MS/MS) with simple and rapid liquid-liquid extraction (LLE)...
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Simulation of Direct-Sequence Spread Spectrum Data Transmission System for Reliable Underwater Acoustic Communications
PublikacjaUnderwater acoustic communication (UAC) system designers tend to transmit as much information as possible, per unit of time, at as low as possible error rate. It is a particularly difficult task in a shallow underwater channel in which the signal suffers from strong time dispersion due to multipath propagation and refraction phenomena. The direct-sequence spread spectrum technique (DSSS) applied successfully in the latest standards...
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The effects of gas exposure on the graphene/AlGaN/GaN heterostructure under UV irradiation
PublikacjaThis work demonstrates a graphene/AlGaN/GaN sensing device with two-dimensional electron gas (2DEG) toward nitrogen dioxide (NO2), tetrahydrofuran, and acetone detection under UV light irradiation. We propose combining measurements of the DC characteristics with a fluctuation-enhanced sensing method to provide insight into the gas detection mechanisms in the synergistic structure of highly stable GaN and gas-sensitive graphene....