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Cadmium complex possessing simultaneously silanethiolato- and dithiocarbamato-ligands. A novel single-source precursor of cadmium sulfide
PublikacjaThermal decomposition of suitable coordination compounds may be used as efficient route for fabrication of semiconducting layers. A new potential CdS precursor—a cadmium complex with all-sulfur Cd-coordination sphere [Cd{l-SSi(OBut)3}(S2CNC4H8)]2 (1) —has been prepared and its properties are investigated. The complex was obtained in the reaction between dimeric bis(tri-tert-butoxysilanethiolato) cadmium(II) [Cd{SSi(OBut)3}2]2 and...
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Concentrations of alfa- and gamma- tocopherols in human breast milk during the first months of lactation and in infant formulas
PublikacjaThe aim of this study was to determine the concentrations of alpha- and gamma-tocopherols in human breast milk samples from different periods of lactation and to compare them with tocopherol content in commercially available formulas for infants at corresponding ages. The study included 93 breast milk samples obtained on the 2nd (colostrum, n=17), 14th (n=30), 30th (n=27) and 90th day of lactation (n=19), along with 90 samples...
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Application of a commercially available derivatization instrument and commonly used reagents to HPLC on-line determination of antioxidants
PublikacjaThis study demonstrates the potential of a commercially available derivatization instrument coupled with HPLC for separation and on-line determination of antioxidants detected with widely used screening reagents - DPPH (2,2-diphenyl-1-picrylhydrazyl), ABTS (2,2'-azino-bis(3-ethylbenzthiazoline-6-sulphonic acid) or FCR (Folin-Ciocalteu's phenol reagent ). As the result of optimization, key parameters of the analytical procedure,...
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Effect of Individual Components of Lignocellulosic Biomass on Methane Production and Methanogen Community Structure
PublikacjaOne of the major factors that influences the economic feasibility of biogas production is the availability of digestible feedstocks. There is little research on the influence of the chemical composition of biomass on biogas synthesis, especially with regard to the content of lignocellulosic materials. Therefore, the aim of this study was to estimate how differences in the content of cellulose and lignin in lignocellulosic biomass...
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Sample preparation procedure using extraction and derivatization of carboxylic acids from aqueous samples by means of deep eutectic solvents for gas chromatographic-mass spectrometric analysis
PublikacjaThe paper presents a new procedure for the determination of organic acids in a complex aqueous matrixusing ultrasound-assisted dispersive liquid–liquid microextraction followed by injection port derivati-zation and GC–MS analysis. A deep eutectic solvent (choline chloride: 4-methylphenol in a 1:2 mol ratio)was used both as an extracting solvent and as a derivatizing agent to yield ion pairs which were next con-verted to methyl...
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Phosphorus and nitrogen forms in liquid fraction of digestates from agricultural biogas plants
PublikacjaThe novelty of the presented research is the determination of the nitrogen and phosphorus fraction in the liquid fraction of digestate from agricultural biogas plants. This information is important because it can help in proposing possible further liquid fraction management or developing of new technologies for their purification. The research covered digestates from agricultural biogas plants, obtained from the fermentation of...
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MACHINE LEARNING–BASED ANALYSIS OF ENGLISH LATERAL ALLOPHONES
PublikacjaAutomatic classification methods, such as artificial neural networks (ANNs), the k-nearest neighbor (kNN) and selforganizing maps (SOMs), are applied to allophone analysis based on recorded speech. A list of 650 words was created for that purpose, containing positionally and/or contextually conditioned allophones. For each word, a group of 16 native and non-native speakers were audio-video recorded, from which seven native speakers’...
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Processing of acoustical data in a multimodal bank operating room surveillance system
PublikacjaAn automatic surveillance system capable of detecting, classifying and localizing acoustic events in a bank operating room is presented. Algorithms for detection and classification of abnormal acoustic events, such as screams or gunshots are introduced. Two types of detectors are employed to detect impulsive sounds and vocal activity. A Support Vector Machine (SVM) classifier is used to discern between the different classes of...
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Audio-visual surveillance system for application in bank operating room
PublikacjaAn audio-visual surveillance system able to detect, classify and to localize acoustic events in a bank operating room is presented. Algorithms for detection and classification of abnormal acoustic events, such as screams or gunshots are introduced. Two types of detectors are employed to detect impulsive sounds and vocal activity. A Support Vector Machine (SVM) classifier is used to discern between the different classes of acoustic...
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Próba oceny dokładności pomiarów satelitarnych toru kolejowego
PublikacjaW pracy przedstawiono rozwój technik pomiarów satelitarnych GPS, na tle zmieniających się rozwiązań wyznaczania fazowej poprawki pseudoodległościowej. Wskazano na występujące różnice w wykorzystaniu pomiarów RTK z pojedynczej stacji oraz aktywnych sieci geodezyjnych. Na podstawie uzyskanych danych z ok. 40-kilometrowego odcinka linii kolejowej dokonano analizy błędu wyznaczeń współrzędnych sieci ASG-EUPOS, w porównaniu do badań...
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Connected searching of weighted trees
PublikacjaW artykule rozważamy problem spójnego przeszukiwania drzew obciążonych. Autorzy w [L. Barriere i inni, Capture of an intruder by mobile agents, SPAA'02 (2002) 200-209] twierdzą, że istnieje wielomianowy algorytm dla problemu obliczania optymalnej strategii przeszukiwania obciążonego drzewa. W niniejszej pracy pokazano, że problem ten jest obliczeniowo trudny nawet dla wierzchołkowo-obciążonych drzew (wagi krawędzi równe 1) oraz...
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Visible light photoactivity and structure of doped TiO2
PublikacjaOmówiono strukturą i właściwości TiO2 domieszkowanego siarką, węglem oraz borem. Aktywność fotokatalityczna zbadano w reakcji degradacji fenolu pod wpływem światła z zakresu widzialnego (l > 400 nm). Aktywność fotokatalizatorów odniesiono do ich właściwości takich jak powierzchnia właściwa, struktura krystaliczna oraz charakter chemiczny domieszki. Stwierdzono, że fotokatalizatory o najwyższej aktywności mają strukturę anatazu...
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A lower bound on the total outer-independent domination number of a tree
PublikacjaA total outer-independent dominating set of a graph G is a set D of vertices of G such that every vertex of G has a neighbor in D, and the set V(G)D is independent. The total outer-independent domination number of a graph G, denoted by gamma_t^{oi}(G), is the minimum cardinality of a total outer-independent dominating set of G. We prove that for every nontrivial tree T of order n with l leaves we have gamma_t^{oi}(T) >= (2n-2l+2)/3,...
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The cohomological span of LS-Conley index
PublikacjaIn this paper we introduce a new homotopy invariant – the cohomological span of LS-Conley index. We prove the theorems on the existence of critical points for a class of strongly indefinite functionals with the gradient of the form Lx+K(x), where L is bounded linear and K is completely continuous. We give examples of Hamiltonian systems for which our methods give better results than the Morse inequalities. We also give a formula...
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The analysis of raw spirits – a review of methodology
PublikacjaAgricultural distillates (raw spirits) are alc oholic l iquids obtained thro ugh dis till ation (preceded by alcoholic ferm entation)of specific agricultural products that do not have the properties of ethyl alcohol or a spirit, but still retain th e aroma andtaste of the raw ingredients used. This review is a brief overview of agricultural distillates and of some methods commonlyused (GC-MS, GC-FID, GC-O, electronic nose) for...
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Histaminol and Its Complexes with Copper(II) - Studies in Solid State and Solution
PublikacjaHistaminol [4(5)-(B-hydroxyethyl)imidazole, 4-(1H-imidazol-2-yl)ethanol, L] is an analogue of histamine and its minor metabolite. So far its properties have not been studied in detail due to the synthetic difficulties. Here, the structure and acid-base properties of histaminol, as well as the results of studies on its copper(II) complexes in solid state and aqueous solution are reported. Stability constants of the histaminol–CuII...
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Simultaneous detrmination of selected phenoxyacid herbicides and chlorophenols in surface and seawater by HPLC coupled to DAD.
PublikacjaDo badań wykorzystano metodę ekstrakcji do fazy stałej (SPE) w celu wzbogacenia analitów. Ekstrakty analizowano techniką wysokosprawnej chromatografii cieczowej (HPLC) z detekcją DAD. Opracowana metoda umożliwia oznaczenie 14 związków z grupy kwasów fenoksyoctowych i chlorofenoli w czasie 22 min. Odzysk analitów wynosił powyżej 60% dla fenoksykwasów i powyżej 70% w przypadku chlorofenoli. Granica oznaczalności dla oznaczania...
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Effect of WC on electroposition and corossion behaviour of chromium coatings
PublikacjaWłaściwości warstw chromowych zawierających różne ilości drobin WC zbadano metodą XPS, EPS oraz XRD. Metody te pozwoliły określić morfologię i skład chemiczny powłok. Właściwości antykorozyjne określono dla różnych czasów ekspozycji próbek w elektrolicie zawierającym 0,01 mol L-1 za pomocą metody woltamperometrycznej oraz spektroskopii impedancyjnej. Badania wykazały, że obecność WC w warstwach chromowych otrzymanych z kąpieli...
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Raman microscopy in the studies of microphase-separated polyurethanes.
PublikacjaPorównano możliwości badawcze różnych odmian spektroskopowych do analizy po-limerów. Podano przykłądy wykorzystania połączonych technik mikroskopowych ispektroskopowych do badania polimerów wielofazowych. Na tej podstawie wyka-zano zasadność zastosowania po raz pierwszy mikroskopii Ramana w badaniachwielofazowych poliuretanów. Wykazano różnice składu chemicznego poszczegól-nych elementów mikromorfologii wielofazowych, segmentowych...
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Crystal structures of the DsbG disulfide isomerase reveal an unstable disulfide
PublikacjaDsb proteins control the formation and rearrangement of disulfide bonds during the folding of secreted and membrane proteins in bacteria. DsbG, a member of this family, has disulfide bond isomerase and chaperone activity. Here, we present two crystal structures of DsbG at 1.7- and 2.0-Angstrom resolution that are meant to represent the reduced and oxidized forms, respectively. The oxidized structure, however, reveals a mixture...
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An updated method identifying collision-prone locations for ships. A case study for oil tankers navigating in the Gulf of Finland
PublikacjaTo ensure the risk level associated with continuously increasing maritime traffic through particularly sensitive sea areas remains at acceptable level, a periodic risk assessment needs to be carried out by the relevant authorities. As a part of such assessment, allowing for proactive countermeasures to mitigate risk, the frequency of accidents is estimated along with the assessment of geographical locations where the accidents...
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Validation of high-resolution 3D patient QA for proton PBS and IMPT using laser CT of improved polymer gel dosimeters
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3D dose verification with polymer gel detectors of brain-spine match line for proton pencil beam cranio-spinal: A preliminary study
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Assessing therapeutic relevance of biologically interesting, ampholytic substances based on their physicochemical and spectral characteristics with chemometric tools
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Molecular Heteroconjugation Equilibria in (n-Butylamine + Acetic Acid) Systems in Binary (Dimethyl Sulfoxide + 1,4-Dioxane) Solvent Mixtures
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Observation and analysis of transient luminous events in the Earth's atmosphere
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Population modelling of <i>Acartia</i> spp. in a water column ecosystem model for the South-Eastern Baltic Sea
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Continuous Monitoring of Thermooxidative Degradation Products of Polystyrene by Membrane Extraction with Sorbent Interface and Gas Chromatography
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Microdosimetric analysis of response of LiF:Mg,Cu,P (MCP-N) TL detectors for alpha-particles and ultra-high doses of gamma-rays
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Syntheses, structures, and chiroptical and magnetic properties of chiral clusters built from Schiff bases: a novel [MnIIMnIII6NaI2] core
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Thermoluminescent response of differently doped lithium magnesium phosphate (LiMgPO4, LMP) crystals to protons, neutrons and alpha particles
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Artificial neural network model of hardness, porosity and cavitation erosion wear of APS deposited Al2O3 -13 wt% TiO2 coatings
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Flow structure, heat transfer and scaling analysis in the case of thermo-magnetic convection in a differentially heated cylindrical enclosure
PublikacjaThe experimental, numerical and scaling analysis in the case of thermo-magnetic convection in a thermosyphon-like enclosure filled with a paramagnetic fluid is presented. Visualization of temperature field together with the numerical simulation gave an information about the flow structure, which indicated “finger-like” structures of hot and cold streams advecting each other. Their number depended on the Rayleigh number and also...
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Evaluation of possibilities of genotyping of Candida glabrata clinical isolates with RAPD-PCR method and microsatellite analysis
PublikacjaThe aim of the study was to compare the discriminatory power of RAPD-PCR method using RSD10 primer and microsatellite (GACA)4 analysis for genotyping clinical isolates of C. glabrata. Isolates were received from patients of two Polish hospitals: Children's Memorial Health Institute in Warsaw (n=17) and Medical University of Gdansk (n=37). Species identification was confirmed by two phenotypic methods: growth on chromagar plates...
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Measurement of temperature at sliding polymer surface by grindable thermocouples
PublikacjaThis paper is devoted to experimental study of capabilities and limitations of grindable thermocouples as applied to polymer materials sliding on metal. Chromel–alumel and chromel–copel grindable thermocouples have been developed and tested for wide ranges of contact pressure and sliding velocity. The background temperature of the sliding surface can be determined as the lower envelope of the signal from the grindable thermocouple....
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Nanometer structural columns and frustration of magnetic ordering in Nb12O29
PublikacjaDyskutowana jest synteza i właściwości magnetyczne tlenku niobu Nb12O29. Polimorfizm Nb12O29 przejawia się występowaniem dwóch faz: jednoskośnej i ortorombowej. Pomiar podatności magnetycznej pokazuje, że faza jednoskośna wykazuje antyferromagnetyczne przejście ok. 12K.
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Zastosowanie techniki ekstrakcji na fazie stałej (SPE) do zagęszczania wielopierścieniowych węglowodorów aromatycznych z płynów stosowanych w infuzji przy oznaczaniu tych związków techniką HPLC z detektorem fluorescencyjnym i diodowym
PublikacjaPraca zawiera metodykę przygotowania próbki oraz procedurę analityczną oznaczania obecności wielopierścieniowych węglowodorów aromatycznych (WWA) w płynach infuzyjnych stosowanych do wlewów dożylnych dla ludzi oraz wyniki badań stężeń tych węglowodorów w płynach stosowanych do infuzji oraz w stosowanych do produkcji płynów infuzyjnych - substancjach farmaceutycznych. W płynach do infuzji stwierdzono 0,2-7,6 ng/l Benzo(a)pirenu,...
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Marcinkiewicz Averages of Smooth Orthogonal Projections on Sphere
PublikacjaWe construct a single smooth orthogonal projection with desired localization whose average under a group action yields the decomposition of the identity operator. For any full rank lattice \Gamma ⊂ R^d , a smooth projection is localized in a neighborhood of an arbitrary precompact fundamental domain R^d / \Gamma. We also show the existence of a highly localized smooth orthogonal projection, whose Marcinkiewicz average under the...
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Inexpensive Helical Antenna for Global Navigation Satellite Systems
PublikacjaZaprezentowane zostały wyniki badań teoretycznych oraz eksperymentalnych niskobudżetowej anteny na pasmo L. Wyjściowa geometria struktury została obliczona na podstawie ogólnych wzorów. Efekt przesunięcia częstotliwości wywołany przez użycie rdzenia PU został również uwzględniony. Równolegle przeprowadzono badania wrażliwości parametrów anteny na proces produkcji. Zaprojektowano i wykonano układ dopasowania impedancyjnego. W paśmie...
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Sterowanie silnikiem asynchronicznym w układzie zamkniętym z filtrem wyjściowym falownika napięcia
PublikacjaW artykule przedstawiono zamknięty układ sterowania silnikiem asynchronicznym klatkowym pracujący bez pomiaru prędkości obrotowej przy zasilaniu z falownika napięcia z filtrem wyjściowym. Filtr wyjściowy falownika stanowi układ zawierający elementy bierne L, C , R umieszczone między falownikiem a silnikiem, które wprowadzają do układu spadek napięcia oraz powoduje występowanie przesunięcia fazowego prądów i napięć na wejściu i...
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Quasi-resonant DC-link voltage inverter with enhanced zero-voltage switching control
PublikacjaA new topology modification of the parallel quasi-resonant circuit for a dc-link voltage inverter enables regulation of the zero voltage dc-link subperiods and the dc-link voltage gradient settings. The proposed circuit is based on four MOSFET switches with free-wheeling diodes for controlled quasi-resonant recharging between L-C tank in order to assure inverter zero voltage switching (ZVS) conditions. Design optimization of the...
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Application of Headspace Solid-phase Microextraction with Poly(1-vinyl-3- Hexylimidazolium Chloride) Polymeric Ionic Liquid Coating using GC - MS to Determine Volatile Fatty Acids in Dairy Wastewater
PublikacjaVolatile fatty acids were determined in this study using headspace solid-phase microextraction (HS-SPME) with a poly(1-vinyl-3-hexylimidazolium chloride) polymeric ionic liquid coated fiber followed by gas chromatography - mass spectrometry. Experimental parameters such as extraction time and temperature, sample volume as well as desorption time and temperature were optimized. Detection limits of the method were in the range of...
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Pompy satelitowe
PublikacjaW artykule opisano budowę oraz wyniki badań pompy satelitowej będące efektem zrealizowanego w latach 2007 - 2010 projektu badawczo-rozwojowego nr R0300103. Badania prowadzono z wykorzystaniem oleju, wody i emulsji HFA-E. Przedstawione w artykule wyniki badań dotyczą strat objętościowych, mechanicznych, ciśnieniowych oraz poziomu hałasu emitowanego przez pompę. Laboratoryjne badania trwałościowe pomp satelitowych są jednym z zadań...
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Finding small-width connected path decompositions in polynomial time
PublikacjaA connected path decomposition of a simple graph $G$ is a path decomposition $(X_1,\ldots,X_l)$ such that the subgraph of $G$ induced by $X_1\cup\cdots\cup X_i$ is connected for each $i\in\{1,\ldots,l\}$. The connected pathwidth of $G$ is then the minimum width over all connected path decompositions of $G$. We prove that for each fixed $k$, the connected pathwidth of any input graph can be computed in polynomial-time. This answers...
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Expermental investigation on adsorption of methylene blue dye from waste water using corncob cellulose-based hydrogel
PublikacjaHydrogel from corncob cellulose was synthesized in this investigation. The synthesized Hydrogel was characterized by SEM, XRD, and FTIR instruments. As the results indicate the synthesized hydrogel has required and important features, these suggest the suitability of hydrogel for the adsorption of methylene blue dye (MBD). Three important process variables (dosage, contact time, and initial concentration) with three levels were...
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Arctic catchment as a sensitive indicator of the environmental changes: distribution and migration of metals (Svalbard)
PublikacjaArctic regions experience metal pollution, despite their remote location, and the distribution and migration of those metals determine their potential impact on the local environment. Here, a High-Arctic catchment (Revelva, Svalbard) located remotely from human-induced pollution sources is studied with respect to the distribution and migration of chosen trace elements (Ag, Al, As, B, Ba, Bi, Ca, Cd, Co, Cr, Cu, Cs, Mo, Ni, Pb,...
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Overcoming carboxylic acid inhibition by granular consortia in high-load liquefied food waste fermentation for efficient lactate accumulation
PublikacjaGranular sludge, a self-aggregating spherical biofilm, possesses better stability compared to flocculent sludge under extreme conditions. This study compared the ability of anaerobic granular sludge (AnGS) and flocculent waste activated sludge (WAS) to convert food waste (FW) into highly-valuable optically active lactic acid (LA), a central and versatile intermediate platform molecule. Different loadings (30–60 g volatile suspended...
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Sonocatalytic degradation of Bisphenol A from aquatic matrices over Pd/CeO2 nanoparticles: Kinetics study, transformation products, and toxicity
PublikacjaIn this work, different ratios of palladium – cerium oxide (Pd/CeO2) catalyst were synthesized and characterized, while their sonocatalytic activity was evaluated for the degradation of the xenobiotic Bisphenol A (BPA) from aqueous solutions. Sonocatalytic activity expressed as BPA decomposition exhibited a volcano-type behavior in relation to the Pd loading, and the 0.25Pd/CeO2 catalyst characterized by the maximum Pd dispersion...
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Chemistry of non-precipitation components of wet deposition with Poland as an example
PublikacjaW pracy przedstawiono badania dotyczące chemizmu osadów atmosferycznych pobieranych na terenie Polski w okresie od 2004 do 2007 roku. Średni skład jonowy (TIC) dla rosy, szronu i mgły (w stanie ciekłym i stałym) wynosił odpowiednio 2147, 1929 i 1014 µeq/l, gdzie typowy skład jonowy TIC dla opadów atmosferycznych wynosi 318 µeq/l. Dla wszystkich typów osadów atmosferycznych różne jony pełnią ważną rolę: Ca2+ i SO42-...
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Seasonal changes in organotin compounds in water and sediment samples from the semi-closed Port of Gdynia
PublikacjaThe effect of seasonal changes on the distribution of organotin compounds (OTC) in the sediments and seawaterfrom the docks of the Port of Gdynia was investigated. Sediment and seawater samples were collectedfrom four industrial docks in February (winter) and June (summer) in 2009. The samples were analyzed forbutyltin, phenyltin, octyltin, and tricyclohexyltin (total of 9 OTC derivatives). The fine fraction (b0.063 mm)accumulated...