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Application and optimization of headspace solid-phase microextraction (HS-SPME) coupled with gas chromatography - flame-ionization detector (GC-FID) to determine products of the petroleum industry in aqueous samples
PublikacjaA simple and solvent-free analytical method has been optimized for the determination of hydrocarbons (C6 - C20) from products of the petroleum industry in aqueous samples. Extraction and analysis was carried out using headspace solid-phase microextraction (HS-SPME) and gas chromatography coupled with flame-ionization detector (GC-FID). A ZB-5 capillary column (30 m × 0.25 mm inner diameter, 0.25 µm film thickness) was used for...
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A New Type of Macro-Elements for Efficient Two-Dimensional FEM Analysis
PublikacjaThis letter deals with a model order reduction technique applicable for driven and eigenvalue problems solved using the finite element method (FEM). It allows one to efficiently compute electromagnetic parameters of structures comprising small features that require strong local mesh refinement. The subdomains of very fine mesh are separated from the global domain as so called macro-elements that undergo model reduction. The macro-elements...
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Thermoplastic polyurethanes derived from petrochemical or renewable resources: A comprehensive review
PublikacjaThermoplastic polyurethanes (TPUs) materials are obtained by the reaction of polyol (ether-, ester-, and carbonate-based diols with average molecular weight in the range from 1,000 to 3,000 g/mol) with aliphatic or aromatic diisocyanates. Synthesized materials consist of the hard and soft segments which are separated in different level. All mechanical and thermal properties of TPUs depend on the chemical structure of used monomers,...
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Estimation of fracture toughness and shear yield stress of orthotropic materials in cutting with rotating tools
PublikacjaThe cutting force is an energetic effect of splitting material, and might be considered from a point of view of modern fracture mechanics. Forecasting of the shear plane angle in cutting broaden possibilities for modelling of the cutting process even for thin uncut chips. Such mathematical model has been developed here for description of the orthotropic materials’ cutting on the base of fracture theory, and includes work of separation...
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Implicit Space Mapping for Variable-Fidelity EM-Driven Design of Compact Circuits
PublikacjaSpace mapping (SM) belongs to the most successful surrogate-based optimization (SBO) methods in microwave engineering. Among available SM variations, implicit SM (ISM) is particularly attractive due to its simplicity and separation of extractable surrogate model parameters and design variables of the circuit/system at hand. Unlike other SM approaches, ISM exploits a set of preassigned parameters to align the surrogate with the...
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Thermal-FSI modeling of flow and heat transfer in a heat exchangerbased on minichanels
PublikacjaIn this paper selected numerical modelling problems for an advanced thermal-FSI ("Fluid Solid Interaction") mini-channel heat exchanger model are presented. Special attention is given to the heat transfer between the separated mediums for different mass flows. Similar modelling problems have also been discussed in the literature dedicated to numerical and theoretical modelling problems for typical heat exchangers [1, 2, 3]. Basic...
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Computer-aided evaluation of the railway track geometry on the basis of satellite measurements
PublikacjaIn recent years, all over the world there has been a period of intensive development of GNSS (Global Navigation Satellite Systems) measurement techniques and their extension for the purpose of their applications in the field of surveying and navigation. Moreover, in many countries a rising trend in the development of rail transportation systems has been noticed. In this paper, a method of railway track geometry assessment based...
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A Multi-Antenna Scheme for Early Detection and Mitigation of Intermediate GNSS Spoofing
PublikacjaThis article presents a method for detecting and mitigating intermediate GNSS spoofing. In this type of attack, at its early stage, a spoofer transmits counterfeit signals which have slight time offsets compared to true signals arriving from satellites. The anti-spoofing method proposed in this article fuses antenna array processing techniques with a multipath detection algorithm. The latter is necessary to separate highly correlated...
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Enzymatic activities behind degradation of glucosinolates
PublikacjaMyrosinase (thioglucosidase, EC 3.2.1.147) is the enzyme responsible for the hydrolysis of glucosinolates (GLs). In plant tissue, myrosinase and GLs are sequestered in separate cellular compartments. As a result of cell disruption, e.g., after pathogen attack or on chopping or grinding during food preparation, the myrosinase comes into contact with GLs and catalyzes the hydrolysis of thioglucosidic bond in GL structure. Consequently,...
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Application of the discrete Green's function-based antenna simulations for excitation of the total-field/scattered-field interface in the FDTD method
PublikacjaIn this article, the discrete Green's function formulation of the finite-difference time-domain (DGF-FDTD) method is proposed for simulation of wire antennas irradiating inhomogeneous dielectric scatterers. Surface equivalence theorem in the discrete domain is used to separate the problem into an inhomogeneous domain and a wire antenna that are simulated with the use of FDTD and DGF-FDTD, respectively. Then, the excitation of the...
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Study of preference for surround microphone techniques, used in the recording of choir and instrumental ensemble
PublikacjaThe aim of this paper is to describe the process of choosing the best surround microphone technique for recording of choir with an instrumental ensemble. First, examples of multichannel microphone techniques including those used in the recording are described. Then, the assumptions and details of music recording in Radio Gdansk Studio are provided as well as the process of mixing of the multichannel recording. The extensive subjective...
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Hybrid Technique Combining the FDTD Method and Its Convolution Formulation Based on the Discrete Green's Function
PublikacjaIn this letter, a technique combining the finite-difference time-domain (FDTD) method and its formulation based on the discrete Green's function (DGF) is presented. The hybrid method is applicable to inhomogeneous dielectric structures that are mutually coupled with wire antennas. The method employs the surface equivalence theorem in the discrete domain to separate the problem into a dielectric domain simulated using the FDTD method...
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Running performance of an aerodynamic journal bearing with squeeze film effect
PublikacjaResults of theoretical and experimental studies concerning the performance of an aerodynamic journal bearing of which running is assisted by squeeze film ultrasonic levitation (SFUL) are presented in this paper. The SFUL mechanism not only can separate journal from the bearing at the start and stop phases of operation but also can significantly contribute to the dynamic stability of the bearing when it runs at speed. Computer calculations...
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A tool for integrating Web Site services over User Interface
PublikacjaCompanies and organizations are building information systems by integrating previously independent applications, together with new developments. This integration process has to deal with existing applications, which can only be used through their specific interfaces, and often cannot be modified. Integration of web applications running remotely and controlled by separate organizations becomes even more complicated, as their user...
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Reliable low-cost surrogate modeling and design optimisation of antennas using implicit space mapping with substrate segmentation
PublikacjaAbstract: In this work, a reliable methodology for fast simulation-driven design optimisation of antenna structures is proposed. The authors’ approach exploits implicit space mapping (ISM) technology. To adopt it for handling antenna structures, they introduce substrate segmentation with separate dielectric permittivity value assigned for each segment as ISM preassigned parameters. At the same time, the coarse model for space mapping...
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A spatio-temporal approach to intersectoral labour and wage mobility
PublikacjaThe article presents the spatio-temporal approach for intersectoral labor and wage mobility. Analyses of interindustry mobility were performed with the use of general entropy mobility indices (GEMM). Spatio- temporal approach was obtained thanks to the separate measurement of spatial autocorrelation and regression for each set of sectoral wage and employment structure and was conducted in each year of the research period separately....
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A Spatio-temporal Approach to Intersectoral Labour and Wage Mobility
PublikacjaThe article presents the spatio-temporal approach for intersectoral labor and wage mobility. Analyses of interindustry mobility were performed with the use of general entropy mobility indices (GEMM). Spatio-temporal approach was obtained thanks to the separate measurement of spatial autocorrelation and regression for each set of sectoral wage and employment structure and was conducted in each year of the research period separately....
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Classifying type of vehicles on the basis of data extracted from audio signal characteristics
PublikacjaThe aim of this study is to find and optimize a feature vector for an automatic recognition of the type of vehicles, extracted form an audio signal. First, the influence of weather-based conditions of road surface on spectral characteristic of the audio signal recorded from a passing vehicle in close proximity to the road is discussed. Next, parameterization of the recorded audio signal is performed. For that purpose, the MIRtoolbox,...
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Investigations on strength and fracture in RC beams scaled along height or length
PublikacjaThe objective of the present paper is to identify experimentally and theoretically differing failure mechanisms in reinforced concrete beams subjected to four-point bending for a separate variation of the depth and length at the constant thickness. Experiments were performed on reinforced concrete beams under four-point bending. Different failure mechanisms included steel yielding, diagonal tension or shear- compression depending...
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The Characteristics of New SSB Proteins from Metagenomic Libraries and Their Use in Biotech Applications
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Czas inżynierów
PublikacjaKażdego roku budowlane wydziały politechnik krajowych organizują coraz bardziej atrakcyjne wydarzenia, na które składają się seminaria, konferencje naukowe, prezentacje firm, a także wzbudzające najwięcej emocji konkursy konstruktorskie. Nasza Alma Mater szczyci się od wielu lat cyklicznym konkursem „wyKOMBinuj mOst” organizowanym przez Koło Naukowe Mechaniki Budowli KOMBO (Katedra Mechaniki Budowli i Mostów, Wydział Inżynierii...
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Sztuczna słodzycz wokół nas
PublikacjaSyntetyczne słodziki o dużej mocy słodzącej stanowią ważną klasę dodatków do żywności, które są szeroko stosowane w przemyśle spożywczym. Główną cechą tych zwykle niskokalorycznych środków jest bardzo intensywny słodki smak. Producenci żywności, mając na uwadze osiągnięcie lepszych doznań smakowych, stosują coraz to nowe typy słodzików bądź ich różne mieszaniny. Zapotrzebowanie na żywność z substancjami słodzącymi nieustannie rośnie....
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Synthesis, characterization, and application of 2D/2D TiO2-GO-ZnFe2O4 obtained by the fluorine-free lyophilization method for solar light-driven photocatalytic degradation of ibuprofen
PublikacjaIn this study, we report the potential of 2D/2D TiO2- GO-ZnFe2O4 photocatalyst obtained using the fluorine-free lyophilization technique for the degradation of ibuprofen belonging to the group of active pharmaceutical ingredients (API). The improved ibuprofen degradation under simulated solar light was achieved in the presence of a composite of 2D TiO2 combined with GO and embedded ZnFe2O4, which additionally provides superparamagnetic...
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Femtosecond Er-doped fiber laser source tunable from 872 to 1075 nm for two-photon vision studies in humans
PublikacjaWe report the development of a widely-tunable femtosecond fiber laser system and its application for two-photon vision studies. The source is based on an Er-doped fiber laser with spectral shift up to 2150 nm, followed by a second harmonic generation module to generate a frequency-doubled beam tunable from 872 to 1075 nm. The source delivers sub-230 fs pulses with nearly-constant duration over the entire tuning range, with output...
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Determinants of Directionality and Efficiency of the ATP Synthase Fo Motor at Atomic Resolution
PublikacjaFo subcomplex of ATP synthase is a membrane-embedded rotary motor that converts proton motive force into mechanical energy. Despite a rapid increase in the number of high-resolution structures, the mechanism of tight coupling between proton transport and motion of the rotary c-ring remains elusive. Here, using extensive all-atom free energy simulations, we show how the motor’s directionality naturally arises from the interplay...
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Low-power microwave-induced fabrication of functionalised few-layer black phosphorus electrodes: A novel route towards Haemophilus Influenzae pathogen biosensing devices
PublikacjaIn this paper, various passivation schemes were applied at few-layer black phosphorus (FLBP) to achieve covalent functionalisation with 4-azidobenzoic acid, improving its electrochemical response intended for analytical and biosensing applications. The thermal and microwave assisted modification procedures in toluene and dime-thylformamide resulted in high reversibility of reactions on functionalised FLBP using a ferricyanide/ferrocya-nide...
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Baseline-free debonding detection in reinforced concrete structures by elastic wave propagation
PublikacjaThe article presents the results of the numerical and experimental analysis concerning wave propagation in reinforced concrete (RC) beams with various extent of debonding between the steel rod and concrete cover. The main aim of the paper was to consider the unsolved research gaps, which considerably limit the application of wave-based methods in practice. The propagation of the flexural wave modes excited and registered on the...
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Mass Spectrometry-Based Direct Analytical Techniques
PublikacjaDirect analysis of samples is considered as one of the most environmentally sustainable solutions in analytical chemistry. In the ideal case, such solutions do not require sample preparation and analytes separation steps, therefore do not consumpt harmful substances (or consumpt only minimum amounts of them) and do not generate hazardous waste. Technical solutions for direct analysis also offer miniaturized and field-portable analyzers...
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Effect of the Catalytic Center on the Electron Transfer Dynamics in Hydrogen-Evolving Ruthenium-Based Photocatalysts Investigated by Theoretical Calculations
PublikacjaThe light-induced relaxation pathways in the molecular photocatalyst [(tbbpy)2Ru(tpphz)PtCl2]2+ are investigated with time-dependent density functional theory calculations together with the Marcus theory of electron transfer (ET). The calculations show that metal (Ru) to ligand (tpphz) charge transfer (MLCT) triplet states are populated following an excitation in the longer wavelength range of the absorption spectrum, but that an...
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The Laboratory Stand for the Evaluation of Heat Dissipation from the Power Cable in a Casing Pipe
PublikacjaThe current carrying capacity of a power cable determines its efficiency, which depends on its capability to dissipate heat produced inside the cable, as a result of current flow, into the surrounding. The studies were conducted to determine how the characteristics of the medium around the cable affected its temperature and, as a result, its ability to transport electricity. The experimentation in the lab and real measurements...
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Reducing common mode voltage and bearing currents in quasi - resonant DC - link inverter
PublikacjaIn the paper, a concept of separation of an inverter-fed induction motor drive from its mains supply by two transistor switches inserted in the dc-link circuit is reexamined based on the proposed parallel quasi-resonant dc-link inverter (PQRDCLI). The objective of the paper is to show an advantage of the proposed topology in limiting high frequency common mode voltage and bearing currents. In the laboratory setup, an induction...
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Economics of credit scoring management
PublikacjaCredit scoring models constitute an inevitable element of modern risk and profitability management in retail financial lending institutions. Quality,or separation power of a credit scoring model is usually assessed with the Gini coefficient. Generally, the higher Gini coefficient the better, as in this way a bank can increase number of good customers and/or reject more bad applicants. In...
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Metal-Organic Framework (MOF)/Epoxy Coatings: A Review
PublikacjaEpoxy coatings are developing fast in order to meet the requirements of advanced materials and systems. Progress in nanomaterial science and technology has opened a new era of engineering for tailoring the bulk and surface properties of organic coatings, e.g., adhesion to the substrate, anti-corrosion, mechanical, flame-retardant, and self-healing characteristics. Metal-organic frameworks (MOFs), a subclass of coordinative polymers...
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Segmented bio-based polyurethane composites containing powdered cellulose obtained from novel bio-based diisocyanate mixtures
PublikacjaA considerable number of research works focus on the positive influence of cellulose on the properties of polymer-based composites and their wide range of application possibilities. The present work is focused on the synthesis of novel bio-based polyurethane (bio-PU) composites filled with powdered cellulose (microcellulose, MC) in an amount of 5 wt.%. Bio-PU composites were synthesized via a non-solvent prepolymer method. First,...
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Determination of parent and methylated polycyclic aromatic hydrocarbons in water samples by dispersive liquid–liquid microextraction–two dimensional gas chromatography–time-of-flight mass spectrometry
PublikacjaPolycyclic aromatic hydrocarbons (PAHs) are contaminants frequently found in environmental waters. Owing to their toxic effects, it is important to develop analytical methodologies that allow their fast and reliable determination. Dispersive liquid–liquid microextraction (DLLME) allows a quick extraction of analytes with little organic solvent consumption. The best results regarding sample preparation are obtained when 40 mL of...
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Application of normal-phase high-performance liquid chromatography followed by gas chromatography for analytics of diesel fuel additives
PublikacjaThe paper presents the results of investigations on new procedures of determination of selected cleaning additives in diesel fuel. Two procedures: one-step analysis using gas chromatography with flame ionization detection (GC-FID) or mass spectrometry (GC-MS) and a two-step procedure in which normal-phase high-performance liquid chromatography (NP-HPLC) was used for preliminary separation of the additives, were compared. The additive...
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Pounding between Inelastic Three-Storey Buildings under Seismic Excitations
PublikacjaStructural interactions between adjacent, insufficiently separated buildings have been repeatedly observed during damaging ground motions. This phenomenon, known as the structural pounding, may result in substantial damage or even total collapse of structures. The aim of the present paper is to show the results of the nonlinear numerical analysis focused on pounding between inelastic three-storey buildings under seismic excitations....
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Porosity and swelling properties of novel polyurethane–ascorbic acid scaffolds prepared by different procedures for potential use in bone tissue engineering
PublikacjaIn this work, a novel polyurethane (PU) system based on poly(ethylene-butylene) adipate diol, 1,6-hexamethylene diisocyanate, 1,4-butanediol, and ascorbic acid was used to prepare scaffolds with potential applications in bone tissue engineering. Two fabrication methods to obtain porous materials were chosen: phase separation (PS)/salt particle leaching (PL) and solvent casting (SC)/salt PL. The calculated porosity demonstrated...
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The effect of polyamide PA12 and polyester PBT blocks' lengths on the structure and propertries of multiblock terpoly(amide-block-ester-block-amide) (TPAEA)
PublikacjaThe ternary multiblock system terpoly(amide-b-ester-b-amide) (TPAEA) of the chemical structure: poly[(oligoamide-6.36)-block-(tetramethylene terephthalate)-block-laurolactam)] -(PA6.36-b-PBT-b-PA12)n- has been obtained (Table 1). In this system the third component (PBT block here), characterized with the proper molecular weight, is dissolved in hard phase of PA12 blocks and partially dissolved in soft phase of PA6.36. The effects...
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SAWING PROCESS AS A NEW ALTERNATIVE WAY OF DETERMINING SOME WOOD PROPERTIES
PublikacjaCutting forces (power) could be considered from a point of view of modern fracture mechanics. The developed cutting model, derived from fracture mechanics, includes work of separation (fracture toughness) in addition to plasticity and friction, and also dullness of the cutting edge described by the cutting edge radius. Moreover, forecasting of the shear plane angle for the cutting models, broaden possibilities of energetic effects...
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Partial Admission Stages of High Efficiency for a Microturbine
PublikacjaThe paper presents the results of a design analysis of a microturbine for a cogeneration micro-power plant working in accordance with organic Rankine cycle. The heat power of the plant is assumed equal to 20kW and the corresponding available electric output is estimated to be about 3 kW. After the design analysis, the axial turbine with partial admission in all stages was built and tested experimentally. Special attentionwas paid...
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Video Semantic Analysis Framework based on Run-time Production Rules - Towards Cognitive Vision
PublikacjaThis paper proposes a service-oriented architecture for video analysis which separates object detection from event recognition. Our aim is to introduce new tools to be considered in the pathway towards Cognitive Vision as a support for classical Computer Vision techniques that have been broadly used by the scientific community. In the article, we particularly focus in solving some of the reported scalability issues found in current...
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Information content of systems as a physical principle
PublikacjaTo explain the conceptual gap between classical and quantum and other, hypothetical descriptions of the world, several principles have been proposed. So far, all these principles have not explicitly included the uncertainty relation. Here we introduce an information content principle ( ICP ) which represents a constrained uncertainty principle. The principle, by taking into account the encoding and decoding properties of a single physical...
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Vegetable derived-oil facilitating carbon black migration from waste tire rubbers and its reinforcement effect
PublikacjaThree dimensional chemically cross-linked polymer networks present a great challenge for recycling and reutilization of waste tire rubber. In this work, the covalently cross-linked networks of ground tire rubber (GTR) were degraded heterogeneously under 150 °C due to the synergistic effects of the soybean oil and controlled oxidation. The degradation mechanism was discussed using Horikx theory and Fourier transformation infrared...
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Simultaneous determination of individual isothiocyanates in plant samples by HPLC-DAD-MS following SPE and derivatization with N-acetyl-l-cysteine
PublikacjaThe procedure for the isothiocyanates (ITCs) determination that involves derivatization with N-acetyl-l-cysteine (NAC) and separation by HPLC was developed. Prior to derivatization, plant ITCs were isolated and purified using solid-phase extraction (SPE). The optimum conditions of derivatization are: 500 μL of isopropanolic eluate obtained by SPE combined with 500 μL of derivatizing reagent (0.2 M NAC and 0.2 M NaHCO3 in water)...
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WYBRANE WŁAŚCIWOŚCI FIZYCZNO-CHEMICZNE MIKROSFER I MOŻLIWOŚĆ ICH WYKORZYSTANIA W KOMPOZYTACH CEMENTOWYCH : The selected physico-chemical properties of microspheres and possibility of their use in cement composites
PublikacjaMicrospheres are formed during the mineral transformation stage in coal combustion. Their content in fly ashes from the combustion of different types of coals varies over a rather wide range from 0.01 to 4.8 wt.%. The microspheres have three main elements, silicon, aluminum and iron, the oxides of which account for about 89.0 wt.% of the material. Mineralogical analysis using XRD shows that microspheres mainly contain mullite and...
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Partial Admission Stages of High Efficiency for a Microturbine
PublikacjaThe paper presents the results of a design analysis of a micro-turbine for a co-generation micro-power plant working in accordance with organic Rankine cycle. The heat power of the plant is assumed equal to 20kW and the corresponding available electric output is estimated to be about 3kW. After the design analysis, the axial turbine with partial admission in all stages was built and tested experimentally. Special attention was...
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Linear viscoelastic modelling of damage-involved structural pounding during earthquakes
PublikacjaDamage-involved structural pounding during earthquakes has been recently intensively studied using different impact force models. The results of the previous studies indicate that the linear viscoelastic model is relatively simple yet accurate in modelling pounding-involved behaviour of structures during earthquakes. The only shortcoming of the model is a negative value of the pounding force occurring just before separation, which...
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Ultrasound assisted extraction
PublikacjaThe use of green and sustainable extraction techniques is very popular topic in the multidisciplinary area of chemistry, biology and technology. There is no doubt that extraction constitutes a very important step of analytical procedures of separation, detection, identification and determination of wide spectrum analytes from samples characterized by complex and very often nonhomogeneous composition of matrix. Traditional techniques...
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Spectral Clustering Wikipedia Keyword-Based search Results
PublikacjaThe paper summarizes our research in the area of unsupervised categorization of Wikipedia articles. As a practical result of our research, we present an application of spectral clustering algorithm used for grouping Wikipedia search results. The main contribution of the paper is a representation method for Wikipedia articles that has been based on combination of words and links and used for categoriation of search results in this...