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Wyniki wyszukiwania dla: HDI
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Chiral Schiff base complexes as an effective catalyst in Diels-Alder reaction
PublikacjaDiels Alder reaction is a very important tool in carbon-carbon bond formation. It is a cycloaddition between a conjugated diene and a second compound called dienophile. Where one or more heteroatoms are present in the diene and/or dienophile framework, the cycloaddition is called hetero-Diels-Alder reaction (HDA). The asymmetric Diels-Alder reaction is among the most powerful available methodologies for that construction of optically...
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Niching mechanisms in evolutionary computations
PublikacjaDozorowanie nisz stanowi mechanizm, którego celem jest utrzymanie gorzej przystosowanych osobników tak, aby populacja była różnorodna, zawierała odpowiednią liczbę istniejących gatunków, zarówno tych bardziej licznych, jak i tych mniej licznych, a przez to nie powodowała przedwczesnej zbieżności algorytmów ewolucyjnych. Efekt taki uzyskuje się poprzez odpowiednią modyfikację stopnia przystosowania lub rang osobników (zwiększa się...
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Effects of Urea and Trimethylamine-N-oxide on the Properties of Water and the Secondary Structure of Hen Egg White Lysozyme
PublikacjaW celu określenia sposobu hydratacji mocznika i N-tlenku trimetyloaminy, wykorzystano spektroskopię oscylacyjną FTIR. Dane eksperymentalne, otrzymane z pomiarów widm oscylacyjnych wody półciężkiej (HDO) rozcieńczonej izotopowo w wodnych roztworach badanych związków, analizowane były za pomocą "metody widm różnicowych". Strukturalno-energetyczna charakterystyka wody zaburzonej przez cząsteczki osmolitów wskazuje, że woda zaburzona...
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Synthesis, structure and properties of poly(ether-urethane)s synthesized using a tri-functional oxypropylated glycerol as a polyol
PublikacjaThe main aim of this work was to obtain poly(ether-urethane)s using tri-functional polyoxyalkylene polyol (Rokopol G1000), which introducing the chemical cross-links into the structure of polyurethanes. Poly(ether-urethane)s were prepared using two-step method, called prepolymer method, which involves in the first step the reaction of 4,4'-diphenylmethane diisocyanate (MDI) and tri-functional polypropylene glycol glycerol triether...
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Synthesis and characterisation of polyurethane elastomers with semi-products obtained from polyurethane recycling
PublikacjaIn this work polyurethane elastomers were synthesised by using different mixtures of a petrochemical and glycerolysate polyols and 4,4-diphenylmethane diisocyanate (MDI). Glycerolysate polyol was produced from polyurethane foam decomposition using crude glycerine as a decomposition agent. The structure and thermal properties of obtained semi-product were similar to the polyol used in the synthesis of original foam. Glycerolysate...
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Evaluation of the glycerolysis process and valorisation of recovered polyol in polyurethane synthesis
PublikacjaIn this study, the glycerolysis of polyurethane (PU) foam and the applicability of obtained glycerolysate (GLY) for cast PUs were investigated. It was found that crude glycerine with purity grade of 84% might be successfully used for the glycerolysis. The optimal conditions were determined as follows: reaction time of 60 min at 220 °C using dibutyltin dilaurate catalyst (0.5%). Moreover, the purification of GLY by means of liquid-liquid...
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Bio polyetherurethane composites with high content of natural ingredients: hydroxylated soybean oil based polyol, bio glycol and microcrystalline cellulose
PublikacjaIn our study, we focused on obtaining bio-polyurethane composites using bio-components such as bio glycol, modified natural oil-based polyol, and microcrystalline cellulose (MCC). The pre-polymer method was used to prepare the bio polyurethane matrix. Prepolymer was synthesized using 4,4’-diphenylmethane diisocyanate (MDI) and a polyol mixture containing 50 wt.% of commercial polyether and 50 wt.% of hydroxylated soybean oil (H3)....
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Thermoplastic polyurethanes with glycolysate intermediates from polyurethane waste recycling
PublikacjaThe polyol is a major component in polyurethane formulations and therefore introducing to the formulation recycled polyol (obtained during decomposition process) allows decreasing the usage of pure petrochemical components. In this work, thermoplastic polyurethanes were prepared using various mixtures of a petrochemical macrodiol poly(ethylene-butylene adipate)diol (PEBA) and a recycled glycolysate intermediate, called glycolysate...
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GIUSEPPE VOLPI. IL GRANDE MEDIATORE TRA ISTITUZIONI, POLITICA ED ECONOMIA
PublikacjaGiuseppe Volpi di Misurata represented a mediation point between different interests both in the economic field and in the complex national – but also regional and local – political balance that long underpinned the fascist regime. This article intends to revisit this figure between the 1920s and the Second World War. The attempt will be made to identify, through an approach that will be chronological and thematic, the passages...
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Bi-based halide perovskites: Stability and opportunities in the photocatalytic approach for hydrogen evolution
PublikacjaIn this study, we successfully prepared Bi-based single perovskites of the A3Bi2I9 type (A = Cs, Rb, MA, FA), and, for the first time, attempted to experimentally obtain double perovskites Cs2B’BiI6 type (B′ = Ag, Au, In, Cu). Despite the premises available in theoretical studies, our research has proven the impossibility of the existence of double perovskites of this type. Nevertheless, both types of obtained materials were subjected...
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Induced circularly polarized luminescence for revealing DNA binding with fluorescent dyes
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Symmetry-Dependent Vibrational Circular Dichroism Enhancement in Co(II) Salicylaldiminato Complexes
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A framework for risk matrix design: A case of MASS navigation risk
PublikacjaRisk matrix, a tool for visualizing risk assessment results, is essential to facilitate the risk communication and risk management in risk-based decision-making processes related to new and unexplored socio-technical systems. The use of an appropriate risk matrix is discussed in the literature, but it is overlooked for emerging technologies such as Maritime Autonomous Surface Ships (MASS). In this study, a comprehensive framework...
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Advanced Bayesian study on inland navigational risk of remotely controlled autonomous ship
PublikacjaThe arise of autonomous ships has necessitated the development of new risk assessment techniques and methods. This study proposes a new framework for navigational risk assessment of remotely controlled Maritime Autonomous Surface Ships (MASS). This framework establishes a set of risk influencing factors affecting safety of navigation of a remotely-controlled MASS. Next, model parameters are defined based on the risk factors, and...
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Programowo-sprzętowa platforma symulacyjna - Hardware In the Loop - zaawansowanego układu sterowania poziomem wody w pionowej wytwornicy pary elektrowni jądrowej
PublikacjaW artykule przedstawiono koncepcję programowo-sprzętowej platformy symulacyjnej wykorzystującej technikę symulacji w pętli sprzętowej HIL (ang. Hardware In The Loop simulation), wykorzystanej dla potrzeb projektowania i weryfikacji w czasie rzeczywistym (ang. Real Time) zaawansowanych algorytmów sterowania poziomem wody w pionowej wytwornicy pary elektrowni jądrowej. Jej głównymi elementami są: środowisko czasu rzeczywistego Matlab/Simulink...
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Programowo-sprzętowa platforma symulacyjna - Hardware In the Loop - zaawansowanego układu sterowania poziomem wody w pionowej wytwornicy pary elektrowni jądrowej
PublikacjaW artykule przedstawiono koncepcję programowo-sprzętowej platformy symulacyjnej wykorzystującej technikę symulacji w pętli sprzętowej HIL (ang. Hardware In The Loop simulation), wykorzystanej dla potrzeb projektowania i weryfikacji w czasie rzeczywistym (ang. Real Time) zaawansowanych algorytmów sterowania poziomem wody w pionowej wytwornicy pary elektrowni jądrowej. Jej głównymi elementami sa: środowisko czasu rzeczywistego Matlab/Simulink...
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Structure, morphology and mechanical behaviour of novel bio-based polyurethane composites with microcrystalline cellulose
PublikacjaThe aim of this work was to obtain bio-based polyurethane composites using biocomponents such as, bio-glycol, modified natural oil-based polyol, and microcrystalline cellulose (MCC). The prepolymer method was used to prepare the bio-based polyurethane matrix. Prepolymer synthesised from 4,4’-diphenylmethane diisocyanate (MDI) and a polyol mixture containing 75% wt. commercial polyether and 25% wt. hydroxylated soybean oils (H3)...
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Banking concentration in the Baltic and Western Balkan states — selected issues
PublikacjaResearch background: In a rapidly changing economic environment companies deepen their cooperation, which entails in all sectors of the economy. The progressive increase in market concentration, especially in the banking sector, is caused by various reasons. Purpose of the article: The purpose of this article is to compare the tendencies within market structures in few countries which origin from similar political systems and...
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Synteza, struktura chemiczna i właściwości bezizocyjanianowych poliuretanów otrzymywanych z wykorzystaniem CO2 oraz surowców pochodzenia naturalnego.
PublikacjaZ uwagi na wciąż rosnącą świadomość proekologiczną, politykę zrównoważonego rozwoju, a także nurt zielonej chemii wiodącym trendem w przemyśle tworzyw sztucznych jest poszukiwanie alternatywnych metod otrzymywania materiałów polimerowych. Komercyjnie poliuretany otrzymywane są w wyniku reakcji poliaddycji di- lub poliizocyjanianów z poliolami i małocząsteczkowymi przedłużaczami łańcucha. Z uwagi na niekorzystne właściwości diizocyjanianów,...
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Transport deficiency is the molecular basis of Candida albicans resistance to antifungal oligopeptides
Publikacja(FMDP), an inhibitor of glucosamine-6-phosphate synthase, exhibited growth inhibitory activity against Candida albicans, with minimal inhibitory concentration values in the 0.05–50 mg/L range. Uptake by the peptide permeases was found to be the main factor limiting an anticandidal activity of these compounds. Di- and tripeptide containing FMDP (F2 and F3) were transported by Ptr2p/Ptr22p peptide transporters (PTR) and FMDP-containing...
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A wireless network for off-shore marine research
PublikacjaThis paper presents functionality, the most important technology developments and potential use cases of digital communication system, developed to facilitate selected tasks commonly required during off-shore operations and marine research, including: broadband information sharing between platforms isolated from an on-shore communication infrastructure, acquisition of large data-sets from variety of off-shore...
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Remote command and control capabilities for data acquisition systems provided by delay-tolerant network mechanisms
PublikacjaThe paper presents an assessment of a remote device reconfiguration service employing a Delay Tolerant Network (DTN) mechanisms. This service has been implemented as a part of a communication appliance dedicated to marine data transfer in off-shore and open sea areas. The service has been successfully deployed and validation test have been completed. The practical use-case has been defined as remote access to the equipment operating...
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Hidden Champions of Poland
PublikacjaPoland is a country with a strong entrepreneurial spirit. The hidden champions’ performance has been closely related to political and economic changes: the fall of communism in 1989 and the transition from a centrally planned economy to a market economy. This led to the emergence of small private businesses focused on the domestic market. The accession to the European Union in 2004 created new perspectives for the hidden champions’...
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Mechanical Properties, Microstructure and Surface Quality of Polypropylene Green Composites as a Function of Sunflower Husk Waste Filler Particle Size and Content
PublikacjaAgricultural waste is a still untapped source of materials that can, in case of proper utilization, significantly improve the sustainability of polymers and their composites. In this work, polymer composites based on isotactic polypropylene were produced incorporating ground sunflower husk in the amount of 10 wt% and 20 wt%. The work’s main objective is to evaluate how preliminary fractioning of this agricultural waste filler affects...
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Detekcja i lokalizacja przecieków w rurociągach przemysłowych.
PublikacjaZadanie monitorowania przepływu mediów ciekłych lub gazowych przez rurociągi przemysłowe realizuje się za pomocą algorytmów obserwacji, skonstruowanych odpowiednio do nieliniowego modelu procesu transportowego, z zastosowaniem pomiarów ciśnienia i natężenia przepływu medium na krańcach nadzorowanego odcinka rurociągu. Uwagę skupiono na dwu metodach analitycznej redundancji i filtracyjnej generacji sygnału resztowego, będącego...
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Detection and localization of leaks in transmission pipelines
PublikacjaZadanie monitorowania przepływu mediów ciekłych lub gazowych przez rurociągiprzemysłowe realizuje się za pomocą algorytmów obserwacji, skonstruowanychodpowiednio do nieliniowego modelu procesu transportowego, z zastosowaniempomiarów ciśnienia i natężenia przepływu medium na krańcach nadzorowanegoodcinka rurociągu. Uwagę skupiono na dwu metodach analtycznej redundancji ifiltracyjnej generacji sygnału resztowego, będącego...
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STUDY ON THE RELATIONSHIP BETWEEN VEHICLE MAINTENANCE AND FUEL CONSUMPTION
PublikacjaA contemporary road vehicle (RV) is a rather complex system, consisting of a large number of subsystems, assemblies, units, and elements (parts). While operating, an RV interacts with the environment, and its elements interact with each other. Consequently, the properties (parameters) of these elements change in the process - hardness, roughness, size, relative position, gapping, etc. A partial solution to the presented problems...
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The changes of crosslink density of polyurethanes synthesised with using recycled component. Chemical structure and mechanical properties investigations.
PublikacjaThis paper aims at the utilisation of glycerolysate (Gly) obtained in polyurethane recycling process by means of crude glycerine, which has in its structure hydroxyl end groups that allow for further processing. Polyurethanes (PUs) were synthesised using prepolymer method with the mixture of neat polyol and glycerolysate, in different ratios, with 4,4-diphenylmethane diisocyanate (MDI). The prepolymer was subsequently extended...
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Refurbishment of a historical building - design issues
PublikacjaOver a 10-year modernization of the main building of Gdansk University of Technology is coming to the end. The ever increasing number of students requires not only the development of the campus with new facility buildings, also the existing buildings are subject to adaptation and modernization. In addition to high-impact solutions, as restoring the former glory of the building (reconstruction of the clock tower), or introducing...
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Amides as models to study the hydration of proteins and peptides — spectroscopic and theoretical approach on hydration in various temperatures
PublikacjaInteractions with water are one of the key factors which determine protein stability and activity in aqueous solutions. However, the protein hydration is still insufficiently understood. N-methylacetamide (NMA) is regarded as a minimal part of the peptide backbone and the relative simplicity of its structure makes it a good model for studies on protein–water interactions. In this paper, the influence of NMA and N,N-dimethylacetamide...
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Carbon nanowalls: A new versatile graphene based interface for laser desorption/ionization-mass spectrometry detection of small compounds in real samples.
PublikacjaCarbon nanowalls, vertically aligned graphene nanosheets, attract attention owing to their tunable band-gap, high conductivity, high mechanical robustness, high optical absorbance and other remarkable properties. In this paper, we report for the first time, the use of hydrophobic boron-doped carbon nanowalls (CNWs) for laser desorption/ionization of small compounds and their subsequent detection by mass spectrometry (LDI-MS). The...
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Polyhydric SiO2 coating assistant to graft organophosphorus onto glass fabric for simultaneously improving flame retardancy and mechanical properties of epoxy resin composites
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N-alkyl derivatives of 2-amino-2-deoxy-D-glucose
PublikacjaMono- i di-N-alkilowe pochodne 1,3,4,6-tetra-O-acetylo-2-amino-2-deoksy-beta-D-glukozy (alkil = metyl, etyl, propyl, butyl, pentyl, heksyl, benzyl) otrzymano w wyniku redukcyjnej alkilacji per-O-acetylo-D-glukozaminy. (N-etylo, N-propylo, N-butylo, N-pentylo, N-heksylo)-1,3,4,6-tetra-O-acetylo-2-amino-2-deoksy-beta-D-glukozy deacetylowano w celu podjęcia prób enzymatycznej fosforylacji. Wszystkie produkty scharakteryzowano za pomocą...
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NUMERICAL SIMULATIONS OF GAP FLOW ABOVE ROTATING DISK
PublikacjaA rotating disk can be considered a basic configuration for the investigati ons of the impact of various conditions on the flow through the clearance between the s hrouded turbine blade and the casing. Numerical calculations using Fine/Turbo Numeca were conducted to examine the influence of the rotational velocity and the pressure differ ence across the disk on the flow conditions, especially the mass flow through the clearance....
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L'economia mondiale dopo la guerra fredda
PublikacjaChe cosa è successo negli equilibri economici mondiali a partire dal 1989 e dalla dissoluzione del vecchio ordine sovietico? Dopo aver esaminato gli Usa e i suoi competitori asiatici, Giappone e Cina, il libro si concentra sull’Europa e sulle grandi trasformazioni portate dalla riunificazione tedesca, da Maastricht e dalla nascita dell’euro. Infine analizza, nell’ambito della globalizzazione, il ruolo dei BRICS, lo sviluppo economico...
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Advanced XAS analysis for investigating fuel cell electrocatalysts
PublikacjaW pracy została zaprezentowana analiza XAFS nanocząstek platyny używanych jako materiał katalityczny w niskotemperaturowych ogniwach paliwowych. Analiza danych EXAFS została przeprowadzona za pomocą zaawansowanej metody GNXAS, w której wzięto pod uwagę rozkład rozmiaru granul nano-platyny i niejednorodność warstwy katalitycznej elektrody, badane za pomocą SEM (skaningowy mikroskop elektronowy), TEM (transmisyjny mikroskop elektronowy)...
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Performance of a fuel cell optimized for in situ X-ray absorption experiments
PublikacjaKomercyjna komórka ogniwa paliwowego typu PEM została zmodyfikowana w celu realizacji pomiaru XAS w warunkach pracy ogniwa. Modyfikacja komórki miała na celu optymalizację jej parametrów pod kątem eksperymentu XAS realizowanego w modzie transmisyjnym i fluorescencyjnym, poprzez minimalizację absorpcji komórki, przy zachowaniu jej parametrów elektrochemicznych. W pracy zostały zaprezentowane szczegóły techniczne komórki a jej efektywność...
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The bismuth atom neighbourhood in bismuth-silicate glasses from X-ray absorption experiment
PublikacjaPraca zawiera wyniki strukturalnej analizy EXAFS lokalnego otoczenia atomów bizmutu w krystalicznym tlenku bizmutu (odmiana alfa) i w szklach bizmutowo-krzemianowych o składzie xBi2O3 (1-x)SiO2,x=0.3, 0.4, 0.5, 0.6. Analizę XA- FS realizowano w oparciu o metodę GNXAS. Otrzymane wyniki porównano z danymi literaturowym.
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Using contextual conditional preferences for recommendation taska: a case study in the movie domain
PublikacjaRecommendation engines aim to propose users items they are interested in by looking at the user interaction with a system. However, individual interests may be drastically influenced by the context in which decisions are taken. We present an attempt to model user interests via a set of contextual conditional preferences. We show that usage of proposed preferences gives reasonable values of the accuracy and the precision even when...
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Nano-structured Pt embedded in the acidic salts of heteropolymolybdate matrices: MS XAFS study
PublikacjaMultiple-scattering extended X-ray absorption fine structure (MS EXAFS) study combined with TEM and XRD analysis of a novel Pt-based catalyst operating at low temperature fuel cells (FCs) is presented. Innovation in the case of the considered catalyst resides in the use of a porous inorganic matrix of acidic heteropolymolybdate salts as a catalyst support. Obtained results show the relation between the matrix composition and the...
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Rating Prediction with Contextual Conditional Preferences
PublikacjaExploiting contextual information is considered a good solution to improve the quality of recommendations, aiming at suggesting more relevant items for a specific context. On the other hand, recommender systems research still strive for solving the cold-start problem, namely where not enough information about users and their ratings is available. In this paper we propose a new rating prediction algorithm to face the cold-start...
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Modification of Ground Tire Rubber—Promising Approach for Development of Green Composites
PublikacjaGround tire rubber (GTR) was mechano-chemically modified using a road bitumen 100/150 and two types of organic peroxides: di-(2-tert-butyl-peroxyisopropyl)-benzene (BIB) and dicumyl peroxide (DCP). The impact of used additives on reactive sintering efficiency and physico-mechanical properties of modified GTR was investigated using oscillating disc rheometer measurements, followed by tensile tests and swelling behavior studies....
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Cyfrowy akcelerator wybranych modułów standardu kompresji wideo H.264
PublikacjaW komunikacie przedstawiono konfigurowalny cyfrowy akcelerator estymacji ruchu (motion estimation) przeznaczony dla enkodera wideo standardu H.264. Akcelerator został wstępnie zaimplementowany w układzie FPGA VIRTEX6-VLX365T, a następnie w układzie ASIC w technologii UMC 90 nm. Obie implementacje zostały zweryfikowane pozytywnie, a szczegółowe wyniki symulacji i pomiarów akceleratora ASIC zostały porównane z innymi dostępnymi w...
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Indirect Measurement of Motor Current Derivatives in PMSM Sensorless Drives
PublikacjaMotor current derivatives contain useful information for control algorithms, especially in sensorless electric drives. The measurement of motor current derivatives in electric motors supplied by voltage source inverter can be performed using di/dt transducers. However, in such a solution additional sensors have to be installed, e.g. Rogowski coils. Another approach is to measure current derivatives indirectly – by oversampling...
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On the complex formation of iron(III) bromide in the space-demanding solvent N,N'-dimethylpropyleneurea and the structure of the trisbromoiron(III) complex i solution and crystalline state
PublikacjaPrzeprowadzono badania kalorymetryczne równowag kompleksów koordynacyjnych jonu żelaza(III) z jonami bromkowymi w DMPU. Stwierdzono, że w DMPU powstają trzy: mono-, di- i tribromkowe kompleksy żelaza(III) a ich powstawanie jest uwarunkowane zmianą entropii. Badania krystalograficzne dowiodły, że FeBr3 w roztworze DMPU ma konfigurację płaskiego trójkąta równobocznego, żadna cząsteczka rozpuszczalnika nie jest związana z jonem metalu,...
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Renewable natural resources as green alternative substrates to obtain bio-based non-isocyanate polyurethanes-review
PublikacjaCommercially available polyurethanes are synthesized by the polyaddition of diisocyanates with polyols and low molecular weight chain extenders. A new approach to polyurethanes synthesis is realized via non-isocyanate routes. Negative impacts of petroleum-based chemicals on the environment and human health as well as gradual reduction of fuel-based resources, which leads to an increase in their prices, are an incentive to looking...
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Intelligent system supporting diagnosis of malignant melanoma
PublikacjaMalignant melanomas are the most deadly type of skin cancers. Early diagnosis is a key for successful treatment and survival. The paper presents the system for supporting the process of diagnosis of skin lesions in order to detect a malignant melanoma. The paper describes the development process of an intel-ligent system purposed for the diagnosis of malignant melanoma. Presented sys-tem can be used as a decision support system...
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Numerical simulation of temperature distribution of heat flow on reservoir tanks connected in a series
PublikacjaThe flow of temperature distribution through a medium in thermodynamic studies plays an important role in understanding physical phenomena in chemical science and petroleum engineering, while temperature distribution indicates the degree of reaction that must be undergone to obtain the final product. Therefore, this paper aims to present and apply the exponential matrix algorithm (EMA), differential transformation algorithm (DTA),...
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MOLECULAR SIMULATIONS OF NEOCARZINOSTATIN CHROMOPHORE RELEASE MECHANISM
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Molecular simulations study of ligand-release mechanism in an odorant-binding protein from the southern house mosquito
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