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Wyniki wyszukiwania dla: FT-MIR
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Influence of sintering temperature of porous SrTi0.65Fe0.35O3-d oxygen electrode on electrochemical impedance spectroscopy spectra measured at 800 °C
Dane BadawczeThis dataset contains results electrochemica impedance spectroscopy (EIS) of symmetrical cells with porous SrTi0.65Fe0.35O3-d oxygen electrodes sintered at different temperatures (800 °C; 900 °C and 1000 °C). Measure temperature was 800 °C (syntetic air, 40 ml min-1). Results converted to electrode surfaces area and dived by two electrodes.
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The TEC measurement of LSCNT (dilatometry) in air
Dane BadawczeThe dataset includes dilatometry results for La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s measured in air from 100 to 800C using Netzsch DIL 402 PC.
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Circulating miRNA profiles and the risk of hemorrhagic transformation after thrombolytic treatment of acute ischemic stroke: a pilot study
PublikacjaBackground: Hemorrhagic transformation (HT) in acute ischemic stroke is likely to occur in patients treated with intravenous thrombolysis (IVT) and may lead to neurological deterioration and symptomatic intracranial hemorrhage (sICH). Despite the complex inclusion and exclusion criteria for IVT and some useful tools to stratify HT risk, sICH still occurs in approximately 6% of patients because some of the risk factors for this...
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Decomposition kinetics of vanadium xerogel powder
Dane BadawczeThe DataSet contains the TGA curves of vanadium As-prepared xerogel powder with different heating rates. The information about sol synthesis is described in the Journal of Nanomaterials.
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Deposition and characterization of organic polymer thin films using a dielectric barrier discharge with different C2Hm/N2 (m = 2, 4, 6) gas mixtures
PublikacjaOrganic polymer thin films have been deposited on Si(100) and aluminum coated glass substrates by a dielectric barrier discharge (DBD) operated at medium pressure using different C2Hm/N2 (m = 2, 4, 6) gas mixtures. The deposited films were characterized by various spectroscopic techniques. Fourier transform infrared reflection absorption spectroscopy (FT-IRRAS) revealed the chemical functional groups present in the films. The surface...
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Dobór kształtu widma sygnału UWB IR do aktualnego stanu zajętości widma elektromagnetycznego
PublikacjaReferat przedstawia praktyczne zasady stosowania metod modyfikacji widma sygnału radia impulsowego do poprawy warunków międzysystemowej kompatybilności elektromagnetycznej. Zaprezentowano przykład doboru kryteriów zmian widma UWB do rzeczywistego stanu zajętości widma elektromagnetycznego występującego na terenie trójmiasta.
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Authentication of whisky due to its botanical origin and way of production by instrumental analysis and multivariate classification methods
PublikacjaHeadspacemass-spectrometry (HS-MS), mid infrared (MIR) and UV–vis spectroscopywere used to authenticate whisky samples from different origins and ways of production ((Irish, Spanish, Bourbon, TennesseeWhisky and Scotch). The collected spectra were processed with partial least-squares discriminant analysis (PLS-DA) to build the classification models. In all cases the five groups ofwhiskieswere distinguished, but the best resultswere...
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Music Mood Visualization Using Self-Organizing Maps
PublikacjaDue to an increasing amount of music being made available in digital form in the Internet, an automatic organization of music is sought. The paper presents an approach to graphical representation of mood of songs based on Self-Organizing Maps. Parameters describing mood of music are proposed and calculated and then analyzed employing correlation with mood dimensions based on the Multidimensional Scaling. A map is created in which...
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Facile synthesis of accordion-like porous carbon from waste PET bottles-based MIL-53(Al) and its application for high-performance Zn-ion capacitor
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Zastosowanie analizy szeregów czasowych do oceny zanieczyszczenia powietrza atmosferycznego w rejonie Trójmiasta. Application of time series analysis on air quality assessment in the region of Tricity
PublikacjaNa podstawie analizy wyników pomiarów poziomów stężenia: NO3-, SO42-, F- ,Cl-, NH4+, PO43-, Ca2+, K+, Mg2+ oraz pomiarów pH i przewodności elektrolitycznej próbek wód opadowych na terenie Trójmiasta z zastosowaniem techniki analizy szeregów czasowych wykazano, że cykliczne wahania poziomów depozycji SO42-, F-, NO3- i Ca2+ w próbkach są skorelowane z cyklicznymi 9 zmianami przeważających kierunków wiatrów. Analiza struktury szeregów...
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Use of Near Infrared Transillumination/Back Scattering Sounding (NIR-T/BSS) to assess effects of elevated intracranial pressure on width of subarachnoid space and celebrovascular pulsation in animals
PublikacjaW pracy dokonano ocenę zmiany szerokości przestrzeni podpajęczynówkowej i tętnienia naczyń mózgowych w czasie chwilowego zwiększenia ciśnienia śródczaszkowego u królików doświadczalnych. Badania zostały przeprowadzone przy wykorzystaniu metody transiluminacji w bliskiej podczerwieni z rozpraszaniem zwrotnym NIRT-BSS.
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An air-assisted dispersive liquid phase microextraction method based on a hydrophobic magnetic deep eutectic solvent for the extraction and preconcentration of melamine from milk and milk-based products
PublikacjaIn the current research, a fast and sustainable air-assisted hydrophobic magnetic deep eutectic solvent-based dispersive liquid phase microextraction followed by UV–Vis spectrophotometry measurements was optimized for the extraction and determination of melamine in milk and milk-based products. The central composite design was applied for the optimization of factors affecting the recovery of melamine. Quantitative extraction of...
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Crystallization kinetics of V2O5 nanorods
Dane BadawczeThe DataSet contains the DSC curves of As-prepared xerogel powder with different heating rates. The information about sol synthesis is described in the Journal of Nanomaterials.
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Jakub Szczepański prof. dr hab. inż. arch.
OsobyJakub Szczepański jest profesorem nadzwyczajnym na Wydziale Architektury Politechniki Gdańskiej, a od 2016 r. prodziekanem ds. nauki. Architekt, historyk architektury i konserwator zabytków. Jego badania koncentrują się na historii i architekturze Gdańska i miast Regionu Bałtyckiego, a także konserwacji dziedzictwa architektury osadzonych w problematyce współczesnych miast. Równolegle z pracą naukową na Politechnice Gdańskiej...
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Studies on novel BiyXz-TiO2/SrTiO3 composites: Surface properties and visible light-driven photoactivity
PublikacjaA series of novel BiyXz-TiO2/SrTiO3 composites were prepared by multistep synthesis route. The asprepared photocatalysts were characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), diffuse reflectance spectroscopy (DRS), Fourier transform infrared (FT-IR), Raman spectra and BET analysis. The photocatalytic activity test was performed in aqueous solution of phenol under...
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Extractive detoxification of hydrolysates with simultaneous formation of deep eutectic solvents
PublikacjaThe hydrolysis of lignocellulosic biomass results in the production of so-called fermentation inhibitors, which reduce the efficiency of biohydrogen production. To increase the efficiency of hydrogen production, inhibitors should be removed from aqueous hydrolysate solutions before the fermentation process. This paper presents a new approach to the detoxification of hydrolysates with the simultaneous formation of in-situ deep eutectic...
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Potentiometric sensor with lipid-polymer membranes for quality assessment of French red wines
PublikacjaThe quality of wines resulting from vineyard management is important for consumers due to the taste and price of wines. In this work, the quality of red wines of three vintages has been investigated by potentiometric sensors with six all-solid-state electrodes. Two series of experiments were carried out. The first involved a qualitative analysis of wine of different vintages from freshly opened bottles. The second consisted of...
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Thermogravimetric measurement (TG) of 10 wt.% Ce0.8La0.2O2-NiO-YSZ anode for DIR-SOFC
Dane BadawczeThe daataset includes the thermogravimetric measurement (TG) of Ce0.8La0.2O2-NiO-YSZ anode for DIR-SOFC. The mesurement was performed under synthestic air atmosphere. The anode was composed of NiO-YSZ cermet composite (90 wt%) and Ce0.8La0.2O2-s additive (10wt%) with the addition of poroformer - PMMA granules 8um diameter (40 vol.% of whole powder volume)....
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Thermogravimetric measurement (TG) of 20wt.% Ce0.8La0.2O2-NiO-YSZ anode for DIR-SOFC
Dane BadawczeThe daataset includes the thermogravimetric measurement (TG) of Ce0.8La0.2O2-NiO-YSZ anode for DIR-SOFC. The mesurement was performed under synthestic air atmosphere. The anode was composed of NiO-YSZ cermet composite (80 wt%) and Ce0.8La0.2O2-s additive (20wt%) with the addition of poroformer - PMMA granules 8um diameter (40 vol.% of whole powder volume)....
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Electrochemical impedance spectroscopy spectra measured at 700 °C on porous SrTi0.30Fe0.70O3-d oxygen electrodes sintered at different temperatures
Dane BadawczeThis dataset contains results electrochemica impedance spectroscopy (EIS) of symmetrical cells with porous SrTi0.30Fe0.70O3-d oxygen electrodes sintered at different temperaturs (800 °C, 900 °C and 1000 °C). EIS spectra were measured at 700 °C with synthetic air flow (21% O2, 40 ml min-1). Results converted to electrode surfaces area and dived by two...
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Electrochemical impedance spectroscopy spectra measured at 700 °C on porous SrTi0.65Fe0.35O3-d oxygen electrodes sintered at different temperatures
Dane BadawczeThis dataset contains results electrochemica impedance spectroscopy (EIS) of symmetrical cells with porous SrTi0.65Fe0.35O3-d oxygen electrodes sintered at different temperaturs (800 °C, 900 °C and 1000 °C). EIS spectra were measured at 700 °C with synthetic air flow (21% O2, 40 ml min-1). Results converted to electrode surfaces area and dived by two...
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Electrochemical impedance spectroscopy spectra measured at 700 °C on porous SrTi0.50Fe0.50O3-d oxygen electrodes sintered at different temperatures
Dane BadawczeThis dataset contains results electrochemica impedance spectroscopy (EIS) of symmetrical cells with porous SrTi0.50Fe0.50O3-d oxygen electrodes sintered at different temperaturs (800 °C, 900 °C and 1000 °C). EIS spectra were measured at 700 °C with synthetic air flow (21% O2, 40 ml min-1). Results converted to electrode surfaces area and dived by two...
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Structure and Molecular Dynamics in Renewable Polyamides from Dideoxy-Diamino Isohexide
PublikacjaThe chemical structure, the conformation, andthe flexibility of the polymer chain fragments present in thepolyamides synthesized from 2,5-diamino-2,5-dideoxy-1,4;3,6-dianhydrosorbitol, 1,4-diaminobutane, and either sebacic orbrassylic acid have been studied by liquid-state 2D NMRspectroscopy viz. correlation spectra (COSY) and heteronuclearmultiple-bond correlation spectra (gHMBC), by 13Ccross-polarization/magic-angle spinning...
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Obtaining and Characterization of the PLA/Chitosan Foams with Antimicrobial Properties Achieved by the Emulsification Combined with the Dissolution of Chitosan by CO2 Saturation
PublikacjaA new method of obtaining functional foam material has been proposed. The materials were created by mixing the poly lactic acid (PLA) solution in chloroform, chitosan (CS) dissolved in water saturated with CO2 and polyethylene glycol (PEG), and freeze-dried for removal of the solvents. The composite foams were characterized for their structural (SEM, FT-IR, density, porosity), thermal (DSC), functional (hardness, elasticity, swelling...
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Superconductivity and appearance of negative magnetocaloric effect in Ba1–xKxBiO3 perovskites, doped by Y, La and Pr
PublikacjaRecently, substantial attention is given to the bismuth-based perovskites for variety of electronic applications. The perovskites are used for quantum dots displays (QLED), photovoltaic systems and superconducting (HTS) devices. In this paper comprehensive studies of Ba1–xKxBi1–yREyO3 bismuth perovskites (REBKBO, RE = Y , La or Pr) are reported. Apart from structural anomalous behavior at low temperatures, the electronic properties...
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Obtaining and Characterization of the PLA/Chitosan Foams with Antimicrobial Properties Achieved by the Emulsification Combined with the Dissolution of Chitosan by CO2 Saturation
PublikacjaA new method of obtaining functional foam material has been proposed. The materials were created by mixing the poly lactic acid (PLA) solution in chloroform, chitosan (CS) dissolved in water saturated with CO2 and polyethylene glycol (PEG), and freeze-dried for removal of the solvents. The composite foams were characterized for their structural (SEM, FT-IR, density, porosity), thermal (DSC), functional (hardness, elasticity, swelling...
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Novel, Fully Biobased Semicrystalline Polyamides
PublikacjaNovel, semicrystalline polyamides and co(polyamides) were synthesized from biobased sebacic acid (SA), 2,5-diamino-2,5-dideoxy-1,4;3,6-dianhydroiditol (diaminoisoidide, DAII) as well as from 1,4-diaminobutane (DAB), also known as putrescine in nature. Low molecular weight polyamides were obtained by melt polycondensation of the salts based on these monomers or by interfacial polycondensation. In order to increase their molecular...
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Chemical characteristics of new nanopowder of titania doped with nitrogen atoms
PublikacjaW pracy zaprezentowano charakterystykę domieszkowanego azotem ditlenku tytanu otrzymanego na drodze jednoetapowej syntezy z kompleksu tytanu (IV) z ligandami zawierającymi atomy azotu. ikrostruktura i morfologia nowego materiału została określony za pomocą badań XRD, AFM, UV-VIS i FT-IR. Raport przedstawia również badania elektrochemiczne, które pozowliły na wyznaczenie potencjału pasma płaskiego na podstawie wykresu Mott
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Electrochemical glucose sensor based on the glucose oxidase entrapped in chitosan immobilized onto laser-processed Au-Ti electrode
PublikacjaThe study on novel electrode material composed of structured titanium foil with embedded Au nanoparticles and modified with chitosan with entrapped glucose oxidase is presented. To confirm the successful immobilization of glucose oxidase FT-IR analysis was performed. The response of electrodes were tested towards glucose in the presence of different interference compounds and biological fluids. The prepared material exhibits excellent...
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WEiA (AiR) - Matematyka (mgr inż. D.Żarek)
Kursy Online -
Area specific resistance (at 800 °C - 500 °C) of the SrTi0.50Fe0.50O3 porous oxygen electrodes sintered at different temperatures
Dane BadawczeIn this dataset are presented results of the polarization resistance of differently sintered SrTi0.50Fe0.50O3 porous oxygen electrodes in symetrical cell. Applied sintering temperatures were 900 °C, 950 °C and 1000 °C. The measurement temperature range was between 800 °C and 500 °C with synthetic air flow (21% O2, 40 ml min-1). Results converted to...
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Area specific resistance (at 800 °C - 500 °C) of the SrTi0.30Fe0.70O3 porous oxygen electrodes sintered at different temperatures
Dane BadawczeIn this dataset are presented results of the polarization resistance of differently sintered SrTi0.30Fe0.70O3 porous oxygen electrodes in symetrical cell. Applied sintering temperatures were 900 °C, 950 °C and 1000 °C. The measurement temperature range was between 800 °C and 500 °C with synthetic air flow (21% O2, 40 ml min-1). Results converted to...
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Area specific resistance (at 800 °C - 500 °C) of the SrTi0.65Fe0.35O3 porous oxygen electrodes sintered at different temperatures
Dane BadawczeIn this dataset are presented results of the polarization resistance of differently sintered SrTi0.65Fe0.35O3 porous oxygen electrodes in symetrical cell. Applied sintering temperatures were 900 °C, 950 °C and 1000 °C. The measurement temperature range was between 800 °C and 500 °C with synthetic air flow (21% O2, 40 ml min-1). Results converted to...
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Low temperature electrical conductivity of the SrFeO3-d pellet
Dane BadawczeThis dataset contains results of low temperature electrical conductivity measurements of dense SrFeO3-d (SFO) pellet. DC electrical conductivity measurements of SFO were performed by the Van der Pauw method between 400 °C and room temperature with 20 °C step. Studies were performed at Synthetic Air flow under humidified (~4 vol%) gas flow rate of 40...
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Low temperature electrical conductivity of the SrTi0.65Fe0.35O3-d pellet
Dane BadawczeThis dataset contains results of low temperature electrical conductivity measurements of dense SrTi0.65Fe0.35O3-d (STF35) pellet. DC electrical conductivity measurements of STF35 were performed by the Van der Pauw method between 400 °C and room temperature with 20 °C step. Studies were performed at Synthetic Air flow under humidified (~4 vol%) gas...
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Low temperature electrical conductivity of the SrTi0.30Fe0.70O3-d pellet
Dane BadawczeThis dataset contains results of low temperature electrical conductivity measurements of dense SrTi0.30Fe0.70O3-d (STF70) pellet. DC electrical conductivity measurements of STF70 were performed by the Van der Pauw method between 400 °C and room temperature with 20 °C step. Studies were performed at Synthetic Air flow under humidified (~4 vol%) gas...
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Low temperature electrical conductivity of the SrTi0.50Fe0.50O3-d pellet
Dane BadawczeThis dataset contains results of low temperature electrical conductivity measurements of dense SrTi0.50Fe0.50O3-d (STF50) pellet. DC electrical conductivity measurements of STF50 were performed by the Van der Pauw method between 400 °C and room temperature with 20 °C step. Studies were performed at Synthetic Air flow under humidified (~4 vol%) gas...
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Low temperature electrical conductivity of the SrTi0.10Fe0.90O3-d pellet
Dane BadawczeThis dataset contains results of low temperature electrical conductivity measurements of dense SrTi0.10Fe0.90O3-d (STF90) pellet. DC electrical conductivity measurements of STF90 were performed by the Van der Pauw method between 400 °C and room temperature with 20 °C step. Studies were performed at Synthetic Air flow under humidified (~4 vol%) gas...
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Lech Rowiński dr hab. inż.
Osoby -
Passive sampling techniques in monitoring of BTEX in urban air = Technika dozymetrii pasywnej w monitoringu analitów z grupy BTEX w powietrzu atmosferycznym na obszarach miejskich
PublikacjaLotna związki organiczne, a wśród nich związki z grupy BTEX, odgrywają istotną rolę w chemii środowiska. Mogą one oddziaływać znacząco na abiotyczną jak i biotyczną część środowiska. Nie bez znaczenia jest również wpływ LZO na organizmy żywe w tym na zdrowie ludzkie. Ponadto posiadają one zdolność do kumulowania się w organizmach żywych zwiększając ryzyko zachorowań. Niektóre z nich mogą również niekorzystnie oddziaływać na organizmy...
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Mapping of concentration of BTEX in atmospheric air in the area of Tricity Agglomeration = Mapowanie poziomów zanieczyszczeń związków z grupy BTEX w powietrzu atmosferycznym na terenie Aglomeracji Trójmiejskiej
PublikacjaUzyskanie informacji o poziomie zanieczyszczeń powietrza atmosferycznego przez związki z grupy BTEX na terenie aglomeracji Trójmiejskiej i Tczewa, pozwoli na ocenę i prognozowanie stanu środowiska w celu wyjaśnienia zmian zachodzących w środowisku w wyniku działalności człowieka. Sporządzenie map poziomu zanieczyszczeń powietrza atmosferycznego posłuży do opisu przestrzennego rozkładu zanieczyszczeń oraz szacowania poziomu zanieczyszczeń...
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Passive sampling techniques in monitoring of BTEX in urban air = Technika dozymetrii pasywnej w monitoringu analitów z grupy BTEX w powietrzu atmosferycznym na obszarach miejskich
PublikacjaLotna związki organiczne, a wśród nich związki z grupy BTEX, odgrywają istotną rolę w chemii środowiska. Mogą one oddziaływać znacząco na abiotyczną jak i biotyczną część środowiska. Nie bez znaczenia jest również wpływ LZO na organizmy żywe w tym na zdrowie ludzkie. Ponadto posiadają one zdolność do kumulowania się w organizmach żywych zwiększając ryzyko zachorowań. Niektóre z nich mogą również niekorzystnie oddziaływać na organizmy...
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Evaluation of the significance of the effect of the active cross-sectional area of the inlet air channel on the specific enthalpy of the exhaust gas of a diesel engine using statistics F of the Fisher-Snedecor distribution
PublikacjaThis paper presents the application of Fisher-Snedecor distribution F statistics to assess the significance of the influence of changes in the active cross-sectional area of the inlet air channel (Adol) flow in a diesel engine on the observed diagnostic parameter determined on the basis of measurements of the quick changing exhaust gas temperature in the outlet channel, which is the specific enthalpy of the exhaust gas stream within...
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Badanie próbek materiałów (HDPE, LLDPE) metodami FTIR, DSC, MFI i oznaczenie własności w statycznej próbie rozciągania oraz ustalenie przyczyny zniszczenia elementu wykonanego z LLDPE -
PublikacjaBadania próbek materiałów HDPE i LLDPE obejmowały: analizę struktury chemicznej materiałów (metodą FTIR), wyznaczenie wskaźnika szybkości płynięcia własności (MFR i MVR), własności termicznych (metodą DSC) oraz własności w statycznej próbie rozciągania. Na podstawie otrzymanych wyników ustalono prawdopodobną przyczynę zniszczenia elementu konstrukcyjnego wykonanego z LLDPE.
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Modeling of the alcohol dehydrogenase active site. Two different modes of alcohol binding in crystals of zinc and cadmium tri-tert-butoxysilanethiolates evidenced by X-ray diffraction and solid state vibrational spectroscopy
PublikacjaOpisano syntezę, struktury cząsteczkowe oraz widma FT-IR, 1H. 13C, 29Si, 113Cd NMR dziesięciu nowych, mieszanoligandowych kompleksów cynku i kadmu z ligandem tri-tert-butoksysilanotiolanowym i pochodnymi imidazolu. Za pomocą rentgenowskiej analizy strukturalnej i spektroskopii w podczerwieni udokumentowano dwa różne sposoby wiązania etanolu i metanolu w kryształach tych związków. Opisane kompleksy stanowią modele miejsca aktywnego...
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Impact analysis of surface roughness of the plate-plate measuring system on resistance torque in interaction with MR fluid
PublikacjaMagnetorheological (MR) fluids are complex suspensions of magnetic particles in a non-magnetic carrier fluid. They exhibit ‘smart’ properties that enable them to change their rheological parameters in response to a change in the external magnetic field applied. This behavior is used in some engineering solutions, e.g. MR clutches or brakes. For such systems to work correctly, the resistance torque achieved by contact with the...
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The Use of Calcium Phosphate-Based Starter Pellets for the Preparation of Sprinkle IR MUPS Formulation of Rosuvastatin Calcium
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Free-air anomaly grid on the Gulf of Gdańsk
Dane BadawczeWe present an attempt to determine the accuracy of shipborne gravimetry for the needs of geoid determination. The shipborne gravity campaign, is the beginning of a series of gravimetry measurements in the Polish Exclusive Economy Zone. The campaign was conducted in the area where the accuracy of geoid determination is crucial for the safety of navigation...
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The supramolecular organization of self-assembling chlorosomal bacteriochlorophyll c, d, or e mimics
PublikacjaBacteriochlorophylls (BChls) c, d, and e are the main light-harvesting pigments of green photosynthetic bacteria that self-assemble into nanostructures within the chlorosomes forming the most efficient antennas of photosynthetic organisms. All previous models of the chlorosomal antennae, which are quite controversially discussed because no single crystals could be grown so far from these organelles, involve a strong hydrogen-bonding...
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Direct amination of boron-doped diamond by plasma polymerized allylamine film
PublikacjaA novel microwave pulsed-plasma based method for the modification of the hydrogen-terminated polycrystalline boron-doped diamond (BDD) with a thin film of polymerized allylamine (PPAAm) is reported. A modified BDD surface is resistant to hydrolysis and delamination and is characterized by a high density of positively charged amino groups. Pulsed microwave plasma was applied to improve the degree of cross-linking and bonding of...