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Wyniki wyszukiwania dla: "cold" extraction
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Hydrophobic deep eutectic solvents in microextraction techniques–A review
PublikacjaOver the past decade, deep eutectic solvents (DES) have been widely studied and applied in sample preparation techniques. Until recently, most of the synthesized DES were hydrophilic, which prevented their use in the extraction of aqueous samples. However, after 2015 studies on the synthesis and application of hydrophobic deep eutectic solvents (HDES) has rapidly expanded. Due to unique properties of HDES i.e. density, viscosity,...
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Rain Gardens GC_MS analysis dataset
Dane BadawczeThis dataset contains the results of samples analysis (no-target analysis: scan mode) using gas chromatography coupled with mass spectrometry GC–MS (GC-2030 NEXIS MS, Shimadzu, Japan or Thermo Scientific, Waltham, USA).
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Vehicle Dynamics - L-15/C-15/L-15/P-15, Design and Production Engineering, WIMiO, undergraduate studies, engineering studies, full-time (stationary) studies, 2021/2022, se06, (M:320383W0), summer semester 2023/2024
Kursy OnlineModuł przedmiotów wybieralnych, MiBM, I stopień, specjalność w j. angielskim: Design and Production Engineering (DaPE), semestr 6?, (przedmiot dla Chińczyków), Lecture: Throttle by tyred wheel: slip rolling, rolling with tyre strain, vertical and lateral surface reactions, traction, energetic looses, forces in contact path. Drugs of movement: rolling, air, gradient, inertia, cornering and towing. Forces ant torques acting to vehicle...
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Beata Krawczyk dr hab.
Osobydr hab. Beata Krawczyk, prof. uczelni Stopnie naukowe, wykształcenie, kwalifikacje Beata Krawczyk uzyskała tytuł magistra biologii na Wydziale Biologii (wówczas: Wydział Biologii i Nauk o Ziemi), Uniwersytetu Gdańskiego w 1986 roku, a doktorat z biologii molekularnej na Wydziale Biologii (wówczas: Wydział Biologii, Geografii i Oceanologii) Uniwersytetu Gdańskiego w 1996 roku. Stopień doktora habilitowanego w zakresie nauk biologicznych...
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Green analytical chemistry : theory and practice
PublikacjaThis tutorial review summarises the current state of green analytical chemistry with special emphasis on environmentally friendly sample preparation techniques. Green analytical chemistry is a part of the sustainable development concept; its history and origins are described. Miniaturisation of analytical devices and shortening the time elapsing between performing analysis and obtaining reliable analytical results are important...
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Porównanie efektywności wybranych technik ekstrakcji/ługowania metabolitów wtórnych z suchego materiału roślin owadożernych z hodowli in vitro = Acomparison of effciency of secondary metabolites extraction/leaching techniques from carnivorous plants dry material from in vitro culture
PublikacjaW roślinach owadożernych za efekt terapeutyczny odpowiadają głównie pochodne 1,4-naftochinonu (juglon), oraz flawonoidy. Interesujące właściwości tych związków oraz możliwość synergicznego działania wielu innych metabolitów na efekt terapeutyczny, podjęto pracę przygotowania technologii efektywnego wyodrębniania metabolitów. W tej publikacji porównano efektywności technik ekstrakcji/ługowania. Jako materiał badany posłużyły wysuszone...
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Nowoczesne techniki przygotowania próbki do oznaczania analitów organicznych z zastosowaniem chromatografii gazowej. Część I. Podstawy teoretyczne ekstrakcji. Modern techniques of preparation of samples for determining organic analytes by gas chromatography. Part I. Theoretical principles of extraction.
PublikacjaPrzedstawiono podstawy teoretyczne technik izolacji i wzbogacania analitów organicznych z próbek gazowych oraz ciekłych. Już pobieżna analiza literatury dotyczącej omawianych zagadnień, pokazuje jak różnorodne i bogate spektrum technik jest stosowane na etapie przygotowania próbki. Z drugiej strony, z punktu widzenia podstaw fizykochemicznych, większość technik opiera się na dwóch zjawiskach: adsorpcji analitów na medium zatrzymującym...
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Początki piśmiennictwa staropermskiego. Stefanowski anbur jako jeden z najstarszych zabytków uralskich [The beginnings of Old Permian writings. Anbur (abur) as one of the oldest Uralian scripts]
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Deep eutectic solvents with solid supports used in microextraction processes applied for endocrine-disrupting chemicals
PublikacjaThe determination of endocrine-disrupting chemicals (EDCs) has become one of the biggest challenges in Analytical Chemistry. Due to the low concentration of these compounds in different kinds of samples, it becomes necessary to employ efficient sample preparation methods and sensitive measurement techniques to achieve low limits of detection. This issue becomes even more struggling when the principles of the Green Analytical Chemistry...
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Rapid Characterization of the Human Breast Milk Lipidome Using a Solid-Phase Microextraction and Liquid Chromatography-Mass Spectrometry-Based Approach.
PublikacjaHuman breast milk (HBM) is a biofluid consisting of various biomolecules such as proteins, lipids, carbohydrates, minerals and bioactive substances. Due to its unique and complex composition, HBM provides not only nutritional components required for the growth of the infant, but also additional protection against infections. Global insight into the composition of HBM is crucial to understanding the health benefits infants receive...
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Esteraza GDSL z psychrotolerancyjnego szczepu Pseudomonas sp. S9 - konstrukcja systemów ekspresyjnych opartych o komórki Escherichia coli i Pichia pastoris, produkcja, oczyszczanie i charakterystyka uzyskanych białek rekombinowanych
PublikacjaW rozprawie doktorskiej celu opracowania wydajnej metody produkcji rekombinantowych wariantów sekwencyjnych enzymu esterolitycznego z psychrotolerancyjnego szczepu Pseudomonas sp. S9 zaprojektowano układy ekspresyjne umożliwiające ich produkcję w bakteriach Escherichia coli oraz drożdżach Pichia pastoris. W systemie ekspresyjnym E. coli wyprodukowano dwa warianty białek: EstS9Auto (białko zbudowane z domeny katalitycznej, domeny...
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Gracjana Klein-Raina dr hab.
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OTHER AND UNSPECIFIED MALE GENITAL ORGANS, Spermatic cord - Male, 30 - Tissue image [6110730021431501]
Dane BadawczeThis is the histopathological image of OTHER AND UNSPECIFIED MALE GENITAL ORGANS tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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OTHER AND UNSPECIFIED MALE GENITAL ORGANS, Spermatic cord - Male, 27 - Tissue image [10130730023083861]
Dane BadawczeThis is the histopathological image of OTHER AND UNSPECIFIED MALE GENITAL ORGANS tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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OTHER AND UNSPECIFIED MALE GENITAL ORGANS, Spermatic cord - Male, 30 - Tissue image [6110730021432311]
Dane BadawczeThis is the histopathological image of OTHER AND UNSPECIFIED MALE GENITAL ORGANS tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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OTHER AND UNSPECIFIED MALE GENITAL ORGANS, Spermatic cord - Male, 27 - Tissue image [6080730009644901]
Dane BadawczeThis is the histopathological image of OTHER AND UNSPECIFIED MALE GENITAL ORGANS tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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OTHER AND UNSPECIFIED MALE GENITAL ORGANS, Spermatic cord - Male, 39 - Tissue image [7220729599717211]
Dane BadawczeThis is the histopathological image of OTHER AND UNSPECIFIED MALE GENITAL ORGANS tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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OTHER AND UNSPECIFIED MALE GENITAL ORGANS, Spermatic cord - Male, 30 - Tissue image [10100730045417201]
Dane BadawczeThis is the histopathological image of OTHER AND UNSPECIFIED MALE GENITAL ORGANS tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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OTHER AND UNSPECIFIED MALE GENITAL ORGANS, Spermatic cord - Male, 20 - Tissue image [10130730023075511]
Dane BadawczeThis is the histopathological image of OTHER AND UNSPECIFIED MALE GENITAL ORGANS tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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OTHER AND UNSPECIFIED MALE GENITAL ORGANS, Spermatic cord - Male, 39 - Tissue image [7220729599715031]
Dane BadawczeThis is the histopathological image of OTHER AND UNSPECIFIED MALE GENITAL ORGANS tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Discovery of Stylistic Patterns in Business Process Textual Descriptions: IT Ticket Case
PublikacjaGrowing IT complexity and related problems, which are reflected in IT tickets,create a need for new qualitative approaches. The goal isto automate the extraction of main topics described in tickets in order to provide high quality support for the IT process workers and enablea smooth service delivery to the end user. Present paper proposes a method of knowledge extraction in a form of stylistic patterns in business...
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Assessment of the ice jam potential on regulated rivers and reservoirs with the use of numerical model results
PublikacjaThis study presents an attempt at estimating the jam potential on rivers with significant anthropogenic intervention in the course or flow characteristics of the river. The DynaRiCE model was used for forecasting both the place and time of an ice jam occurrence. In this modified method, two ice parameters are subjected to analysis, namely the relative ice-to-water velocity (vi/vw),and the ice thickness to single floe thickness...
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Finding safe and efficient shipping routes in ice-covered waters: A framework and a model
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Towards probabilistic models for the prediction of a ship performance in dynamic ice
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Estimating operability of ships in ridged ice fields
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Comparative analysis of the quality parameters and the fatty acid composition of two economically important Baltic fish: cod, Gadus morhua and flounder, Platichthys flesus (Actinopterygii) subjected to iced storage
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Lower rim substituted p-tert-butyl-calix[4]arene. Part 17. synthesis, extractive and ionophoric properties of p-tert-butylcalix[4]arene appended with hydroxamix acid moieties
PublikacjaThe synthesis and characterization of four p-tert-butylcalix[4]arene-hydroxamic acidc are reported. The dependence of the metal ion binding, assessed by liquid extraction of the metal nitrates from water into dichloromethane in individual and competitive experiments, on the ligand structure, is presented. The results showed that those ligands could be successfully used in separation process of trnasition and heavy metals often...
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TRANSFORMATION OF WORLD ECONOMY AFTER THE END OF COLD WAR - Nowy
Kursy OnlineThe course focuses the main trends of the world economy in the last 30 years. National and macro-regional, as well as sectorial case studies will be used to offer a clearer understanding of the main global dynamics. The approach is multidisciplinary and mainly qualitative, including economic and business history, international political economy, economic sociology and political science.
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A comprehensive review on Ginger (Zingiber officinale) as a potential source of nutraceuticals for food formulations: Towards the polishing of gingerol and other present biomolecules
PublikacjaCurrently, ginger is one the most consumed plants when dealing with the treatments of various illnesses. So far, it is known that various biologically active molecules, such as gingerols, shogaols and zingerone, among others, are the main responsible for specific biological activities, opening a new window for its utilization as a nutraceutical in foods. In pioneering extraction processes, solvent extraction has been initially...
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The effect of chitosan concentration and molecular weight on endotoxin content
Dane BadawczeThe dataset includes results to determine the effect of chitosan concentration and molecular weight on endotoxin content as well as the effect of purification methods. The endotoxin concentration was determined using the PyroGene Recombinant Factor C Endpoint Fluorescent Assay. Chitosan 0.6% in 0.1M glycolic acid from Chemat LMW, MMW, and HMW were used...
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Piotr Dworakowski dr
OsobyPiotr Dworakowski received the MSc degree and PhD degree with distinction in electrical engineering from Gdansk University of Technology, Poland, in 2007 and 2020 respectively. From 2008 to 2013 he was working in Alstom Transport, Tarbes, France on traction drives control. Since 2014 he has been a Power Converters Team Leader in SuperGrid Institute, Lyon, France. His research interests include high efficiency power converters for...
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Lower rim substituted p-tert-butyl-calix[4]arene. Part 17. Synthesis, extractive and ionophoric properties of p-tert-butylcalix[4]arene appended with hydroxamic acid moieties
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Michał Lech dr inż.
OsobyMichał Lech was born in Gdynia in 1983. In 2007 he graduated from the faculty of Electronics, Telecommunications and Informatics of Gdansk University of Technology. In June 2013, he received his Ph.D. degree. The subject of the dissertation was: “A Method and Algorithms for Controlling the Sound Mixing Processes with Hand Gestures Recognized Using Computer Vision”. The main focus of the thesis was the bias of audio perception caused...
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Study of the influence of the presence of Dr fimbriae on the sedimentation of recombinant Escherichia coli strains: AAEC191A and BL21(DE3)
Dane BadawczeCell sedimentation in the medium is a common phenomenon in most bacterial enviroments. This study specifically investigated the impact of Dr fimbriae presence on cell deposition. To explore this, recombinant Escherichia coli strains were employed, including BL21(DE3)/pCC90, BL21(DE3)/pACYCpBAD, BL21(DE3)/pCC90 Dra D-mut, BL21(DE3)/pCC90 D54-STOP, AAEC191A/pCC90,...
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An in situ derivatization – dispersive liquid–liquid microextraction combined with gas-chromatography – mass spectrometry for determining biogenic amines in home-made fermented alcoholic drinks
PublikacjaA novel dispersive liquid–liquid microextraction (DLLME) gas chromatography mass-spectrometry(GC–MS) method was developed for the determination of 13 biogenic amines in home-made wine sam-ples. The method allows to simultaneous extraction and derivatization of the amines providing a simpleand fast mode of extract enrichment. During the study, two different procedures were examined. Sta-tistical analysis was performed to choose...
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Ionogel sorbent coatings for determining organophosphorus and pyrethroid insecticides in water and fresh juice samples by headspace-solid phase microextraction
PublikacjaThe sol–gel method yielded three different ionogel sorbent coatings that were obtained based on a silica material containing ionic liquids (ILs) immobilized in its pores. Two ILs, triethylsulfonium bis(trifluoromethylsulfonyl) imide [Set3][TFSI] and 1-butyl-1-methylpiperidinium bis(trifluoromethylsulfonyl)imide [C4C1Pip][TFSI], as well as their equimolar mixture [Set3/C4C1Pip], were used to obtain ionogel fibers. The developed...
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Head-Space SPME for the Analysis of Organophosphorus Insecticides by Novel Silica IL-Based Fibers in Real Samples
PublikacjaThis work demonstrates the suitability of a newly developed ionic liquid (IL)-based silica SPME fiber for the determination of seven organophosphorus insecticides in cucumber and grapefruit samples by headspace solid-phase microextraction (HS-SPME) with a gas chromatography–flame ionization detector (FID). The sol-gel method released four different sorbent coatings, which were obtained based on a silica matrix containing ILs immobilized...
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Organic and conventional kiwifruit myths versus reality: antioxidant, antiproliferative and health effects
PublikacjaComparison between organic and conventional kiwifruit cultivars ''Hayward'' and ''Bidan'', which was done by four redical scavenging assays, ESI-MS, and DSC measurements, showed significant differences between cultivars. Such results were not estimated in kiwifruit growing under organic and conventional conditions. The extraction of bioactive compounds was done by two different methods: sequential extraction with ethyl acetate...
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Research on the phenomena of warming up and free cooling down the car engine
PublikacjaThe average cold start temperature in Europe is 9 degrees C. However, not the average is the most important for the composition of exhaust gases and associated air pollution. The most onerous for the environment are the winter starts when automotive emissions of harmful gases add up in cities with those of home heating systems. The paper presents preliminary studies of warming up and cooling down processes in various environmental conditions....
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Analysis of the Capability of Deep Learning Algorithms for EEG-based Brain-Computer Interface Implementation
PublikacjaMachine learning models have received significant attention for their exceptional performance in classifying electroencephalography (EEG) data. They have proven to be highly effective in extracting intricate patterns and features from the raw signal data, thereby contributing to their success in EEG classification tasks. In this study, we explore the possibilities of utilizing contemporary machine learning algorithms in decoding...
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Involvement of human glutathione S-transferase M1-1 in the glutathione conjugation of the antitumor unsymmetrical bisacridine derivative C-2028.
Dane BadawczeUnsymmetrical bisacridines (UAs) are a novel potent class of antitumor-active therapeutics. The aim of this study was to investigate the possible role of human glutathione S-transferase M1-1 (hGSTM1-1) in the glutathione (GSH) conjugation of a representative UA, C‑2028.
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D.C. electrical measurements of Bi2VO5.5 ceramic measured at high temperature region
Dane BadawczeD.C. electrical properties of Bi2VO5.5 ceramic was measured.
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World Politics
Kursy OnlineThe course aims to familiarize stdnets with the most important theories of the international relations. This instrument will enable them to understand a series of case studies that will be presented starting with the first wordl war and going until today. The case studies will include the main aspects of the Cold War period, the role of USA and Soviet Union in shaping the international relations according to a political and ideological...
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Safeguarding democracy during pandemics. Social distancing, postal, or internet voting—the good, the bad, or the ugly?
PublikacjaDuring a pandemic, many countries and organizations must decide whether to postpone upcoming elections or to hold them (Krimmer et al., 2020a). If the decision is made to hold the election, three main scenarios come to mind: continue using the existing system but include measures to ensure the health of participants; or look for alternatives among remote voting channels which could ensure social distancing is guaranteed either...
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Automatic Analysis of Trajectories of Moving Objects
PublikacjaOngoing monitoring is essential to providing security and safety of maritime and air operations. This paper presents the research in the area of automatic analysis of movement of unrestricted vehicles like ships and air-planes. The analysis is aimed at extraction of trajectory information, and the results can be used to identify anomalous behaviour in archived and real-time data. In this paper we focus on data acquired using the...
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Two highly thermostable paralogous single-stranded DNA-binding proteins from Thermoanaerobacter tengcongensis
PublikacjaThe thermophilic bacterium Thermoanaerobacter tengcongensis has two single-stranded DNA-binding (SSB) proteins, designated TteSSB2 and TteSSB3. In a SSB complementation assay in Escherichia coli, only TteSSB3 took over the in vivo function of EcoSSB. We have cloned the ssb genes obtained by PCR and have developed E. coli overexpression systems. The TteSSB2 and TteSSB3 consist of 153 and 150 amino acids with a calculated molecular...
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Study of the influence of the presence of Dr fimbriae on the hydrophobicity of cells of recombinant Escherichia coli strains: AAEC191A and BL21(DE3)
Dane BadawczeThe ability of a cell surface to repel or adhere to surfaces is crucial, and it was assessed through a microbiological adhesion test involving hexadecane and xylene. In this method, microorganisms in an aqueous layer are mixed with an organic layer, and after completion, the absorbance of each sample is measured at a 570 nm wavelength. The results obtained...
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Solid phase microextraction: state of the art, opportunities and applications
PublikacjaSolid phase microextraction is one of the most popular green techniques used for sample preparations in analytical chemistry. It is a simple, rapid, sensitive, and solvent-free technique. Since SPME was first introduced in the early 1990s, there has been an intensification of research in order to elaborate new methodical solutions in many research facilities around the world, which could increase the use of this technique. More...
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Plasmon-enhanced photoluminescence from TiO2 and TeO2 thin films doped by Eu3+ for optoelectronic applications
PublikacjaIn this work we study the luminescence properties of europium-doped titanium dioxide and tellurium oxide thin films enhanced by gold plasmonic nanostructures. We propose a new type of plasmon structure with an ultrathin dielectric film between plasmonic platform and luminescent material. Plasmonic platforms were manufactured through thermal annealing of the gold thin film. Thermal dewetting of gold film results in spherical gold...
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Analysis of antibiotic resistance in Escherichia coli isolated from the Reda River and the Oliwski Stream using basic statistical methods = Zastosowanie metod ststystycznych do analizy antybiotykoodporności bakterii wskaźnikowych pochodzących z rzeki Redy i Potoku Oliwskiego
PublikacjaIn this study distribution of antimicrobial resistance patterns among fecal indicator bacteria (Escherichia coli and Enterococcus spp.) was examined in two watercourses. The susceptibility analyses were carried out against the antimicrobial agents, important in treating human E. coli and enterococcal infection. Water samples were obtained from the Oliwski Stream and from the Reda River. On each watercourse the five representative...