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Search results for: SAMPLE PREPARATION TECHNIQUES
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An Overview on Materials and Techniques in 3D Bioprinting Toward Biomedical Application
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Non- and low-alcoholic beer – popularity and manufacturing techniques [pdf]
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Comparison of extraction techniques of robenidine from poultry feed samples
PublicationW publikacji opisano wykorzystanie różnych technik ekstrakcji kokcydistatyków (na przykładzie robenidyny) z próbek pasz zwierzęcych. W trakcie badań porównano wpływ różnych parametrów ekstrakcji na współczynniki odzysku analitu. Wśród wykorzystanych technik ekstrakcji wymienić należy: ekstrakcję za pomocą rozpuszczalnika wspomaganą ultradźwiękami oraz mikrofalami, ekstrakcję w aparatach Soxhleta i Soxteca a także ekstrakcję przez...
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Adaptation of various persons' identification techniques as a solution for security and safety
PublicationPrzedstawiono różne metody identyfikacji osób w oparciu o ich cechy biometryczne w zastosowaniu do bezpieczeństwa i zabezpieczeń. Takimi biometrycznymi cechami mogą być właściwości fizjologiczne jak odciski palców, kształt dłoni, właściwości tęczówki jak również cechy behawioralne jak sposób pisania lub wypowiadania się.
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Modern techniques of extraction of organic analytes from environmental matrices.
PublicationW pracy przedstawiono usystematyzowane informacje dotyczące dostępnych jak i nowych technik izolacji i wzbogacania analitów organicznych przed etapem oznaczeń końcowych.
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Analytical techniques used in monitoring of atmospheric air andstack gases
PublicationPrzedstawiono klasyfikację metod i technik analitycznych wykorzystywanych w badaniach powietrza atmosferycznego i gazów odlotowych. Przedstawiono również typowe urządzenia wykorzystywane na etapie pobierania próbek.
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Innovative Techniques of Processing Human Milk to Preserve Key Components
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Applications of compression techniques for reducing the size of multibeam sonar records
PublicationJednym z najczęściej używanych urządzeń służących do szeroko rozumianego telemonitoringu morskiego są sonary wielowiązkowe (ang. Multibeam systems - MBS). Ich wysoka wydajność w tworzeniu informacji o obiektach znajdujących się pod wodą skutkuje w dużych ilościach danych pozyskiwanych podczas rejsów badawczych i pomiarowych. W tym kontekście, proces przechowywania i zarządzania takim magazynem danych staje się istotnym problemem...
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Comparison of Volatile Constituents ofAcorus calamusandAsarum europaeumObtained by Different Techniques
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Computational Techniques in Numerical Simulations of Arc and Laser Welding Processes
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A hybrid speech codec employing parametric and perceptual coding techniques
PublicationW referacie przedstawiono hybrydowy kodek mowy dla zastosowan w komunikacji VoIP wykorzystujący kodowanie parametryczne i percetualne. Sygnał mowy jest dzielony na składowe dźwięczne, które podlegają kodowania perceptualnemu, składowe bezdźwięczne, które kodowane są metodą parametryczną oraz transjenty, które nie są kodowane żadną stratną metodą. Dodatkowo przedstawiono architekturę kodeka, w której perceptualnie kodowana i przesyłana...
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Usability Techniques Possible to Use in Diagnostic Tools Interface Improvement
PublicationThe development of diagnostic tools has caused a rapid increase in the amount of information generated and presented, necessitating the use of computer displays as an interface to data presentation and the use of modern diagnostic tools. The paper presents methods for testing usability that can be used in designing and improving the quality of interfaces of modern diagnostic tools that use communication through graphical user interfaces.
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Cognitive Systems, Concepts, Processes, and Techniques for the Age of Industry 4.0
PublicationThe aim of this Guest Edition of Cybernetics and Systems is to present a wide-ranging scale of concepts and processes being currently researched, developed, and evaluated in real life settings in anticipation of incoming Industry 4.0 era. With the fourth industrial revolution expectation, the broad spectrum of cognitive approaches have emerged as an attempt to mimic and augment, in some way, human intelligence. Intelligence, in...
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Determination of Sodium Ion Diffusion Coefficient in Tin Sulfide@Carbon Anode Material Using GITT and EIS Techniques
PublicationThe electroanalytical behavior of SnSx (x = 1, 2) encapsulated into a carbon phase was studied using the galvanostatic intermittent titration technique (GITT) and electrochemical impedance spectroscopy (EIS). These techniques are widely utilized in battery systems to investigate the diffusion of alkali metal cations in anode and cathode materials depending on the concentration of ions in the host material. Here, we report different...
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Study of microstress state of P91 steel using complementary mechanical Barkhausen, magnetoacoustic emission, and X-ray diffraction techniques
PublicationThe paper deals with assessment of microstress state of martensite P91 steel using three complementary techniques: mechanical Barkhausen emission, magnetoacoustic emission (MAE), and X-ray diffraction (XRD) profile analysis. Magnetic coercivity Hc and microstructure were investigated with inductive magnetometry and magnetic force microscopy (MFM), respectively. Internal stress level of P91 steel was modified by heat treatment....
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Application of different building representation techniques in HEC-RAS 2-D for urban flood modeling using the Toce River experimental case
PublicationThis paper presents the impact of the choice of building representation techniques and hydrodynamic models on urban flood simulations using HEC-RAS 2-D for the Toce River physical model. To this end, eight numerical models based on previous laboratory experiments were prepared to simulate unsteady urban flooding on each side of building units. Two simplified building layouts (aligned and staggered) were examined, where models were...
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Predicting seismic response of SMRFs founded on different soil types using machine learning techniques
PublicationPredicting the Maximum Interstory Drift Ratio (M-IDR) of Steel Moment-Resisting Frames (SMRFs) is a useful tool for designers to approximately evaluate the vulnerability of SMRFs. This study aims to explore supervised Machine Learning (ML) algorithms to build a surrogate prediction model for SMRFs to reduce the need for complex modeling. For this purpose, twenty well-known ML algorithms implemented in Python software are trained...
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Medical Image Segmentation Using Deep Semantic-based Methods: A Review of Techniques, Applications and Emerging Trends
PublicationSemantic-based segmentation (Semseg) methods play an essential part in medical imaging analysis to improve the diagnostic process. In Semseg technique, every pixel of an image is classified into an instance, where each class is corresponded by an instance. In particular, the semantic segmentation can be used by many medical experts in the domain of radiology, ophthalmologists, dermatologist, and image-guided radiotherapy. The authors...
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The issue of uncertainty of visual measurement techniques for long distance measurements based on the example of applying electric traction elements in diagnostics and monitoring
PublicationRail transport is the most economical and energy-effective in the field of land transport, in particular electrified. In order to ensure efficient and reliable operation of electrified rail transport, the issues of monitoring and diagnostics of the traction infrastructure and vehicles are extremely important. The most critical point in the transmission of electric energy to the vehicle is the sliding contact of the current collector...
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Preparation of 1-[Ω-(1,4,5,6-Tetrahydropyrimidin-2-yl)alkyl]thymines
PublicationOne-stage prepn. of the hydrochloride salts of 1-[ω-(1,4,5,6-tetrahydropyrimidin-2-yl)alkyl]-thymines, e.g. I, from 1-(ω-cyanoalkyl)thymines and a 1:1-mixt. of 1,3-diaminopropane and ethanol satd. with hydrogen sulfide is described. 1-(2-Cyanoethyl)-thymine gave a facile reversal of the Michael reaction to thymine under the conditions used. The reaction of 1,3-bis(3-cyanobenzyl)thymine with the above reagent produced 1,3-bis[3-(1,4,5,6-tetrahydropyrimidin-2-yl)benzyl]thymine.
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Poly(vinyl alcohol)/GO-MMT nanocomposites: Preparation, structure and properties
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Preparation of Activated Carbon from the Biodegradable film for Co2 Capture Applications
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Preparation of fluorescent nanodiamond suspensions using bead-assisted ultrasonic disintegration
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Preparation, properties and potential applications of a photocurable varnish with pleasant limonene smell
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Preparation of environmental samples for gas chromatographic determination of selected organic pollutants
PublicationOpisano różne metody izolacji i wzbogacania zanieczyszczeń organicznych z ciekłych, gazowych i stałych próbek środowiskowych. Opisano konstrukcję i testowanie nowych systemów do przygotowania próbek oraz ich zastosowanie w połączeniu z chromatografią gazową do oznaczania zanieczyszczeń organicznych w póbkach rzeczywistych.
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Preparation and characterisation of visible light responsive iodine doped TiO2 electrodes
PublicationPraca przedstawia charakterystykę domieszkowanego jodem ditlenku tytanu (I-TiO2) otrzymanego na drodze hydrotermicznej syntezy, gdzie prekursor stanowiły komplesy tytanu (IV) z ligandami zawierającymi atom jodu. Struktura nowego materiału została opisana za pomocą technik XPS, XRD, UV-vis i FT-IR-ATR. Badania te potwierdziły, że otrzymany proszek I-TiO2 ma zmniejszoną przerwę energetyczną. Praca prezentuje również badania elektrochemiczne...
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Preparation of TiO2-nitrogen-doped photocatalyst active under visible light
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Preparation, composition and properties of fish silage produced with post-coagulation sludge
PublicationPost-coagulation sludge was added to fish fydrolyzates (silage). Silage was prepared using whole sprats. Technology of the process has been modified and sulphuric acid was replaced with phosphoric acid. The objective was to evaleuate the quality of produced silage during storage, particulary the changes of peroxide value and amount of free acids in silage fat.
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Facile preparation of extremely photoactive boron-doped TiO2 nanotubes arrays
PublicationDoping of TiO2 nanotube arrays with boron was realized via electrochemical treatment of as-anodized titania immersed in electrolyte containing boric acid. The photoactivity of doped and pure titania was examined by means of photoelectrochemical and photocatalytic response under UV-vis irradiation. The results showed that photocurrent density of B-TNTs is remarkably higher (7.5 times) than density of pure TiO2 nanotube arrays. Furthermore,...
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Preparation and some properties of multiblock copoly(amide-b-amide)s
PublicationThe paper concerns the polymers built of oligoamide hard blocks and oligoamide soft blocks (KPAA, formula I). Oligo(laurolactam) (PA12) was used as hard block and the product of reaction of dimerized fatty acid and hexamethylene diamine (PA6,36) was used as a soft one. Effects of molar ratio of these blocks on the following properties of KPAA have been investigated: limiting viscosity number ([2]), degrees of swelling in water...
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Preparation and structure of nanocrystalline sol-gel derived lithium titanate powder
Publicationw pracy szczegółowo opisano nowatorską metodę wytwarzania nanokrystalicznych proszków tytanianu litu. przedstawiono wyniki badań wykonanych próbek.
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Non-matrix reference materials-the challenges in the preparation of standard gas mixtures
PublicationIn the last few years particularly great pressure is exerted on quality control and assurance of analytical measurement results. An invaluable role in this process is played by reference materials. The paper presents the characteristics of basic types of reference materials, with particular attention to gaseous reference materials.
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Liquefaction of macroalgae Enteromorpha biomass for the preparation of biopolyols by using crude glycerol
PublicationThis article describes the liquefaction process of macroalgae Enteromorpha with the use of crude glycerol as a solvent and a reagent, aimed at obtaining of new bio-polyols, which are characterized with respect to their chemical structure, physical and thermal properties. Six different biopolyols were prepared. In order to optimize the liquefaction of algal biomass for the best bio-polyol properties, two catalysts (sulfuric or orthophosphoric...
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MMA fighters's technical-tacticak preparation-fight analysis: a case study
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THE APPLICATION OF THE MECHANOCHEMICAL SYNTHESIS FOR THE PREPARATION OF ADVANCED CERAMICS BASED ON BARIUM TITANATE
PublicationIn the present study, the lead-free BaTi1-xZrxO3 (for x = 0, 0.05 and 0.15) ceramics were prepared by High-Energy Ball Milling and heat treatments. The performed X-ray, SEM and EDS measurements confirmed high purity, good quality and the expected quantitative composition of the obtained samples. The study of dielectric properties was performed by means of broadband dielectric spectroscopy at the frequency ranging from 0.1 Hz to...
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Preparation and Properties of Thermoplastic Polyurethane Composites Filled with Powdered Buckwheat Husks
PublicationBio-based fillers for the polymer composites are still interesting from the scientific and industrial point of view, due to their low cost and renewable nature. In this work partially green composites were obtained by the mixing of thermoplastic poly(ester-urethane) with the unmodified and modified (by acetylation) grinded buckwheat husks. Obtained biocomposites were characterized in the terms of their chemical structure (FTIR),...
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Preparation and characterization of asphaltene based adsorbents for gas-solid adsorption systems
PublicationThe dissertation presents results of the experimental research on asphaltene-based adsorbents (support coated with asphaltene layer) for gas-solid adsorption systems, with special reference to volatile organic compounds (VOCs) removal from gas streams. Analysis of gas adsorption properties revealed that asphaltenes isolated from oxidized bitumen have strong affinity toward VOCs. Interactions with target gas molecules, and selectivity...
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Monitoring of crosslinking of a DGEBA-PAMAM adhesive in composite/aluminium bonded joint using mechanical and ultra-sound techniques
PublicationAdhesive cure is an important and determining aspect of strength and stability of bonded structures. Crosslinking of the polymer leads to the adhesive strength, stiffness and durability. Depending on the resin and curing agent used, cure time can vary from minutes to weeks, even then 100% crosslinking not being guaranteed. Standard methods based on dynamic mechanical analysis (DMA) or calorimetric techniques (DSC, DTA) are valuable...
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Comparison of different techniques for extracting Polychlorinated Biphenyls from bottom sediment samples using Isotope Dilution Mass Spectrometry
PublicationIn this work, problems that may occur during determination of trace levels of polychlorinated biphenyls in sediment samples are described. The main error sources are connected with extraction of analytes prior to final determination. During model studies, polychlorinated biphenyls have been extracted from sediment reference material (METRANAL 2) with the use of different solvents (dichloromethane, hexane, and toluene); the process...
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RF Multi-Functional Input-Reflectionless Dispersive-Delay Structure With Sharp-Rejection Filtering Using Channelization Techniques
PublicationA class of RF multi-functional input-reflectionless dispersive-delay structure (DDS) with linear-type in-band groupdelay variation and sharp-rejection bandpass-filtering capability is reported. It exploits a two-branch-channelized/balanced-type circuit with similar low-order reflective DDS units inside its channels, which are connected through input/output 3-dB quadrature wideband couplers. The adopted DDS unit is based on a coupledresonator...
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First deep eutectic solvent-based (DES) stationary phase for gas chromatography and future perspectives for DES application in separation techniques
PublicationThe paper presents the first application of deep eutectic solvents (DES) as stationary phases for gas chromatography. DES obtained by mixing tetrabutylammonium chloride (TBAC) as a hydrogen bond acceptor (HBA) with heptadecanoic acid being a hydrogen bond donor (HBD) in a mole ratio of HBA:HBD equal to 1:2 was characterized by its ability to separate volatile organic compounds (VOCs). The Rohrschneider – McReynolds constants determined...
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Chapter 6 : Non-intrusive measurement techniques in bubble dynamics investigation
PublicationPrzedstawiono wyniki badań dynamiki pęcherzyków parowych i gazowych przy użyciu nieinwazyjnych metod optycznych i akustycznych.
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Assessment of river water quality in the South Baltic coast by multivariate techniques
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Shaping coherence function of sources used in low-coherent measurement techniques
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Shaping coherence function of sources used in low-coherent measurement techniques
PublicationW niskokoherencyjnych technikach pomiarowych kształt funkcji koherencji wykorzystywanego źródła ma bezpośredni wpływ na parametry metrologiczne układu pomiarowego. Z tego względu, w wielu aplikacjach niezbędne jest użycie metod pozwalających na zmianę kształtu tej funkcji. W artykule przeanalizowano możliwości kształtowania funkcji koherencji, a przedstawione analizy teoretyczne i wyniki symulacji komputerowych wskazują, że kształtowanie...
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Analytical techniques in studies of the environmental fate of pharmaceuticals and personal-care products
PublicationW pracy przedstawiono dane literaturowe odnośnie źródeł emisji, dróg transportu, przemian i metabolizmu, pomiomu stężeń ksenobiotyków z grupy farmaceutyków i środków higieny osobistej w próbkach pobranych z różnych elementów środowiska (woda, gleba, osady denne) oraz próbek bioty. Szczególną uwagę zwrócono na techniki analityczne wykorzystywane w badaniach losu środowiskowego w/w zanieczyszczeń.
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Recent Trends in the Application of Chromatographic Techniques in the Analysis of Luteolin and Its Derivatives
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Ultrahigh-resolution detection techniques for biomedical applications of optical coherent tomography.
PublicationOptyczne metody pomiarowe odgrywają w ostatnich latach coraz większą rolę w badaniach i diagnostyce medycznej. Mają one szereg zalet, do których zaliczyć można odporność na promieniowanie elektromagnetyczne, bezinwazyjność, bezpieczeństwo pomiaru oraz wysoką rozdzielczość. Jedną z najważniejszych technik stosowanych w diagnostyce medycznej jest koherentna tomografia optyczna (OCT). Jest to wysokorozdzielcza metoda obrazowania wewnętrznych...
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Comparison of the measurement techniques employed for evaluation of ambient air odour quality
PublicationThe paper presents the results of investigation on ambient air odour quality in a vicinity of the industrial sewage treatment plant being a part of the crude oil processing plant. The investigation was performed during spring-winter season using a prototype of electronic nose and the Nasal Ranger field olfactometers. The prototype was equipped with a set of six semiconductor sensors by FIGARO Co. and one PID-type sensor. The field...
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Remediation techniques for elimination of heavy metal pollutants from soil: A review
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