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Search results for: PTR-MS
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Sprawozdanie z XIII Ogólnopolskiej konferencji z cyklu „Ekologia humanistyczna” pt. „Przyroda wyzwaniem dla kultury. Społeczności lokalne wobec obszarów chronionych” (Warszawa, 16-17.10.2019)
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Opinia o konspekcie pracy doktorskiej Natalii Balcerzak pt. Rewitalizacja historycznych obiektów pobrowarnych w Polsce na przykładzie zespołu dawnego browaru w Gdańsku-Wrzeszczu
PublicationW opinii przedstawiono wskazówki merytoryczne do sformułowania tez rozprawy w dalszych nad nią pracach
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Uptake, accumulation, and translocation of Zn, Cu, Pb, Cd, Ni, and Cr by P. australis seedlings in an urban dredged sediment mesocosm: impact of seedling origin and initial trace metal content
PublicationThe study presents results from 6 months of phytoremediation of sediments dredged from three urban retention tanks carried out in a mesocosm setup with the use of P. australis. Two kinds of P. australis seedlings were considered: seedlings originating from natural (uncontaminated - Suncont) and anthropogenically changed environments (contaminated – Scont); this distinction was reflected in the baseline concentrations of trace metals...
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Determination of the chemical structure of potencial organic impurities occuring in the drug substance opopramol
PublicationThe tricyclic antipsychotic and antidepressant drug opipramol was examined with regard to the chemical structure of its organic impurities. Impurities were isolated from the technical product by chromatographic methods and their chemical structures were estabilished by HMNR, MS and FTIR.
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Real-Time Volatilomics: A Novel Approach for Analyzing Biological Samples
PublicationThe use of the ‘omics techniques in environmental research has become common-place. The most widely implemented of these include metabolomics, proteomics, genomics, and transcriptomics. In recent years, a similar approach has also been taken with the analysis of volatiles from biological samples, giving rise to the so-called ‘volatilomics’ in plant analysis. Developments in direct infusion mass spectrometry (DI-MS) techniques have...
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Low Cost Method for Location Service in the WCDMA System
PublicationA new and low cost method for a location service (LCS) in the Wideband Code Division Multiple Access (WCDMA) system is outlined. This method, which is called TDOA + RTT, enables calculation of the geographical position of a mobile station (MS) without knowledge of relative time differences (RTDs) between base stations (BSs). The TDOA+RTT method is based on the measurement of round trip times (RTTs) between the MS and the serving...
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The structure of nystatin A2
PublicationBudowa chemiczna składnika kompleksu nystatyn (nystatyny A2) została ustalona na podstawie analizy estru metylowego N-acetylonystatyny A2 przy pomocy metod spektroskopowych UV, MS i NMR. Widmo UV wskazało obecność w badanym związku chromoforu tetraenowego. Ciężar cząsteczkowy ustalono jako 909 j.m. na postawie analizy MS z wykorzystaniem techniki FAB, co pozwoliło wydedukować skład elementarny nystatyny A2 jako C47H75NO16. Analizy...
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Synthesis, physical properties and preliminary investigation of hemocompa-tibility of polyurethanes from aliphatic resources with castor oil participation
PublicationWykonano syntezy PUR z oligoeterodiolu, dioli małocząsteczkowych, oleju rycynowego i 4,4´diizocyjanianudicykloheksylometanu. Oznaczono właściwości mechaniczne PUR, kąty zwilżania i napięcie powierzchniowe. Opisano wstępne badania zgodności PUR z ludzką krwią oraz kalcyfikacji powierzchni PUR w warunkach statycznych in vitro. Napięcie powierzchniowe otrzymanych PUR jest zbliżone do napięcia powierzchniowego naturalnych powierzchni...
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Rapid Characterization of the Human Breast Milk Lipidome Using a Solid-Phase Microextraction and Liquid Chromatography-Mass Spectrometry-Based Approach.
PublicationHuman breast milk (HBM) is a biofluid consisting of various biomolecules such as proteins, lipids, carbohydrates, minerals and bioactive substances. Due to its unique and complex composition, HBM provides not only nutritional components required for the growth of the infant, but also additional protection against infections. Global insight into the composition of HBM is crucial to understanding the health benefits infants receive...
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Usuwanie par substancji organicznych z powietrza w biofiltrze ze złożami naturalnymi.**2003, 150 s. 111 rys. 23 tab. bibliogr. 102 poz. maszyn. Rozprawa doktorska /26.02.2003/ Wydz. Chem. Promotor: prof. dr hab. inż. B. Kawalec-Pietrenko.
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Occurrence and Levels of Biogenic Amines in Beers Produced by Different Methods
PublicationThe concentration of biogenic amines (BAs) in beer depends, among other factors, on the activity of microorganisms, in particular lactic acid bacteria. In this work an analytical method based on derivatization with tosyl chloride and high-performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) was used to determine 17 BAs in samples of commercially available beers, and to monitor the changes in concentration of...
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Sensor Position Estimation Method for IoT Using Mobile Reference Node
PublicationThe paper proposes an innovative method of locating objects for the Internet of Things (IoT). The proposed method allows the position of a fixed measuring sensor (MS) to be estimated using one mobile base station with a known position moving around the MS. The mathematical analysis of the method, and three algorithms — Newton’s (NA), gradient descent (GD) and genetic (GA) — for solving the system of non-linear positional equations...
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Pesticide residues levels in honey from apiaries located of Northern Poland
PublicationConcentration levels of 30 pesticide residues were measured in honey samples collected from apiaries in northern part of Poland (Pomerania) using method based on the QuEChERS extraction followed by liquid chromatography-tandem mass spectrometry with electron spray ionization (LC-ESI-MS/MS). In 29% of the samples were found positive for at least some of the target compounds. Concentration of bifenthrin, fenpyroximate, methidathion,...
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The role of hydrogen bonding on tuning hard-soft segments in bio-based thermoplastic poly(ether-urethane)s
PublicationThis work describes the preparation of bio-based thermoplastic poly(ether-urethane)s (TPU) via a prepolymer method and investigates the effect of varying the interphase hydrogen-bonding (H-bonding) on physicochemical, thermal and mechanical properties. This was achieved by varying the glycol type and molar ratio of [NCO]/[OH] groups used during the prepolymer chain extending step. The TPUs’ chemical structure was analyzed by Fourier...
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Synthesis and structural characterization of bio-based bis(cyclic carbonate)s for the preparation of non-isocyanate polyurethanes
PublicationBio-based cyclic carbonates are of significant research interest as monomers for non-isocyanate polyurethane (NIPU) synthesis. This research describes the synthesis of a series of five-membered bis(cyclic carbonate)s using bio-based polyether polyols (PO3G) with different molecular weights (250, 650 and 1000 g mol−1) and carbon dioxide as green feedstocks. The utilization of CO2 as a source of carbon in the chemical reaction is...
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Synthesis and Physicochemical Characteristics of Chitosan-Based Polyurethane Flexible Foams
PublicationThe use of shrimp waste to obtain chitosan (Ch) is an essential issue, considering a circular economy, waste management, and its application to environmentally friendly materials. In this study, northern prawn shells were utilized to obtain Ch, which could then be used for synthesizing chitosan-based polyurethane (PUR+Ch) foams with different Ch concentration. The chemical structure, morphology, hardness, thermal properties, viscoelastic...
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Reakcje difosfanów R2P-P(SiMe3)2 oraz ich pochodnych litowych R2P-P(SiMe3)Li z fosfanowymi kompleksami [(R3P)2MCl2], M = Pt, Pd, Ni
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Sprawozdanie z XIV Ogólnopolskiej konferencji naukowej z cyklu „Ekologia humanistyczna” pt. „Paradoksy ekologiczne – odpady miarą sukcesu i porażki cywilizowanej ludzkości” (Warszawa, 28‒29.10.2020)
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Ekspertyza dotycząca funkcjonowania dzielnicy Dolna Oliwa w rejonie ulic Kołobrzeska Piastowska (osiedle Przymorze) w ramach przygotowań i realizacji Festiwalu Streetwaves pt "Dobra Samotność"
Publicationprace eksperckie wraz z prelekcją oraz udziałem w panelu dyskusyjnym na temat możliwości rewitalizacji i reurbanizacji wielkich osiedli mieszkaniowych
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Multivariate Statistical Approach for Nephrines in Womenwith Obesity
PublicationCatecholamines are physiological regulators of carbohydrate and lipid metabolism during stress, but their chronic influence on metabolic changes in obese patients is still not clarified. The present study aimed to establish the associations between the catecholamine metabolites and metabolic syndrome (MS) components in obese women as well as to reveal the possible hidden subgroups of patients through hierarchical cluster analysis...
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The Mechanism of a Retro-Diels–Alder Fragmentation of Luteolin: Theoretical Studies Supported by Electrospray Ionization Tandem Mass Spectrometry Results
PublicationThe mechanisms of retro-Diels–Alder fragmentation of luteolin are studied theoretically using the Density Functional Theory method (B3LYP hybrid functional) together with the 6-311++G(d,p) basis set and supported by electrospray ionization tandem mass spectrometry (ESI-MS) results. The reaction paths leading to the formation of 1,3A and 1,3B fragment ions observed as the main spectral features in the ESI-MS spectrum are described...
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Chemical surface etching methods for ground tire rubber as sustainable approach for environmentally-friendly composites development– a review
PublicationGround tire rubber (GTR) has been used as a sustainable low-cost modifier in various composites. However, due to the hydrophobic nature of GTR, it is in compatible with most matrices and results in deterioration in both mechanical and physical properties of composites. This necessitates pre-modification of the powdered rubber to improve the interfacial bonding at the rubber-matric interface. The most common GTR modification research...
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Prediction of Overall In Vitro Microsomal Stability of Drug Candidates Based on Molecular Modeling and Support Vector Machines. Case Study of Novel Arylpiperazines Derivatives
PublicationOther than efficacy of interaction with the molecular target, metabolic stability is the primary factor responsible for the failure or success of a compound in the drug development pipeline. The ideal drug candidate should be stable enough to reach its therapeutic site of action. Despite many recent excellent achievements in the field of computational methods supporting drug metabolism studies, a well-recognized procedure to model...
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The template synthesis and complexation properties of the methoxypyrogal-lo[4]arene
PublicationZaprezentowano metodę syntezy templatowej MPA. Obserwowano kompleksowanie silnych akceptorów elektronów przez MPA. Analiza widm ESI-MS wykazała właściwości kompleksujące w stosunku do kationów metali alkalicznych. Właściwości jonoforowe związku badano w membranowych elektrodach jonoselektywnych.
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Getting to know the potential of social media in forest education
PublicationThe development of social network sites not only facilitates the acquisition and deepening of knowledge but also provides the possibility of easily contacting foresters, specialists in natural sciences and nature enthusiasts. In addition, for some years...
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On a matching distance between rooted phylogenetic trees
PublicationThe Robinson–Foulds (RF) distance is the most popular method of evaluating the dissimilarity between phylogenetic trees. In this paper, we define and explore in detail properties of the Matching Cluster (MC) distance, which can be regarded as a refinement of the RF metric for rooted trees. Similarly to RF, MC operates on clusters of compared trees, but the distance evaluation is more complex. Using the graph theoretic approach...
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The Current State-of-the-Art in the Determination of Pharmaceutical Residues in Environmental Matrices Using Hyphenated Techniques
PublicationSeveral thousand tons of pharmaceuticals and their transformation products (metabolites and degradation products) are introduced into the environment each year. They affect both human health and the environment, therefore, analytical procedures enabling the determination of a wide range of pharmaceuticals at trace levelswithminimal effort, time, and energy are required. Nowadays, hyphenated techniques are commonly applied in pharmaceutical...
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Determination of Pesticide Residues in Honeybees using Modified QUEChERS Sample Work-Up and Liquid Chromatography-Tandem Mass Spectrometry
PublicationIncreasing emissions of chemical compounds to the environment, especially of pesticides, is one of factors that may explain present honeybee colony losses. In this work, an analytical method employing liquid chromatography-tandem mass spectrometry (LC-MS/MS) was optimized for the simultaneous screening of 19 pesticides which have not been yet determined in honeybee samples from northern Poland (Pomerania). The sample preparation,...
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Nowa metoda lokalizowania terminala ruchomego w systemie WCDMA/FDD
PublicationW referacie zaprezentowano nową metodę lokalizowania terminala ruchomego w systemie WCDMA/FDD (Wideband Code Division Multiple Access / Frequency Division Duplex). Metoda ta umożliwia estymację położenia geograficznego terminala ruchomego MS (Mobile Station) bez znajomości różnic czasowych w synchronizacji RTD (Relative Time Difference) poszczególnych stacji bazowych BS (Base Station), biorących udział w tym procesie. Do eliminacji...
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Biobased Ultralow-Density Polyurethane Foams with Enhanced Recyclability
PublicationPolyurethane (PUR) foams are widely used in many engineering applications, but their efficient recycling has remained a major challenge for many years. This study presents a novel strategy of incorporating hydrolyzable ester units into the PUR structure to enhance PUR foam recyclability. The present ecodesign concept of PUR materials enables fully the replacement of petrochemical polyols with biobased alternatives and production...
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Chromium-Catalyzed CO2–Epoxide Copolymerization
PublicationIminopyrrole, aminopyrrole, and aminophosphine ligands were complexed with various chromium sources, producing eight complexes that were tested for their catalytic behavior toward epoxide–CO2 copolymerization. As elucidated by MALDI-TOF-MS, copolymerizations afforded polycarbonates and poly(ether-carbonates) exhibiting linear or cyclic topologies.
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Prediction of protein assemblies, the next frontier: The CASP14‐CAPRI experiment
PublicationWe present the results for CAPRI Round 50, the 4th joint CASP-CAPRI protein assembly prediction challenge. The Round comprised a total of 12 targets, including 6 dimers, 3 trimers, and 3 higher-order oligomers. Four of these were easy targets, for which good structural templates were available either for the full assembly, or for the main interfaces (of the higher-order oligomers). Eight were difficult targets for which only distantly...
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Intensification of catechin extraction from the bark of Syzygium cumini using ultrasonication: Optimization, characterization, degradation analysis and kinetic studies
PublicationCatechin is a prominent polyphenolic component that possesses various medicinal properties. Present work communicates the intensification and optimization of catechin extraction from the bark of Syzygium cumini tree using stirred reactor, soxhlet, ultrasonic bath, and ultrasonic horn technique. The optimization of several parameters such as type of solvent, solid to solvent ratio (1:100 w/v), speed of agitation (300 RPM), extraction...
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The Application of 2,6-Bis(4-Methoxybenzoyl)-Diaminopyridine in Solvent Extraction and Polymer Membrane Separation for the Recovery of Au(III), Ag(I), Pd(II) and Pt(II) Ions from Aqueous Solutions
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100-lecie powstania Zrzeszenia Studentów Polaków Politechniki Gdańskiej. Bratnia Pomoc i Korporacji ZAG Wisła
PublicationW 2021 roku przypada 100-lecie utworzenia Korporacji ZAG Wisła, nawiązującej do tradycji pierwszej polskiej organizacji Związku Akademików Gdańskich, oraz utworzenia i zalegalizowania samopomocowej organizacji zrzeszającej...
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Studies on fluorene stability in different liquid media. Badania stabilności fluorenu w środowiskach ciekłych.
PublicationPrzedstawiono degradację fluorenu w różnych rozpuszczalnikach (acetonitryl,metanol, woda, DMSO, heksan, cykloheksan). Proces monitorowano przy zastosowaniu techniki HPLC-DAD-MS. Zbadano wpływ światła, bakterii i temperatury.Zidentyfikowano produkty degradacji jakimi okazał się kwas salicylowy oraz g-fluorenon.
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Modelowanie ciągów danych z użyciem sieci neuronowych
PublicationRozdział opisuje problematykę przetwarzania ciągów danych. Opisane zostały typy ciągów danych: dane sekwencyjne, sekwencje czasowe oraz przebiegi czasowe. Przedstawiona została architektura sieci rekurencyj
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Performance properties of rigid polyurethane-polyisocyanurate/brewers’ spent grain foamed composites as function of isocyanate index
PublicationIn the presented work, rigid polyurethane-polyisocyanurate (PUR-PIR) foams filled with brewers’ spent grain (BSG) were prepared. The influence of the isocyanate index (II) on its performance was investigated. Foams obtained with higher isocyanate index required a higher amount of hydrofluorocarbon physical blowing agent to provide the same apparent density of material. An increase of isocyanate index resulted in a slight decrease...
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The Hydrolysis of Slowly Biodegradable Substrate in Activated Sludge
PublicationIn a present work a novel procedure, based on the standard batch tests and pretreatment of wastewater sample with coagulation-flocculation method, was proposed to evaluate the effects of hydrolysis of slowly biodegradable substrate (Xs) on biological nutrient removal (BNR) processes in activated sludge systems. The study was conducted at two large BNR wastewater treatment plants (WWTPs) in northern Poland: "Wschod" in Gdansk and...
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Analiza i badania pomiarowe dokładności lokalizowania terminali ruchomych w sieciach komórkowych
PublicationJakość oferowanych przez operatorów sieci komórkowych usług o wartości wzbogaconej (usług dodanych) zależy od efektywności metod estymacji położenia geograficznego terminala ruchomego MS (Mobile Station). Dokładność istniejących w sieciach komórkowych metod lokalizacyjnych jest niewystarczająca, szczególnie w odniesieniu do usług związanych z wywołaniem w niebezpieczeństwie. Obecnie, do najbardziej popularnej w sieciach komórkowych...
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A screening of select toxic and essential elements and persistent organic pollutants in the fur of Svalbard reindeer
PublicationReindeers play an important role in the polar ecosystem, being long-lived sole vegetarians feeding on local vegetation. They can be used as a valuable bioindicator, helping us to understand contaminants’ impact on the polar terrestrial ecosystem. Still, scarce data exist from research in which polar herbivores (especially those from the European parts of the Arctic) were a major study subject for trace elements and persistent organic...
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Nowe metody do badań składników obcych w miodach pszczelich
PublicationPszczoły, zbierając nektar, pyłek kwiatowy i spadź narażone są na częsty kontakt ze szkodliwymi substancjami (stosowanymi w rolnictwie) osadzonymi na roślinach i przenoszą te zanieczyszczenia - na powierzchni ciała lub wraz z pożytkami - do ula, i w konsekwencji zanieczyszczenia przedostają się do miodu.W związku z możliwością zanieczyszczenia miodu przez pestycydy należące do różnych klas związków chemicznych, pomocne okazuje...
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Pozostałości farmaceutyków w środowisku - problem daleki od rozwiązania
PublicationDo środowiska dostaje się coraz więcej związków pochodzenia farmaceutycznego. Zainteresowanie nimi tym bardziej wzrasta ze względu na ich niekorzystny wpływ nie tylko na środowisko, ale także na organizm ludzki. Mogą one powodować m.in. feminizację samców, wzrost odporności bakterii na antybiotyki oraz wzrost lekooporności ludzi. Dodatkowo farmaceutyki mogą przekształcać się w inne związki, których potencjał wywoływania efektów...
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Application of headspace-solid phase microextraction followed by gas chromatography-mass spectrometry to determine short-chain monocarboxylic acids in cattle farm wastewater and waste landfill leachates
PublicationZaproponowano metodykę oznaczania krótkołańcuchowych kwasów monokarboksylowych w ściekach z hodowli bydła i odciekach ze składowisk zawierających organiczne odpady, oparta na technice mikroekstrakcji do fazy stacjonarnej z fazy nadpowierzchniowej próbek ciekłych, w połączeniu ze sprzężonym układem GC-MS.
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Isolation and structure elucidation of phenolic compounds from Cyclopiasubternata Vogel (honeybush) intact plant and in vitro cultures
PublicationZ materiału roślinnego i hodowli tkankowych Cyclopia subternata Vogel (miodokrzew) wyizolowano i zidentyfikowano matodami NMR i MS 10 związków. m.in. z grupy flawonów i glikozydów izoflawonów. 6 z nich po raz pierwszy wykryto w tym gatunku roślin.
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Connection matrix theory for discrete dynamical systems
PublicationIn [C] and [F1] the connection matrix theory for Morse decomposition is developedin the case of continuous dynamical systems. Our purpose is to study the case of discrete timedynamical systems.
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Detekcja obumierania bakterii osadu czynnego
PublicationAnaliza składników głównych (PCA) jest narzędziem służącym wyodrębnieniu podstawowych czynników w rozważanych procesach w oparciu o dostępne pomiary. Zastosowanie PCA w monitorowaniu procesów pozwala na analizę pod kątem diagnostyki nie tylko wielkości mierzonych lecz również wielkości niedostępnych pomiarowo (ograniczenia technologiczne, koszty). Zaleta ta jest szczególnie istotna w przypadku biologicznej oczyszczalni ścieków,...
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Bisphenols and their derivatives in baby diaper samples.
PublicationMany common products contain and leach hazardous chemicals, including endocrine-disrupting chemicals such as bisphenols that are harmful to human health. For toddlers, this dangerousness is higher because of their not fully developed detoxification system. Due to this, bisphenols content in products such as baby diapers, should be monitored. Baby diapers not only remain in close contact with the skin, but are also used from the...
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Platelets in fetal growth restriction: role of reactive oxygen species, oxygen metabolism, and aggregation.
PublicationFetal growth restriction (FGR) is mainly caused by failure of the uteroplacental unit. Theexact pathogenesis remains unclear. The cause is thought to be related to abnormal platelet activation,which may...
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Thermal properties of tetrabutylammonium bromotrichloro-, tribromochloro-and tetrabromoferrates(III)
PublicationW pracy badana jest termiczna dekompozycja związków tetrabutylammonium bromotrichloro-, tribromochloro-and tetrabromoferrates(III). Analizę termiczną (TG-MS, DTA, DTG i DSC) prowadzono w atmosferze argonu w zakresie temperatur 293-1073 K. Stałe produkty dekompozycji identyfikowano metodą dyfrakcji promieniowania rentgenowskiego.