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Search results for: ZIRCONIUM ALLOYS
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Ferromagnetism in Pr-rich binary Pr7Ru3 intermetallic compound
PublicationWe present the synthesis and experimental characterization of the binary intermetallic compound Pr7Ru3. The polycrystalline sample was prepared by arc melting pure Pr and Ru, followed by homogenization at 500 °C and 600 °C for 48 and 89 h, respectively. Powder x-ray diffraction confirms that Pr7Ru3 crystallizes in an orthorhombic crystal structure (Pnma, space group no. 62) with the lattice parameters: a = 7.3606(7) Å, b = 23.120(1)...
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Intergranular Corrosion Detection Using Electromagnetic Transducers for Ultrasonic Testing
PublicationThe aim of this paper is to create a research methodology that allows a quick analysis of the structural state of high alloy austenitic steels using non-destructive ultrasonic tests, in contrast to destructive standard methods. Electromagnetic acoustic transducers (EMAT) are used to generate and receive the ultrasonic wave and detect the microstructural changes caused by sample sensitization in elevated temperature, even after...
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The Concept of a Methodology for Selecting the Optimal Parameters of Heat Received from a Nuclear Power Plant Operating in a Partial Cogeneration Mode
PublicationThe paper presents the concept of the objective function which is to allow the selection of optimal parameters of the district heating system using a nuclear power plant operating in partial cogeneration mode. The concept is based on research carried out a number of years ago. The size of annual expenses was proposed as the objective function, which allows to compare the operation of a nuclear power plant in partial cogeneration...
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“Piglia il bastone e battila molto bene… allora battila, non con animo irato, ma per zelo e carità dell’anima sua.” La violenza domestica secondo alcune testimonianze medievali
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Evaluation of the structures size in the liquid-gas flow by gamma-ray absorption
PublicationThe rapid development of tomography methods particularly electrical, X and gamma rays allows for a wide range of the information about flow structure. However, all of such methods are quite complicated. At the same time much simpler systems as the measuring system of gamma rays absorption, allows to obtain a all key flow information which describe the two-phase flow. In the article the results of analyzes of radiometric signal...
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Cathodic activation of synthesized highly defective monoclinic hydroxyl‐functionalized ZrO2 nanoparticles for efficient electrochemical production of hydrogen in alkaline media
PublicationThe high electrochemical stability of Zirconia (ZrO2) at high potentials strongly suggested it as an alternative to carbon supports, which experience reduced efficiency due to some corrosion problems particularly during prolonged electrocatalysis activity. However, the use of ZrO2 was limited by its low electrical conductivity and surface area. In this work, we developed a methodology for synthesizing monoclinic ZrO2 NPs with increased...
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Spray pyrolysis of doped-ceria barrier layers for solid oxide fuel cells
PublicationGadolinium doped ceria (Ce0.8Gd0.2O2 − x-CGO) layer fabricated by spray pyrolysis is investigated as the diffusion barrier for solid oxide fuel cell. It is deposited between the La0.6Sr0.4FeO3 − δ cathode and the yttria stabilized zirconia electrolyte to mitigate harmful interdiffusion of elements. The parameters of the fabrication process are linked to the measured area specific resistances of the symmetrical cells and the efficiency...
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Synthesis and characterization of novel renewable polyesters based on 2,5-furandicarboxylic acid and 2,3-butanediol
PublicationNovel polyesters from 2,5-furandicarboxylic acid or 2,5-dimethyl-furandicarboxylate and 2,3-butanediol have been synthesized via bulk polycondensation catalyzed by titanium (IV) n-butoxide, tin (IV) ethylhexanoate, or zirconium (IV) butoxide. The polymers were analyzed by size exclusion chromatography, nuclear magnetic resonance spectroscopy, Fourier transform infrared spectroscopy (FTIR), matrix-assisted laser ionization-desorption...
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Reliable method of assessing fracture properties of asymmetric bonded joints
PublicationTwo methods of assessing fracture properties of adhesive joints were studied. Two wedge tests: with continuous deflection and with force measurements were compared. Asymmetric geometry of the bonded joint was considered, i.e. two different plates of aluminium alloys: Al-Cu and Al-Mg, were bonded with epoxy DGEBA adhesive. The analytical model is shown to estimate the values of fracture properties: crack position and critical fracture...
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A Convenient Stereoselective Synthesis of trans-4a,5,8,8a-Tetrahydro-2H-isoquinolin-1-ones via trans 3-Allylation of 4-Allyl-3,4-dihydropyridine-2-thiones and RCM as Key Steps
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Improved performance of LaNi0.6Fe0.4O3 solid oxide fuel cell cathode by application of a thin interface cathode functional layer
PublicationIn this work, novel functional layers were prepared by a low temperature spray pyrolysis method on the oxygen side of the solid oxide cells. Thin layers of Ce0.8Gd0.2O2 and LaNi0.6Fe0.4O3 are prepared between the electrolyte and the porous oxygen electrode. Additionally the influence of the sprayed ceria barrier layer on the zirconia based electrolyte with the new layers is evaluated. Impedance spectroscopy results show improvement...
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Application of BAN Network to Increase Security in Transport Systems
PublicationIn the article general characteristics of the BAN network with M2M communications are presented. These are networks that enable the implementation of wireless transmission of signals using special sensors located on the body or implanted subcutaneously. These sensors allow monitoring of different type life parameters of a human. In the next part of work there is proposed the implementation of BAN networks to transport systems as...
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The dispersive micro-solid phase extraction method for MS-based lipidomics of human breast milk*
PublicationA simple and rapid microextraction method ensuring high lipidome coverage was developed for liquid chromatography mass spectrometry (LC-MS)-based lipidomics of human breast milk. The dispersive microsolid phase extraction (D-µ-SPE) technique, coupled with the design of experiment (DoE) method, enabled the study of the influence of several conditions (desorption solvent, stationary phase ratio, and sorption and desorption time)...
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Adaptation of radar software to work with ambiguous distance measurement
PublicationA software extension for radar stations designed to work in the low-PRF mode that allows them to correctly measure range to targets outside of their instrumented range, is proposed. The solution does not require substantial modifications of the radar software. Additionally, we describe tools that allow one to simulate the output of a low-PRF radar observing targets that are outside its instrumented range. The proposed approach...
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Atomic Force Microscope data post-processing algorithm for higher harmonics imaging
PublicationPrevious works have proved that higher harmonics topography imaging using atomic force microscope (AFM) can significantly enhanced its measurement capabilities. Integrated tools dedicated to most of microscopes allow to visualize the investigated surface only by one selected harmonic. Because of the different characteristics of a sample, scanning tip and the environment, appropriate harmonic selection is time consuming and requires...
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Application of wet powder spraying for anode supported solid oxide fuel cell with a perowskite SrTi0.98Nb0.02O3-d anode
PublicationAnode-supported solid oxide fuel cell with SrTi0.98Nb0.02O3–d anode, yttria-stabilized zirconia electrolyte and La(Ni0.6Fe0.4) O3d cathode has been successfully fabricated and evaluated. Process of anode support fabrication has been presented. Wet powder spraying and high temperature sintering method have been studied and applied to deposit the thin electrolyte layer.In order to improve catalytic properties of the anode, it has...
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Virtual reality technology in architectural education
PublicationContemporary virtual reality (VR) technology allows the recreation of non-existent architectural objects of which there may be no trace remaining. Virtual reality applications allow access to digital models, which visualise the lost architecture. The popularity of VR has resulted in it being applied not only to computer games, but also in visualising the past. Maps allow movement through historical trails and 3D models of architecture...
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Vascular stents - materials and manufacturing technologies
PublicationThe objective of this article is to present materials and technology for the manufacture of vascular stents with appropriate design requirements. The use of the right material is very important in implantology. A biomaterial introduced into the circulatory system must be biocompatible and hemocompatible. At the same time, it should not initiate toxic, mutagenic, or immunological reactions. Currently, 316L stainless steel (316L...
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The Influence of Laser Alloying of Ti13Nb13Zr on Surface Topography and Properties
PublicationThe laser alloying is a continually developing surface treatment because of its significant and specific structuration of a surface. In particular, it is applied for Ti alloys, being now the most essential biomaterials` group for load-bearing implants. The present research was performed on the Ti13Nb13Zr alloy subject to laser modification in order to determine the treatment effects on surface topography and its some mechanical...
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Structural and Transportation Properties of Strontium Titanate Composites with Ion Conductive Oxides
PublicationThis paper has been written based on the author’s doctoral dissertation “Structural and transportation properties of strontium and titanate composites with ion conductive oxides”, prepared under the supervision of Prof. Dr. Hab. Eng. Bogusław Kusz at the Department of Solid State Physics of Gdańsk University of Technology. It reports the idea of the thesis and conclusions from the study. Niobium doped strontium titanate (Sr(Ti,Nb)O3)...
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Bonding in Phosphanylphosphinidene Complexes of Transition Metals and their Correlation with Structures, 31 P NMR Spectra, and Reactivities
PublicationTheoretical studies of the bonding interactions and most important properties are carried out for isolable phosphanylphosphinidene complexes of transition metals. Three main types of phosphanylphosphinidene complexes are distinguished, based on the way in which the phosphanylphosphinidene ligand bonds to the metal center: (i) side-on complexes of platinum, where the R2Pβ–Pα ligand mimics structural features of free singlet phosphanylphosphinidenes...
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Hardware accelerated thin client for virtual reality applications
PublicationThin client applications often make minimal use of hardware available at the client side. This article focuses on the problem of creating portable thin client application for virtual reality applications, which allows use of client graphics hardware to aid rendering process. Some already available potential solutions are presented and entirely new protocol for client-server communication is presented to allow fast and reliable...
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Clonal selection algorithm for vehicle routing
PublicationOver the years several successful computing techniques have been inspired by biological mechanisms. Studies of the mechanisms that allow the immune systems of vertebratesto adapt and learn have resulted in a class of algorithms called artificial immune systems. Clonal selection is a process that allows lymphocytes to launch a quick response to known pathogens and to adapt to new, previously unencountered ones. This paper presents...
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Management of Textual Data at Conceptual Level
PublicationThe article presents the approach to the management of a large repository of documents at conceptual level. We describe our approach to representing Wikipedia articles using their categories. The representation has been used to construct groups of similar articles. Proposed approach has been implemented in prototype system that allows to organize articles that are search results for a given query. Constructed clusters allow to...
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TiO 2 Co x O y composite nanotube arrays via one step electrochemical anodization for visible light–induced photocatalytic reaction
PublicationTiO2CoxOy (x = 1, y = 1 or x = 3, y = 4) composite photocatalysts have been synthesized via one step anodic anodization of TiCo alloys. The effects of the cobalt content in the alloy (5, 10 and 15 wt%), water content (2, 5 and 10%) in the electrolyte solution, and applied voltage (30, 40 and 50 V) during the anodization process on the morphology and surface properties. Additionally, the dependence of cobalt content in the nanotubes...
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Knowledge base views
PublicationThe paper introduces an extension to the NeeK language. In the current shape NeeK allows for selection of fragments of a given ontology. The selected part is automatically mapped to a database schema by Data Views implementation. Experience with a real system using Data Views has shown that the resulting database schema does not necessarily reflect the needs of the business logic of an application that uses a specific Data View....
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Synthesis of 11,12-dihydro benzo[c]phenanthridines via a Pd-catalyzed unusual construction of isocoumarin ring/FeCl3-mediated intramolecular arene-allyl cyclization: First identification of a benzo[c]phenanthridine based PDE4 inhibitor
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The use of plate springs for preloading of a system of tapered roller bearings of a wind turbine gearbox
PublicationThe use of preloaded tapered roller bearings in wind turbine drive systems allows a transfer of load in the case of high variations of axial forces. The examined bearing system, a modification of a current design, consists of a pair of different sized bearings. Previous study showed the high sensitivity of tapered roller bearings on the existing radial interference. Dimensional tolerances used in the original design do not allow...
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The Hough transform in the classification process of inland ships
PublicationThis article presents an analysis of the possibilities of using image processing methods for feature extraction that allows kNN classification based on a ship’s image delivered from an on-water video surveillance system. The subject of the analysis is the Hough transform which enables the detection of straight lines in an image. The recognized straight lines and the information about them serve as features in the classification...
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Formation of Porous Structure of the Metallic Materials Used on Bone Implants
PublicationResearch on improvement of structure and fabrication methods of the bone implants are carried out for many years. Research are aimed to shape the structures, that will have a Young's modulus value similar to the value of the human bones Young's modulus. Depending on theporosity, Young's moduli can even be tailored to match the modulus of bone closer than solid metals can, thus reducing the problems associated with stress shielding...
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Three electrode configuration measurements of electrolyte-diffusion barrier-cathode interface
PublicationMeasurements of a system consisting of cathode/doped ceria diffusion barrier/doped zirconia electrolyte were made using two- and three-electrode configuration. Results obtained on a three-electrode measurement configuration were compared with and reflect the results obtained in two-electrode configuration. Three-electrode measurements allowed separating the impact of the symmetrical interface in the investigated system. They also...
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Effect of TiO2 Concentration on Microstructure and Properties of Composite Cu–Sn–TiO2 Coatings Obtained by Electrodeposition
PublicationIn this work, Cu–Sn–TiO2 composite coatings were electrochemically obtained from a sulfate bath containing 0–10 g/L of TiO2 nanoparticles. The effect of TiO2 particles on kinetics of cathodic electrodeposition has been studied by linear sweep voltammetry and chronopotentiometry. As compared to the Cu–Sn alloy, the Cu–Sn–TiO2 composite coatings show rougher surfaces with TiO2 agglomerates embedded in the metal matrix. The highest...
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Allergic reactions as a defense of the organism to the influence of implants components made of stainless steel
PublicationDue to the increasing number of cases of hypersensitivity caused by direct contact with metals, as well as the increasing demand for implants in humans all ages numerous studies on the effects of the impact of implant components are being carried out. The paper presents the phenomenon of etiology of allergy in general terms and in relation to the biomaterials used in medicine. There have been characterized in terms of impact on...
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Allergic Reactions as a Defense of the Organism to the Influence of Implants Components Made of Stainless Steel
PublicationDue to the increasing number of cases of hypersensitivity caused by direct contact with metals, as well as the increasing demand for implants in humans all ages numerous studies on the effects of the impact of implant components are being carried out. The paper presents the phenomenon of etiology of allergy in general terms and in relation to the biomaterials used in medicine. There have been characterized in terms of impact on...
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LaNi1-xCoxO3-δ(x=0.4 to 0.7) cathodes for solid oxide fuel cells by infiltration
PublicationPerformance of LaNi 1-x Co x O 3−δ (LNC) (x=0.4 to 0.7) as a cathode in solid oxide fuel cell (SOFC) is evaluated. Symmetrical cathode/electrolyte/cathode cells for electrochemical testing are prepared by infiltration of yttria stabilized zirconia (YSZ) backbone with LNC solutions. It is showed that the cathode infiltrated with LaNi 0.5 Co 0.5 O 3−δ (LNC155) has the lowest polarization resistance and activation energy, 197 mΩ cm...
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Information System for Drivers Within the Integrated Traffic Management System - TRISTAR
PublicationAdvanced traveler information systems (ATIS) for drivers are a very important element of modern traffic management. In recent years ITS infrastructure is being developed also in Poland. It allows for delivering to drivers information related to the conditions in the road network through, inter alia, dedicated Variable Message Signs (VMS). Such information enables drivers to take decisions, contributing to improving the efficiency...
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Determination of parent and methylated polycyclic aromatic hydrocarbons in water samples by dispersive liquid–liquid microextraction–two dimensional gas chromatography–time-of-flight mass spectrometry
PublicationPolycyclic aromatic hydrocarbons (PAHs) are contaminants frequently found in environmental waters. Owing to their toxic effects, it is important to develop analytical methodologies that allow their fast and reliable determination. Dispersive liquid–liquid microextraction (DLLME) allows a quick extraction of analytes with little organic solvent consumption. The best results regarding sample preparation are obtained when 40 mL of...
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Auto-tuning methodology for configuration and application parameters of hybrid CPU + GPU parallel systems based on expert knowledge
PublicationAuto-tuning of configuration and application param- eters allows to achieve significant performance gains in many contemporary compute-intensive applications. Feasible search spaces of parameters tend to become too big to allow for exhaustive search in the auto-tuning process. Expert knowledge about the utilized computing systems becomes useful to prune the search space and new methodologies are needed in the face of emerging heterogeneous...
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Glass-ceramic sealants and steel interconnects: accelerated interfacial stability and reactivity tests at high temperature
PublicationHigh-temperature reactions between glass-ceramic sealants and Fe-Cr alloy interconnects may lead to the formation of undesirable phases, and consequently degradation of solid oxide fuel/electrolyser devices. In this work, three different glass-ceramic sealants (Na-containing, Ba-containing, Sr-containing compositions) and Fe22Cr stainless steel powders (raw and pre-oxidised) are considered in order to test their chemical reactivity...
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A Visual Method of Measuring Railway-Track Weed Infestation Level
PublicationThis paper concerns the assessment of railway track surface conditions in relation to the degree of weed infestation. The paper conceptually describes the proposed method using a visual system to analyse weed infestation level. The use of image analysis software for weed detection is also proposed. This new measurement method allows for a mobile assessment of the track’s weed infestation status. Validation of the assessment method...
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Research on Linear Actuators for Active Foil Bearings
PublicationActive foil bearings are a kind of gas foil bearing. They contain actuators which allow for modification of the bearing sleeve size and the shape of the lubrication gap. Rotor vibrations can be actively controlled by these changes. It is possible, among other things, to reduce the starting torque, control the vibration amplitude at different speeds and improve operational safety. Prototypes of active foil bearings are being developed...
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Badania spawalności stali S460N w środowisku wodnym z wykorzystaniem próby Tekken
PublicationSpawanie w środowisku wodnym niesie ze sobą wiele problemów, wśród których najważniejszym jest skłonność stali do powstawania pęknięć zimnych. O ile w przypadku spawania na powietrzu istnieje wiele metod zapobiegania tym pęknięciom, o tyle pod wodą zastosowanie tych metod jest ograniczone. Z tego powodu konieczne jest określenie skłonności danego materiału do pękania zimnego. W pracy oceniono spawalność drobnoziarnistej...
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Fault Diagnostics in PEMFC Stacks by Evaluation of Local Performance and Cell Impedance Analysis
PublicationStarvation, flooding, and dry‐out phenomena occur in polymer electrolyte membrane fuel cells (PEMFCs), due to heterogeneous local conditions, material inhomogeneity, and uneven flow distribution across the single cell active area and in between the individual cells. The impact of the load level and air feed conditions on the performance was identified for individual single cells within a 10‐cell stack. Analysis of the current density...
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CGO as a barrier layer between LSCF electrodes and YSZ electrolyte fabricated by spray pyrolysis for solid oxide fuel cells
PublicationPerovskite La0.6Sr0.4Co0.2Fe0.8O3 − δ (LSCF) is often used as a cathode material for solid oxide fuel cells (SOFC) due to high mixed ionic and electronic conductivity and good catalytic activity. Unfortunately, sintering of the LSCF cathode together with the yttria stabilized zirconia (YSZ) electrolyte, leads to formation of the La2Zr2O7 and SrZrO3 phases in the interface. These phases increase the resistance of the cell. To avoid...
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Old Problems - New Solutions: Conversion of Capitals as a Tool for Shaping the Competitive Position in the Economic Field
PublicationThe acts and operations any social actor effectuates in each of the logically distinguished spheres of reality are conditioned by many factors, among which a reliable analysis of the strengths and weaknesses of an agent should be considered of utmost importance. The concept of capitals presented in this article divides the quantity of resources available to all acting agents into four main categories (which allows for determining...
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Old Problems - New Solutions: Conversion of Capitals as a Tool for Shaping the Competitive Position in the Economic Field
PublicationThe acts and operations any social actor effectuates in each of the logically distinguished spheres of reality are conditioned by many factors, among which a reliable analysis of the strengths and weaknesses of an agent should be considered of utmost importance. The concept of capitals presented in this article divides the quantity of resources available to all acting agents into four main categories (which allows for determining...
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Materials Design for the Titanium Scaffold Based Implant
PublicationThe main objective of here presented research is a design the scaffold/porous titanium(Ti) alloy based composite material demonstrating better biocompatibility, longer lifetime andbioactivity behaviour for load-bearing implants. The development of such material is proposed bymaking a number of consecutive tasks. Modelling the mechanical, biomechanical and biologicalbehavior of porous titanium structure and an elaboration of results...
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Materials Design for the Titanium Scaffold Based Implant
PublicationThe main objective of here presented research is a design the scaffold/porous titanium(Ti) alloy based composite material demonstrating better biocompatibility, longer lifetime andbioactivity behaviour for load-bearing implants. The development of such material is proposed bymaking a number of consecutive tasks. Modelling the mechanical, biomechanical and biologicalbehavior of porous titanium structure and an elaboration of results...
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System setup and software for cyclic, staircase and square wave voltammetry measurements
PublicationHardware dedicated for electrochemical measurement sometimes does not allow performing certain voltammetry experiments. Staircase and square wave voltammetry, techniques which have many advantages comparing with standard voltammetric techniques, are rarely implemented in software controlling electrochemical measuring equipment. These methods, however, can be relatively easy realized with some addition...
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APPLICATION OF APRIORI ALGORITHM IN THE LAMINATION PROCESS IN YACHT PRODUCTION
PublicationThe article specifies the dependence of defects occurring in the lamination process in the production of yachts. Despite great knowledge about their genesis, they cannot be completely eliminated. Authentic data obtained through cooperation with one of the Polish yacht shipyards during the years 2013–2017 were used for the analysis. To perform a simulation, the sample size was observed in 1450 samples, consisting of 6 models of...