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Search results for: L-DOPA
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Methodology of the Morphometry Study on Baltic Herring
PublicationAcoustic techniques are used in the estimation of the abundance of Baltic herring. Investigations of the relationship between the Baltic herring individual target strength TS and the total fish length L, significant in the acoustic assessment, demonstrated its de-pendence on the study area location. It motivated the detailed analysis of the relationship between herring from the southern Baltic ICES Subdivisions 24, 25, and 26,...
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The enantiomeric determination of chloro-precursors of methamphetamine
PublicationImpurity profiling and classification of seized methamphetamine may supply valuable information with respect to the conditions and the chemicals used in the illicit methamphetamine manufacture and may provide information on the original source of the sample. Determination of the stereochemical makeup of forensic samples is important as well for the same reasons. Laboratories in many places are engaged in clandestine manufacture...
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Wyznaczanie współczynnika dyspersji metodą kondultometryczną
PublicationW artykule przedstawiono konduktometryczną metodę wyznaczania współczynnika dyspersji w przypadku jednowymiarowym statystyczną metodą Fischera. Obliczenia wykonano na podstawie pomiarów przewodności nierozkładalnego trasera w postaci roztworu solanki (NaCl). Do tego celu wykonane zostało stanowisko pomiarowe złożone z prostego odcinka rurociągu wykonanego z polipropylenu o średnicy D=15 mm i długości L=44,05 m. Na wlocie i wylocie...
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Treatment of high-quality groundwater by means of one-stage filtration on active filtration beds
PublicationPrzeprowadzone badania pilotowe uzdatniania wody podziemnej wysokiej jakości, wykazały, że wody o niewielkich stężeniach żelaza (< 0,6 mgl) i manganu (<0,1 mg/l) można uzdatniać stosując napowietrznie i jednostopniową filtrację, w układzie zamkniętym, przez aktywne złoża filtracyjne. Wszystkie przebadane złoża (jednowarstwowe z piasku kwarcowego; dwuwarstwowe z piasku kwarcowego i piroluzytu oraz trzywarstwowe z antracytu, piasku...
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The effect of the annual growth and the late wood share upon density of the Polish pine wood as a function of its origin
PublicationW artykule przedstawiono zróżnicowanie gęstości polskiego drewna sosnowego (Pinus sylvestris L.) w zależności od udziału drewna późnego w przyroście rocznym z uwzględnieniem krainy pochodzenia drewna. Wspomniane zróżnicowanie jest w istotne statystycznie w skali globalnej oraz dla większości miejsc pochodzenia. Pomiar gęstości wykonano przy użyciu metody stereometrycznej. Metoda ta polegała na określeniu objętości pryzmy poprzez...
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Determination of chemical oxygen demand (cod) at boron-doped diamond (bdd) sensor by means of amperometric technique
PublicationA boron-doped diamond (BDD) sensor was proposed for effective detection of chemical oxygen demand (COD) by means of amperometric technique. Thin boron doped diamond active sensor layer was deposited on Si wafer and glassy carbon substrate by Microwave Plasma Enhanced Chemical Vapor Deposition (MW PE CVD). The structure of BDD was confirmed by Raman spectra analysis. Broad Raman bands centered at 482 cm-1 and 1219 cm-1 are typical...
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Construction of glucosamine-6-phosphate synthase with an internal hexahistydyl fragment
PublicationL-Glutamine: D-fructose-6-phosphate aminotransferase (EC 2.6.1.16), known also as glucosamine-6-phosphate (GlcN-6-P) syntase, catalyzes the first committed step in the amino sugar biosynthetic pathway in prokaryotic and eukaryotic organisms. The enzyme carries out a complex reaction involving ammonia transfer and sugar phosphate isomerization. GlcN-6-P syntase is an important point of metabolic control of amino sugar biosynthesis...
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Generalized Chebyshev Bandpass Filters With Frequency-Dependent Couplings Based on Stubs
PublicationThis paper presents an accurate synthesis method for inline and cross-coupled generalized Chebyshev bandpass filters with frequency-dependent couplings implemented via open and short stubs. The technique involves the synthesis of a lumped-element prototy pe in the form of a coupling matrix with a frequency-dependent term and the conversion of this prototype to a distributed-element mode l composed of sections of TEM lines. This...
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Determination of Chemical Oxygen Demand (COD) at Boron-doped Diamond (BDD) Sensor by Means of Amperometric Technique
PublicationA boron-doped diamond (BDD) sensor was proposed for effective detection of chemical oxygen demand (COD) by means of amperometric technique. Thin boron doped diamond active sensor layer was deposited on Si wafer and glassy carbon substrate by Microwave Plasma Enhanced Chemical Vapor Deposition (MW PE CVD). The structure of BDD was confirmed by Raman spectra analysis. Broad Raman bands centered at 482 cm-1 and 1219 cm-1 are typical...
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The effect of UV-C irradiation on lipids and selected biologically active compounds in human milk
PublicationThe effect of UV-C irradiation of human milk on lipid oxidation, content of antioxidants (vitamin C and catalase, CAT) and bactericidal compounds (lysozyme), as well as the total antioxidant capacity (TAC), of the breast milk was investigated. In parallel, the extent of inactivation of some bacteria was also determined. UV-C at doses from 85 to 740 J L−1 caused total inactivation of Escherichia coli and Staphylococcus aureus, but...
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Problems and chellenges to determine pesticide residues in bumblebees
PublicationBumblebees play an important role in t he pollination process of many crops and flowers. Therefore, taking action to protect and assess the impact of p esticides on these insects is fully justi fied. Pesticides may cause mortality and also sub-lethal effects that are not always directly visible. Bumblebees, like honeybees, can be used as indicators for environmental monitoring contamination. Two approaches are mainly used for the...
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Influence of different cultivation systems on bioactivity of asparagus
PublicationEvaluation of functional and bioactive compounds of Asparagus officinalis L. growing in conventional and organic greenhouse and conventional open –field farming was the aim of this research. Polyphenols in cladodes grown conventionally were higher than organic. Flavonoids and carotenoids were the highest in cladodes in open field. Organic spears were richer in total phenolics (+6.9% and +19.1%) and flavonoids (+4.7% and 16.8%)...
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SPEKTROSKOPOWE BADANIA WYŁADOWANIA MIKROFALOWEGO W ŹRÓDLE PLAZMY TYPU KOMORA REZONANSOWA ZASILANA FALOWODOWO
PublicationW pracy przedstawiono wyniki spektroskopowych badań wyładowania mikrofalowego (2,45 GHz) pod ciśnieniem atmosferycznym, generowanego w źródle plazmy typu komora rezonansowa. Gazami roboczymi były: argon, azot oraz metan, a także mieszaniny argon/metan oraz azot/metan. Natężenie przepływu gazu roboczego zmieniano w zakresie od 50 do 100 l/min, natomiast moc mikrofal absorbowanych przez wyładowanie wynosiła od 300 do 4000 W. Zmierzone...
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Food analysis using artificial senses.
PublicationNowadays, consumers are paying great attention to the characteristics of food such as smell, taste, and appearance. This motivates scientists to imitate human senses using devices known as electronic senses. These include electronic noses, electronic tongues, and computer vision. Thanks to the utilization of various sensors and methods of signal analysis, artificial senses are widely applied in food analysis for process monitoring...
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ASSESSMENT OF WEAR OF THE BANDSAW TEETH IN INDUSTRIAL CONDITIONS
PublicationA methodology for measuring bandsaw tooth wear is presented in this paper. This type of measurement is proposed as an alternative way of determining tooth wear in industrial conditions. The method is based on determining the KE value, i.e., the distance of the radius of the rounded cutting edge of the tooth and the intersection of the surface of the back and the surface of the face of the cutting wedge of the bandsaw tooth....
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Comparison of the fracture toughness of pine wood determined on the basis of orthogonal linear cutting and frame sawing
PublicationIn this paper, the values of the fracture toughness of Scots pine determined by cutting tests are presented. The cutting tests were carried out using the samples of Scotch pine (Pinus sylvestris L.) from Pomeranian Region, Poland. These experiments were carried out on two research stands: orthogonal linear cutting tests were conducted using the microtome instrument and the frame saw PRW-15M was used for sawing tests. The values...
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Inhibitors of glucosamine-6-phosphate synthase as potential antimicrobials or antidiabetics – synthesis and properties
PublicationGlucosamine-6-phosphate synthase (GlcN-6-P synthase) is known as a promising target for antimicrobial agents and antidiabetics. Several compounds of natural or synthetic origin have been identified as inhibitors of this enzyme. This set comprises highly selective L-glutamine, amino sugar phosphate or transition state intermediate cis-enolamine analogues. Relatively low antimicrobial activity of these inhibitors, poorly penetrating...
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Degradation of 1,4-dioxane by sono-activated persulfates for water and wastewater treatment applications
PublicationThis paper presents a hybrid advanced oxidation process (AOP) based on sonocavitational activation of persulfate (PS) for degradation of 1,4-dioxane during wastewater treatment. Application of sono-cavitation effectively convert PS to radical species demonstrating synergistic effect by increasing the reaction rate and reducing the required energy for activation. It is economically feasible and deployed alternative to the direct...
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Hybrid cross-linked chitosan/protonated-proline:glucose DES membranes with superior pervaporation performance for ethanol dehydration
PublicationThis work explores a protonated L-proline:glucose (molar ratio 5:1) deep eutectic solvent (DES) in fabricating biopolymer membranes utilizing chitosan (CS). Initially, the miscibility of CS and DES to prepare homogeneous dense blend membranes has been investigated. Different techniques, such as scanning electron microscopy, contact angle (CA), atomic force microscopy (AFM), Fourier transformed infrared spectroscopy (FTIR) and swelling...
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Simple smartphone-based methods for the determination of bioactive compounds in wine
PublicationA set of simple smartphone-based methods of bioactive compounds determination were developed for wine analysis. Procedures for smartphone-based determination of the total content of phenolic compounds, flavonoids, anthocyanins and biogenic amines, as well as measurement of antioxidant activity were developed and fully validated. The experimental setup is based on smartphone and 3D-printed device, though it is very simple and can...
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Effect of operating conditions on N 2 O production in an anammox sequencing batch reactor containing granular sludge
PublicationNitrous oxide (N2O) is one of the gases with the greatest impact in the atmosphere due to its persistence and significant contribution to the greenhouse effect. This study provides an insight into the dynamics of N2O production in wastewater nitrogen removal systems. A 10 L sequencing batch reactor containing enriched anammox biomass was subjected to different operational conditions, i.e., temperature, feed time, NO2 /NH4 þ ratio...
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Characterization of herbal teas containing lime flowers – Tiliae flos by HPTLC method with chemometric analysis
PublicationLinden trees are a source of food products called lime flowers (Tiliae flos), traditionally used in the form of infusion for the treatment of feverish colds and coughs. Lime flowers should include flowers of Tilia cordata Mill, T.x europaea L., and T. platyphyllos Scop. or a mixture of these. The aim of current research was to establish a fast, sensitive HPTLC (high-performance thin-layer chromatography) method that would allow...
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Isolation of the GFA1 gene encoding glucosamine-6-phosphate synthase of Sporothrix schenckii and its expression in Saccharomyces cerevisiae
PublicationGlucosamine-6-phosphate synthase (GlcN-6-P synthase) is an essential enzyme involved in cell wall biogenesis that has been proposed as a strategic target for antifungal chemotherapy. Here we describe the cloning and functional characterization of Sporothrix schenckii GFA1 gene which was isolated from a genomic library of the fungus. The gene encodes a predicted protein of 708 amino acids that is homologous to GlcN-6-P synthases...
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Marketing relacji : Geneza relationship marketing i jego cele
PublicationRozdział piąty opracowania dotyczy marketingu relacji. W pierwszym podrozdziale tego rozdziału prezentowana jest geneza relationship marketing. Interpretowane jest, w oparciu o definicje L. Berry'ego, A. Payne'a oraz M. Rydla i S. Ronkowskiego, pojęcie marketingu relacji. Dokonywana jest także prezentacja celów jakie stawiane są przed omawianą koncepcją. Cele te są charakteryzowane w oparciu o model sześciu rynków, model Gummessona,...
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Physical, chemical and biochemical properties of Western Siberia Sphagnum and Carex peat soils
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Benign Acute Childhood Myositis During Influenza B Outbreak
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On the selectivity of nanostructured semiconductor gas sensors
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Magnetism and structure ofLixCoO2and comparison toNaxCoO2
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Attitudes of Lazarski University Medical Students towards Disaster Medicine; Questionnaire Survey
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Observations of Cepheids in Pi of the Sky experiment
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Design Optimization of an Anisotropic Magnetoresistance Sensor for Detection of Magnetic Nanoparticles
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Fabrication of 3D graphene/MoS2 spherical heterostructure as anode material in Li-ion battery
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Formation and electronic properties ofBC3single-wall nanotubes upon boron substitution of carbon nanotubes
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Modeling the pH effects on nitrogen removal in the anammox-enriched granular sludge
PublicationThe aim of the study was to determine the pH effects on nitrogen removal in the anammox-enriched granular sludge. The experimental data were extracted from a 4L completely-mixed batch reactor with the granular sludge at different initial pH values (6.5, 7, 7.5, 8, 8.5, 9, 9.5, 10, 10.5) and constant temperature T=30℃. Simulations were run in GPS-X 6.4 using a comprehensive mechanistic model Mantis2. Two kinetic parameters, including...
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Electron collisions with cyanoacetylene HC3N : Vibrational excitation and dissociative electron attachment
PublicationWe experimentally probe electron collisions with HC3N in the energy range from 0 to 10 eV with the focus on vibrational excitation and dissociative electron attachment. The vibrational excitation cross sections show a number of resonances which are mode specific: the two dominant π∗ resonances are visible in the excitation of all the vibrational modes; however, broad σ ∗ resonances are visible only in certain bond-stretching vibrational...
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Adsorption-assisted transport of water vapour in super-hydrophobic membranes filled with multilayer graphene platelets
PublicationThe effects of confinement of multilayer graphene platelets in hydrophobic microporous polymeric membranes are here examined. Intermolecular interactions between water vapour molecules and nanocomposite membranes are envisaged to originate assisted transport of water vapour in membrane distillation processes when a suitable filler-polymer ratio is reached. Mass transport coefficients are estimated under different working conditions,...
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Interaction of cisplatin and two potential antitumoral platinum(ii) complexes with a model lipid membrane: a combined NMR and MD study
PublicationIn this study, the interaction of cisplatin (1) and two potential antitumoral Pt(II) complexes (2 and 3) with a model DMPC bilayer was investigated by multinuclear NMR spectroscopy and MD simulations in order to understand its implication for the different antitumoral properties shown by the three complexes. In particular, 31P, 13C and 2H solid state NMR experiments were performed to obtain information on the phase structure, phase...
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Edible black ant Smith (Carebara vidua) as human food – A systematic review
PublicationMeeting food security is one of the major global challenges to ensure sufficient supply of food for current and future generations, considering increasing population growth and climate change issues. Consequently, the consumption of edible insects as an alternative food source has recently gained global attention for combating global food insecurity. The present review aims to provide information on the recent progress in consumption...
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The measurement of the velocity field around a ship hull mo-del in a tawing tank using PIV method
PublicationRozdział zawiera wyniki badań eksperymentalnych pola prędkości wokół modelukadłubu statku metodą PIV. Wykazano prawidłowość zastosowania metody PIV wtego typu badaniach.
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Supported superparamagnetic Pd/Co alloy nanoparticles prepared from a silica/cyanogel co-gel
PublicationW pracy opisany jest sposób otrzymywania materiału kompozytowego zawierającego nanocząstki stopu Pd/Co. Obserwowane i dyskutowane jest przejście superparamagnetyczne pomiędzy 50K i 75K.
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Metoda prognozowania mocy skrawania przy przecinaniu piłami polskiego drewna sosnowego z uwzględnieniem wiązkości materiału obrabianego
PublicationW pracy zostały przedstawione wartości właściwości materiałowych tj.: wiązkość R oraz naprężenia tnące w strefie skrawania τy, dla drewna sosnowego (Pinus sylvestris L.). Badane próbki drewna pochodziły z czterech Krain Przyrodniczo - Leśnych Polski: Bałtyckiej Krainy Przyrodniczo - Leśnej (kraina A), Karpackiej Krainy Przyrodniczo - Leśnej (kraina B), Małopolskiej Krainy Przyrodniczo - Leśnej (kraina C) oraz Wielkopolsko - Pomorskiej...
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Comparison of Cadmium Cd2+ and Lead Pb2+ Binding by Fe2O3@SiO2‐EDTA Nanoparticles – Binding Stability and Kinetic Studies
PublicationThis study describes the synthesis and characterization of ethylenediaminetetraacetic acid (EDTA) functionalized magnetic nanoparticles of 20 nm in size – Fe3O4@SiO2‐EDTA – which were used as a novel magnetic adsorbent for Cd(II) and Pb(II) binding in aqueous medium. These nanoparticles were obtained in two‐stage synthesis: covering by tetraethyl orthosilicate and functionalization with EDTA derivatives. Nanoparticles were characterized...
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The antitumor compound triazoloacridinone C-1305 inhibits FLT3 kinase activity and potentiates apoptosis in mutant FLT3-ITD leukemia cells.
PublicationAim: FMS-like receptor tyrosine kinase (FLT3) is expressed in some normal hematopoietic cell types and plays an important role in the pathogenesis of acute myeloid leukemia (AML). In this study, we examined the effects of triazoloacridinone C-1305, an antitumor compound, on AML cells with different FLT3 status in vitro. Methods: A panel of human leukemic cell lines with different FLT3 status was used, including FLT3 internal tandem...
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Disruption of homocitrate synthase genes in Candida albicans affects growth but not virulence
PublicationDwa geny, LYS21 i LYS22, kodujące izoformy syntazy homocytrynianowej, enzymu katalizującego pierwszy wyjątkowy etap w szlaku biosyntezy lizyny, zostały rozbite z komórkach Candida albicans z wykorzystaniem strategii ''SAT flipper''. Podwójny mutant lys21delta/lys22delta nie wykazywał aktywności syntazy homocytrynianowej, natomiast charakteryzował się auksotrofią wzrostową wobec lizyny w podłożach minimalnych, co można było odwrócić...
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Application of single drop extraxtion (SDE) gas chromatography method for the determination of carbonyl compounds in spirits and vodkas
PublicationW pracy przedstawiono metodę oznaczania związków karbonylowych w spirytusach i wódkach, wykorzystującą do izolacji i wzbogacania technikę mikroekstrakcji do pojedynczej kropli (SDE)po derywatyzacji analitów O-(2,3,4,5,6-pentafluorobenzylo)hydroksylaminą. Określono optymalne parametry izolacji i wzbogacania aldehydów z roztworów alkoholowych (objętość próbki, objętość kropli, zawartość alkoholu, temperaturę i czas ekstrakcji)....
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Phenolic composition and antioxidant properties of polish blue-berried honeysuckle genotypes by HPLC-DAD-MS, HPLC postcolumn derivatization with ABTS or FC, and TLC with DPPH visualization
PublicationIn this study, different Polish cultivars of blue-berried honeysuckles (Lonicera caerulea L.), wild and bog bilberry, were analyzed for bioactive compounds. The chemical properties verified included composition of anthocyanins and other polyphenols, antioxidant activity, and profiles of antioxidants by HPLC postcolumn derivatization or TLC. The antioxidant activities of different blue-berried honeysuckle cultivars were similar...
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Application and optimization of headspace solid-phase microextraction (HS-SPME) coupled with gas chromatography - flame-ionization detector (GC-FID) to determine products of the petroleum industry in aqueous samples
PublicationA simple and solvent-free analytical method has been optimized for the determination of hydrocarbons (C6 - C20) from products of the petroleum industry in aqueous samples. Extraction and analysis was carried out using headspace solid-phase microextraction (HS-SPME) and gas chromatography coupled with flame-ionization detector (GC-FID). A ZB-5 capillary column (30 m × 0.25 mm inner diameter, 0.25 µm film thickness) was used for...
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Effect of Microplastics Pollution on Hydrogen Production from Biomass: A Comprehensive Review
PublicationHydrogen production from biomass and organic wastes is considered as a potential alternative energy source and is known as a clean and CO2-free fuel energy carrier. H2 is considered very promising among the other energy sources; therefore, the effective conversion of biomass and organic solid waste to this secondary energy source is urgently sought. As a result, it is of importance to assess the impact of the existence of microplastics...
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Integration of the sulfate reduction and anammox processes for enhancing sustainable nitrogen removal in granular sludge reactors
PublicationThe Anammox and Sulfate Reduction Ammonium Oxidation processes were compared in two granular sequencing batch reactors operated for 160 days under anammox conditions. It was hypothesized that increasing the concentration of SO42− may positively influence the rate of N removal under anaerobic conditions and it was tested whether SO42− reduction and anammox occur independently or are related to each other. The cooperation of N-S...
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Comparison of High Performance Liquid Chromatography Methods with Different Detectors for Determination of Steroid Hormones in Aqueous Matrices
PublicationThis paper presents the development and comparison of procedures for the qualitative and quantitative determination of five estrogenic compounds (17-a-ethynylestradiol, estrone, estradiol, estriol, and progesterone) in drinking water and wastewater samples. Five extraction columns and two disks were tested for their efficiency. The C18 columns were superior on the basis of cost for solid phase extraction of drinking water or sewage....