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Search results for: MASS SPECTROMWETERS
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Evaluation of flavour profiles in e-cigarette refill solutions using gas chromatography–tandem mass spectrometry
PublicationMany flavour compounds that are present in e-liquids for e-cigarettes are responsible for specific tastes and smoking sensations for users. Data concerning content and specific types of flavours is often limited and unknown to users. The aim of the research was to define and compare flavour profiles of e-liquids with the same group taste from different manufacturers. Gas chromatography coupled with tandem mass spectrometry (GC–MS/MS)...
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Exchange-Traded Funds on European Markets: Has Critical Mass been Reached? Implications for Financial Systems.
PublicationExchange-traded funds (ETFs) are one of the most rapidly expanding categories of financial products in Europe. One of the key yet still unanswered questions is whether European ETF markets have reached the size at which they could affect the financial systems. In our study, we examine 13 European countries during the period 2004–2017 in order to trace whether the share of ETFs in the total assets of investment funds has reached...
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Simulations of hydro-fracking in rock mass at meso-scale using fully coupled DEM/CFD approach
PublicationThe paper deals with two-dimensional (2D) numerical modelling of hydro-fracking (hydraulic fracturing) in rocks at the meso-scale. A numerical model was developed to characterize the properties of fluid-driven fractures in rocks by combining the discrete element method (DEM) with computational fluid dynamics (CFD). The mechanical behaviour of the rock matrix was simulated with DEM and the behaviour of the fracturing fluid flow...
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2014 POSTER Serum proteome mass spectrometry analyses for identification of novel diagnostic biomarkers in breast cancer patients
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Headspace Solid-Phase Microextraction Coupled with Gas Chromatography–Mass Spectrometry for the Determination of Volatile Organic Compounds in Urine
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Investigation of the flow, heat and mass transfer and emissions in pulverized fuel fired boiler using physical and numerical modeling.
PublicationPraca przedstawia wykorzystanie techniki modelowania fizycznego trójwymiarowego oraz obliczeń numerycznych umożliwiających symulację rzeczywistych procesów spalania paliw stałych i gazowych w urządzeniach energetycznych. Dodatkowo wyniki obliczeń porównano z wynikami modelowania fizycznego oraz pomiarów na obiekcie rzeczywistym.
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Analytical techniques for trace organic compounds - IV: Tandem mass spectrometry for organic trace analysis (Technical Report)
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Application of dispersive liquid-liquid microextraction for the determination of selected organochlorine pesticides in honey by gas chromatography - mass spectrometry
PublicationDispersive liquid-liquid microextraction (DLLME) is a rapid and easy technique that consumes minute amounts of organic solvents. In this work, we present chemometric study on optimization of DLLME parameters for the extraction of aldrin, endrin, lindane, alfa-endosulfan, 4,4'-DDT and its metabolites from honey matrix. Method quantification limits (MQLs) vary between 0.3 ng/g for 2,4'-DDE and 4,4'-DDE to 13.2 ng/g for alfa-endosulfan...
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Absence of 6-Hydroxydopamine in the Rat Brain After Treatment with Stimulants and Other Dopaminergic Agents: A Mass Fragmentographic Study
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A new silylation reagent dimethyl(3,3,3-trifluoropropyl)silyldiethylamine for the analysis of estrogenic compounds by gas chromatography–mass spectrometry
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Determination of twenty pharmaceutical contaminants in soil using ultrasound-assisted extraction with gas chromatography-mass spectrometric detection
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A targeted mass spectrometry immunoassay to quantify osteopontin in fresh-frozen breast tumors and adjacent normal breast tissues
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Some aspects of the analysis of environmental pollutants in sediments using pressurized liquid extraction and gas chromatography-mass spectrometry
PublicationOpisano wyniki badań nowej procedury oznaczania analitów z grupy wielopierścieniowych węglowodorów aromatycznych oraz polichlorowanych bifenyli w próbkach osadów dennych. Szczególnie dużo uwagi poświęcono zbadaniu możliwości wykorzystania techniki przyspieszonej ekstrakcji analitów za pomocą rozpuszczalnika na etapie izolacji wzbogacania. Ustalono również warunki oznaczeń końcowych z wykorzystaniem techniki GC-MS.
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Post-Chromatographic Derivatization Coupled with Mass Spectrometry as a Method of Profiling and Identification of Antioxidants; Ligustrum vulgare Phytocomplex as an Example
PublicationHigh-performance liquid chromatography (HPLC) and high-performance thin-layer chromatography (HPTLC) coupled with radical scavenging assays, such as 2,2-diphenyl-1-picrylhydrazyl (DPPH) and 2,2′-azinobis-(3-ethylbenzothiazoline-6-sulfonic acid (ABTS) can be both used for the detection of the antioxidants in plant extracts. In this study, the ethanolic (70% v/v) extracts from different morphological parts of Ligustrum vulgare collected...
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Singlet oxygen in the removal of organic pollutants: An updated review on the degradation pathways based on mass spectrometry and DFT calculations
PublicationThe degradation of pollutants by a non-radical pathway involving singlet oxygen (1O2) is highly relevant in advanced oxidation processes. Photosensitizers, modified photocatalysts, and activated persulfates can generate highly selective 1O2 in the medium. The selective reaction of 1O2 with organic pollutants results in the evolution of different intermediate products. While these products can be identified using mass spectrometry...
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Determination of antifreeze substances in the airport runoff waters by solid-phase microextraction and gas chromatography–mass spectrometry method
PublicationA new method has been developed for the determination of antifreeze agents such as ethylene glycol (EG), propylene glycol (PG), and diethylene glycol (DEG) in the samples of airport runoff water. The method is based on headspace solid–phase microextraction (HS–SPME) of target analytes, which is coupled with gas chromatography–mass spectrometry (GC–MS). Until now, there was a lack of appropriate methodology for collecting reliable...
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Analysis of multi-class pharmaceuticals in fish tissues by ultra-high-performance liquid chromatography tandem mass spectrometry
PublicationA new sensitive method based on pressurized liquid extraction (PLE) and purification by gel permeation chromatography (GPC) prior to ultra-high-performance liquid chromatography coupled to tandem mass spectrometry (UHPLC–MS/MS) was developed for the determination in fish homogenate, liver and muscle of twenty pharmaceuticals compounds and metabolites from seven commonly used therapeutic families. An extensive matrix effect evaluation...
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Development of a liquid chromatography–tandem mass spectrometryprocedure for determination of endocrine disrupting compounds infish from Mediterranean rivers
PublicationA new, sensitive and rapid method based on QuEChERS (Quick, Easy, Cheap, Effective, Rugged and Safe)approach followed by ultra high performance liquid chromatography coupled with tandem mass spec-trometry (UHPLC–MS/MS) was developed for the determination of nineteen endocrine disruptors (EDCs)and related compounds belonging to different classes in various fish species. Matrix effect on the analyti-cal performance was evaluated,...
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Determination of nine high-intensity sweeteners in various foods by high-performance liquid chromatography with mass spectrometric detection
PublicationAn analytical procedure involving solid-phase extraction (SPE) and high-performance liquid chromatography-mass spectrometry has been developed for the determination of nine high-intensity sweeteners authorised in the EU; acesulfame-K (ACS-K), aspartame (ASP), alitame (ALI), cyclamate (CYC), dulcin (DUL), neohesperidin dihydrochalcone (NHDC), neotame (NEO), saccharin (SAC) and sucralose (SCL) in a variety of food samples (i.e. beverages,...
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Identification of pollutants at the adjacent areas to the landfill site using two dimensional gas chromatography with mass spectrometry technique
PublicationMunicipal landfills are considered one of the main sources of air pollutants. In this article is presented the use of a modern analytical technique: a two dimensional gas chromatography to identify the substances in the atmospheric air near a waste processing plant located in Gdansk. In order to determine the types of substances occurring in different atmospheric conditions, the study was conducted from February to April 2016....
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Analysis of volatile fraction of hybrid fruit pulp using Proton Transfer Reaction - Time-Of-Flight Mass Spectrometry
PublicationFruits and vegetables are important ingredients in human diet. Because of this, it is very important to know their exact composition and to control their quality. Based on the aroma of food products, it is possible to pre-evaluate their quality and freshness. The aim of this work was to characterize the volatile fraction of the hybrid fruit ‘sweetie’ using the modern analytical device PTR-TOFMS. Hybrid fruit samples are human-made...
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Mass transfer in the bath reactor of the adsorption process of 1,2-dichloropropane from aqueous solution onto the activated carbon
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Uncertainty of mass flow measurement using centric and eccentric orifice for Reynolds number in the range 10,000 ≤ Re ≤ 20,000
PublicationThe article analyses the impact of the Reynolds number on the estimated uncertainty of the mass flow rate measurement using an orifice plate. The objects of the research were two types of orifices: centric (ISA) and eccentric, with the diameter ratio β = 0.5. Studies were performed by Monte Carlo simulation and experiments for Reynolds numbers in the range 10,000 ≤ Re ≤ 20,000. The obtained results have shown that for both orifice...
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Fixed point index for $G$-equivariant multivalued maps
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Struktury mikropaskowe z uszkodzoną warstwą metalizacji masy
PublicationRozważono sekcje linii mikropaskowych z uszkodzeniemi-wytrawieniami w metalizacji masy. Badano możliwości wykorzystania takich struktur w konstrukcji filtrów dolnoprzepustowych oraz górno- bądź pasmowo zaporowych. Zaprojektowano, wykonano i przebadano sekcję z dwuelementowym zaburzeniem w metalizacji. Stwierdzono występowanie efektów spowolnienia fal (prowadzących do miniaturyzacji układu) oraz możliwości wykorzystania struktury...
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Identyfikacja stałej reprezentującej bezwładność masy przepływającej wody
PublicationW artykule przedstawiono sposób identyfikacji wartości parametru reprezentującego bezwładność masy przepływającej wody dla hydrozespołów pracujących przy dużym spadzie i długich rurociągach. Opisany sposób identyfikacji wykorzystywany jest w adaptacyjnej metodzie synchronizacji. Do identyfikacji wykorzystuje się uproszczony model matematyczny układu regulacji prędkości kątowej oraz początkową fazę odpowiedzi synchronizowanego obiektu.
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Struktury mikropaskowe z uszkodzoną warstwą metalizacji masy
PublicationPrzedstawiono struktury linii mikropaskowej ze świadomie wprowadzonymi uszkodzeniami metalizacji masy (DGS - Defected Ground Structure). Zaobserwowano wystąpienie filtracji dolnoprzepustowej oraz pasmowej górnozaporowej. Zaprojektowano, wykonano i przebadano dwelementową strukturę filtru. Zauważono efekt spowolnienia fali prowadzący do redukcji wymiarów układu oraz stwierdzono wystąpienie znaczącego tłumienia przy wyższych częstotliwościach.
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Local fixed point indices of iterations of planar maps
PublicationW artykule podana zostaje postać indeksów iteracji dla pewnej klasy odwzorowań planarnych. Podstawowymi narzędziami stosowanym w pracy są liczba Nielsena i indeks Conleya.
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Statyczne i dynamiczne badania własności masy polimerowej
PublicationPolimer jest materiałem, który coraz częściej znajduje zastosowanie w budownictwie w przypadku konstrukcji narażonych na wpływy dynamiczne. Poprzez dodanie do składu polimeru odpowiednich składników możliwe jest otrzymanie materiału o specjalnych parametrach, np. o zwiększonym tłumieniu. Od kilku lat masa polimerowa stosowana jest w tzw. metodzie złączy podatnych. Potwierdzono również jej efektywność w zastosowaniu do elementów...
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Music Mood Visualization Using Self-Organizing Maps
PublicationDue to an increasing amount of music being made available in digital form in the Internet, an automatic organization of music is sought. The paper presents an approach to graphical representation of mood of songs based on Self-Organizing Maps. Parameters describing mood of music are proposed and calculated and then analyzed employing correlation with mood dimensions based on the Multidimensional Scaling. A map is created in which...
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Evaluation of a Novel Approach to Virtual Bass Synthesis Strategy
PublicationThe aim of this paper is to present a novel approach to the Virtual Bass Synthesis (VBS) strategy applied to portable computers. The developed algorithms involve intelligent, rule-based settings of bass synthesis parameters with regard to music genre of an audio excerpt and the type of a portable device in use. The Smart VBS algorithm performs the synthesis based on a nonlinear device (NLD) with artificial controlling synthesis...
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Shub’s conjecture for smooth longitudinal maps of S^m
PublicationLet f be a smooth map of the m-dimensional sphere Sm to itself, preserving the longitudinal foliation. We estimate from below the number of fixed points of the iterates of f , reduce Shub’s conjecture for longitudinal maps to a lower dimensional classical version, and prove the conjecture in case m = 2 and in a weak form for m = 3.
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The Hopf type theorem for equivariant gradient local maps
PublicationWe construct a degree-type otopy invariant for equivariant gradient local maps in the case of a real finite-dimensional orthogonal representation of a compact Lie group. We prove that the invariant establishes a bijection between the set of equivariant gradient otopy classes and the direct sum of countably many copies of Z.
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Periodic points of latitudinal maps of the $m$-dimensional sphere
PublicationLet f be a smooth self-map of the m-dimensional sphere Sm. Under the assumption that f preserves latitudinal foliations with the fibres S1, we estimate from below the number of fixed points of the iterates of f. The paper generalizes the results obtained by Pugh and Shub and by Misiurewicz.
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Generalized Gradient Equivariant Multivalued Maps, Approximation and Degree
PublicationConsider the Euclidean space Rn with the orthogonal action of a compact Lie group G. We prove that a locally Lipschitz G-invariant mapping f from Rn to R can be uniformly approximated by G-invariant smooth mappings g in such a way that the gradient of g is a graph approximation of Clarke’s generalized gradient of f . This result enables a proper development of equivariant gradient degree theory for a class of set-valued gradient...
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A method to determine the tightening sequence for standing rigging of a mast
PublicationThe article proposes an alternative method to determine the sequence of generation of pre-tension forces in standing rigging of a mast. The proposed approach has been verified on both a virtual simulation experiment and laboratory tests. In this method, the desired tension values are obtained using the influence matrix which allows to calculate the effect of tension change in an individual rope on the tension distribution in the...
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The method of measuring the energy pass-band of a communication receiver
PublicationPrzedstawiono metodę wyznaczania energetycznego pasma odbiornika radiokomunikacyjnego na podstawie charakterystyki gęstości widmowej mocy szumów własnych na wyjściu odbiornika. Podano numeryczny estymator tego pasma. Wyprowadzono zależności na złożoną niepewność standardową wyznaczania szerokości pasma energetycznego odbiornika.
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Ensembling noisy segmentation masks of blurred sperm images
PublicationBackground: Sperm tail morphology and motility have been demonstrated to be important factors in determining sperm quality for in vitro fertilization. However, many existing computer-aided sperm analysis systems leave the sperm tail out of the analysis, as detecting a few tail pixels is challenging. Moreover, some publicly available datasets for classifying morphological defects contain images limited only to the sperm head. This...
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Online Volatile Compound Emissions Analysis Using a Microchamber/Thermal Extractor Coupled to Proton Transfer Reaction-Mass Spectrometry
PublicationIndoor air is a complex and dynamic mixture comprising manifold volatile organic compounds (VOCs) that may cause physiological and/or psychological discomfort, depending on the nature of exposure. This technical note presents a novel approach to analyze VOC emissions by coupling a microchamber/thermal extractor (μ-CTE) system to a proton transfer reaction-mass spectrometer (PTR-MS). This configuration provides an alternative to...
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An evaluation of sucrose as a possible contaminant in e-liquids for electronic cigarettes by hydrophilic interaction liquid chromatography–tandem mass spectrometry
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The use of fast molecular descriptors and artificial neural networks approach in organochlorine compounds electron ionization mass spectra classification
PublicationDeveloping of theoretical tools can be very helpful for supporting new pollutant detection. Nowadays, a combination of mass spectrometry and chromatographic techniques are the most basic environmental monitoring methods. In this paper, two organochlorine compound mass spectra classification systems were proposed. The classification models were developed within the framework of artificial neural networks (ANNs) and fast 1D and...
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Mass spectrometry-based analysis of therapy-related changes in serum proteome patterns of patients with early-stage breast cancer
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High-resolution synthesis of high-density breast mammograms: Application to improved fairness in deep learning based mass detection
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Estimation of platinum in environmental water samples with solid phase extraction technique using inductively coupled plasma mass spectrometry
PublicationZoptymalizowano metodykę oznaczania śladowych poziomów stężeń platyny (IV) w oparciu o technikę ekstrakcji do fazy stałej w połączeniu ze spektrometrią mas z plazmą wzbudzoną indukcyjnie. Na etapie wzbogacania platyny wykorzystano żel krzemionkowy modyfikowany grupami aminopropylowymi. Ilościowy odzysk platyny uzyskano poprzez wykorzystanie 1.0 mol L-1 roztworu tiomocznika jako eluenta. Odchylenie standardowe wyników (RSD) było...
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Comparison of different techniques for extracting Polychlorinated Biphenyls from bottom sediment samples using Isotope Dilution Mass Spectrometry
PublicationIn this work, problems that may occur during determination of trace levels of polychlorinated biphenyls in sediment samples are described. The main error sources are connected with extraction of analytes prior to final determination. During model studies, polychlorinated biphenyls have been extracted from sediment reference material (METRANAL 2) with the use of different solvents (dichloromethane, hexane, and toluene); the process...
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On-line assessment of oil quality during deep frying using an electronic nose and proton transfer reaction mass spectrometry
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The quantification of bisphenols and their analogues in wastewaters and surface water by an improved solid-phase extraction gas chromatography/mass spectrometry method
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Direct injection liquid chromatography-mass spectrometry (DI-LC-MS) analysis for rapid lipidomic profiling of extracellular vesicles
PublicationExtracellular vesicles (EVs) are small, spherical particles produced by eukaryotic and prokaryotic cells, surrounded by a bilayer membrane and carrying various bioactive molecules, such as proteins, surface receptors, membrane and soluble proteins, lipids, and nucleic acids. EVs are of substantial interest because of their important roles in cell communication, epigenetic regulation and possible application in disease diagnosis...
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Characterization of the interactions between human high-molecular-mass kininogen and cell wall proteins of pathogenic yeasts, Candida tropicalis
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An evaluation of sucrose as a possible contaminant in e-liquids for electronic cigarettes by hydrophilic interaction liquid chromatography–tandem mass spectrometry
PublicationThe influence of sucrose combustion products on smoking and nicotine addiction is still controversial because the presence of the sucrose may be treated as a source of aldehydes and organic acids. In e-liquids used as refills for electronic cigarettes, which are made primarily of poly(propylene glycol), glycerine and ethanol, sucrose may be present at trace levels, and its impact on mainstream smoke formation, and hence on human...