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Bis(dithiobenzoato-k2S,S')bis(tetrahydrofuran-kO)magnesium(II)
PublicationTytułowy związek [Mg(C7H5S2)2(C4H8O)2] został otrzymany w reakcji PhMgBr z nadmiarem CS2. Jest to pierwszy kompleks magnezu zawierający dwa ligandy ditiobenzoesanowe. Kompleks posiada zniekształconą geometrię oktaedryczną.
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An investigation on the chemistry of the R2P=P ligand: reactions of a phosphanylphosphinidene complex of tungsten(VI) with electrophilic reagents
PublicationThe nucleophilic properties of the title compound [(2,6-i-Pr2C6H3N)2(Cl)W(η2-t-Bu2PvP)]Li·3DME (1) were investigated in reactions with selected electrophilic reagents such as MeI, M(CO)5THF (M = Cr, Mo, W), AlCl3, and GaCl3. Methylation of 1 by MeI yields phosphanylphosphido complexes [(2,6-i-Pr2C6H3N)2W(X)(1,2-η-t-Bu2PvP–CH3)] (X = Cl, I) (2-Cl/2-I) with the formation of a new P–C bond. Moreover, 1 reacts with electrophilic compounds...
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The Reactivity of Phosphanylphosphinidene Complexes of Transition Metals Toward Terminal Dihaloalkanes
PublicationThe reactivities of phosphanylphosphinidene complexes [(DippN)2W(Cl)(η2-P−PtBu2)]− (1), [(pTol3P)2Pt(η2- P=PtBu2)] (2), and [(dppe)Pt(η2-P=PtBu2)] (3) toward dihaloalkanes and methyl iodide were investigated. The reactions of the anionic tungsten complex (1) with stochiometric Br(CH2)nBr (n = 3, 4, 6) led to the formation of neutral complexes with a tBu2PP(CH2)3Br ligand or neutral dinuclear complexes with unusual tetradentate...
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Syntheses and structures of the first terminal phosphanylphosphido complex of hafnium [cp2hf(cl){η1-(me3si)p-p(net2)2}] and the firstzirconocene-phosphanylphosphinidene dimer [cp2zr{μ2-p-p(net2)2}2zrcp2]
PublicationReactions of (Et2N)2P-P(SiMe3)Li with [Cp2MCl2] (M= Zr, Hf) in toluene or pentane yield the related terminal phosphanylphosphido complexes [Cp2M(Cl){η1-(Me3Si)P-P(NEt2)2}]. The solid statestructure of [Cp2Hf(Cl){η1-(Me3Si)P-P(NEt2)2}] was established by single crystal X-ray diffraction. The reaction of (Et2N)2P-P(SiMe3)Li with [Cp2ZrCl2] in THF or DME solutions leads to the formationof deep red crystals of the first neutral diamagnetic...
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General route for the synthesis of terminal phosphanylphosphido complexes of Zr(IV) and Hf(IV): Structural investigations of the first zirconium complex with a phosphanylphosphido ligand
PublicationReactions of R2P-P(SiMe3)Li with [Cp2MCl2] (M = Zr, Hf) in hydrocarbons yield the related terminal phosphanylphosphidocomplexes [Cp2M(Cl){(Me3Si)P-PR2-jP1}] (R = iPr and tBu). The solid state structures of [Cp2M(Cl){P(SiMe3)-PiPr2-jP1}] (M = Zr, Hf) were established by single crystal X-ray diffraction studies. The phosphido-P atoms adopt almost planar geometries and the phosphanyl P atoms adopt pyramidal geometries. The reaction...
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The new diphosphanylphosphido complexes of tungsten(VI) and molybdenum(VI). Their synthesis, structures and properties
PublicationWe report on the reactivity of R2P–P(Li)–PR’2 (R = tBu, iPr, R’ = NEt2, iPr) towards diimido complexes [(dippN)2MCl2·dme] (M = Mo, W and dipp = 2,6-iPr2C6H3). A series of new complexes with diphosphanylphosphido ligands R2P–P–PR’2 were isolated. The solid-state structures of [(dippN)2M(Cl)(1,2-η-iPr2P–P– PiPr2)] (2Mo and 2W) and [(dippN)2M(Cl){1,2-η-tBu2P–P–P(NEt2)2}] (3Mo and 3W) were established by single-crystal X-ray diffraction...
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Reactions of (Ph)tBuP-P(SiMe3)Li·3THF with [(PNP)TiCl2] and [MeNacNacTiCl2·THF]. Synthesis of first PNP titanium(IV) complex with phosphanylphosphinidene ligand [(PNP)Ti(Cl){η2-P-P(Ph)tBu}]
PublicationLithium derivative of diphosphane (Ph)tBuP-P(SiMe3)Li (1) was isolated for the first time and investigated in reactions with β-diketiminate (MeNacnac− = [Ar]NC(Me)CHC(Me)N[Ar]; Ar = 2,6-iPr2C6H3) and PNP-pincer (PNP = N[2-PiPr2-4-methylphenyl]2) Ti(III) complexes. The β-diketiminate titanium(III) complex containing phosphanylphosphido ligand [MeNacNacTi(Cl){η2-P(SiMe3)-P(Ph)tBu}] (2) was prepared in reaction of [MeNacNacTiCl2·THF]...
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A Comprehensive Experimental and Theoretical Study on the[{(η5-C5H5)2Zr[P(µ-PNEt2)2P(NEt2)2P]}2O Crystalline System
PublicationThe structure of tetraphosphetane zirconium complex C52H100N8OP10Zr21 was determined by single crystal X-ray diffraction analysis. The crystal belongs to the monoclinic system, space group P21/c, with a = 19.6452(14), b = 17.8701(12), c = 20.7963(14)Å, α = γ = 90°, β = 112.953(7)°, V = 6722.7(8)Å3, Z = 4. The electronic structure of the organometallic complex has been characterized within the framework of Quantum Chemical Topology....
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Sulfurization of phosphanylphosphinidene ligand: Access to phosphinothioyltrithiophosphonato platinum(II) complexes
PublicationThe reactivity of phosphanylphosphinidene Pt(0) complexes [DppePt(η2-P–PtBu2)] (1) and [(pTol3P)2Pt(η2-P–PtBu2)] (2) toward sulfur was studied. Reactions of 1 and 2 with an excess of sulfur led to the formation of the first transition metal complexes 3 and 4 with phosphinothioyltrithiophosphonato ligands with the formula [tBu2P(=S)–P(=S)S2]2-. In contrast to previous reports on the phosphanylphosphinidene moiety sulfurization,...
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The Process of Building Civil Society against the Shortcomings of Polish Planning Legislation
PublicationThe article presents the main assumptions of the project of Coastal Strip development in Gdansk. According to the authors best knowledge this is the first pro publico bono project in Poland in a large area of the city formed on the initiative of and elaborated by the city's inhabitants supported by two NGOs. Successive stages of the project preparation are discussed on the background of the shortcomings of Polish planning law...
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Number of seasonal work permits issued in 2018
Open Research DataIn 2018, a total of 121,436 seasonal work permits were issued, the vast majority of which were granted to Ukrainian citizens. The following dataset shows the countries from which citizens have been issued the most permits.
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A Text as a Set of Research Data. A Number of Aspects of Data Acquisition and Creation of Datasets in Neo-Latin Studies
PublicationIn this paper, the authors, who specialise in part in neo-Latin studies and the his-tory of early modern education, share their experiences of collecting sources for Open Research Data sets under the Bridge of Data project. On the basis of inscription texts from St. Mary’s Church in Gdańsk, they created 29 Open Research Data sets. In turn, the text of the lectures of the Gdańsk scholar Michael Christoph Hanow, Praecepta de arte...
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Improving performance of large thrust bearings through modeling and experimentation
PublicationLarge thrust bearings are highly loaded machine elements and their failures cause serious losses. Start ups and stoppages of the bearing under load are specially critical regimes of operation. Load carrying capacity depends on the profile of the oil gap. In transient states this profile is also changing. In the design of large thrust bearings minimizing thermo-elastic deformations is an important goal, which can be accomplished...
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The influence of feed rate and shear forces on the devulcanization process of ground tire rubber (GTR) conducted in a co-rotating twin screw extruder
PublicationThe search for new ways to recycling of rubber waste has been the aim of many studies conducted by research centers and companiesworldwide. The results of our investigations on the process of continuous thermomechanical devulcanization of ground tire rubber using a twin screw extruder are presented.We used a co-rotating twin screw extruder with a special configuration of plasticizing unit, enabling generation of considerable shear...
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The influence of screw configuration and screw speed of co-rotating twin screw extruder on the properties of products obtained by thermomechanical reclaiming of ground tire rubber
PublicationThe results of our investigations on the process of continuous thermomechanical reclaiming of ground tire rubber (GTR) carried out using a twin screw extruder are presented.We used a co-rotating twin screw extruder with a special configuration of plasticizing unit, enabling generation of considerable shear forces. The influence of screw configuration and screw speed on breaking of chemical crosslink bonds contained in ground tire...
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Symbiosis of Art and Technology – From Renaissance to Interactive Art,
PublicationThe article presents the mutual relations between art and technology from the Renaissance to the interactive art of today. It indicates important factors influencing the possibilities of imaging and interpreting reality by artists, ranging from the development of oil painting techniques, linear perspective, the invention of printing and photography, to achievements related to the development of information technologies (computers,...
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Shape-Memory Polyurethane Polymers
PublicationPolyurethanes (PUs) are one of the most widely used polymers in research and industry. They can be synthesized from chemical sources and natural sources. PUs are a very useful class of polymers and exhibit many desirable properties that can be exploited in various applications. PUs are formed by the reaction between polyols and isocyanates. A wide variety of polyols and isocyanates are available for synthesis, and hence we can...
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Quality assessment of low voltage surge arresters
PublicationUsers expect reliable operation of the surge arrester during overvoltages, which may originate from a switching process or a lightning discharge. The necessary conditions to guarantee these expectations are: appropriate construction of the surge arrester, its production being maintained in accordance with technical standards, and a positive results of the type test (as well routine and acceptance tests). The recipient, especially...
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How can HSR promote inter-city collaborative innovation across regional borders?
PublicationMany studies have shown that high-speed rail (HSR) can reshape the spatial pattern of economic geography. However, there needs to be more logical argumentation and rigorous empirical design on the paths and mechanisms involved. This paper considers the impact of the border effect on HSR links and innovation clusters from the perspective of inter-regional collaborative innovation. It provides a logical and compact theoretical...
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Innovative Urban Blue Space Design in a Changing Climate: Transition Models in the Baltic Sea Region
PublicationWaterfront areas in cities are subject to constant changes. The desire to integrate the transformed waterside areas with the urban fabric involves shaping high-quality public spaces related to water, which are often referred to as urban blue spaces (UBS). The aim of the research was to examine the transformation processes of urban waterfront areas in the Baltic Sea Region and identify emerging transition models and types of blue...
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Metody i aplikacje zdalnego szkolenia mieszkańców inteligentnych miast
PublicationSTRONA GŁÓWNAOBSZARY TEMATYCZNERADA NAUKOWARECENZENCIREDAKCJAINFORMACJE DLA AUTORÓWRECENZJAKONTAKT Strona główna > Numer 14/2017 > Metody i aplikacje zdalnego szkolenia mieszkańców inteligentnych miast METODY I APLIKACJE ZDALNEGO SZKOLENIA MIESZKAŃCÓW INTELIGENTNYCH MIAST Jerzy Balicki, Piotr Dryja, Waldemar Korłub, Maciej Tyszka Rozwój nowego rodzaju miast i regionów nazywanych smart cities pociąga za sobą nowy sposób...
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Female entrepreneurship in Kazakhstan
PublicationWomen constitute the majority of the Kazakh population and, even though they live almost 10 years longer than men on average, they are far less economically active. Less than half of the female population take up employment. Women’s wages are often as much as 30% lower than men’s. The subjective reasons for undertaking economic activity as mentioned by women included: independence from the husband, low earnings of the husband and...
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Comparative Analysis of Developed Rainfall Intensity–Duration–Frequency Curves for Erbil with Other Iraqi Urban Areas
PublicationRainfall Intensity–Duration–Frequency (IDF) relationships are widely used in water infrastructure design and construction. IDF curves represent the relationship between rainfall intensity, duration, and frequency, and are obtained by analyzing observed data. These relationships are critical for the safe design of flood protection structures, storm sewers, culverts, bridges, etc. In this study, the IDF curves and empirical IDF formulas...
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An analysis of wind conditions at pedestrian level in the selected types of multi-family housing developments
PublicationThe following article addresses the issue of wind conditions around urban building development at pedestrian level. Factors that depend on those issues include wind comfort and air quality within urbanized spaces. The conditions specific of cities located in a temperate climate zone have been taken into account. The article is intended to identify aerodynamic phenomena characteristic of the three basic types of multi-family building...
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Cycling as a Sustainable Transport Alternative in Polish Cittaslow Towns
PublicationIt is well known that growing motor traffic in urban areas causes air pollution and noise which affects the environment and public health. It is hardly surprising then that cycling should be used as an alternative mode of transport, not just in major cities but also in smaller ones including those that are members of the Cittaslow network. Their approach is based on sustainable development, care for the environment and transport...
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A Review on Metal–Organic Framework as a Promising Catalyst for Biodiesel Production ENERGY & FUELS
PublicationThe rapid depletion of fossil-derived fuels along with rising environmental pollution have motivated academics and manufacturers to pursue more environmentally friendly and sustainable energy options in today’s globe. Biodiesel has developed as an ecologically favorable alternative. However, the mass manufacturing of biodiesel on an industrial scale confronts substantial cost and pricing challenges. To address this issue, high-efficiency...
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Permanent traffic count stations - expressway S6 Poland 2016
Open Research DataThe data includes traffic data from permanent traffic count stations located on the expressway S6 in the Tri-City Agglomeration area in Poland. The data covers the 12 months of 2016.
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Depressive symptoms in elderly people participating in University of the Third Age and residents of Nursing Homes: The role of optimism and acceptance of passing
PublicationThe elderly age group needs particular support in preventing development of depressive symptoms, among others, due to the prospect of passing. This group is heterogenous in terms of characteristics of ways of spending leisure time, which, as an important aspect of everyday life affecting the quality of interpersonal relationships and well-being, might be related to the level of their depressive symptoms. The aim of this study...
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The Corporate Museum: A New Type of Museum Created as a Component of Marketing Company
PublicationA new type of museum appeared – the corporate museum. The museum institution in this instance has been used as a new marketing device for building corporate identity strategies. Their inception is not based on the existing context of a place, but appears to be integrated with the corporate identity program, exposing the company’s values and philosophy. The corporate museums are thematic, commercial buildings, owned by a particular...
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Ryszard F. Sadowski dr hab. prof. uczelni
PeoplePLACE OF EMPLOYMENT: Since 2004 prof. Ryszard F. Sadowski is employed at the Faculty of Christian Philosophy (WFCh) at the Cardinal Stefan Wyszyński University in Warsaw. He is a member of the research team of the Center for Ecology and Ecophilosophy (former Institute of Ecology and Ecophilosophy) UKSW. Since 2020 prof. Sadowski is Chair of Ecophilosophy in the Institut of Philosophy at Cardinal Stefan Wyszyński University in Warsaw....
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Rozwój zrównoważony w planowaniu strategicznym w miastach powiatowych na obszarze peryferyjnym woj. pomorskiego
PublicationCelem pracy było rozpoznanie, czy i w jakim zakresie zasady rozwoju zrównoważonego są obecne w planowaniu strategicznym w miastach powiatowych na obszarach peryferyjnych województwa pomorskiego. Wybrano taki zestaw miast, ponieważ ich rozwój może odegrać istotną rolę w aktywizacji obszarów peryferyjnych (miasta w obszarach metropolitalnych mają odrębną specyfikę). Cechy rozwoju zrównoważonego opisane w teorii oraz dokumentach krajowych...
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Analiza holenderskich doświadczeń w zakresie logistyki miejskiej
PublicationW artykule dokonano analizy holenderskich doświadczeń w zakresie logistyki miejskiej i organizacji systemu dostaw towarów na przykładzie Utrechtu. Wybór miasta podyktowany był ponad 20 letnim konsekwentnym zaangażowaniem i doświadczeniem w tej dziedzinie. Przedstawiono zmiany w podejściu do problemów miejskiego transportu ładunków z punktu widzenia polityki krajowej oraz przebieg procesu decentralizacji odpowiedzialności na poziom...
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Site-selective magnetic order of neptunium inNp2Ni17
PublicationWe present the results obtained by superconducting quantum interference device (SQUID) magnetometry, specific heat, and Mossbauer spectroscopy measurements carried out on Np2Ni17 polycrystalline samples. We show that long-range magnetic order, with a moment mu((2b)) similar to 2.25 mu(B), occurs below T-N = 17.5 K on the Np (2b) sites. A nontrivial situation is observed in that the other Np sites (2d) do not take part to the order...
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S.O.S. Climate waterfront A Strategy of Excellence in Research and Innovation to Design Tools for the Waterfront to face Climate Change.
ProjectsProject realized in Faculty of Architecture according to 823901 — sosclimatewaterfront — H2020-MSCA-RISE-2018 agreement from 2018-10-04
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HEALTH SAFETY OF BREAD IN SMALL BAKERIES
PublicationThe aim of the article is to present the safety and health risks in the production process of bread, supported by research in small bakeries located in the Pomeranian Voivodeship. Health safety of bread is one of the features that decide its quality. This article additionally presents other determinants influencing the quality of bread. It also demonstrates opinions showing food safety as a separate attribute of quality. The paper...
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Marek Wójcikowski dr hab. inż.
PeopleMarek Wójcikowski graduated in 1993 from the Department of Electronics at Gdansk University of Technology (GUT). In 2002 he obtained a doctoral degree in the field of electronics and in 2016 he obtained a habilitation at the Faculty of Electronics, Telecommunications and Informatics at GUT. From the beginning of his career he is associated with GUT: first as an assistant (years 1994-2002) and then as assistant professor (since...
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20232024_Elective design II_CULTURAL HERITAGE ROUTES_Gdańsk Measuring the city, advanced digital surveying techniques for cultural heritage documentation
e-Learning CoursesCultural Heritage Routes – Gdańsk. This course explores challenges, conflicts and concepts of cultural heritage preservation and protection at urban level, their connection to architectural and urban design in the time of digitalisation and their importance for a future of the cities. The aim of this course, based on the case study city of Gdańsk, is to understand the problem of cultural heritage and develop innovative...
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SUMMER SCHOOL: Arch Drawing 2/ Elective design II: CULTURAL HERITAGE ROUTES – GDAŃSK FORTIFICATION SYSTEM _2023
e-Learning CoursesCultural Heritage Routes – Gdańsk Fortification System This course explores challenges, conflicts and concepts of cultural heritage preservation and protection in urban level, their connection to architectural and urban design in the time of digitalisation and their importance for a future of the cities. The aim of this course, based on the case study city of Gdańsk, is to understand the problem of cultural heritage and...
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20232024_Elective design II_CULTURAL HERITAGE ROUTES_Gdańsk Drawing architecture to understand the city
e-Learning CoursesCultural Heritage Routes – Gdańsk. This course explores challenges, conflicts and concepts of cultural heritage preservation and protection at urban level, their connection to architectural and urban design in the time of digitalisation and their importance for a future of the cities. The aim of this course, based on the case study city of Gdańsk, is to understand the problem of cultural heritage and develop innovative...
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Ultra-Compact Self-Quadruplexing Microfluidically Frequency Reconfigurable Slot Antenna Using Half-Mode SIW
PublicationIn this brief, the design of an ultra-compact self-quadruplexing frequency reconfigurable antenna (SQFRA) utilizing a half-mode substrate-integrated waveguide (HMSIW) and microfluidic channels is discussed. Four HMSIW cavities fed by four microstrip lines and slots are used to construct a highly compact antenna. The microstrip feedings to the HMSIW cavities are applied in such a way that the proposed antenna exhibits self-quadruplexing...
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POLDER AND CITY: SUSTAINING WATER LANDSCAPES ON AN URBAN EDGE
PublicationThe question investigated in this paper is how to maintain the environmental quality of the polder landscape encompassing the city in the condition of urban pressure on this landscape. On the basis of theoretical approaches, historical surveys and introductory study models new ideas are tested on the case study of Gdansk, a city located in the Vistula River delta in northern Poland. Research shows that the city was created as a...
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Architecture in the field of art on the example of author’s realizations
PublicationThe aim of the article was to show the place of architecture in the space of art on the example of original projects. In the author's opinion, architecture, using an artistic object as a means of expression, influences the process of living by showing the recipient, who is an inhabitant, important values from the point of view of creating a house that ensures a good quality of life and strengthening the understanding of both various...
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Automatic Threat Detection for Historic Buildings in Dark Places Based on the Modified OptD Method
PublicationHistoric buildings, due to their architectural, cultural, and historical value, are the subject of preservation and conservatory works. Such operations are preceded by an inventory of the object. One of the tools that can be applied for such purposes is Light Detection and Ranging (LiDAR). This technology provides information about the position, reflection, and intensity values of individual points; thus, it allows for the creation...
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Urban city lights. Light pollution as one of the effects of incorrectly designed external illumination. How can a successful lighting masterplan diminish its impact?
PublicationIn the modern world, artificial lighting brings many tangible benefits such as the ability to extend working hours and so increase production, recreational use of the city after dark, or the possibility to travel regardless of the time of day. However, this flexibility comes at a price and negatively impacts on the environment. One such negative phenomenon is Light Pollution ‐ a term used to describe excessive nighttime artificial...
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WHY SHOULD WE ADOPT NON-USED ATTICS OF MONUMENTAL SACRAL CATHOLIC CHURCHES FOR SECULAR PURPOSES?
PublicationA motive for adapting the desecrated churches to new purposes is a broadly discussed matter, progressively better investigated and defined. Is it advisable to introduce a new, permanent function, complementary to the sacred one in the historical ecclesial buildings? This paper presents the results of the research on benefits of adapting the non-utilized attics of monumental churches still performing their sacred function, located...
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Janusz Datta prof. dr hab. inż.
PeopleIn 1988, Janusz Datta finished his studies at the Gdańsk University of Technology (GUT), Faculty of Chemistry. Since then he has been employed at the Faculty of Chemistry in the Department of Polymer Technology. During the first six years of employement he was worked as a scientist. In this period, he travelled extensively to ZACHEM company located in Bydgoszcz to gain practical experience related to chemical processing. In 1994,...
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π-Indenyl substituted zirconium compounds containing terminal bonded phosphanylphosphido ligands [Ind2Zr(Cl){(Me3Si)P–PR2-κP1}]. Synthesis, X-ray analysis and NMR studies
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Syntheses and crystal structures of lithium derivatives of diphosphanes R2P-P(SiMe3)Li·3L, R = Ph, iPr and iPr2N, L = THF or DME
PublicationW wyniku reakcji R2P-P(SiMe3)2 z BuLi w THF lub DME powstają pochodne litowe difosfanów R2P-P(SiMe3)Li·3L. Dla R = iPr oraz iPr2N powstają sole R2P-P(SiMe3)Li·3THF, w których atom litu jest czterokrotnie koordynowany a dla R = Ph powstaje sól [Li·3DME]+[Ph2P-PSiMe3]-, która posiada budowę jonową. W reakcji BuLi z Ph2P-P(SiMe3)2 powstają znaczne ilości produktów ubocznych: Ph2P-PPh2 i LiP(SiMe3)2.
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π-Indenyl substituted zirconium compounds containing terminal bondedphosphanylphosphido ligands [Ind2Zr(Cl){(Me3Si)P-PR2-jP1}]. Synthesis,X-ray analysis and NMR studies
PublicationPraca prezentuję reakcję kompleksów indenylowych cyrkonu z solami litowymi difosfanów o ogólnym wzorze R2P-P(SiMe3)Li, gdzie R = tBu, Et2N, iPr2N. W wyniku tych reakcji otrzymano 3 nowe kompleksy fosfanylofosfidowe.Otrzymane nowe kompleksy zbadano przy pomocy technik rentgenowskiej analizy strukturalnej i NMR.Dichloro-bis(indenyl)zirconium(IV) reacts with lithium derivatives of diphosphanes R2P-P(SiMe3)Li (R = tBu, Et2N, iPr2N)...
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Naturally occurring mitochondrial DNA heteroplasmy in the MRL mouse
PublicationThe MRL/MpJ mouse is an inbred laboratory strain of Mus musculus, known to exhibit enhanced autoimmunity, increased wound healing, and increased regeneration properties. We report the full-length mitochondrial DNA (mtDNA) sequence of the MRL mouse (Accession # EU450583), and characterize the discovery of two naturally occurring heteroplasmic sites. The first is a T3900C substitution in the TpsiCloop of the tRNA methionine gene...