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Search results for: REALTIME PCR
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PTR-MS and GC-MS as complementary techniques for analysis of volatiles: A tutorial review
PublicationThis tutorial review is a critical commentary on the combined use of two instrumental analytical techniques, namely GC-MS and PTR-MS. The first mention of such an analytical approach likely appeared after the year 2000 and despite many advantages, it has not been applied very often. Therefore, the aim of this article is to elaborate on the concept of their combined use and to provide a curse tutorial for those considering taking...
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Złożone oddziaływanie smarów na własności warstw wierzchnich stalowych par ciernych
PublicationWęglowodory zawarte w smarach w specyficzny sposób działają na elementy par ciernych wykonane z metali i ich tlenków, będących katalizatorami. Znanymi katalizatorami są: żelazo, nikiel, platyna i pallad. W smarowanych, stalowych parach ciernych zachodzi katalityczna, chemisorbcyjna dysocjacja węglowodorów zawartych w smarze. Opisano badania wpływu tej dysocjacji na sprężyste i tłumiące własności próbek stalowych. Wynik tych badań...
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Współczynnik przewodzenia ciepła λ izolacji PIR w świetle polityki zgodności
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Revealing dynamic changes of the volatile profile of food samples using PTR–MS
PublicationVolatile compounds carry valuable information regarding the properties of foodstuffs. Volatiles emitted from food can be used as, for example, indicators of quality, shelf-life, or authenticity. A better understanding of the multitude of transformations which occur during food processing could facilitate the optimisation of production, increase the desirability of food products, and also their wholesomeness. However, as some of...
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PTR-MS and electronic nose application for volatile fraction analysis of cigar tobacco
PublicationCigar consumers attach great importance to the quality of these products. At the same time, cigars are often expensive, so destructive analytical methods of quality control are not being desired. However, it has been found that there are many volatile organic compounds in their headspace. Because of that, proton transfer reaction–mass spectrometry and electronic nose were used to analyse it. The obtained results were used to distinguish...
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Etyczne dylematy PR-owca
PublicationPraca jest analizą wybranych dylematów etycznych osoby pełniącej funkcję specjalisty public relations, podstawowych wartości i zasad koniecznych do pełnienia tych funkcji.
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Experimental and theoretical studies on the photodegradation of 2-ethylhexyl 4-methoxycinnamate in the presence of reactive oxygen and chlorine species
Publication2-Ethylhexyl 4-methoxycinnamate (EHMC) is one of the most commonly used sunscreen ingredient. In this study we investigated photodegradation of EHMC in the presence of such common oxidizing and chlorinating systems as H2O2, H2O2/HCl, H2O2/UV, and H2O2/HCl/UV. Reaction products were detected by gas chromatography with a mass spectrometric detector (GC-MS). As a result of experimental studies chloro-substituted 4-methoxycinnamic...
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Photodynamic Inactivation of Candida albicans with Imidazoacridinones: Influence of Irradiance, Photosensitizer Uptake and Reactive Oxygen Species Generation
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Effect of the Relative Position of the Face Milling Tool towards the Workpiece on Machined Surface Roughness and Milling Dynamics
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Effect of nitrogen doping on TiOxNy thin film formation at reactive high-power pulsed magnetron sputtering
PublicationThe paper is focused on a study of formation of TiOxNy thin films prepared by pulsed magnetron sputtering of metallic Ti target. Oxygen and nitrogen were delivered into the discharge in the form of reactive gases O2 and N2. The films were deposited by high-power impulse magnetron sputtering working with discharge repetition frequency f = 250 Hz at low (p = 0.75 Pa) and high (p = 10 Pa) pressure. The substrates were on floating...
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Occlusion phenomenon of redox probe by protein as a way of voltammetric detection of non-electroactive C-reactive protein
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Cast polyurethanes obtained from reactive recovered polyol intermediates via crude glycerine decomposition process
PublicationIn this work, the possibility of applying intermediates from polyurethane waste recycling in polyurethane synthesis was presented. Polyurethanes were synthesised in a two-step method using a mixture of petrochemical polyol and glycerolysate, used as a reactive component, 4,4-diphenylmethane diisocyanate (MDI) and 1,4-buthanediol (BD). Glycerolysates were produced during decomposition of polyurethane elastomer by crude glycerine...
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Reclaimed rubber in-situ grafted with soybean oil as a novel green reactive plasticizer in SBR/silica compounds
PublicationPolymer recycling and biodegradable polymeric materials are two major routes towards the sustainable development of polymer materials which contributes to the management of waste. In this regard, an eco-friendly approach is presented wherein high reclaiming degree of ground tire rubber (GTR) was achieved by low-temperature oxidation under swollen action of soybean oil. In-situ reclaimed GTR with soybean oil was cured into reactive...
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A reactive algorithm for deducing nodal forwarding behavior in a multihop ad-hoc wireless network in the presence of errors
PublicationA novel algorithm is presented to deduce individual nodal forwarding behavior from standard end-to-end acknowledgments. The algorithm is based on a well-established mathematical method and is robust to network related errors and nodal behavior changes. The proposed solution was verified in a network simulation, during which it achieved sound results in a challenging multihop ad-hoc network environment.
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A measurement method for lossy capacitive relative humidity sensors based on a direct sensor-to-microcontroller interface circuit
PublicationA new time-domain measurement method for determining the capacitance and resistance values of lossy relative humidity capacitive sensors is presented. The method is based on a direct sensor-to-microcontroller interface for microcontrollers with internal analog comparators and timers. The interface circuit consists only of four reference resistors (two reference resistors if a microcontroller includes a voltage reference source),...
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Measurements of reactive power distribution in a ship power station with two generators working in parallel
Open Research DataThe presented dataset is part of research focusing on the assessment of metrological properties of the instrument, Estimator/Analyzer (E/A v.2), developed and made at the Faculty of Electrical Engineering, Department of Marine Electrical Power Engineering of Gdynia Maritime University. The attached dataset contains processed data, expressing a reactive...
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The role of cytochrome P450 reductase (CPR) in metabolism of potent nitroacridine antitumor, C-1748
PublicationCelem pracy było poznanie molekularnego mechanizmu działania pochodnych 9-amino-1-nitroakrydyny. Zbadano przemiany enzymatyczne tych związków w różnych układach enzymatycznych: I. Szczurza frakcja mikrosomalna z reduktazą cytochromu P450. II. Rekombinantowe izoenzymy cytochromu P450 z wysokim i niskim poziomem reduktazy cytochromu P450. III. Frakcje mikrosomalne dzikiego typu oraz pozbawione genu kodującego reduktazę cytochromu...
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Employment and export specialization patterns versus GDP per capita performance - unifying approach
PublicationThis paper analyses the evolution of specialization patterns along the process of economic development. The scope of the paper is twofold: first of all, it aims at understanding if the evolution of employment specialization is reflected in the same manner in trade specialisation patterns. Secondly, it explores the link between the degree of specialization on one side and cross country GDP per capita performance on the other. We...
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Influence of H2S on degradation of 9Cr-1Mo steel in advanced stage of metal dusting process
PublicationPrzedstawiono wyniki badań stali 9Cr-1Mo w zaawansowanym stadium procesu pylenia metalu po 10 latach eksploatacji w piecu rafineryjnej instalacji platformingu CCR, przeprowadzonych w celu podjęcia decyzji o dozowaniu związków siarki do wsadu instalacji. Na podstawie długotrwałej ekspozycji próbek stali w 600C w mieszaninie wodoru i siarkowodoru wykazano, że siarka może być powodem procesów wpływających niekorzystnie na stan materiału...
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Thermal stabilization and permanent deformation resistance of LWA/PCM-modified asphalt road surfaces
PublicationThis paper presents the results of attempts at reducing the problem of solar overheating of asphalt road pavement surfaces, resulting in weakening and accelerated destruction of the aforementioned structures. To protect pavement surfaces against periodic overheating, standard asphalt mixture AC 16 W 35/50, used for binder course, has been modified by replacing one of the aggregate fractions from the mineral mixture with lightweight...
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Implementation of the FOPID Algorithm in the PLC Controller - PWR Thermal Power Control Case Study
PublicationIn the paper authors describe proposition of design and verification procedures of the discrete Fractional Order PID (FOPID) algorithm for control of the Pressurized Water Reactor (PWR) thermal power near its nominal operating point. The FOPID algorithm synthesis consists of: off-line optimal tunning of its parameters in continuous time-domain with LQ (Linear Quadratic) performance index and simplified models of nuclear reactor...
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Medical-Grade PCL Based Polyurethane System for FDM 3D Printing—Characterization and Fabrication
PublicationThe widespread use of three-dimensional (3D) printing technologies in medicine has contributed to the increased demand for 3D printing materials. In addition, new printing materials that are appearing in the industry do not provide a detailed material characterization. In this paper, we present the synthesis and characterization of polycaprolactone (PCL) based medical-grade thermoplastic polyurethanes, which are suitable for forming...
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Multi-nodal PWR reactor model — Methodology proposition for power distribution coefficients calculation
PublicationIn the paper the multi-nodal Pressurized Water Reactor (PWR) model called Mann’s model is presented. This models is used for modelling purposes of the heat transfer from fuel to coolant in reactor core. The authors expand widely used in literature approach by defining additional coefficients for the heat transfer model. These parameters approximate the power generation distribution in the PWR reactor core according to the to the...
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Identyfikacja i diagnostyka procesu oczyszczania ścieków przy użyciu metody MS-PCA
PublicationPołączenie algorytmu PCA z dekompozycją falkową pozwala na wiarygodną identyfikację i diagnostykę procesu z wieloma skalami czasu. Niniejszy artykuł pokazuje jak przy pomocy wspomianego narzedzia określić stan pracy obiektu oraz odpowiednio szybko wykryć uszkodzenia (np. czujników pomiarowych) lub stany awaryjne obiektu jakim jest oczyszczalnia ścieków. Przedstawiony jest przykład detekcji błędów pomiarowych (stężenie tlenu w komorze...
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Prediction of the fatigue lifetime of PUR structural elements using a combined experimental-numerical approach
PublicationThis paper presents a method for estimating the fatigue life of polyurethane elastomeric components. A rubber replacement - polyurethane of hardness 80ShA commonly used in vibration damping systems, for example, in motor vehicle suspensions, was used for the study. A metal-rubber bushing component was selected for analysis, and numerical analysis was carried out along with a fatigue model proposal based on a modification of the...
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Metoda szybkiego wyznaczania par węzłowo rozłącznych tras dla ochrony transmisji unicast
PublicationW celu ochrony transmisji przed awarią węzłów/łączy wykorzystuje się alternatywne trasy transmisji. Jednakże, złożoność obliczeniowa dostępnych algorytmów doboru tras rozłącznych często istotnie wstrzymuje producentów sprzętu od implementacji tychże rozwiązań. W pracy prezentujemy nowe podejście wyznaczania par rozłącznych tras bazujące na transformacji grafu sieci w meta strukturę. Wyniki badań odnośnie czasu wyznaczania tras...
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Per mare ad astra
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Per Linguam-A Journal of Language Learning
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Investigating the use of ozonation process with calcium peroxide for the removal of reactive blue 19 dye from textile wastewater.
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Investigating the use of ozonation process with calcium peroxide for the removal of reactive blue 19 dye from textile wastewater
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Vitiligo pathogenesis: autoimmune disease, genetic defect, excessive reactive oxygen species, calcium imbalance, or what else?
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Eye-Tracking Examination of the Anthropological Race, Gender and Verbal-Pictorial Relative Positions on Ergonomics of Visual Information Presentation
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Reactive oxygen species (ROS) production in human peripheral blood neutrophils exposedin vitroto static magnetic field
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Genetic variation in C-reactive protein (CRP) gene is associated with retinopathy and hypertension in adolescents with type 1 diabetes
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Isolation of the relative decrease in magnetic permeability contribution to reluctance of an open magnetic circuit based on stray field measurements
PublicationThe goal of the study was to evaluate a relative decrease in magnetic permeability in open magnetic circuits based on stray magnetic field measurements. The boundary element method was used to simulate magnetic circuits with variable geometry and variable magnetic permeability. The simulated magnetic circuits were rectangular or bone-shaped flat samples. Reluctance was increased in the middle of the samples resulting in leakage...
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On the Possibility of Improving the Oxidation Resistance of High-Chromium Ferritic Stainless Steel Using Reactive Element Oxide Nanoparticles
PublicationHigh-chromium ferritic steels are current the only viable candidates for cheap interconnect materials for application in high-temperature solid oxide fuel and electrolyzer cells (HT-SOFCs/SOECs). The durability and operating characteristics of interconnects manufactured using these materials may be improved significantly by applying a protective-conducting MoCo2O4 coating and depositing an intermediate layer consisting of nanoparticles...
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Reactive imines: Addition of 2-aminopyrimidine to the imine bond and isolation of the aminal from the equilibrium mixture aminal/imine
PublicationThe reaction between o-vanillin and 2-aminopyrimidine leads to the formation of a single crystalline product: aminal, 1, which results from the reaction of the initially formed imine with 2-aminopyrimidine. The reaction was followed by the NMR spectroscopy. VT NMR studies prove that in solution two major species are observed: aminal and imine and their ratio depends on the time or/and temperature with the imine content increasing...
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Frequency-Variant Double-Zero Single-Pole Reactive Coupling Networks for Coupled-Resonator Microwave Bandpass Filters
PublicationIn this work, a family of frequency-variant reactive coupling (FVRC) networks is introduced and discussed as new building blocks for the synthesis of coupled-resonator bandpass filters with real or complex transmission zeros (TZs). The FVRC is a type of nonideal frequency-dependent inverter that has nonzero elements on the diagonal of the impedance matrix, along with a nonlinear frequency-variation profile of its transimpedance...
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Novel Cast Polyurethanes Obtained by Using Reactive Phosphorus-Containing Polyol: Synthesis, Thermal Analysis and Combustion Behaviors
PublicationPhosphorus-containing polyol applications in polyurethane synthesis can prevent volatilization of flame retardants and their migration on the surface of a material. In this work, novel cast polyurethanes were prepared by a one-step method with the use of different amounts of phosphorus-containing polyol, 4,4′–diphenylmethane diisocyanate and 1,4-butanediol. The chemical structure, thermal, physicochemical and mechanical properties...
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Structure and optical parameters of Eu doped tellurium oxide thin films prepared by reactive magnetron sputtering method
PublicationIn this work the structural properties and photoluminescence of tellurium dioxide thin films doped by europium were described. Thin films were deposited by magnetron sputtering method and simultaneously heated at 200 °C. Presence of Eu ions and their valence states was confirmed by X-ray photoemission spectroscopy measurements. The structure of the films as well as the influence of europium dopant on crystalline structure of the...
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Influence of reactive oxygen species during deposition of iron oxide films by high power impulse magnetron sputtering.
PublicationIron oxide films were deposited using high power impulse magnetron sputtering (HiPIMS) of an iron cathode in an argon/oxygen gas mixture at different gas pressures (0.5~Pa, 1.5~Pa, and 5.0~Pa). The HiPIMS system was operated at a repetition frequency $f = 100$~Hz with a duty cycle of 1~\%. A main goal is a comparison of film growth during conventional and electron cyclotron wave resonance-assisted HiPIMS. The deposition plasma...
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Intensity Ratio of Kβ/Kα in Selected Elements from Mg to Cu, and the Chemical Effects of Cr Kα1,2 Diagram Lines and Cr Kβ/Kα Intensity Ratio in Cr Compounds
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Per far midaglie di gesso: Giovanni Bernardino Bonifacio i sztuka portretu all'antica.
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Scenariusze emisji metali ciężkich, dioksyn i PCB w Europie do 2020 roku
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Scenariusze emisji metali ciężkich, dioksyn i PCB w Europie do 2020 roku
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The Risk Indicators of Construction Projects’ Cost Overruns Assessed with PCA, Decision Trees, and Pearson’s Correlations
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Automatic Regularization by Quantization in Reducible Representations of CCR: Point-Form Quantum Optics with Classical Sources
PublicationElectromagnetic fields are quantized in a manifestly covariant way by means ofa class of reducible "center-of-mass N-representations" of the algebra of canonical commutationrelations (CCR). The four-potential Aa(x) transforms in these representations as aHermitian four-vector field in Minkowski four-position space (without change of gauge), butin momentum space it splits into spin-1 massless photons and two massless scalars. Whatwe...
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Study on Technological Effects of a Precise Grooving of AlSi13MgCuNi Alloy with a Novel WCCo/PCD (DDCC) Inserts
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Porównanie efektywności metod ponownego wykorzystania częstotliwości PFR i SFR w systemie LTE
PublicationW referacie przedstawiono porównawcze wyniki badań efektywności metod powtórnego wykorzystania pasma – PFR i SFR w systemie LTE. Porównanie dotyczy zarówno pojemności interfejsów radiowych w przypadku użycia tych metod, jak również osiąganej przepływności dla pojedynczych połączeń. Wyniki badań mogą być użyteczne do oceny efektywności obu metod oraz do projektowania i optymalizacji sieci komórkowej LTE.
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Wielopierścieniowe węglowodory aromatyczne (WWA), Polichlorowane bifenyle (PCB), Lotne związki organiczne (VOC),Pestycydy.
PublicationW raporcie (2 wersje językowe) przedstawiono wyniki badań dorzecza rzeki Odry w ramach Międzynarodowego Programu Badań Odry (IOP) realizowanego w okresie 1997-2000 przez 12 jednostek badawczych z Polski i Niemiec. Badania były finansowane przez Federalne Ministerstwo Edukacji i Badań oraz Fundację Współpracy Polsko-Niemieckiej. Badaniom poddawano próbki wody, osadów dennych oraz zawiesiny pobierane w trakcie 8 kampanii...