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Sensitive method for determination of benzoic acid in beverages and food samples using air–assisted hydrophobic deep eutectic solvent-based dispersive liquid-liquid microextraction
PublikacjaA simple, reliable and rapid air–assisted hydrophobic deep eutectic solvent-based dispersive liquid–liquid microextraction (AA-HDES-DLLME) was developed for analysis of benzoic acid in various beverages and food samples. The final determination stage was performed via UV–visible spectrophotometry. The key parameters (extraction time, HDES type and volume, dispersant volume, pH and sample volume) of the AA-HDES-DLLME method were...
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Ultrasound-Assisted Dispersive Liquid-Liquid Microextraction Using Deep Eutectic Solvents (DESs) for Neutral Red Dye Spectrophotometric Determination
PublikacjaDeep eutectic solvents (DES), which have low toxicity and are low cost, biodegradable, and easily synthesized, were used for the extraction of neutral red (NR) dye before its spectrophotometric analysis. DES, containing choline chloride as a hydrogen bond acceptor and phenol as a hydrogen bond donor with a molar ratio of 1:2, was used for the extraction of NR dye from aqueous media. The possible interaction of different DESs with...
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Assessing the time effectiveness of trust management in fully synchronised wireless sensor networks
PublikacjaThe paper presents the results of the time effectiveness assessment of the distributed WSN Cooperative Trust Management Method - WCT2M in a fully synchronized Wireless Sensor Network (WSN). First we introduce some basic types of synchronization patterns in WSN based on the idea of sleep scheduling. Then we explain how WCT2M works in the network applying the fully synchronized sleep scheduling pattern. Such networks were subjected...
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A Time Delay Controller Included Terminal Sliding Mode and Fuzzy Gain Tuning for Underwater Vehicle-Manipulator Systems
PublikacjaAn improved Time Delay Control (TDC) method for an Underwater Vehicle-Manipulator System (UVMS) is proposed. The proposed controller consists of three terms: a time-delay-estimation term that cancels nonlinearities of the UVMS dynamics, a Terminal Sliding Mode (TSM) term that provides a fast response and a PID term that reduces the tracking error. In addition the proposed controller uses fuzzy rules to adaptively tune the gains...
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Optimization of a Fabric Phase Sorptive Extraction protocol for the isolation of six bisphenols from juice pouches to be analysed by high performance liquid chromatography coupled with diode array detector
PublikacjaFabric Phase Sorptive Extraction (FPSE) combined with high pressure liquid chromatography using to diode array detection (HPLC-DAD) was applied for the simultaneous determination of bisphenols (BPA, BPB, BPC, BPE, BPF, BPS) in juice pouches. The FPSE procedure was optimized with regards to the critical parameters that affect the performance of the method including the selection of the FPSE membrane type and size, adsorption time,...
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DETERMINING THE TIME CONSTANT USING TWO METHODS AND DEFINING THE THERMOCOUPLE RESPONSE TO SINE EXCITATION OF GAS TEMPERATURE
PublikacjaThis paper describes the two methods of determining the time constant of type K thermocouple, for two construction solutions: the exposed weld and the mantle fillet weld. This is an important parameter indicating the response time of the thermocouple on the recorded signal. The first method consists of determining the value of τ in the way of numerical simulation of heat exchange between the thermocouple and the current of gas...
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Transcriptomic Effects of Estrogen Starvation and Induction in the MCF7 Cells. The Meta-analysis of Microarray Results
PublikacjaEstrogen is one of the most important signaling molecules which targets a number of genes. Estrogen levels regulate cell proliferation and a plethora of metabolic processes, which may interfere with a range of medical conditions and drug metabolism. The MCF7 breast cancer cell line, expressing the estrogen receptor α, is a well-studied model of cellular answer to estrogen. The aim of this study was to characterize transcriptomic...
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Impulse Impedance Measurements of Lightning Protection Earthings
PublikacjaLightning protection earthing systems should be tested at currents with time parameters similar to those of lightnings. A method and definition of a measured value of impulse impedance are introduced. The impulse impedance was determined by a quotient of voltage drop on the tested earthing to a value of current in measure circuit. The usefulness of the impulse method for lightning protection evaluation is tested on radio base stations...
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Influence analysis of selected parameters on the ASON/GMPLS control plane performance
PublikacjaThe paper regards the problem of ASON/GMPLS performance. The authors present influence analysis of selected parameters on the ASON/GMPLS control plane performance represented in mean Connection Set-up Time E(CST) and mean Connection Release Time E(CRT). The selected parameters are: offered traffic, request intensity and proportion of requests class. The influence analysis is performed with simulation method by using OMNeT++ discrete-event...
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Hybridization of the FDTD method with use of the discrete Green's function
PublikacjaIn this contribution, a hybrid technique is presented which combines the finite-difference time-domain (FDTD) method and the discrete Green's function (DGF) formulation of this method. FDTD is a powerful technique for the analysis of complex penetrable objects but its application is not efficient when the computational domain includes many free-space cells. Therefore, the hybrid method was developed which is applicable to complex...
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Estimation of Selected Synchronous Generator Parameters Based on the Gradient Method
PublikacjaThe authors present a method for the estimation of synchronous generator model parameters using a gradient algorithm. The paper shows an example of model parameter estimation for a turbogenerator and hydrogenerator, based on the generator voltage time responses obtained during an active and reactive power rejection test.
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Application of response surface methodology to optimize solid-phase microextraction procedure for chromatographic determination of aroma-active monoterpenes in berries
PublikacjaMost of scientific papers concern the qualitative or semi-quantitative analysis of aroma-active terpenes in liquid food matrices. Therefore, the procedure based on solid-phase microextraction and comprehensive two-dimensional gas chromatography-time-of-flight mass spectrometry for determination of monoterpenes in fresh berries was developed. The optimal extraction conditions using divinylbenzene-carboxen-polydimethylsiloxane fiber...
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IR-THERMAL IMAGING IN CARDIOSURGERY
PublikacjaA method for monitoring the state of the myocardium during cardiosurgical interventions based on thermal IR imaging is presented. These methods called Static Thermography and Active Dynamic Thermography (ADT) uses information about distribution of temperature on the surface and an external excitation source to induce thermal transient processes in a tested object. Recording time series of thermograms allows to calculate parametric...
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Framework of an Evolutionary Multi-Objective Optimisation Method for Planning a Safe Trajectory for a Marine Autonomous Surface Ship
PublikacjaThis paper represents the first stage of research into a multi-objective method of planning safe trajectories for marine autonomous surface ships (MASSs) involved in encounter situations. Our method applies an evolutionary multi-objective optimisation (EMO) approach to pursue three objectives: minimisation of the risk of collision, minimisation of fuel consumption due to collision avoidance manoeuvres, and minimisation of the extra...
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Determination of Pesticide Residues in Honey using the GC×GC-TOFMS Technique
PublikacjaIn this study, a QuEChERS method and gas chromatography coupled with time-of-flight mass spectrometry (GCxGC-TOFMS) was developed for rapid extraction and simultaneous determination of 12 pesticide residues in honey. The GCxGC-TOFMS method was validated according to the SANCO guidance in terms of linearity, selectivity, reproducibility and recovery. Regarding the results, recovery rates ranged between 70-120% with relative standard...
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Exact modal absorbing boundary condition for waveguide simulations - discrete Green's function approach
PublikacjaA modal absorbing boundary condition (ABC) based on the discrete Green's function (DGF) is introduced and applied for termination of waveguides simulated by means of the finite-difference time-domain (FDTD) method. The differences between the developed approach and implementations already demonstrated in the literature are presented. By applying DGF, a consistent theoretical approach to modal ABC in the FDTD method is obtained....
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A New Approach of Solidification Analysis in Modular Latent Thermal Energy Storage Unit Based on Image Processing
PublikacjaThe solidification process of RT18HC in a cylindrical shell and tube storage unit has been studied using a new methodology based on image processing. The main idea of the algorithm is to label the region of solidification and use statistical functions to calculate the dimensions of the solidification front over time. Said analysis includes two methods. The first method is to measure the solid fraction changes during solidification....
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Hybrid Multi-Criteria Method of Analyzing the Location of Distributed Renewable Energy Sources
PublikacjaThis paper presents the development and the application of a hybrid multi-criteria method, the combination of the Analytic Hierarchy Process (AHP), and numerical taxonomy (NT),to support the decision making on the location of distributed renewable energy sources meetingvarious types of assessment criteria. Finding criteria weights, using the AHP method, eliminates thedisadvantage of NT—which, in current form, is defined by its...
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Coherent-wave Monte Carlo method for simulating light propagation in tissue
PublikacjaSimulating propagation and scattering of coherent light in turbid media, such as biological tissues, is a complex problem. Numerical methods for solving Helmholtz or wave equation (e.g. finite-difference or finite-element methods) require large amount of computer memory and long computation time. This makes them impractical for simulating laser beam propagation into deep layers of tissue. Other group of methods, based on radiative...
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ECHOES REDUCTION DURING DIGITAL DATA TRANSMISSION IN HYDROACOUSTIC CHANNEL – LABORATORY EXPERIMENT
PublikacjaThe possibility of using a hydroacoustic channel for digital data transmission is very limited. This is due to the effect of multipath propagation of the emitted acoustic wave and the damping of the mechanical wave in this medium, which increase with frequency. The first of these phenomena results in inter-symbol interference disturbances in data transmission systems, including even hundreds of symbols. Due to the number of reflections...
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Using the Fingerprinting Method to Customize RTLS Based on the AoA Ranging Technique
PublikacjaReal-time Locating Systems (RTLSs) have the ability to precisely locate the position of things and people in real time. They are needed for security and emergency applications, but also for healthcare and home care appliances. The research aims for developing an analytical method to customize RTLSs, in order to improve localization performance in terms of precision. The proposed method is based on Angle of Arrival (AoA), a ranging...
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Testing the Wide-Sense Stationarity of Bandpass Signals for Underwater Acoustic Communications
PublikacjaThe Underwater Acoustic Communication (UAC) systems work in communication channels characterized by a large variety of multipath propagation conditions that can additionally change over time. Designing a reliable communication system requires knowledge of the transmission parameters of the channel. There is a need for the development of adaptive signaling schemes that would dynamically optimize the signal parameters of the physical...
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Customized crossover in evolutionary sets of safe ship trajectories
PublikacjaThe paper presents selected aspects of evolutionary sets of safe ship trajectories-a method which applies evolutionary algorithms and some of the assumptions of game theory to solving ship encounter situations. For given positions and motion parameters of the ships, the method finds a near optimal set of safe trajectories of all ships involved in an encounter. The method works in real time and the solutions must be returned within...
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NUMERICAL SIMULATION OF CRATER CREATING PROCESS IN DYNAMIC REPLACEMENT METHOD BY SMOOTH PARTICLE HYDRODYNAMICS
PublikacjaA theoretical base of SPH method, including the governing equations, discussion of importance of the smoothing function length, contact formulation, boundary treatment and finally utilization in hydrocode simulations are presented. An application of SPH to a real case of large penetrations (crater creating) into the soil caused by falling mass in Dynamic Replacement Method is discussed. An influence of particles spacing on method...
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Position and Orientation Estimation in Radio Network With Groups of Locally Synchronized Nodes
PublikacjaThis article presents a positioning system with groups of locally synchronized nodes. A mobile object is equipped with a group of several synchronized receivers that are able to measure the difference in the time of arrival of signals from reference transmitters. The reference transmitters are synchronized only in local groups, with no global synchronization between groups. It is assumed that the synchronous operation of transmitters...
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Designing efficient A-D-A1-D-A type fullerene free acceptor molecules with enhanced power conversion efficiency for solar cell applications
PublikacjaThe achievement of highly efficient power conversion efficiency (PCE) is a big concern for non-fullerene organic solar cells (NF-OSCs) because PCE can depend on numerous variables. Here, new five novel acceptor molecules without fullerenes were developed and investigated using DFT (density functional theory) and TD-DFT (time dependent-density functional theory). Compared to the recently synthesized molecule (PZ-dIDTC6), the developed...
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Fast-response optoelectronic detection of explosives’ residues from the nitroaromatic compounds detonation: field studies approach
PublikacjaWe are presenting an application of optoelectronic nitrogen dioxide (NO2) analyzer based on cavity enhanced absorption spectroscopy in the detection of traces of explosives after detonation. It has been shown that the analyzer using blue-violet laser is able to detect explosive residues after the detonation of various amounts of nitroaromatic compounds (75g-1kg) with higher efficiency than the HPLC soil sample testing equipment,...
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Interdependence between Power Grids and Communication Networks: A Resilience Perspective
PublikacjaPower network resilience is increasingly dependent on communication networks. Besides traditional generation, power networks need to accommodate increasingly high penetration levels of dispersed micro generation, mostly based on renewable sources, and increasing and challenging demand, such as electric vehicles. At the same time the deployment of enabling technologies throughout the power grid makes available new demand resources...
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Preconditioners with Low Memory Requirements for Higher-Order Finite-Element Method Applied to Solving Maxwell’s Equations on Multicore CPUs and GPUs
PublikacjaThis paper discusses two fast implementations of the conjugate gradient iterative method using a hierarchical multilevel preconditioner to solve the complex-valued, sparse systems obtained using the higher order finite-element method applied to the solution of the time-harmonic Maxwell equations. In the first implementation, denoted PCG-V, a classical V-cycle is applied and the system of equations on the lowest level is solved...
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Reservoir Influence on Pressure Wave Propagation in Steel Pipes
PublikacjaThe relation between the length of steel pipe and the pressure wave period in the system, reservoir-pipe-valve, is discussed. Experiments carried out for the short steel pipes showed that in such a system, the pressure wave celerity estimated using the measured wave cycles systematically increases with the increase of the pipe length. The observed differences can exceed even 90 m=s. As the pressure wave traveling in the pipe with...
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Fast Low-fidelity Wing Aerodynamics Model for Surrogate-Based Shape Optimization
PublikacjaVariable-fidelity optimization (VFO) can be efficient in terms of the computational cost when compared with traditional approaches, such as gradient-based methods with adjoint sensitivity information. In variable-fidelity methods, the directoptimization of the expensive high-fidelity model is replaced by iterative re-optimization of a physics-based surrogate model, which is constructed from a corrected low-fidelity model. The success...
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Quality control of cheese samples for the presence of natamycin preservative – A natural deep eutectic solvent (NADES) based extraction coupled with HPLC
PublikacjaA new protocol for the determination of natamycin – an antifungal agent used as a food preservative - in cheese samples – is described. This new method is based on a natural deep eutectic solvent (NADES) green extraction procedure. High-performance liquid chromatography (HPLC) was used for detection and quantification. NADESs with different molar ratios were evaluated for efficient and selective extraction. NADES made of thymol...
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Longitudinal drug synergy assessment using convolutional neural network image-decoding of glioblastoma single-spheroid cultures
PublikacjaAbstract Background In recent years, drug combinations have become increasingly popular to improve therapeutic outcomes in various diseases, including difficult to cure cancers such as the brain cancer glioblastoma. Assessing the interaction between drugs over time is critical for predicting drug combination effectiveness and minimizing the risk of therapy resistance. However, as viability readouts of drug combination experiments...
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City scan as a tool to assess resilience challenges and vulnerabilities at the community level
PublikacjaThe majority of the world’s population lives in cities and cities are the key to achieving resilience. Local governments own only part of the land and can only partially decide about measures that should be taken ‘on the ground’. Local governments are therefore highly dependent on individuals, communities, and businesses to adapt and transform and take action in their own backyards or neighbourhoods. Since, for many people, climate...
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Voltage Dependence of Supercapacitor Capacitance
PublikacjaElectronic Double-Layer Capacitors (EDLC), called Supercapacitors (SC), are electronic devices that are capable to store a relatively high amount of energy in a small volume comparing to other types of capacitors. They are composed of an activated carbon layer and electrolyte solution. The charge is stored on electrodes, forming the Helmholtz layer, and in electrolyte. The capacitance of supercapacitor is voltage- dependent. We...
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Estimation of Synchronous Generator and AVR Parameters Based on Gradient and Genetic Methods
PublikacjaThe author present a method for the estimation of selected synchronous generator model and AVR parameters using a gradient and a genetic algorithm. The paper shows an example of model parameter estimation for a turbogenerator, based on the generator voltage time responses obtained during an active and reactive power rejection test
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A New Expression for the 3-D Dyadic FDTD-Compatible Green's Function Based on Multidimensional Z-Transform
PublikacjaIn this letter, a new analytic expression for the time-domain discrete Green's function (DGF) is derived for the 3-D finite-difference time-domain (FDTD) grid. The derivation employs the multidimensional Z-transform and the impulse response of the discretized scalar wave equation (i.e., scalar DGF). The derived DGF expression involves elementary functions only and requires the implementation of a single function in the multiple-precision...
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On the convergence of a finite-difference discretization à la Mickens of the generalized Burgers–Huxley equation
PublikacjaIn this note, we establish the property of convergence for a finite-difference discretization of a diffusive partial differential equation with generalized Burgers convective law and generalized Hodgkin–Huxley reaction. The numerical method was previously investigated in the literature and, amongst other features of interest, it is a fast and nonlinear technique that is capable of preserving positivity, boundedness and monotonicity....
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The 5S methodology as a tool for improving organization of production
PublikacjaThe chapter presents the 5S method as a tool for continuous improving lean management processes, whose task is to create a highly efficient, clean, and ergonomic working environment. The method is presented as a collection of 5 simple rules, and at the same time it is a tool that allows you to control the workplace visually. The history of the 5S tool originates from Japanese philosophy, namely the five basic elements of the system: Seiri...
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Footbridges. Dynamic Design – Selected Problems
PublikacjaModern footbridges create challenge in esthetic and structural design. Breaking the proven canons is a recipe for architectural success. However esthetic form has to be also a functional pedestrian bridge. Therefore a good FEM modeling is a key element in engineering part of design. The paper presents selected problems related to the modeling of the dynamic construction of footbridges. Several basic dynamic problems concerning...
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Chirp Rate and Instantaneous Frequency Estimation: Application to Recursive Vertical Synchrosqueezing
PublikacjaThis letter introduces new chirp rate and instantaneous frequency estimators designed for frequency-modulated signals. These estimators are first investigated from a deterministic point of view, then compared together in terms of statistical efficiency. They are also used to design new recursive versions of the vertically synchrosqueezed short-time Fourier transform, using a previously published method (D. Fourer, F. Auger, and...
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Evolutionary sets of safe ship trajectories with speed reduction manoeuvres within traffic separation schemes
PublikacjaIn the previous paper the author presented the evolutionary ship trajectory planning method designed to support Traffic Separation Schemes (TSS). This time the extensions of this method are described which allow to combine evolutionary trajectory planning with speed reduction manoeuvres. On TSS regions with higher than usual density of traffic and smaller distances between ships, the course alterations alone are not always sufficient...
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Multi-objective weather routing of sailboats considering wave resistance
PublikacjaThe article presents a method to determine the route of a sailing vessel with the aid of deterministic algorithms. The method assumes that the area in which the route is to be determined is limited and the basic input data comprise the wind vector and the speed characteristic of the vessel. Compared to previous works of the authors, the present article additionally takes into account the effect of sea waves with the resultant resistance...
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Optymalizacja efektywności hamowania odzyskowego w transporcie szynowym przez sterowanie czasem przyjazdu na stację
PublikacjaArtykuł nawiązuje do poprzednich prac autorów, w których przedstawiono model organizacji ruchu kooperujących pociągów z uwzględnieniem optymalizacji wykorzystania energii zwracanej do sieci jezdnej. W przedstawionej pracy zmodyfikowano model zmieniając główną zmienną sterującą, mającą wpływ na efektywne wykorzystanie energii, z czasu odjazdu na czas przyjazdu pociągu na stację lub przystanek. Optymalizacja dokonywana jest przez...
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Metal (Mo, W, Ti) Carbide Catalysts: Synthesis and Application as Alternative Catalysts for Dry Reforming of Hydrocarbons—A Review
PublikacjaDry reforming of hydrocarbons (DRH) is a pro-environmental method for syngas production. It owes its pro-environmental character to the use of carbon dioxide, which is one of the main greenhouse gases. Currently used nickel catalysts on oxide supports suffer from rapid deactivation due to sintering of active metal particles or the deposition of carbon deposits blocking the flow of gases through the reaction tube. In this view,...
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Numerical solutions for blood flow in elastic vessels
PublikacjaWe consider the differential–algebraic system for the blood flow and pressure in the systemic arteries. By the operator splitting method, we transform the system into the hyperbolic one, introduce the bicharacteristics, and perform the time–space nonuniform discretization, obtaining the innovative difference scheme. Our results are illustrated with numerical experiments.
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Multi-objective weather routing of sailing vessels
PublikacjaThe paper presents a multi-objective deterministic method of weather routing for sailing vessels. Depending on a particular purpose of sailboat weather routing, the presented method makes it possible to customize the criteria and constraints so as to fit a particular user’s needs. Apart from a typical shortest time criterion, safety and comfort can also be taken into account. Additionally, the method supports dynamic weather data:...
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Local basis function method for identification of nonstationary systems
PublikacjaThis thesis is focused on the basis function method for the identification of nonstationary processes. The first chapter describes a group of models that can be identified using the basis function method. The next chapter describes the basic version of the basis function method, including its algebraic and statistical properties. The following section introduces the local basis function (LBF) method: its properties are described...
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The ONETEP linear-scaling density functional theory program
PublikacjaWe present an overview of the ONETEP program for linear-scaling density functional theory (DFT) calculations with large basis set (planewave) accuracy on parallel computers. The DFT energy is computed from the density matrix, which is constructed from spatially localized orbitals we call Non-orthogonal Generalized Wannier Functions (NGWFs), expressed in terms of periodic sinc (psinc) functions. During the calculation, both the...
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Imidazoacridinone antitumor agent C-1311 as a selective mechanism- based inactivator of human cytochrome P450 1A2 and 3A4 isoenzymes.
Publikacja5-Diethylaminoethylamino-8-hydroxyimidazoacridinone (C-1311), a promising antitumor agent that is also active against autoimmune diseases, was determined to be a selective inhibitor of the cytochrome P450 (CYP) 1A2 and 3A4 isoenzymes. Therefore, C-1311 might modulate the effectiveness of other drugs used in multidrug therapy. The present work aimed to identify the mechanism of the observed C-1311-mediated inactivation of CYP1A2...