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- Dane Badawcze 269 wyników po odfiltrowaniu
Wyniki wyszukiwania dla: WYKRYWANIE MIN PRZECIWPIECHOTNYCH
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DIAGNOSTYKA KABLI ŚREDNIEGO NAPIĘCIA W ENERGA-OPERATOR SA
PublikacjaW referacie przedstawiono wyniki pomiarów diagnostycznych kabli średniego napięcia (SN) o izolacji polietylenowej, o różnym czasie eksploatacji do lat 15. Analizowano poziom wyładowań niezupełnych (wnz) oraz współczynnik strat dielektrycznych tg mierzony przy oddziaływaniu napięcia o częstotliwości 0,1 Hz (VLF). Znaczne zróżnicowanie otrzymanych wyników pomiarów wskazuje na skuteczność wykrywania zachodzących procesów starzeniowych...
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Mechanizmy ochrony integralności plików na poziomie monitora maszyny wirtualnej
PublikacjaMechanizmy ochrony integralności plików umożliwiają wykrywanie nieautoryzowanych zamian w kluczowych do działania systemu operacyjnego plików. Dotychczas rozwiązania tego typu działały jako aplikacje systemowe lub były integrowane z jądrem systemu operacyjnego. Wraz ze zwiększeniem dostępności technik wirtualizacji pojawiła się możliwość przeniesienia systemu ochrony na poziom monitora maszyny wirtualnej, co zapewnia izolację mechanizmu...
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FTIR spectra of SOFC with LSCNT layer fueled by biogas mixture at 750 C (pure)
Dane BadawczeThe dataset contains the FTIR spectra collected during the electrical measurements DIR-SOFC with LSCNT layer. The SOFC was reduced at 800degC in H2 prior to mesurements. The spectra were collected every 10 min.
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The thermostability, bioactive compounds and antioxidant activity of some vegetables subjected to different durations of boiling: investigation in vitro
PublikacjaThis research was performed in order to compare the water and acetone extracts of raw and boiled for 10, 20, 40 and 60 min Korean lotus roots (KLR) and Polish white onion (PWO) in the contents of theirbioactive compounds, antioxidant activity and thermostability.It was found that polyphenols (mg GAE/g), flavanols (mg GAE/g), flavonoids (mg CE/g), anthocyanins (mg CGE/kg) and tannins (mg CE/g) in water extract of raw lotus roots...
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Ti/TiO2 nanotubes sensitized PbS quantum dots as photoelectrodes applied for decomposition of anticancer drugs under simulated solar energy
PublikacjaOne of the challenges in research into photoelectrocatalytic (PEC) degradation of pollutants is finding the appropriate photoanode material, which has a significant impact on the process efficiency. Among all others, photoelectrodes based on an ordered TiO2 nanotube arrays are a promising material due to well-developed surface area and efficient charge separation. To increase the PEC activity of this material, the SILAR method was...
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Internal friction in pure Co and CoPt alloy during ordering
PublikacjaZbadano tarcie wewnętrzne, wskaźnik modułu sprężystości postaciowej i podatność magnetyczną stopu CoPt (50% at. Pt) w stanie nieuporządkowanym, uzyskanym w wyniku oziębienia, podczas wyżarzania do 850 K przy wzrostach temperatury 6K/min. i 2K/min., stosując odwróconą skręcarkę wahadłową. Zaobserwowano maksimum tarcia wewnętrznego w CoPt przy 700 K oraz w monokrysztale kobaltu w 720 K w pobliżu martenzytycznej przemiany fazowej,...
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Video traffic data - Interchange Sulno (S1-94), Poland
Dane BadawczeThe data includes video traffic data registered with 8 video cameras at weaving area (weaving section type A) of the Sulno interchange within S1 expressway in Poland (interchange of expressway S1 and national road 94), located in the Silesian Agglomeration. The data covers the two days: 12.09.2017 (expressway S1) and 13.09.2017 (road 94).
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TiN coating in ring-on-ring sliding with saline solution (0.9%) lubrication 5MPa, 0.1m/s specimn. #B48/#A45
Dane BadawczeWear tests in sliding friction of TiN coating on 1.4021 (EN 10088-1) heat treated stainless steel. Ring - on - ring contact in unidirectional sliding, TiN over TiN . Mean contact stress: 5MPa. Sliding velocity: 0,1 m/s. Mean friction radius: 9.5mm. Lubricant: SALINE SOLUTION (0.9%). Tribometer: PT-3. Overall test time till coating penetration 12 min....
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TiC coating in ring-on-ring sliding with saline solution (0.9%) lubrication 5MPa, 0.1m/s specimn. #B41/#A39
Dane BadawczeWear tests in sliding friction of TiC coating on 1.4021 (EN 10088-1) heat treated stainless steel. Ring - on - ring contact in unidirectional sliding, TiC over TiC . Mean contact stress: 5MPa. Sliding velocity: 0,1 m/s. Mean friction radius: 9.5mm. Lubricant: SALINE SOLUTION (0.9%). Tribometer: PT-3. Overall test time till coating penetration 9 min....
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CrN coating in ring-on-ring sliding with distlled water lubrication 5MPa, 0.1m/s specimn. #A23/#B22
Dane BadawczeWear tests in sliding friction of CrN coating on 1.4021 (EN 10088-1) heat treated stainless steel. Ring - on - ring contact in unidirectional sliding, CrN over CrN . Mean contact stress: 5MPa. Sliding velocity: 0,1 m/s. Mean friction radius: 9.5mm. Lubricant: DISTILLED WATER. Tribometer: PT-3. Overall test time till coating penetration 12 min. The...
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TiC coating in ring-on-ring sliding with distlled water lubrication 5MPa, 0.1m/s specimn. #B39/#A41
Dane BadawczeWear tests in sliding friction of TiC coating on 1.4021 (EN 10088-1) heat treated stainless steel. Ring - on - ring contact in unidirectional sliding, TiC over TiC . Mean contact stress: 5MPa. Sliding velocity: 0,1 m/s. Mean friction radius: 9.5mm. Lubricant: DISTILLED WATER. Tribometer: PT-3. Overall test time till coating penetration 3 min. The test...
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SiC coating in ring-on-ring sliding with distlled water lubrication 5MPa, 0.1m/s specimn. #B34/#A33
Dane BadawczeWear tests in sliding friction of SiC coating on 1.4021 (EN 10088-1) heat treated stainless steel. Ring - on - ring contact in unidirectional sliding, SiC over SiC. Mean contact stress: 5MPa. Sliding velocity: 0,1 m/s. Mean friction radius: 9.5mm. Lubricant: DISTILLED WATER. Tribometer: PT-3. Overall test time till coating penetration 3 min. The test...
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TiN coating in ring-on-ring sliding with saline solution (0.9%) lubrication 5MPa, 0.1m/s specimn. #A45/#B48
Dane BadawczeWear tests in sliding friction of TiN coating on 1.4021 (EN 10088-1) heat treated stainless steel. Ring - on - ring contact in unidirectional sliding, TiN over TiN . Mean contact stress: 5MPa. Sliding velocity: 0,1 m/s. Mean friction radius: 9.5mm. Lubricant: SALINE SOLUTION (0.9%). Tribometer: PT-3. Overall test time till coating penetration 12 min....
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TiC coating in ring-on-ring sliding with distlled water lubrication 5MPa, 0.1m/s specimn. #A41/#B39
Dane BadawczeWear tests in sliding friction of TiC coating on 1.4021 (EN 10088-1) heat treated stainless steel. Ring - on - ring contact in unidirectional sliding, TiC over TiC . Mean contact stress: 5MPa. Sliding velocity: 0,1 m/s. Mean friction radius: 9.5mm. Lubricant: DISTILLED WATER. Tribometer: PT-3. Overall test time till coating penetration 3 min. The...
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CrN coating in ring-on-ring sliding with saline solution (0.9%) lubrication 5MPa, 0.1m/s specimn. #A25/#B21
Dane BadawczeWear tests in sliding friction of CrN coating on 1.4021 (EN 10088-1) heat treated stainless steel. Ring - on - ring contact in unidirectional sliding, CrN over CrN . Mean contact stress: 5MPa. Sliding velocity: 0,1 m/s. Mean friction radius: 9.5mm. Lubricant: SALINE SOLUTION (0.9%). Tribometer: PT-3. Overall test time till coating penetration 9 min....
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CrN coating in ring-on-ring sliding with distlled water lubrication 5MPa, 0.1m/s specimn. #B22/#A23
Dane BadawczeWear tests in sliding friction of CrN coating on 1.4021 (EN 10088-1) heat treated stainless steel. Ring - on - ring contact in unidirectional sliding, CrN over CrN. Mean contact stress: 5MPa. Sliding velocity: 0,1 m/s. Mean friction radius: 9.5mm. Lubricant: DISTILLED WATER. Tribometer: PT-3. Overall test time till coating penetration 6 min. The test...
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SiC coating in ring-on-ring sliding with distlled water lubrication 5MPa, 0.1m/s specimn. #A33/#B34
Dane BadawczeWear tests in sliding friction of SiC coating on 1.4021 (EN 10088-1) heat treated stainless steel. Ring - on - ring contact in unidirectional sliding, SiC over SiC. Mean contact stress: 5MPa. Sliding velocity: 0,1 m/s. Mean friction radius: 9.5mm. Lubricant: DISTILLED WATER. Tribometer: PT-3. Overall test time till coating penetration 3 min. The test...
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A highly thermostable, homodimeric single-stranded DNA-binding protein from Deinococcus radiopugnans
PublikacjaWe report the identification and characterization of the single-stranded DNA-binding protein (SSB) from the mesophile and highly radiation-resistant Deinococcus radiopugnans (DrpSSB). PCR-derived DNA fragment containing the complete structural gene for DrpSSB protein was cloned and expressed in Escherichia coli. The gene consisting of an open reading frame of 900 nucleotides encodes a protein of 300 amino acids with a calculated...
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The Influence of Tool Shape and Process Parameters on the Mechanical Properties of AW-3004 Aluminium Alloy Friction Stir Welded Joints
PublikacjaThe purpose of the following study was to compare the effect of the shape of a tool onthe joint and to obtain the values of Friction Stir Welding (FSW) parameters that provide the bestpossible joint quality. The material used was an aluminium alloy, EN AW-3004 (AlMn1Mg1). To theauthors’ best knowledge, no investigations of this alloy during FSW have been presented earlier. Fivebutt joints were made with a self-developed, cylindrical,...
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Termowizyjna metoda oceny ochrony cieplnej
PublikacjaMetody diagnostyki, tj. wykrywania i rozróżniania usterek, a w szczególności techniki termowizyjne, mają bardzo szerokie zastosowanie. Pozwalają na wykrycie anomalii, zanim pojawią się ich widoczne konsekwencje. Na podstawie dostępnej literatura tego tematu dostrzec można wielki teoretyczny i praktyczny rozwój tej dziedziny.Metody termowizyjne stosuje się z powodzeniem w budownictwie, w celu wykrycia mostków cieplnych oraz nieszczelności...
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The photocatalytic activity of MoS2 electrodes under sunlight illumination
Dane BadawczeThis dataset contains the results of the photocatalytic activities of the MoS2 and MoS2 modified by SnO2 were assessed through the photocatalytic reduction of Cr6+ under the sunlight illumination. In the experiment, 20 mg of the catalyst was distributed in the K2Cr2O7 aqueous solution (50 mL, 100 mg•L-1). The mixed solution was stirred for 30 min to...
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Thermal behavior of TeOx xerogel powder under different atmospheres
Dane BadawczeThe DataSet contains the results of the thermal behavior of the TeOx xerogel powder measured under different atmospheres. The material was obtained by the sol-gel method. The starting solution was prepared by mixing telluric acid (precursor) with thetraetylene glycol, water, and ethanol. The sol was obtained by vigorously stirring precursor solution...
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CrN coating in ring-on-ring sliding with saline solution (0.9%) lubrication 5MPa, 0.1m/s specimn. #B21/#A21
Dane BadawczeWear tests in sliding friction of CrN coating on 1.4021 (EN 10088-1) heat treated stainless steel. Ring - on - ring contact in unidirectional sliding, CrN over CrN . Mean contact stress: 5MPa. Sliding velocity: 0,1 m/s. Mean friction radius: 9.5mm. Lubricant: SALINE SOLUTION (0.9%). Tribometer: PT-3. Overall test time till coating penetration 25 min....
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TiN coating in ring-on-ring sliding with distlled water lubrication 5MPa, 0.1m/s specimn. #A45/#A47
Dane BadawczeWear tests in sliding friction of TiN coating on 1.4021 (EN 10088-1) heat treated stainless steel. Ring - on - ring contact in unidirectional sliding, TiN over TiN. Mean contact stress: 5MPa. Sliding velocity: 0,1 m/s. Mean friction radius: 9.5mm. Lubricant: DISTILLED WATER. Tribometer: PT-3. Overall test time till coating penetration 20 min. The test...
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TiN coating in ring-on-ring sliding with distlled water lubrication 5MPa, 0.1m/s specimn. #A45/#B45
Dane BadawczeWear tests in sliding friction of TiN coating on 1.4021 (EN 10088-1) heat treated stainless steel. Ring - on - ring contact in unidirectional sliding, TiN over TiN. Mean contact stress: 5MPa. Sliding velocity: 0,1 m/s. Mean friction radius: 9.5mm. Lubricant: DISTILLED WATER. Tribometer: PT-3. Overall test time till coating penetration 90 min. The test...
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The termostability, bioactive compounds and antioxidant activity of some vegetables subjected to different durations of boiling: investigation in vitro.
PublikacjaThis research was performed in order to compare the water and acetone extracts of raw and boiled for 10, 20, 40 and 60 min Korean lotus roots (KLR) and Polish white onion (PWO) in the contents of theirbioactive compounds, antioxidant activity and thermostability. It was found that polyphenols (mg GAE/g), flavanols (mg GAE/g), flavonoids (mg CE/g), anthocyanins(mg CGE/kg) and tannins (mg CE/g) in water extract of raw lotus roots...
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Intensyfikacja procesów w przemyśle chemicznym [Moduł dyscyplinarny do wyboru, Grupa B]
Kursy OnlineProwadząca: dr hab. inż. Donata Konopacka-Łyskawa Terminy realizacji: 6.11 (ndz), godz. 12-13:45 (2x45 min. + przerwa) 10.12(sob), godz. 9:15-11 (2x45 min. + przerwa) 11.12 (ndz), godz. 9:15-11 14.01 (sob), godz. 9:15-11 15.01 (ndz), godz. 9:15-11 21.01 (sob), godz. 9:15-11 22.01 (ndz.), godz. 9:15-11:45 (3x45 min. + przerwa) Celem realizacji przedmiotu jest zapoznanie doktorantów wdrożeniowych z metodami i strategiami...
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FTIR spectra of SOFC with LSCNT layer fueled by H2 and 20ppm H2S/biogas mixture at 750 C - cyclic measurements (12h per cycle)
Dane BadawczeThe dataset contains the FTIR spectra collected during the cyclic measurements of H2S poisoning in DIR-SOFC with LSCNT layer. The H2S poisoning and H2 regenrating cycles were 12 h each. The spectra were collected every 10 min.
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Video traffic data - Interchange Zakrzewo (S11-307), Poland
Dane BadawczeThe data includes video traffic data registered with 8 video cameras at weaving area (weaving section type A) of the Zakrzewo interchange within S11 expressway in Poland (interchange of expressway S11 and regional road 307), located in the Poznan Agglomeration. The data covers the two days: 20.09.2017 (expressway S11) and 21.09.2017 (road 307).
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Determining diagnostic coverage of elements and analysis of subsystems` architectural constraints
PublikacjaWypełnienie funkcji bezpieczeństwa przez systemy E/E/PE łączy się z niezawodnym działaniem podsystemów, których struktura i właściwości muszą gwarantować skuteczne i szybkie wykrywanie uszkodzeń. Do określenia przeciętnego prawdopodobieństwa niewypełnienia funkcji bezpieczeństwa na żądanie (PFDavg) niezbędna jest znajomość pokrycia diagnostycznego w odniesieniu do wszystkich podsystemów. Najlepiej, aby podsystemy były zaliczane...
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Ocena odporności na zużycie ścierne stopów Ti na elementy pary trącej endoprotez stawu kolanowego
PublikacjaNajczęściej stosowanym biomateriałem tytanowym na elementy endoprotez stawu kolanowego jest stop Ti6Al4V. Z uwagi na zawartość wanadu, zaliczanego do pierwiastków o dużej toksyczności podejmowane są działania w kierunku zastąpienia wskazanego stopu - stopami bezwanadowymi. Jednym z najbardziej obiecujących jest stop Ti13Nb13Zr zawierający w swoim składzie jedynie pierwiastki witalne, niewywołujące stanów zapalnych i odczynów...
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Beta-galactosidase activity of Meiothermus ruber cells
PublikacjaFreeze-dried cells of Meiothermus ruber catalyses cleavage of o-nitrophenyl-b-D-galactopiranoside (oNPb-gal) and conversion of lactose into glucose and galactose. The permeabilization with 2%toluene,20%ethanol and 20%acetone increased enzymatic activity from 74.87 U/g of lyophilized cells up to 129.44,114.38 and 90.19 U/g,respectively. Ethanol was an effective permeabilizing agent and its efficiency was dependent on the concentration,...
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Fusion of DNA-binding domain of Pyrococcus furiosus ligase with TaqStoffel DNA polymerase as a useful tool in PCR with difficult targets
PublikacjaThe DNA coding sequence of TaqStoffel polymer- ase was fused with the DNA-binding domain of Pyrococcus furiosus ligase. The resulting novel recombinant gene was cloned and expressed in E. coli. The recombinant enzyme was purified and its enzymatic features were studied. The fusion protein (PfuDBDlig-TaqS) was found to have enhanced processivity as a result of the conversion of the Taq DNA polymerase from a relatively low processive...
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Microwave heat treatment application to pasteurization of human milk
PublikacjaA prototype of microwave pasteurizer has been proposed as an alternative for holder pasteurization (HP) routinely used in Human Milk Bank (HMB), ensuring microbiological safety of human milk (HM). It was shown that the time of heat generation was about 15–16 min shorter by applying the microwave than in HP. Total inactivation of heat-sensitive bacteria Escherichia coli, Pseudomonas aeruginosa, Staphylococcus aureus, and Staphylococcus...
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Removal efficiency of phenol by ozonation process with calcium peroxide from aqueous solutions
PublikacjaPhenol has been introduced as a priority pollutant by the US Environmental Protection Agency. Advanced oxidation processes (AOPs) are one of the most efcient methods for removal of non-degradable organic pollutants in aqueous solutions. The removal efciencies of phenol and COD under optimal conditions pH=3, phenol concentration=5 mg/L, CaO2 concentration=0.025 mg/L, temperature 25 °C, 1 g/min ozonation rate and contact time=90...
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Effect of convection and microwave heating on the retention of bioactive components in human milk
PublikacjaBioactive substances are very important components of human milk (HM), especially for premature newborns. The effects of convection (CH) and microwave heating (MWH) at 62.5 and 66 °C, on the level of selected bioactive components of HM: lysozyme (LZ), lactoferrin (LF), secretory immunoglobulin A (sIgA), basal lipase (BL), cytokine TGF-2, vitamin C and total antioxidant capacity (TAC) was compared. Regardless of the used heating methods...
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Optimization of liquid chromatographic separation of pharmaceuticals within green analytical chemistry framework
PublikacjaThe contribution is aimed at the development of methodology that allows to consider green analytical chemistry criteria during optimization of liquid chromatographic separation with design of experiment. The objectives of the optimization are maximization of peak areas of five non-steroid anti-inflammatory drugs, maximization of resolution between peaks, with simultaneous shortening of chromatographic separation time and minimization...
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FTIR spectra of reference SOFC fueled by H2 and 20ppm H2S/biogas mixture at 750 C - cyclic measurements (12h per cycle)
Dane BadawczeThe dataset contains the FTIR spectra collected during the cyclic measurements of H2S poisoning in DIR-SOFC without LSCNT layer. The H2S poisoning and H2 regenrating cycles were 12 h each. The spectra were collected every 10 min.
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Electrical performance measurement of reference and SOFC with LSCNT layer fueled by H2 and 20ppm H2S/biogas mixture at 750 C - cyclic measurements (12h per cycle)
Dane BadawczeThe dataset contains the electrical IV measurements collected during the cyclic measurements of H2S poisoning in DIR-SOFC with/-out LSCNT layer. The H2S poisoning and H2 regenrating cycles were 12 h each. The spectra were collected every 10 min.
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Jumping Wave 2D Profiles
Dane BadawczeThe file contains 2D profiles obtained from a jumping wave study in front of the tool during burnishing of 1.0562 steel by the toroidal-cone tool. Burnishing speed 30.5 m/min, feed of burnishing 0.2mm/rev Force 550 and 800 N.
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Wpływ azotowania jarzeniowego i laserowego nadtapiania na odporność kawitacyjną stali X5CrNi18-10
PublikacjaNierdzewne stale austenityczne charakteryzują się doskonałą odpornością korozyjną, aczkolwiek niskimi właściwościami mechanicznymi. W wielu przypadkach ogranicza to ich eksploatację w warunkach przemysłowych. Ponadto, nierdzewne stale austenityczne są wrażliwe na korozję lokalną w obecności jonów halogenkowych. Technologie materiałowe, które dają potencjalne możliwości otrzymywania korzystnego wpływu na właściwości mechaniczne...
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Linear impedance of V2O5 nanorods obtained at 903K
Dane BadawczeThe DataSet contains the linear electrical properties of V2O5 nanorods which were measured by the impedance spectroscopy method. V2O5 nanorods were obtained by the sol-gel method. The information about xerogel powder synthesis is described in the Journal of Nanomaterials. The precursor powder was pressed into the disk-shaped pellets (12mm in diameter...
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Linear impedance of V2O5 nanorods obtained at 913K
Dane BadawczeThe DataSet contains the linear electrical properties of V2O5 nanorods which were measured by the impedance spectroscopy method. V2O5 nanorods were obtained by the sol-gel method. The information about xerogel powder synthesis is described in the Journal of Nanomaterials. The precursor powder was pressed into the disk-shaped pellets (12mm in diameter...
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Thermal behavior of TeOx powder
Dane BadawczeThe DataSet contains the results of the thermal behavior of the TeOx powder. The material was obtained by the sol-gel method. The starting solution was prepared by mixing telluric acid (precursor) with thetraetylene glycol, water, and ethanol. The sol was obtained by vigorously stirring precursor solution at 50°C for 2h, then the temperature was raised...
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Linear impedance of V2O5 nanorods obtained at 893K
Dane BadawczeThe DataSet contains the linear electrical properties of V2O5 nanorods which were measured by the impedance spectroscopy method. V2O5 nanorods were obtained by the sol-gel method. The information about xerogel powder synthesis is described in the Journal of Nanomaterials. The precursor powder was pressed into the disk-shaped pellets (12mm in diameter...
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Sposób i urządzenie do zwalczania min morskich
Wynalazki -
Impact of high-pressure processing on the bioactive compounds of milk - A comprehensive review
PublikacjaHigh-pressure processing (HPP) is a promising alternative to thermal pasteurization. Recent studies highlighted the effectivity of HPP (400–600 MPa and exposure times of 1–5 min) in reducing pathogenic microflora for up to 5 logs. Analysis of modern scientific sources has shown that pressure affects the main components of milk including fat globules, lactose, casein micelles. The behavior of whey proteins under HPP is very important...
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Cavitation based cleaner technologies for biodiesel production and processing of hydrocarbon streams: A perspective on key fundamentals, missing process data and economic feasibility – A review
PublikacjaThe present review emphasizes the role of hydrodynamic cavitation (HC) and acoustic cavitation in clean and green technologies for selected fuels (of hydrocarbon origins such as gasoline, naphtha, diesel, heavy oil, and crude oil) processing applications including biodiesel production. Herein, the role of cavitation reactors, their geometrical parameters, physicochemical properties of liquid media, liquid oxidants, catalyst loading,...
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Modelling and optimisation of MXene-derived TiO2/Ti3C2 synthesis parameters using Response Surface Methodology based on the Box–Behnken factorial design. Enhanced carbamazepine degradation by the Cu-modified TiO2/Ti3C2 photocatalyst
PublikacjaIn the present study, a hydrothermal method in a water/ethanol environment was used for the first time to obtain novel Cu/TiO2/Ti3C2 composites with high photocatalytic activity for the degradation of carbamazepine (CBZ) under simulated solar light. The Box–Behnken factorial design was coupled with Response Surface Methodology (RSM) for synthesis parameter optimisation. The effect of different synthesis parameters, including temperature, time...
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Kinetics of Intermetallic Phase Precipitation in Manual Metal Arc Welded Duplex Stainless Steels
PublikacjaThe article presents the influence of heat treatment on the kinetics of transformations in lean duplex LDX2101 steel and a weld made of standard duplex 2209 material, which was welded by manual metal arc welding. Changes in the microstructure, hardness, and magnetic phase content were analyzed after heat treatment was conducted at a temperature of 800 °C for a period ranging from 15 to 1440 min. Light and scanning microscopy, Vickers...