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Wyniki wyszukiwania dla: DISORDERED ALLOYS
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<i>N,N,N</i>-Trimethyl-N-(methyl 5-deoxy-2,3-<i>O</i>-isopropylidene-β-D-ribofuranosid-5- yl)ammonium 4-methylbenzenesulfonate sesquihydrate.
PublikacjaThe structure of the title compound, [C12H24NO4][C7H7O3S]·1.5H2O, contains alternating layers parallel to (001) of hydrophobic and polar character, stabilized by C-H...O hydrogen bonding. The furan ring adopts an envelope conformation with the C(OMe) atom as the flap, and the dioxolane ring is twisted about one of the O-C(methine) bonds. A comparison to related compounds is presented. The tosylate-O atoms were disordered over two...
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Modyfikacja powierzchni stopu Ti16Al4V przez nadtapianie laserowe w niskich temperaturach = Surface modification of the Ti6A14V alloy by laser melting in low temperature
PublikacjaPrzedstawiono założenia projektu badawczego zmierzającego do modyfikacji powierzchniowej stopu Ti6Al4V i uzyskaniu lepszej odporności na zużycie ścierne, tribokorozję i zmęczenie korozyjne dzięki nadtopieniu powierzchni stopu laserem w warunkach kriogenicznych.
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Notch fatigue analysis and life assessment using an energy field intensity approach in 7050-T6 aluminium alloy under bending-torsion loading
PublikacjaThis paper studies the fatigue crack initiation and fatigue crack propagation of notched cylindrical bars made of 7050-T6 aluminium alloy subjected to multiaxial bending-torsion loading. The sites of crack initiation and the angles of crack initiation were successfully predicted from the distribution of the first principal stress at the notch surface. Fatigue crack initiation lives were computed through the new concept of energy...
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Correlation between partial inhibition of hydrogen evolution using thiourea and catalytic activity of AB5-type hydrogen storage alloy towards borohydride electrooxidation
PublikacjaDirect borohydride fuel cells (DBFCs) are devices which directly convert the chemical energy stored in the borohydride ion and oxidant into electrical energy as a result of redox reactions. Unfortunately, a significant amount of fuel is lost as a result of the undesirable hydrolysis reaction. The selection of an efficient borohydride hydrolysis inhibitor requires detailed knowledge regarding the interaction mechanism between the...
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Wpływ procesów utleniania na budowę warstwy napawanej ze stopu kobaltu = Oxidation process influence on the morphology the cobalt alloy clad layer
PublikacjaWarstwę napawaną laserowo ze stopu kobaltu poddano utlenianiu w różnych warunkach. Na powierzchni otrzymano różniące się warstwy tlenków o zróżnicowanej morfologii. Brak było widocznych zmian w mikrostrukturze napoiny. Zbadano także wpływ utleniania na twardość warstwy.
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Preparation of Allyl Alcohol Oligomers Using Dipicolinate Oxovanadium(IV) Coordination Compound
PublikacjaCurrently, new precatalysts for olefin oligomerization are being sought in the group of vanadium(IV) complexes. Thus, the aim of our research was to examine the catalytic activity of the oxovanadium(IV) dipicolinate complex [VO(dipic)(H2O)2] 2 H2O (dipic = pyridine-2,6-dicarboxylate anion) in 2-propen-1-ol oligomerization as well as to characterize oligomerization products using matrix-assisted laser desorption/ionization–time-of-flight...
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High temperature corrosion evaluation and lifetime prediction of porous Fe22Cr stainless steel in air in temperature range 700–900 °C
PublikacjaThis work describes a high temperature corrosion kinetics study of ~30% porous Fe22Cr alloys. The surface area of the alloy (~0.02 m2 g-1) has been determined by tomographic microscopy. The weight gain of the alloys was studied by isothermal thermogravimetry in the air for 100 hours at 700 - 900 °C. Breakaway oxidation was observed after oxidation at 850 °C (~100 hours) and 900 °C (~30 hours). The lifetime prediction shows the...
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Stable nanoconjugates of transferrin with alloyed quaternary nanocrystals Ag–In–Zn–S as a biological entity for tumor recognition
PublikacjaOne way to limit the negative effects of anti-tumor drugs on healthy cells is targeted therapy employing functionalized drug carriers. Here we present a biocompatible and stable nanoconjugate of transferrin anchored to Ag-In-Zn-S quantum dots modified with 11-mercaptoundecanoic acid (Tf-QD) as a drug carrier versus typical anticancer drug, doxorubicin. Detailed investigations of Tf-QD nanoconjugates without and with doxorubicin...
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Surface Layer Properties of Sintered Ferritic Stainless Steel Remelted and Alloyed with FeNi and Ni by HPDL Laser
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Analysis of the Surface Stereometry of Alloyed Austenitic Steel after Fibre Laser Cutting using Confocal Microscopy
PublikacjaThe paper extends the concept of cut edge quality and examines the fibre laser cutting process. A Prima Power Platino Fiber Evo device with a reference speed (RS) of 3500 mm/min was used for laser cutting. In order to analyse the influence of the laser cutting speed on the cut edge quality of X5CrNi18-10 stainless steel sheets, macroscopic studies were conducted on a stereoscopic microscope and surface stereometry on a confocal...
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The influence of plastic working on the selection properties of the nickel - aluminium alloy coatings = Wpływ obróbki plastycznej na wybrane właściwości powłok stopowych nikiel - aluminium
PublikacjaW pracy przedstawiono wyniki badań nad możliwością zastosowania technologii obróbki plastycznej (walcowania na zimno i gorąco, oraz prasowania) do kształtowania wybranych właściwości natryskiwanych płomieniowo powłok stopowych Ni-5%Al o strukturze jednofazowej, a mianowicie granicznego roztworu stałego , o maksymalnej 10% rozpuszczalności glinu w sieci krystalograficznej niklu. Celem pracy jest wstępna analiza możliwości zastąpienia...
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Artificial neural network based fatigue life assessment of friction stir welding AA2024-T351 aluminum alloy and multi-objective optimization of welding parameters
PublikacjaIn this paper, the fracture behavior and fatigue crack growth rate of the 2024-T351 aluminum alloy has been investigated. At first, the 2024-T351 aluminum alloys have been welded using friction stir welding procedure and the fracture toughness and fatigue crack growth rate of the CT specimens have been studied experimentally based on ASTM standards. After that, in order to predict fatigue crack growth rate and fracture toughness,...
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Określenie szybkości korozji stopu AlSi13Mg1CuNi nadtopionego laserowo w warunkach kriogenicznych = Corrosion rate determination of AlSi13Mg1CuNi alloy laser remelted at cryogenic conditions
PublikacjaW pracy przedstawiono wyniki badania szybkości korozji stopu AlSi13Mg1CuNi nadtopionego laserowo w warunkach kriogenicznych. Stop eksponowano w 0,01 M roztworze kwasu siarkowego H2SO4
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Dynamic Behavior of Aluminum Alloy Aw 5005 Undergoing Interfacial Friction and Specimen Configuration in Split Hopkinson Pressure Bar System at High Strain Rates and Temperatures
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Wpływ stanu warstwy wierzchniej na mikrostrukturę i właściwości korozyjne stopu SUPERSTON = Influence of the state of surface layer on microstructure and corrosion properties of SUPERSTON alloy
PublikacjaW artykule przedstawiono rezultaty nadtapiania laserowego w warunkach kriogenicznych stopu SUPERSTON. Dokonano oceny mikrostruktury powierzchni i przekroju stopu SUPERSTON po obróbce laserowej. Określono właściwości stopu, które porównano ze stanem powierzchni po nadtapianiu oraz nadtapianiu i szlifowaniu.
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Social media as an opportunity or a blind alley in social communication and forest education? – Experiences from Poland
PublikacjaThe article characterizes the experiences, problems, and prospects for the development of forest education on social media, which in Poland has been carried out by the Państwowe Gospodarstwo Leśne Lasy Państwowe (National Forest Holding ‘State...
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Fracture surface topography measurements analysis of low-alloyed corrosion resistant steel after bending-torsion fatigue tests
PublikacjaIn this paper, an assessment of a topography measurement method for fracture surfaces of 10HNAP steel after bending-torsion fatigue tests was performed. Surface roughness was measured by using a non-contact Focus Variation Microscopy (FVM) technique in which the non-measured points (NMPs) and outliers (spikes) were removed by the application of general methods. The results revealed, that the optical measurement method introduced...
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Masked hypertension in type 2 diabetes: never take normotension for granted and always assess out-of-office blood pressure
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P92 steel and inconel 617 alloy welds joint produced using ERNiCr-3 filler with GTAW process: Solidification mechanism, microstructure, mechanical properties and residual stresses
PublikacjaThe objective of the current study was to analyse the microstructure, mechanical characteristics, and residual stresses of a dissimilar welded joint (DWJ) made of P92 steel and the Inconel alloy 617 (IN617) using the gas tungsten arc welding (GTAW) method. The ERNiCr-3 filler was selected to produce the conventional V groove (VG) and narrow V groove (NVG) butt joint. The filler deficient zones in the weldments, such as the filler...
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Influence of dispersed phase content on the mechanical properties of electroless nanocomposite Ni-P/Si3N4 and hybrid Ni-P/Si3N4/graphite layers deposited on the AW-7075 alloy.
PublikacjaThe article presents the results of mechanical testing of Ni-P/Si3N4 nanocomposite and hybrid Ni-P/Si3N4/graphite coatings deposited on AW-7075 aluminum alloy using the chemical reduction method. In terms of mechanical testing, microhardness was measured, and surface roughness and adhesion of the coatings to the aluminum substrate were determined using the “scratch test” method. The surface morphology of the deposited layers was...
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Analiza budowy i własności napoiny wykonanej z proszku 1606 ze stopu kobaltu = Morphology and property analyze of the layer made of 1606 powder of cobalt alloy
PublikacjaW pracy analizowano budowę i zmiany zachodzące w strukturze napawanej laserowo warstwy wykonanej ze stopu kobaltu pod wpływem korozyjnego środowiska gazów spalinowych. Warstwa wykazywała się znaczną niejednorodnością chemiczną i składem różnym od założonego jednakże te nieprawidłowości nie wpłynęły znacząco na jej odporność korozyjną w gorących gazach spalinowych.
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An improved methodology for the synthesis of 1-C-allyl imino-d-xylitol and -l-arabinitol and their rapid functionalization
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Properties of Spark Plasma Sintered Compacts and Magnetron Sputtered Coatings Made from Cr, Mo, Re and Zr Alloyed Tungsten Diboride
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Construction of heterometallic and mixed-valence copper(I/II) chloride π-complexes with 1,2,4-triazole allyl-derivative
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Copper(I) π-coordination compounds with allyl derivatives of disubstituted pseudothiohydantoin: synthesis, structure investigation and nonlinear optical features
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Effect of the Cooling Time in Annealing at 350°C on the Phase Transformation Temperatures of a Ni<sub>5</sub><sub>5</sub>Ti<sub>4</sub><sub>5</sub> wt. Alloy
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Magnetic Phase Transition and Exchange Bias in $$\hbox {Ni}_{45}\hbox {Co}_{5}\hbox {Mn}_{35.5}\hbox {In}_{14.5}$$ Ni 45 Co 5 Mn 35.5 In 14.5 Heusler Alloy
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Wpływ nadtapiania laserowego w warunkach kriogenicznych na strukturę warstwy wierzchniej stopu Ti-6Al-4V = Effect of laser melting at cryogenic conditions on structure of the surface layer of the Ti-6Al-4V alloy
PublikacjaWykonano nadtapianie laserowe stopu Ti-6Al-4V zanurzonego w środowisku ciekłego azotu. Badania mikroskopowe wykazały znaczący wpływ parametrów nadtapiania na grubość, mikrostrukturę i mikrotwardośc warstwy wierzchniej.
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Goblet Cell Ratio in Combination with Differentiation and Stem Cell Markers in Barrett Esophagus Allow Distinction of Patients with and without Esophageal Adenocarcinoma
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Compulsive sexual behavior and dysregulation of emotion
PublikacjaIntroduction Dysregulation of emotion (DE) is commonly seen in individuals suffering from compulsive sexual behavior (CSB), as well as represents a crucial element of its common comorbidities like mood, anxiety, and substance use disorders. Aim To investigate the links between CSB and DE. Methods A review of pertinent literature on CSB and DE was performed using EBSCO, PubMed, and Google Scholar databases. Main Outcome Measure...
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Trichloridobis(ethyldiphenylphosphine)-(tetrahydrofuran)molybdenum(III)
PublikacjaIn the mononuclear title compound, [MoCl3(C4H8O)(C14H15P)2], obtained by the reaction of trichlorotris(tetrahydrofuran)molybdenum(III) and ethyldiphenylphosphine in tetrahydrofuran (THF) solution, the MoIII atom is six-coordinated by one O atom of a THF molecule, two P atoms from two ethyldiphenylphosphine ligands and three Cl atoms in a distorted octahedral geometry. The C atoms of the THF molecule are disordered over two positions...
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Kobieta ciężarna i alkohol-toksyczny związek. Smółka noworodków jako materiał w diagnostyce spożywania alkoholu w czasie ciąży
PublikacjaKażda ilość alkoholu spożyta przez ciężarną kobietę może spowodować poronienie, przedwczesny poród, patologię łożyska, zahamowanie wzrostu wewnątrzmacicznego płodu i wystąpienie licznych wad wrodzonych wywołanych alkoholem, określanych wspólnie mianem spektrum płodowych zaburzeń alkoholowych - FASD. Mogą one objawiać się zaburzeniami psychicznymi i/lub fizycznymi. Współczesna diagnostyka u noworodków zespołu FASD opiera się najczęściej...
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Fluorine ions in photocatalysts’ synthesis: an obstacle or an ally? The investigation of photocatalysts in Ti-O-F system
PublikacjaTitanium(IV) oxide (TiO2) is one of the most promising photocatalysts, which is expected to be applied in the photocatalytic degradation of xenobiotics. For sustainable development and green chemistry approach recently, much effort has been paid to enhance TiO2 photocatalytic activity in UV-vis light by modifying its structure. The photocatalytic process’s complexity cannot be simply described as electron-hole pairs generations...
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Activation of Metabotropic Glutamate Receptor (mGlu2) and Muscarinic Receptors (M1, M4, and M5), Alone or in Combination, and Its Impact on the Acquisition and Retention of Learning in the Morris Water Maze, NMDA Expression and cGMP Synthesis
PublikacjaThe Morris water maze (MWM) is regarded as one of the most popular tests for detecting spatial memory in rodents. Long-term potentiation and cGMP synthesis seem to be among the crucial factors involved in this type of learning. Muscarinic (M1, M4, and M5 receptors) and metabotropic glutamate (mGlu) receptors are important targets in the search for antipsychotic drugs with the potency to treat cognitive disabilities associated with...
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Rediscovering Automatic Detection of Stuttering and Its Subclasses through Machine Learning—The Impact of Changing Deep Model Architecture and Amount of Data in the Training Set
PublikacjaThis work deals with automatically detecting stuttering and its subclasses. An effective classification of stuttering along with its subclasses could find wide application in determining the severity of stuttering by speech therapists, preliminary patient diagnosis, and enabling communication with the previously mentioned voice assistants. The first part of this work provides an overview of examples of classical and deep learning...
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Investigation of magnetic order in a new intermetallic compound Nd2PtGe3
PublikacjaIn the present study we report a successful synthesis of the new intermetallic compound Nd2PtGe3 by an arc-melting method. The powder X-ray diffraction analysis indicates that this compound crystallizes in an disordered variant of the AlB2-type structure (space group P6/mmm, no. 191) with lattice parameters a = 4.2455 Å and c = 4. 1933 Å. The compound exhibits a cluster-glass transition below Tf = 2.9 K, characterized through ac...
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Localized impedance measurements of AA2024 and AA2024-T3 performed by means of AFM in contact mode
PublikacjaPurpose: The purpose of this paper is to present the results of an atomic force microscopy (AFM) based approach to local impedance spectroscopy (LIS) measurement performed on AA2024 and AA2024-T3 aluminium alloys. Design/methodology/approach: AFM-LIS measurements were performed ex-situ without the electrolyte environment, so in fact the electrical not electrochemical impedance was obtained. Findings: Relative local impedance values...
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Up-regulation of ferritin ubiquitination in skeletal muscle of transgenic rats bearing the G93A hmSOD1 gene mutation
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Ocena odporności na zużycie ścierne stopów Ti na elementy pary trącej endoprotez stawu kolanowego
PublikacjaNajczęściej stosowanym biomateriałem tytanowym na elementy endoprotez stawu kolanowego jest stop Ti6Al4V. Z uwagi na zawartość wanadu, zaliczanego do pierwiastków o dużej toksyczności podejmowane są działania w kierunku zastąpienia wskazanego stopu - stopami bezwanadowymi. Jednym z najbardziej obiecujących jest stop Ti13Nb13Zr zawierający w swoim składzie jedynie pierwiastki witalne, niewywołujące stanów zapalnych i odczynów...
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Cavitation resistance of OH18N9 steel alloyed with vaidus amount of TiC or Mn by means of laser beam. XIV International Symposium on Gas Flow, Chemical Lasers and High Power Lasers.
PublikacjaPrzedstawiono badania odporności kawitacyjnej stali OH18N9T po laserowym stopowaniu jej powierzchni węglikiem TiC oraz manganem. Wykazano, że wzbogacenie obrabianej stali manganem powoduje przemiany fazowe pod wpływem działania obciążeń kawitacyjnych, co przyczynia się do wzrostu odporności kawitacyjnej. Wzmacnianie stali węglikiem TiC powoduje natomiast zanik zdolności stali do wzmacniania odkształceniowego.
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Local structural and chemical ordering of nanosized Pt(3±δ)Co probed by multiple-scattering x-ray absorption spectroscopy
PublikacjaThis work reports a detailed investigation of the local structure and chemical disorder of a Pt(3±δ)Co thin film and Pt(3±δ)Co nanoparticles. We have used a combination of techniques including x-ray absorption spectroscopy (XAS), x-ray diffraction (XRD), and high-resolution transmission electron microscopy (TEM). The important effect of chemical ordering on pair and three-atom configurations has been studied using computer simulations...
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Superconducting properties of vn-sio 2 sol-gel derived thin films
Publikacjain this work studies of structure and superconducting properties of vnsio2 films are reported. the films were obtained through thermal nitridation (ammonolysis) of solgel derived v2o3sio2 coatings (in a proper v2o3/sio2 ratio) at 1200 ◦c. this process leads to the formation of disordered structure with vn metallic grains dispersed in the insulating sio2 matrix. the structural transformations occurring in the lms as a result...
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Photoluminescence as a probe of phosphorene properties
PublikacjaHere, we provide a detailed evaluation of photoluminescence (PL) as a comprehensive tool for phosphorene characterization with the emphasis on a prominent quantitative role of PL in providing fingerprint-like features due to its extreme sensitivity to the band structure details, anisotropy, disorder, external fields, etc. Factors such as number of layers, dimensionality, structural and chemical disorder, and environmental factors...
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Shoulder ultrasound in the diagnosis of the suprascapular neuropathy in athletes
PublikacjaPurpose: Shoulder pain and weakness are common symptoms in athletes who play sports connected with overhead throwing. Suprascapular neuropathy may be one of the reason of such signs.The aim of the study was to find out if ultrasound examination of the shoulder in athletes reveals signs of suprascapular neuropathy. Methods: This was a cross-sectional study in which 67 pro- fessional volleyball, handball and rugby players of polish...
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Improvements to the two-phase sandwich method for calculating the melting points of pure metals
PublikacjaThe thermophysical properties of metal alloys are often investigated via molecular dynamics (MD) simulations.An exact and reliable estimation of the thermophysical parameters from the MD data requires a properly and carefullyelaborated methodology. In this paper, an improved two-phase sandwich method for the determination of the metal meltingtemperature is proposed, based on the solid-liquid equilibrium theory. The new method was...
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Catena-Poly[[(tetrahydrofuran-[kappa]O)lithium(I)]-bis([mu]-trimethylsilanolato-[kappa]2O:O)-gallium(III)-bis([mu]-trimethylsilanolato-[kappa]2O:O)-[(tetrahydrofuran-[kappa]O)lithium(I)]-[mu]-bromido]
PublikacjaThe title chain polymer compound, [GaLi2Br(C3H9OSi)4(C4H8O)2]n, was obtained in the reaction of GaBr3 with Me3SiOLi in toluene/tetrahydrofuran. The GaIII atom, located on a twofold rotation axis, is coordinated by four trimethylsilanolate ligands and has a distorted tetrahedral geometry. The LiI atom is four coordinated by one bridging Br atom located on an inversion centre, two trimethylsilanolate ligands and one tetrahydrofurane...
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Wnikanie wodoru z paliwa i oleju do stali stopowych 26h2mf i 34hnm oraz jego oddziaływanie z defektami struktury = The hydrogen entry from fuel and oil to the 26h2mf and 34hnm alloy steels, and its interaction with structure defects
PublikacjaWykonano badania skłonności do korozji naprężeniowej przy rozciąganiu próbek ze stałą małą prędkością 10-6s-1, przy obciążeniu cyklicznie zmiennym w środowisku gorącego paliwa kotłowego i gliceryny oraz badania absorpcji wodoru dla stali stopowych 26H2MF i 34HNM w paliwie kotłowym, przepracowanym oleju mineralnym oraz glicerynie jako środowisku referencyjnym. Wykazano największą wrażliwość stali przy obciążeniach zmiennych oraz...
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Crystal structure, DFT-study and NLO properties of the novel copper(I) nitrate π,σ-coordination compound based on 1-allyl-3-norbornan-thiourea
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In situ transformation boosts the pseudocapacitance of CuNi-MOF via cooperative orientational and electronic governing
PublikacjaThe disordered arrangement and thereof inferior conductivity of 2D MOF sheets seriously hinder their practical application. Herein, we propose in situ transformation strategy to architect vertically oriented bimetallic CuNi-MOF as a self-supporting electrode, leading to a decuple high specific capacitance of 1262 C g-1 in comparison with the pristine Ni-MOF powder of 114 C g-1 at 2 A g-1. DFT calculations reveal that introduction...
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Electro-chemo-mechanical properties in nanostructured Ca-doped ceria (CDC) by field assisted sintering
PublikacjaRecent investigations have shown that highly oxygen defective cerium oxides generate non-classical electrostriction that is superior to lead-based ferroelectrics. In this work, we report the effect of field-assisted spark plasma sintering (SPS) on electro-chemo-mechanical properties of calcium doped ceria (CDC). Nanometric powders of Ca.10 nm are rapidly consolidated to form polycrystalline nanostructures with a high degree of...