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Anisotropic optical properties of few-layer black phosphorus coatings: from fundamental insights to opto-electrochemical sensor design
PublikacjaFew-layer black phosphorus (FLBP) is characterised by a tuneable bandgap, high carrier mobility and anisotropic optical properties. It therefore has the potential to find applications in electronics and photonics. FLBP oxidizes upon exposure to air, limiting its utility in devices and components. To address this issue, the thesis introduces methods and tools developed for studying FLBP's optical parameters, with a particular emphasis...
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Monitoring the gas turbine start-up phase on the platform using a hierarchical model based on Multi-Layer Perceptron networks
PublikacjaVery often, the operation of diagnostic systems is related to the evaluation of process functionality, where the diagnostics is carried out using reference models prepared on the basis of the process description in the nominal state. The main goal of the work is to develop a hierarchical gas turbine reference model for the estimation of start-up parameters based on multi-layer perceptron neural networks. A functional decomposition...
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Tailoring optical constants of few-layer black phosphorus coatings: Spectroscopic ellipsometry approach supported by ab-initio simulation
Publikacja2D black phosphorus (BP) has attracted extensive attention as an anisotropic platform for novel optoelectronic and polarizing optics applications. Insight into the factors that tune the optical and polarizing properties of 2D BP reveals their essential influence on BP-based photonic and optoelectronic devices. In this work, studies of the optical constants of few-layer black phosphorus coatings are studied and discussed, with particular...
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Improving the Performance of a Graphite Foil/Polyaniline Electrode Material by a Thin PEDOT:PSS Layer for Application in Flexible, High Power Supercapacitors
PublikacjaIn this study, we present a novel strategy for enhancing polyaniline stability and thus obtaining an electrode material with practical application in supercapacitors. A promising (graphite foil/polyaniline/poly(3,4-ethylenedioxythiophene):poly(styrenesulfonate) GF/PANI/PEDOT:PSS) electrode material was characterized and used in the construction of a symmetric supercapacitor that provides an outstanding high power density. For this...
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Electrochemical synthesis of 2D copper coordination-polymers: Layer-stacking deviation induced by the solvent and its effect on the adsorptive properties
PublikacjaA 2D Cu-based Metal-Organic Framework (MOF), namely copper-terephthalate (Cu(1,4-BDC)), was successfully synthesized by electrochemical method for effective methylene blue (MB) sorption from aqueous solutions. The composition, morphology, and the presence of functional groups in the obtained material were verified by Fourier Transform Infrared spectroscopy (FTIR), Powder X-Ray Diffraction (PXRD), Thermal (TGA), and Elemental (EA)...
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Enhanced stability of electrochemical performance of few-layer black phosphorus electrodes by noncovalent adsorption of 1,4-diamine-9,10-anthraquinone
PublikacjaIn this paper, the novel noncovalent functionalisation strategy of few-layer black phosphorus by 1,4-diamine-9,10-anthraquinone electrode was proposed and studied. The degradation of few-layer black phosphorus under exposure to oxygen and water is a significant obstacle to its use as an electroanalytical electrode. The anthraquinone compound adsorbed at black phosphorus flakes results in improved prevention of the phosphorus surface...
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The effect of beech wood (Fagus sylvatica L.) steaming process on the colour change versus depth of tested wood layer
PublikacjaThe results of experimental research on the colour changes of beech wood at different depths of the tested layer are presented. Beech wood (Fagus sylvatica L.) dried in a conventional kiln was tested. Half of the wood samples were steamed prior to the drying process. Colour changes were measured at various depths after the face milling process was used to remove the material to expose to the deeper surface. The colour changes were...
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Optimal conditions of naphthoquinones separation from carnivorous plants extracts using thin-layer chromatography and high performance liquid chromatography
PublikacjaDroseraceae plants are owned by the family of carnivorous plants, which in an unusual way adapt to environments poor in nutrients. Droseraceae obtain essential nutrients catching insects and other small invertebrantes. Plumbagin, chloroplumbagin, ramentaceon and droseron are naphthoquinones, which could be found in leaves and shoots of plants from Droseraceae family. In the literature there are a lot of information about the pharmacological...
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Particle rotation effects in Cosserat-Maxwell boundary layer flow with non-Fourier heat transfer using a new novel approach
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Wpływ podwyższonych temperatur na napawane warstwy na bazie kobaltu = The elevated temperatures influence on the cobalt base cladding layer
Publikacjaw pracy przeanalizowano wpływ temperatur utleniania (850, 950 i 110 stopni C) na mikrostrukturę i twardośc napawanych plazmowo warstw zykonanych z proszku na bazie kobaltu zdodatkiem 28,8% chromu, 4,9% wolframu, 2,2% niklu, 2,09% żelaza, 1,2% krzemu i 1,2% węgla. W wyniku utleniania na powierzchni napoiny powstaje warstwa tlenku chromu stanowiaca dobrą ochronę w niższych temperaturach, jednak w temperaturach wyższych ulega ona...
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Visible light activity of pulsed layer deposited BiVO4/MnO2 films decorated with gold nanoparticles: The evidence for hydroxyl radicals formation
PublikacjaThin films containing BiVO4 and MnO2 deposited on FTO and modified by Au nanoparticles were studied towards their photoelectrochemical and photocatalytical activities in an aqueous electrolyte. Electrodes were prepared by the pulsed laser deposition (PLD) method. The surfactant-free ablation process was used for preparation of the gold nanoparticles (GNP) water suspension. Obtained layers of varied thicknesses (27–115 nm) were...
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Kinetics of adsorption of hydrocarbon chloro-derivatives from seven-component aqueous solution onto a thin layer of DTO-activated carbon
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Experimental verification of the theoretical modelof heat transfer between a liquid layer formed by a two-phase impinging jet and a solid surface
PublikacjaW pracy przedstawiono eksperymentalną weryfikacje modelu teoretycznego wymiany ciepła pomiędzy warstwą wody a stałą powierzchnią. Warstwa cieczy powstała z uderzającej o powierzchnię dwufazowej strugi uderzającej
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Fingerprint comparison of low-volatile petroleum products by means of Thin Layer Chromatography (TLC) for identification of process leakages and environmental pollution
PublikacjaW pracy zbadano możliwość zastosowania stosunkowo prostej i szybkiej procedury przygotowania próbki, rozdzielania grup składników techniką cienkowarstwowej chromatografii cieczowej (TLC), wizualizacji w świetle UV 254 oraz 360 nm i analizy porównawczej cech plamek na płytkach TLC do określenia rodzaju niskolotnego materiału ropopochodnego stanowiącego zanieczyszczenie wód procesowych, lub wyciek z instalacji w rafinerii ropy naftowej....
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STUDIES ON THE USE OF TERRESTRIAL LASER SCANNING IN THE MAINTENANCE OF BUILDINGS BELONGING TO THE CULTURAL HERITAGE
PublikacjaWithin the frames of the use of terrestrial laser scanning we find numerous examples of registration of building facilities, including also historical and valuable in their culture. In the case presented in this paper, at the root of the problem there is a preservation of the historic blacksmith’s forge located in Gdansk Orunia. The facility dating from the early nineteenth century was intended to repair involving the complete...
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THE METHOD OF MEASURING THE MEMBRANE COVER GEOMETRY USING LASER SCANNING AND SYNCHRONOUS PHOTOGRAMMETRY
PublikacjaThe authors present the experience and results of field studies carried out at the technical acceptance of Forest Opera (name in Polish: Opera Leśna) in Sopot (Poland). An unusual design of covering made in the form of “Sheerfill I” technical fabric membrane required spanned in the form of sails, required the use of terrestrial laser scanning. Such approach allowed for the fast and accurate record of the surface of individual panels...
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THE METHOD OF ANALYSIS OF DAMAGE REINFORCED CONCRETE BEAMS USING TERRESTRIAL LASER SCANNING
PublikacjaThe authors present an analysis of the possibility to assess deformations and mode of failure of R-C beams using terrestrial laser scanning. As part of experiments carried out at the Regional Laboratory of Construction (at Gdansk University of Technology), reinforced concrete beams were subjected to destruction by bending and by shear. The process of press impact on the reinforced concrete beam was recorded using terrestrial laser...
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Studies on the use of terrestrial laser scanning in the maintenance of buildings belonging to the cultural heritage
PublikacjaWithin the frames of the use of terrestrial laser scanning we find numerous examples of registration of building facilities, including also historical and valuable in their culture. In the case presented in this paper, at the root of the problem there is a preservation of the historic blacksmith's forge located in Gdansk Orunia. The facility dating from the early nineteenth century was intended to repair involving the complete...
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Microstructure and properties of the cobalt base clad layers after long time service
PublikacjaBadaniu poddano napawane laserowo warstwy ze stopu na bazie kobaltu. Warstwy wykonane na przylgni grzybka zaworu wylotowego silnika diesla badano po dwóch latach eksploatacji w dwóch silnikach laboratoryjnych. Badania mikrostruktury nie wykazały znaczących zmian. Przeprowadzono również badania chemiczne oraz pomiary twardości warstw po eksploatacji. Badany typ napoin nie wykazał znaczących uszkodzeń po długim czasie eksploatacji.
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The Characteristic of Surface Layers on Austenitic Stainless SteelAfter Glow-discharge Nitriding Process.
PublikacjaThis paper presents investigation of surface layers. The diffusion layers were produced by using different parameters of reactive atmosphere (N2:H2). The research of the surface layers was performed using scanning electron microscope (SEM). The results of energy dispersive X-ray (EDX) analysis and X-ray diffraction (XRD) analysis are presented. Research reveals the influence of chemical constitution of reactive atmosphere on the...
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Wear and corrosion characteristics of the layers type (mn-p) formed on aluminium alloys
Publikacjaopisano multipleksową metodę wytwarzania warstw zawierających mangan i fosfor (mn-p) na stopach aluminium. przedstawiono wyniki badań mikrostruktury, właściwości tribologicznych i korozyjnych tych warstw. stwierdzono obecność tlenku manganu i fosforku manganu w wytworzonych warstwach oraz ich wysoką twardość, rzędu 1272 hv0,02. warstwy typu (mn-p) zmniejszają podatność stopu alsi13mg1cuni na korozję w 0,01 mh2so4.
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Comparision of mechanical properties of nitrided cases and remelted layers of austenitic stainless steel
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Engineering Au nanoparticle arrays on SiO2 glass by pulsed UV laser irradiation
PublikacjaWe study semi-regular arrays of Au nanoparticles (NP) obtained via UV laser irradiation of thin Au films on glass substrate. The NP structures are prepared from films of a thickness up to 60 nm produced by discharge sputtering or pulsed laser deposition, and annealed by nanosecond laser pulses at 266 or 308 nm, respectively, at fluencies in the range of 60-410 mJ/cm2. For the rare- and close-packed NP structures, consistent description...
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Preparation of porous TiO2 films by means of pulsed laser deposition for photocatalytic applications
PublikacjaIn this work the preparation and structure properties of porous thin films of TiO2 were investigated. The films were produced by means of the pulsed laser deposition technique using laser pulses at 266nm (10Hz) and at fluencies of 1-3.5J/cm2. The process was performed in vacuum using O2 buffer gas and films were deposited on the SiO2 glass or Si substrate. X-ray diffraction (XRD) and Raman analysis of the structure and chemical...
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An Optical Low-Coherence System for 2-Dimensional Visualization of Thin Polymer Layers
PublikacjaW artykule omówiono zasadę działania i przedstawiono podstawowe właściwości systemu OCT (Optical Coherence Tomography). Na przykładzie folii polietylenowej przedyskutowano możliwości wykorzystania systemu do badanie wewnętrznej struktury warstwowej obiektów niebiologicznych. Przedstawiono i omówiono wyniki przeprowadzonych badań nad warstwowymi materiałami przeźroczystymi.
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Chemical, thermal and laser processes in recycling of photovoltaic silicon solar cells and modules
PublikacjaIn recent years, photovoltaic power generation systems have been gaining unprecedented attention as an environmentally beneficial method to solve the energy problem. From the economic point of view the pure silicon, which can be recapture from the used cells, is the most important material due to its cost and shortage. In the paper selected methods of used or damaged module and cells recycling and experimental results are presented....
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Laser Investigations of Flow Patterns in Electrostatic Precipitators and Non Thermal Plasma Reactors
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Measurement of sub-nanometer molecular layers with ISFET without a reference electrode dependency
PublikacjaA new method of detection and measurement with sub-nanometer resolution of layers adsorbed or bonded to the ISFET's gate dielectric was presented. The sensitivity of this method is high enough to detect even partial mono-layer covering. The transconductance measurement of the ISFET provides independence of the output signal from pH changes and the driving electrode electrochemical potential instabilities. The stable reference electrode...
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Development of free electron laser and accelerator technology in Poland (CARE and EuCARD projects)
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Acousto-optic interaction of a Gaussian laser beam with an ultrasonic wave of cylindrical symmetry
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SEM investigations of the mechanism of formation and growth of nanohydroxyapatite layers coated with ultrasonic method
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Double wedge prism based beam deflector for precise laser beam steering
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Influence of Laser Modification on the Surface Character of Biomaterials: Titanium and Its Alloys—A Review
PublikacjaLaser surface modification is a widely available and simple technique that can be applied to different types of materials. It has been shown that by using a laser heat source, reproducible surfaces can be obtained, which is particularly important when developing materials for medical applications. The laser modification of titanium and its alloys is advantageous due to the possibility of controlling selected parameters and properties...
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Magnetic anisotropy in the exchange-biased laser-patterned thin Co/CoO films
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Fabrication Of Scaffolds From Ti6Al4V Powders Using The Computer Aided Laser Method
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Surface area investigation of materials with transition layers of continuously changing electron density
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Effect of temperature and gaseous medium on the structure and microhardness of the cobalt base clad layers
PublikacjaBadano wpływ temperatury utleniania na mikrostrukturę i mikrotwardość napawanych warstw ze stopu kobaltu. Warstwy wytwarzano za pomocą napawania plazmowego (pta) na przylgniach zaworów wylotowych wykonanych ze stali x40CrSiMo10-2. Stop kobaltu był poddany utlenianiu w powietrzu w temperaturach od 750 °C to 1100 °C i w gazach wylotowych w temperaturze 750 °C. W wyniku utleniania zaobserwowano zmanę w mikrotwardości warstw. W zewnętrznej...
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Influence of laser remelting at cryogenic conditions on corrosion resistance of non-ferrous alloys
PublikacjaCelem nadtapiania laserowego elementów wytwarzanych z stopów aluminium, miedzi i tytanu jest uzyskanie wysokiej twadrości i odporności na korozję dla wydłużenia okresu ich eksploatacji w rezultacie ich szybkiej krystalizacji. Końcowa mikrostruktura, skład fazowy i właściwości wymienionych stopów zależą od parametrów obróbki laserowej oraz budowy wykresów równowagi fazowej. W artykule przedstawiono wpływ laserowego nadtapiania...
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Spray pyrolysis of doped-ceria barrier layers for solid oxide fuel cells
PublikacjaGadolinium doped ceria (Ce0.8Gd0.2O2 − x-CGO) layer fabricated by spray pyrolysis is investigated as the diffusion barrier for solid oxide fuel cell. It is deposited between the La0.6Sr0.4FeO3 − δ cathode and the yttria stabilized zirconia electrolyte to mitigate harmful interdiffusion of elements. The parameters of the fabrication process are linked to the measured area specific resistances of the symmetrical cells and the efficiency...
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Verification of the new viscoelastic method of thermal stress calculation in asphalt layers of pavements
PublikacjaThe new viscoelastic method of thermal stress calculations in asphalt layers has been developed and published recently by the author. This paper presents verification of this method. The verification is based on the comparison of the results of calculations with results of testing of thermal stresses in Thermal Stress Restrained Specimen Test. The calculations of thermal stresses according to the new method were based on rheological...
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APPLYING RANSAC ALGORITHM FOR FITTING SCANNING STRIPS FROM AIRBORNE LASER SCANNING
PublikacjaDuring the development of the data acquired by airborne laser scanning the important issue is the fitting and georeferencing of ALS point clouds by means of the tie surfaces and the reference planes. The process of scanning strips adjustment is based on mutual integration of point clouds (scanning strips) and their adaptation to the reference planes.In simultaneous adjustment all strips are combined into one geometrically coherent...
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Assessing Acute Toxicity of Selected Packages Internal Layers Extracts using Microtox®
PublikacjaIn the scientific literature related to the widely understood issue of packaging materials designed to have contact with food (food contact materials), there is much information on raw materials used for their production, as well as their physiochemical properties, types and parameters. Unfortunately, not much attention is given to the issues concerning migration of toxic substances from packaging and its actual influence on the...
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Application of the laser diode with central wavelength 975 nm for the therapy of neurofibroma and hemangiomas
PublikacjaThis paper presents newly developed dermatological laser (with central wavelength 975 nm) for application in therapies requiring deep penetration of tissue, e.g. cutaneous (dermal) neurofibroma (Recklinghausen disease) and hemangiomas. This laser can work either in pulse or continues wave mode. Laser radiation is transmitted toward the application region by optical fiber with a diameter of 0.6 mm. The compact design of the laser...
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Surface Property Modification of Collagen, Hyaluronic Acid, and Chitosan Films with the Neodymium Laser
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Problems of analysis of axially loaded steel behavior under laser welded panel
PublikacjaWprowadzanie do praktyki nowych rozwiązań konstrukcyjnych wymaga posiadania danych wejściowych do procesu modelowania ich zachowania. Takim nowym elementem jest stalowy, spawany laserowo panel typu sandwich. W pracy pokazano wy-brane problemy towarzyszące modelowaniu zachowań takiej struktury. Pokazano podstawy teoretyczne wyznaczania sztyw-ności panelu a następnie omówiono wyniki badań wyboczenio-wych serii modeli o zmiennej geometrii.
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Prosthetic Elements Made of the Ti-13Zr-13Nb Alloy by Selective Laser Melting
PublikacjaThe fabrication of the prosthetic foundations and bridges from the Ti-13Zr-13Nb alloy is described. The process was started from CAD/CAM design of 3D models of the foundations based on scanning of patient`s mouth. Next, 3D models were transformed into *.stl files for the manufacturing stage and then the manufacturing process by means of the selective laser melting with the SLM Realizer 100 equipment was made. The intrinsic structure...
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Combined Close Range Photogrammetry and Terrestrial Laser Scanning for Ship Hull Modelling
PublikacjaThe paper addresses the fields of combined close-range photogrammetry and terrestrial laser scanning in the light of ship modelling. The authors pointed out precision and measurement accuracy due to their possible complex application for ship hulls inventories. Due to prescribed vitality of every ship structure, it is crucial to prepare documentation to support the vessel processes. The presented methods are directed, combined...
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Influence of Parameters of Laser Beam Welding on Structure of 2205 Duplex Stainless Steel
PublikacjaLaser welding is used in modern industry, having many advantages comparing to traditional welding technologies. Nowadays, industry sectors such as shipbuilding, automotive and aviation can’t be imagined without laser processing technologies. Possibility of increase of welded joint properties, autogenous welding and high level of process automation makes the technology of laser welding perspective part of the industry. Physical...
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Stability Assessment of Coastal Cliffs Incorporating Laser Scanning Technology and a Numerical Analysis
PublikacjaWe investigated the cli coast in Jastrzebia Gora, Poland. The measurements that were taken between 2014 and 2018 by applying terrestrial, mobile, and airborne laser scanning describe a huge geometric modification involving dislocations in a 2.5 m range. Dierential maps and a volumetric change analysis made it possible to identify the most deformed cli’s location. Part of the monitoring of coastal change involved the measurement...
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Surface texture formation in precision machining of direct laser deposited tungsten carbide
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