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Analiza wpływu produktów biodegradacji polikaprolaktonu modyfikowanego skrobią na populację cyjanobakterii
PublikacjaBiodegradacja, jako jedna z najnowszych metod remediacji środowiska naturalnego, znalazła swoje zastosowanie również w przypadku tworzyw sztucznych. Na rynku pojawiły się nowe polimery de-gradowalne ulegające destrukcji na drodze procesów biologicznych. Tradycyjne polimerowe opako-wania, stwarzające problem z utylizacją, są wypierane przez opakowania biodegradowalne (m.in. z Mater-Bi, PLA czy PCL), przeznaczone głównie do kompostowania....
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Laminaty FRP w budownictwie - charakterystyka materiału i aspekty projektowania
PublikacjaW artykule przedstawiono charakterystykę laminatów polimerowych wzmacnianych włóknami. W pierwszej części zaprezentowano teoretyczne modele materiałowe, podstawowe zależności naprężenie-odkształcenie włókien, matrycy oraz laminatu powstałego przez połączenie obydwu składników. Na tej podstawie sformułowano zalecenia dotyczące praktycznego wykorzystania laminatu w kontekście jego wytężenia w projektowaniu elementów konstrukcyjnych....
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Anion–cation interactions in a series of salts with substituted Hphen, Hbpy and H2bpy cations and [W(CN)8]4− anion: polymer with “super-short” N–H⋯N hydrogen bridges containing exclusively anions and H+
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Selected biotrends in development of epoxy resins and their composites
PublikacjaEpoxy resins and their fibre or particulate composites are widely used in various industries, including building, naval, aircraft, automotive and aerospace. Modern polymer science and technology focus on the development of green polymers and composites. There are two major areas of interest in the case of epoxy resins: the development of bio-based resins and the production of composites with natural fibers. One of the most interesting...
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THE IMPACT OF GROUND TIRE RUBBER TREATMENT ON THE THERMAL CONDUCTIVITY OF FLEXIBLE POLYURETHANE/GROUND TIRE RUBBER COMPOSITES
PublikacjaWaste car tires are burdensome waste, and their utilization is crucial for the natural environment. In many countries, the primary method of their recycling is energy recovery, performed by simple combustion. However, material recycling is much more effective and significantly more beneficial for the natural environment. It results in the generation of ground tire rubber, which can be used to produce polymerrubber composites. It...
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Pervaporation Zeolite-Based Composite Membranes for Solvent Separations
PublikacjaThanks to their well-defined molecular sieving and stability, zeolites have been proposed in selective membrane separations, such as gas separation and pervaporation. For instance, the incorporation of zeolites into polymer phases to generate composite (or mixed matrix) membranes revealed important advances in pervaporation. Therefore, the goal of this review is to compile and elucidate the latest advances (over the last 2-3 years)...
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Semicrystalline Polyesters Based on a Novel Renewable Building Block
PublikacjaIsohexides, like e.g. isosorbide, are well-known carbohydrate-based rigid diols which are capable of dramatically increasing the glass transition temperature of polyesters. However, their relatively low reactivity has thus far hampered large-scale industrial applications in the polymer field. Recently, with the aim to increase reactivity while at the same time retain rigidity, we have developed a new isoidide dicarboxylic acid...
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Zastosowania chromatografii wykluczania (SEC) w analityce technicznej i preparatyce – część I-sza.
PublikacjaW pracy scharakteryzowano założenia teoretyczne oraz mechanizm rozdzielania w warunkach chromatografii wykluczania (SEC). Przeanalizowano wady i zalety tej techniki rozdzielania. Przedstawiono przegląd zastosowań obejmujący wykorzystanie SEC w analityce technicznej oraz w preparatyce. SEC w warunkach liofilowych znajduje zastosowanie do rozdzielania mieszanin polimerów t.j. polistyren, polibutadien, poliizopren, poli(dimetylosiloksan),...
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Recycled Polyurethane as a Second Phase in Thermoset Blends and Its Effect on Thermal Degradation Kinetics Studies
PublikacjaA new approach is introduced in the modification of thermosetting polymer by using different amount of polyurethane of waste origin. The post consumer polyurethane foam coatings are degraded using glycolysis process and the recycled product is further converted into new polyurethane. The blending of recycled polyurethane with epoxy exhibits transparency and produces nanostructures. The effective interaction between two polymers...
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A novel method of creating thermoplastic chitosan blends to produce cell scaffolds by FDM additive manufacturing
PublikacjaDue to its remarkable and promising biological and structural properties, chitosan has been widely studied in several potential applications in the biomedical sector. Attempts are being made to use this polymer and its properties in thermoplastics dedicated to 3D printing in FDM technology. However, chitosan can be processed only from acid solution, which limits its applications. The paper presents a new path for the production...
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Simple synthesis route for fabrication of protective photo‐crosslinked poly(zwitterionic) membranes for application in non‐enzymatic glucose sensing
PublikacjaThis work focuses on the fabrication of non-enzymatic glucose sensing materials based on laser-formed Au nanoparticles embedded in Ti-textured substrates. Those materials possess good catalytic activity toward glucose oxidation in 0.1 × phosphate buffered saline as well as resistance to some interferants, such as ascorbic acid, urea, and glycine. The electrodes are further coated with three different polymers, that is, Nafion,...
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Commercially produced and modified starches
PublikacjaThis book presents some fascinating phenomena associated with the remarkable features of high performance polymers and also provides an update on applications of modern polymers. It offers new research on structure–property relationships, synthesis and purification, and potential applications of high performance polymers. The collection of topics in this book reflects the diversity of recent advances in modern polymers with a broad...
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Topological behavior mimicking ethylene–hexene copolymers using branched lactones and macrolactones
PublikacjaPolyolefins are of paramount importance in the world of polymers due to their technological and economic potential.1 However, their nonpolar character significantly restricts the compatibility and adhesion properties, which consequently limits their versatility. Moreover, an intensified demand for materials from renewable resources can also become a problematic venture for the current polyolefin industry.2 Although Braskem and...
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Interactions of fish gelatin and chitosan in uncrosslinked and crosslinked with EDC films: FT-IR study
PublikacjaFilms based on fish gelatin, chitosan and blend of fish gelatin and chitosan before and after cross-linking with EDC have been characterized by FT-IR spectroscopy. The FT-IR spectrum of fish gelatin film showed the characteristic amide I, amide II and amide III bands, and the FT-IR spectrum of chitosan film confirmed that the polymer was only a partially deacetylated product, and included CH3-C=O and NH2 groups, the latter both...
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Ex situ XANES, XPS and Raman studies of poly(3,4-ethylenedioxythiophene)modified by iron hexacyanoferrate
PublikacjaPraca dotyczy badań XANES, XPS i Ramana polimeru przewodzącego poli(3,4-etylenodioksytiofenu) modyfikowanego heksacyjanożelazianem żelaza. Badania XANES potwierdziły oktaedryczne otoczenie atomu żelaza, którego najbliższymi sąsiadami są atomy węgla oraz atomy azotu. Badania XPS wykazały istnienie wiązań Fe-C, Fe-N oraz chemicznego oddziaływania między atomem siarki polimeru a atomem żelaza błękitu pruskiego. Obecność oddziaływań...
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Advancing sustainable hybrid bitumen systems: A compatibilization solution by functionalized polyolefins for enhanced crumb rubber content in bitumen
PublikacjaPolymer waste pollution has a profound effect on the environment and, consequently, on the lifestyle of hu- mankind. The massive production and disposal of cross-linked polymers clearly exemplify the challenges of recycling. Increasing efforts are being undertaken to introduce recycled polymers, especially crumb rubber (CR), into asphalt formulations. Due to the rather poor processability and phase separation associated with CR- modified...
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Otrzymywanie i charakterystyka funkcjonalnych biomateriałów ksero- i hydrożelowych na bazie chitozanu oraz ocena ich możliwości aplikacyjnych.
PublikacjaMateriały polimerowe powszechnie wykorzystuje się praktycznie we wszystkich dziedzinach życia. Aspekt ekologiczny związany z utylizacją produktów wytwarzanych na bazie polimerów syntetycznych wywołał bardzo duże zainteresowanie możliwościami zastąpienia ich analogami pochodzenia naturalnego, które uważane są za niemal niewyczerpywalne źródło trwałych materiałów na świecie. Źródłem chitozanu, jednego z czołowych biopolimerów będących...
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Effect of Polymerization Statistics on the Electronic Properties of Copolymers for Organic Photovoltaics
PublikacjaStatistical block copolymers, composed of donor (D) and acceptor (A) blocks, are a novel type of material for organic photovoltaics (OPVs) devices. In particular a new series of polymers based on PBTZT-stat-BDTT-8, recently developed by Merck, offers high solubility in different solvents, and a high power conversion efficiency (PCE) in different device architectures. Although it is known that the electronic properties of these...
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Thermomechanical and Fire Properties of Polyethylene-Composite-Filled Ammonium Polyphosphate and Inorganic Fillers: An Evaluation of Their Modification Efficiency
PublikacjaThe development of new polymer compositions characterized by a reduced environmental impact while lowering the price for applications in large-scale production requires the search for solutions based on the reduction in the polymer content in composites’ structure, as well as the use of fillers from sustainable sources. The study aimed to comprehensively evaluate introducing low-cost inorganic fillers, such as copper slag (CS),...
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Dynamic analysis of temporary steel grandstand equipped with different types of bracing system
PublikacjaIn the paper, behaviour of a temporary steel grandstand equipped with two different types of bracing system has been analysed through the numerical study. A typical solution concerning application of a diagonal tubular members has been compared with elements proposed by authors and called polymer dampers. A polymer element consists of two L-shape steel members bonded with polymer mass. The aim of the paper is to verify the effectiveness...
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Enhancing the Seismic Resistance of Columns by GFRP Confinement Using Flexible Adhesive-Experimental Study
PublikacjaIn this paper, the results of two experiments, focused on testing the effectiveness of a method of enhancing the seismic (dynamic) resistance of masonry columns with the use of flexible polymer adhesive, are shown. The first experiment was devoted to investigate the damping properties of a polymer working between two stiff layers, whereas the aim of the second one was to verify if the identified damping properties of the polymer...
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Synteza i właściwości warstw poli(3,4-etylenodioksytiofenu) modyfikowanego heksacyjanożelazianami (II/III) wybranych metali przejściowych
PublikacjaPraca dotyczy modyfikacji warstw polimeru elektroatywnego poli(3,4-etylenodioksytiofenu) heksacyjanożelazianami (II/III) wybranych metali przejściowych (Fe, Co, Ni).
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Influence of e-beam irradiation on poly(aliphatic/aromatic-ester) multiblock copolymers used as biomaterials
PublikacjaThe use of polymers became more relevant in medical applications for the versatility in processing and enhanced material properties of polymers. In order to be suitable as a biomaterial, it is of medical importance that these polymers are biocompatible and do not elicit negative responses from the body after implantation. Furthermore during the course of usage under load-bearing conditions, these biomaterials must sustain dynamical...
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Usuwanie lotnych związków organicznych z fazy gazowej z zastosowaniem cieczy jonowych
PublikacjaUżycie cieczy jonowej do usuwania LZO jest limitowane przez rozpuszczalność usuwanych związków. Dane literaturowe sugerują, że ciecze jonowe jako faza membranowa mogą być z powodzeniem stosowane do selektywnej separacji węglowodorów aromatycznych z mieszanin węglowodorów aromatycznych i alifatycznych. Przedmiotem pracy było kompleksowe opisanie procesu separacji LZO z fazy gazowej z uwzględnieniem czynników wpływających na efektywność...
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A novel method for drop in drop edible oils encapsulation with chitosan using a coaxial technique
PublikacjaThe presented work concerns a novel one step method for oil encapsulation. In this coaxial system the oil constitutes the core of the capsule, while the chitosan solution is the polymer shell surrounding the core to provide separation of the core from the external environment. The paper contains a diagram of the encapsulation equipment and explains the principle of its operation. The experimental results showed the impact of the...
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Silver(I) complexes with nitrile ligands: New materials with versatile applications
PublikacjaIn the present study, the structure, thermal stability, conductive properties, and antimicrobial activity of silver(I) complexes with nitrile ligands were investigated. For the construction of the materials, 2-cyanopyridine (2-cpy), 4-cyanopyridine (4-cpy), 1,2-dicyanobenzene (1,2-dcb), and 1,3-dicyanobenzene (1,3-dcb) were used in addition to the silver nitrite and nitrate. Four new compounds were isolated and structurally characterized:...
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Cytocompatibility of stabilized black phosphorus nanosheets tailored by directly conjugated polymeric micelles for human breast cancer therapy
PublikacjaThe novel procedure of few-layer black phosphorus (FLBP) stabilization and functionalisation was here proposed. The cationic polymer PLL and non-ionic PEG have been involved into encapsulation of FLBP to allow sufficient time for further nanofabrication process and overcome environmental degradation. Two different spacer chemistry was designed to bind polymers to tumor-homing peptides. The efficiency of functionalisation was examined...
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Thermal and dynamic mechanical analysis of cross-linked poly(esterurethanes)
PublikacjaW pracy przedstawiono wyniki badań termograwimetrycznych oraz termomechanicznych usieciowanch za pomocą styrenu i metakrylanu metylu poli(estrouretanów). Uzyskane wyniki pozwoliły stwierdzić, że stabilność termiczna poli(estrouretanów) jest wystarczająca do wielu zastosowań technicznych. Przeprowadzone analizy wykazały również, iż polimery sieciowane styrenem wykazują separację fazową.
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Rozdrobione odpady polimerowe- nowy problem i świadek historii wpływu człowieka na najnowsze dzieje ziemi.
PublikacjaSyntetyczne polimery są nieodłącznym towarzyszem współczesnego człowieka i dowodem jego działalności obecnym w osadach, szczególnie od połowy XX wieku. Przeciętny konsument wprowadza dziennie do środowiska około 2,4 mg mikroplastiku. Terminem "mikroplastik" określa się odpady z tworzyw sztucznych, ktorych wielkość nie przekracza 5 mm.
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THE MELT FLOWABILITY AND TENSILE PERFORMANCE OF POLY (-CAPROLACTONE)/BREWERS’ SPENT GRAIN COMPOSITES AS A FUNCTION OF FILLER MODIFICATION
PublikacjaNowadays, it is essential to reduce the environmental impact of products and technologies. Such an approach should be highlighted in all research activities. In the case of polymer composites, it can be realized by introducing by-products or waste materials as fillers. An auspicious example of such material is the brewers’ spent grain, the major byproduct of the beer production. Its chemical composition, relatively similar to conventional...
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Experimental Study on the Effectiveness of Polyurethane Flexible Adhesive in Reduction of Structural Vibrations
PublikacjaThe aim of the present study is to consider the idea of using polyurethane flexible adhesive in to reduce the vibrations in structures exposed to dynamic loads and evaluate their damping properties in relation to large deformations. Firstly, two aluminium cantilever beams, simulating structural elements (without and with polyurethane layer in the form of tape), were analysed, in order to check the damping of the unconstrained polymer...
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Proposal of New Starch-Blends Composition Quickly Degradable in Marine Environment
PublikacjaThe aim of this paper was to obtain a quickly degradable in seawater polymer blend as an alternative proposal for classical polymer packaging. For preliminary studies: poly(lactic acid) (PLA), starch, calcium carbonate (CaCO3), gelatin and glycerol were chosen. PLA was pointed out due to its biodegradability and comparable properties to polyethylene or polypropylene. Whereas starch was chosen as abundant, renewable and cheap polymer...
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Materiały i fabrykacja w kontekście paradygmatu cyfrowego w architekturze
PublikacjaOpracowanie dotyczy wpływu jaki na współczesną architekturę ma rozwój nauki o materiałach i technologii CNC. Nowe technologie pozwalają na realizację wielokrzywiznowej geometrii oraz uzyskiwanie unikalnych efektów materiałowych z wykorzystaniem zarówno nowych budulców jakimi są materiały kompozytowe i polimery jak również tradycyjnych materiałów takich jak cegła i kamień.
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Materiały i fabrykacja w kontekście paradygmatu cyfrowego w architekturze
PublikacjaOpracowanie dotyczy wpływu jaki na współczesną architekturę ma rozwój nauki o materiałach i technologii CNC. Nowe technologie pozwalają na realizację wielokrzywiznowej geometrii oraz uzyskiwanie unikalnych efektów materiałowych z wykorzystaniem zarówno nowych budulców jakimi są materiały kompozytowe i polimery jak również tradycyjnych materiałów takich jak cegła i kamień.
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Self-healing mechanism of metallopolymers investigated by QM/MM simulations and Raman spectroscopy
PublikacjaThe thermally induced self-healing mechanisms in metallopolymers based on bisterpyridine complexes of iron(II) sulfate and cadmium(II) bromide, respectively, were studied by means of combined quantum mechanical/molecular mechanical (QM/MM) simulations and Raman spectroscopy. Two possible healing schemes, one based on a decomplexation of the cross-linking complexes and a second one relying on the dissociation of ionic clusters,...
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Integration of antifouling properties into epoxy coatings: a review
Publikacjahe need for nontoxic antifouling coatings has encouraged material scientists to develop a class of organic coatings for diverse applications. As a versatile thermosetting resin and well known for coating application, antifouling characteristics have been integrated into epoxy along with anticorrosion and adhesive functions. Accordingly, both micro- and macro-biofoulings have been successfully controlled by using epoxy-based antifouling...
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Transdermal transport of collagen and hyaluronic acid using water in oil microemulsion
PublikacjaCollagen and hyaluronic acid (HA) are biopolymers that affect the appearance and condition of the skin. Delivery of these compounds into the skin is highly challenging since have a number of disadvantageous properties, such as high molecular weight and hydrophilicity. Here, we evaluated the transdermal penetration of low and high molecular weight collagen and HA from microemulsions. A number of microemulsion formulations, differing...
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Polysaccharides in fabrication of membranes: A review
PublikacjaSustainability concerns have motivated and directed a great deal of interest over the past decade towards the development of green technologies. Polysaccharides are green polymers, which experienced growing demand to substitute chemically synthetic polymers. Different types of polysaccharides i.e. cellulose-, starch-, chitin- alginate-, and chitosan-based carbohydrate polymers have been applied in the fabrication of separation...
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Spectroelectrochemical characteristics of poly(3,4-ethylenedioxythiophene) / iron hexacyanoferrate film-modified electrodes
PublikacjaPraca dotyczy pomiarów spektroelektrochemicznych materiałów hybrydowych złożonych z polimeru elektroaktywnego poli(3,4-etylenodioksytiofenu) i Błękitu Pruskiego. Dla porównania badano również filmy polimerowe z wybranymi przeciwjonami: heksacyjanożelazowym (Fe(CN)63-/4-), chlorkowym (Cl-) i polistyrenosulfonowym (PSS-). Materiały w postaci cienkich filmów otrzymano na elektrodzie szklanej pokrytej tlenkiem indowo-cynowym. Widma...
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Hyaluronan-Chondroitin Sulfate Anomalous Crosslinking Due to Temperature Changes
PublikacjaGlycosaminoglycans are a wide class of biopolymers showing great lubricating properties due to their structure and high affinity to water. Two of them, hyaluronic acid and chondroitin sulfate, play an important role in articular cartilage lubrication. In this work, we present results of the all-atom molecular dynamics simulations of both molecules placed in water-based solution. To mimic changes of the physiological conditions,...
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Synergistic Effects of Bitumen Plasticization and Microwave Treatment on Short-Term Devulcanization of Ground Tire Rubber
PublikacjaGround tire rubber (GTR) was mechano-chemically modified with road bitumen 160/220 and subsequently treated using a microwave radiation. The combined impact of bitumen 160/220 content and microwave treatment on short-term devulcanization of GTR was studied by thermal camera, wavelength dispersive X-ray fluorescence spectrometry (WD-XRF), static headspace, and gas chromatography-mass spectrometry (SHS-GC-MS), thermogravimetric analysis...
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Fabrication and Characterization of Flexible Medical-Grade TPU Filament for Fused Deposition Modeling 3DP Technology
PublikacjaThe possibility of using additive manufacturing (AM) in the medicine area has created new opportunities in health care. This has contributed to a sharp increase in demand for 3D printers, their systems and materials that are adapted to strict medical requirements. We described herein a medical-grade thermoplastic polyurethane (S-TPU) which was developed and then formed into a filament for Fused Deposition Modeling (FDM) 3D printers...
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Microporous Polyurethane Thin Layer as a Promising Scaffold for Tissue Engineering
PublikacjaThe literature describes that the most efficient cell penetration takes place at 200–500 µm depth of the scaffold. Many different scaffold fabrication techniques were described to reach these guidelines. One such technique is solvent casting particulate leaching (SC/PL). The main advantage of this technique is its simplicity and cost efficiency, while its main disadvantage is the scaffold thickness, which is usually not less than...
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The Influence of Calcium Glycerophosphate (GPCa) Modifier on Physicochemical, Mechanical, and Biological Performance of Polyurethanes Applicable as Biomaterials for Bone Tissue Scaffolds Fabrication
PublikacjaIn this paper we describe the synthesis of poly(ester ether urethane)s (PEEURs) by using selected raw materials to reach a biocompatible polyurethane (PU) for biomedical applications. PEEURs were synthesized by using aliphatic 1,6-hexamethylene diisocyanate (HDI), poly(ethylene glycol) (PEG), α,ω-dihydroxy(ethylene-butylene adipate) (Polios), 1,4-butanediol (BDO) as a chain extender and calcium glycerolphosphate salt (GPCa) as...
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The Drop-in-Drop Encapsulation in Chitosan and Sodium Alginate as a Method of Prolonging the Quality of Linseed Oil
PublikacjaNowadays, the encapsulation of sensitive products by various techniques has become popular as a promising preservation method. In particular, this applies to oils with a high content of unsaturated fatty acids and a high susceptibility to deterioration. This work presents the possibility of using a chitosan and sodium alginate in the form of a hydrogel membrane to protect food ingredients such as linseed oil, which is stored in...
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Structural and Thermo-Mechanical Properties of Poly(ε-caprolactone) Modified by Various Peroxide Initiators
PublikacjaThe modification of poly(ε-caprolactone) (PCL) was successfully conducted during reactive processing in the presence of dicumyl peroxide (DCP) or di-(2-tert-butyl-peroxyisopropyl)-benzene (BIB). The peroxide initiators were applied in the various amounts of 0.5 or 1.0 pbw (part by weight) into the PCL matrix. The effects of the initiator type and its concentration on the structure and mechanical and thermal properties of PCL were...
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The Production Possibility of the Antimicrobial Filaments by Co-Extrusion of the PLA Pellet with Chitosan Powder for FDM 3D Printing Technology
PublikacjaThe last decades have witnessed a major advancement and development in three-dimensional (3D) printing technology. In the future, the trend’s utilization of 3D printing is expected to play an important role in the biomedical field. This work presents co-extrusion of the polylactic acid (PLA), its derivatives (sPLA), and chitosan with the aim of achieving filaments for printing 3D objects, such as biomedical tools or implants. The...
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Optimization of FFF Process Parameters by Naked Mole-Rat Algorithms with Enhanced Exploration and Exploitation Capabilities
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Microscopic and Spectroscopic Imaging and Thermal Analysis of Acrylates, Silicones and Active Pharmaceutical Ingredients in Adhesive Transdermal Patches
PublikacjaDermal or transdermal patches are increasingly becoming a noteworthy alternative ascarriers for active pharmaceutical ingredients (APIs), which makes their detailed physicochemical evaluation essential for pharmaceutical development. This paper demonstrates mid-infrared (FTIR) and Raman spectroscopy with complementary microscopic methods (SEM, optical and confocal Raman microscopy) and differential scanning calorimetry...
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Physical and Mechanical Evaluation of Silicone-Based Double-Layer Adhesive Patch Intended for Keloids and Scar Treatment Therapy
PublikacjaGrowing interest in silicone elastomers for pharmaceutical purposes is due to both theirbeneficial material effect for scar treatment and their potential as drug carriers. Regarding their morphological structure, silicone polymers possess unique properties, which enable a wide range of applicability possibilities. The present study focused on developing a double-layer adhesive silicone film (DLASil) by evaluating its physical...