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Extraction of acidic herbicides from soil by means of accelerated solvent extraction.
PublikacjaZaprezentowano opracowanie procedury izolacji herbicydów kwasowych z gleby z zastosowaniem urządzenia DIONEX ASE 200. Celem było zoptymalizowanie warunków pracy urządzenia: czasu, temperatury, ciśnienia oraz ilości cykli ekstrakcji. Ostatecznie ekstrakty, po przeprowadzeniu analitów w pochodne metylowe, poddano analizie chromatograficznej (GC).
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Determination of environmental pollutants in soil and sediments - some aspects of sample clean-up and GC analysis
PublikacjaPrzedstawiono wstępne wyniki badań nowej procedury analitycznej przeznaczonej do badań próbek i osadów dennych na zawartość związków organicznych (WWAPCB). Procedura składa się z następujących etapów: - ekstrakcji analitów z wykorzystaniem techniki ASE, - oczyszczania ekstraktów (kolumienki), - chromatograficznego rozdzielania i oznaczania analitów.
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Zagrożenia bezpieczeństwa protokołów komunikacji morskiej, lotniczej i lądowej
PublikacjaW artykule przedstawiono przykładowe zagrożenia wykorzystujące słabości wybranych protokołów komunikacji morskiej, lotniczej i lądowej. Wskazano, jakie czynności należy podjąć, żeby się przed nimi ustrzec (przynajmniej częściowo). Opisano również kierunek, w jakim powinny być rozwijane analizowane protokoły, aby zwiększyć bezpieczeństwo osób je używających.
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Stress Detection of Children with Autism using Physiological Signals in Kaspar Robot-Based Intervention Studies
PublikacjaThis study aims to develop a stress detection system using the blood volume pulse (BVP) signals of children with Autism Spectrum Disorder (ASD) during robot-based interven- tion. This study presents the heart rate variability (HRV) analysis method to detect the stress, where HRV features are extracted from raw BVP signals recorded from an E4 wristband during interaction studies with the social robot Kaspar. Low frequency power...
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Selected concentration techniques for gas chromatographic analysis of environmental samples
PublikacjaThe paper describes the role and tasks of environmental analysis and monitoring. It emphasises the leading role played by gas chromatography, especially when coupled with suitable sample preparation. This is demonstrated by some literature evidence and mainly by the author's original work on the design of sample preparation apparatus and development of GC-based methods of determination of a wide variety of organic pollutants in...
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Limited selectivity of amperometric gas sensors operating in multicomponent gas mixtures and methods of selectivity improvement
PublikacjaIn recent years, smog and poor air quality have became a growing environmental problem. There is a need to continuously monitor the quality of the air. The lack of selectivity is one of the most important problems limiting the use of gas sensors for this purpose. In this study, the selectivity of six amperometric gas sensors is investigated. First, the sensors were calibrated in order to find a correlation between the concentration...
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WSPÓŁCZESNE OCHŁODZENIE REJONU SZETLANDÓW POŁUDNIOWYCH I PÓŁNOCO-ZACHODNICH KRAŃCÓW PÓŁWYSPU ANTARKTYCZNEGO
PublikacjaThe paper discusses changes of hydro-climatic conditions occurring in the South Shetland Islands and in NW parts of the Antarctic Peninsula in the 1979–2016 years period. These changes are important for evaluation of the transformation of marine and coastal ecosystems. The general feature of these changes was a transition from the strong warming phase to the cooling phase, which took place around the year 2000. The paper presents...
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Experimental tests of lintel hybrid beams
PublikacjaThe results of experimental tests of lintel hybrid beams made of air concrete and prestressed concrete were presented in paper. Blocks of air concrete was a protective element for the construction one. The length of hybrid beams was 3.0 m, while total height 27 cm. It was assumed that hybrid beams will work in the simply-supported scheme (with a 10 cm support) loaded uniformly over the entire length. The object of the tests were...
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Constrained aerodynamic shape optimization using neural networks and sequential sampling
PublikacjaAerodynamic shape optimization (ASO) involves computational fluid dynamics (CFD)-based search for an optimal aerodynamic shape such as airfoils and wings. Gradient-based optimization (GBO) with adjoints can be used efficiently to solve ASO problems with many design variables, but problems with many constraints can still be challenging. The recently created efficient global optimization algorithm with neural network (NN)-based prediction...
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Możliwości zamiany elektrycznych przepływomierzy powietrza stosowanych w silnikach spalinowych samochodów
PublikacjaW artykule przedstawiono podstawowe typy przepływomierzy powietrza, stosowane w silnikach spalinowych samochodów: z klapąspiętrzającą, HLM, HFM, Vortex i MAP. Przedstawiono wyniki badania tych przepływomierzy na specjalnie przygotowanym stanowisku pomiarowym. Przeanalizowano możliwość ich zamiany i zweryfikowano taką możliwość w praktyce.
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Production of fuel briquette from solid waste biomass using natural resin as a binder
PublikacjaBackground: This research aimed to evaluate the use of natural resin as a binder for the production of fuel briquette from solid waste biomass.Methods: Proximate analyses were made for fuel briquette prepared from solid waste biomass using natural resin as a binder in comparison with using starch as a binder.Results: The results for density, percent content of moisture, percent content of volatile matter, percent...
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Experimental Study of the Resistance to Influence of Aggressive Liquids on Lightweight Concrete
PublikacjaIn light of the scientific research, the corrosion of concrete structures is one of the main problems that may reduce their durability due to the negative impact of the natural environment. The paper analyzes the influence of the type of component on the selected properties of lightweight concrete subjected to the influence of aggressive liquids. Four concrete mixes were prepared with a granular aggregate made of foamed glass (GEGA)...
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Production of fuel briquette from solid waste biomass using natural resin as a binder
PublikacjaAbstract Background: This research aimed to evaluate the use of natural resin as a binder for the production of fuel briquette from solid waste biomass. Methods: Proximate analyses were made for fuel briquette prepared from solid waste biomass using natural resin as a binder in comparison with using starch as a binder. Results: The results for density, percent content of moisture, percent content of volatile matter, percent content...
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Study of the Resistance to Influence of Aggressive Liquids on Concrete with Lightweight Aggregate
PublikacjaThe corrosion of the structure of concrete caused by the aggressive external environment is one of the main problems that can reduce the durability of buildings. The paper analyzes the influence of the type of component on selected properties of lightweight concrete (LWC) exposed to aggressive liquids. When lightweight concrete containing porous aggregates is used, the influence of an aggressive environment may be of particular...
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Investigation of Acoustic Properties of Poroelastic Asphalt Mixtures in Laboratory and Field Conditions
PublikacjaMeasures for the improvement of acoustic conditions in the vicinity of roads include the construction of pavement structures with low-noise surfaces with optimal macrotexture and the highest possible sound absorption coefficient. Laboratory evaluation of acoustic properties of a designed asphalt mixture before its placement in the pavement is a good solution. Currently, the most popular method for the determination of the sound...
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Interactions in aqueous solutions of K-peptide and DMSO – spectroscopic and calorimetric studies
PublikacjaIntroduction K-peptide (GILQINSRW) – short 9 amino acid fragment of the hen egg white lysozyme has the ability to form amyloid structures. Dimethyl sulfoxide (DMSO) is an osmolyte which can alter this ability. Our goal was to get an insight into the mechanism of Kpeptide-DMSO interactions in aqueous solutions. Such a knowledge can be helpful to understand processes leading to various neurodegenerative diseases. Methods ATR-FTIR...
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Preconditioners with Low Memory Requirements for Higher-Order Finite-Element Method Applied to Solving Maxwell’s Equations on Multicore CPUs and GPUs
PublikacjaThis paper discusses two fast implementations of the conjugate gradient iterative method using a hierarchical multilevel preconditioner to solve the complex-valued, sparse systems obtained using the higher order finite-element method applied to the solution of the time-harmonic Maxwell equations. In the first implementation, denoted PCG-V, a classical V-cycle is applied and the system of equations on the lowest level is solved...
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Urządzenie do wytwarzania gazowych mieszanin wzorcowych z wykorzystaniem procesu barbotażu oraz permeacji
PublikacjaReference gas mixtures are classified to reference materials and are mainly used for quality monitoring and identification of impurities in atmospheric air. They can be also used for calibration of measuring devices. Nowadays, there is a need to develop a new techniques for the preparation of reference gas mixtures [1, 2]. In this paper the design and the operating principles of instrument based on the use of barbotage and permeation...
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CAES – Energy storage providing stability for national power system
PublikacjaThis paper presents a short characteristics of the power system. It also describes various types of energy storage technologies. The suggested solution of accumulation and generation of electric power is based on the cooperation of gas turbine with Compressed Air Storage Energy systems – CAES. This analysis describes also various types of cooperation of CAES and renewable sources of energy, particularly wind power systems.
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Determination of organotin compounds in biological samples using accelerated solvent extraction, sodium tetraethylborate ethylation, and multicapillary gas chromatography flame photometric detection.
PublikacjaPrzedstawiono metodę oznaczania związków cynoorganicznych w próbkach biologicznych. Procedura oparta jest na wykorzystaniu ekstrakcji pod zwiększoną temperaturą i ciśnieniem (ASE) do izolacji związków cynoorganicznych z próbek wątroby morświnów odłowionych w Morzu Bałtyckim. Walidacji metody dokonano na podstawie analizy materiału odniesienia NIES No 11.
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Udział Politechniki Gdańskiej w projekcie RECO
PublikacjaReco jest projektem opartym na współpracy partnerów z Białorusi, Estonii, Finlandii, Litwy, Łotwy, Niemiec, Polski, Rosji i Szwecji w zakresie gospodarki odpadami i planowania przestrzennego. Liderem projektu jest Urząd Administracji Regionu Sztokholm. Projekt Reco realizowany jest w ramach Programu BSR Interreg III B
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Uzbrojenie sieci kanalizacyjnych
PublikacjaCele uzbrojenia sieci. Kanalizacyjne studzienki rewizyjne - zasady, rozwiązania konstrukcyjne, rozwiązania materiałowe, współpraca z podłożem. Spoczniki, studzienki spadowe, płuczki, przewietrzniki, syfony, przelewy, separatory, wpusty deszczowe, zbiorniki retencyjne. Separacja olejów, specjalna konstrukcja KSR, ochrona przed cofką. Przepompownie ścieków, wyloty. Obiekty hydrotechniczne w infrastrukturze drogowej.
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Wideband Radio Direction Finder Implemented in Software Defined Radio Technology
PublikacjaIn the paper a wideband radio direction finder (RDF) implemented in software defined radio (SDR) technology and the results of hardware layer research, including developed antenna switching unit (ASU), are presented. The results of tests of the devices, which are the part of the software defined radio platform (SDRP), and antenna switching unit, confirmed the possibility of using selected components in the final solution.
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Wdrożenie nowych regulacji prawnych w ochronie powietrza atmosferycznego w Polsce
PublikacjaW artykule przedstawiono zmiany prawne wynikające z przystosowania dyrektyw 2008/50/WE i 2004/107/WE do prawodawstwa polskiego. Nowe regulacje odnoszące się do ochrony powietrza stanowią jedynie rozbudowanie i modyfikację istniejacych dotychczas przepisów. W ratykule podano istotne informacje wynikajace z decyzji Komisji Europejslkiej 2011/850/UE
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Assessing agri-environmental schemes for semi-natural grasslands during a 5-year period: can we see positive effects for vascular plants and pollinators?
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Biowaste chicken eggshell powder as a potential cure modifier for epoxy/anhydride systems: competitiveness with terpolymer-modified calcium carbonate at low loading levels
PublikacjaBiowaste chicken eggshell (ES) powder was applied as a potential cure modifier in epoxy/anhydride systems. Cure behaviour and kinetics of composites filled with very low content (0.1 wt% based on epoxy resin) of ES, calcium carbonate (CaCO3), and terpolymer-modified fillers, mES and mCaCO3, were discussed comparatively. Surface analysis was performed by X-ray photoelectron spectroscopy. Cure kinetics was investigated by differential...
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Aproksymacja przebiegu trasy kolejowej na przykładzie krzywoliniowego odcinka połączenia Somonino-Gdańsk Osowa
PublikacjaW artykule zaprezentowano wyniki wyznaczenia współrzędnych przebiegu trasy kolejowej metodami aproksymacji wielomianowej i interpolacji krzywą kubiczną w oparciu o pomiary czasu rzeczywistego GPS zrealizowane z wykorzystanie polskiej aktywnej sieci geodezyjnej ASG-EUPOS. Rozważania teoretyczne poparte zostały praktycznym przykładem aplikacyjnym opartym o zrealizowane pomiary inwentaryzacyjne zmodernizowanego odcinka toru kolejowego...
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Pressure Pulsations in Turbine Blade Seal
PublikacjaThe paper presents the results of experimental investigations into pressure forces generated in a turbine labyrinth seal. The experiments were performed on a single-stage air model turbine of the impulse type. The performed experimental research proved that in a shroud clearance the pressure pulsates and the effects of the nozzle trailing edge thickness as well as the influence of the rotor blades are observed. The exemplary results...
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Evaluation of cathode materials for electrochemical photocatalyst deposition
PublikacjaElectrochemical deposition of photocatalyst, especially TiO2, onto several cathode materials was investigated and evaluated. The deposited films were characterized by scanning electron microscopy (SEM), energy dispersive X-ray spectrometer (EDX) and electrochemical measurements. Photocatalytic activity was determined by the decomposition of cyclohexane in air by irradiation with ultraviolet light emitting diodes. It was found that...
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Fault Diagnostics in PEMFC Stacks by Evaluation of Local Performance and Cell Impedance Analysis
PublikacjaStarvation, flooding, and dry‐out phenomena occur in polymer electrolyte membrane fuel cells (PEMFCs), due to heterogeneous local conditions, material inhomogeneity, and uneven flow distribution across the single cell active area and in between the individual cells. The impact of the load level and air feed conditions on the performance was identified for individual single cells within a 10‐cell stack. Analysis of the current density...
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Study of oxygen electrode reactions on symmetrical porous SrTi0.30Fe0.70O3-δ electrodes on Ce0.8Gd0.2O1.9 electrolyte at 800 °C–500 °C
PublikacjaIron doped strontium titanates (SrTi1-xFexO3-δ) are an interesting mixed ionic-electronic conductor model used to study basic oxygen reduction/oxidation reactions. In this work, we performed an impedance spectroscopy study on symmetrical porous SrTi0.30Fe0.70O3-δ (STF70) electrodes on a ceriabased electrolyte. The sample was measured in varying oxygen concentration: from 0.3% to 100% in 800 °C - 500 °C temperature range. Low polarisation...
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RESEARCH ON ORGANIC COATINGS DESIGNED FOR UNDERWATER APPLICATIONS
PublikacjaUnderwater steel structures require periodic maintenance. In the case of vessels, anti-corrosion works are carried out in the shipyard, where very good conditions for applying organic protective coatings can be provided. Very good surface preparation can be obtained by the use of abrasive blasting. The well-prepared metal surface is free from impurities (particularly inorganic salts). Suitable conditions for the application and...
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Numerical analysis of CO2-water separation in a horizontal double T-junction
PublikacjaCarbon dioxide is considered one of the main factors leading to global warming. Considering the significant impacts of CO2 on climate change, various technologies have been developed in recent decades to control carbon emission, such as for example CO2 capture and storage. The developed cycle of a negative CO2 emission power plant includes some devices, out of which, separator plays an indispensable role. To this end, T-junction...
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Shear fracture of longitudinally reinforced concrete beams under bending using Digital Image Correlation and FE simulations with concrete micro-structure based on X-ray micro-computed tomography images
PublikacjaThe paper presents experimental and numerical investigations of the shear fracture in rectangular concrete beams longitudinally reinforced with steel or basalt bar under quasi-static three point bending. Shear fracture process zone formation and development on the surface of beams was investigated by Digital Image Correlation (DIC) whereas thorough analyses of 3D material micro-structure, air voids, width and curvature of shear...
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Conductivity, structure, and thermodynamics of Y2Ti2O7–Y3NbO7 solid solutions
PublikacjaThe defect fluorite yttrium niobate Y3NbO7 and pyrochlore yttrium titanate Y2Ti2O7 solid solutions have been synthesized via a solid state synthesis route. The resulting stoichiometry of the oxides is Y2+xTi2−2xNbxO7, where x = 0 to x = 1. All of the samples were single-phase; however, for those with a predominant fluorite phase, a small amount of additional pyrochlore phase was detected. The volume of the solid solution unit cells...
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In-situ and ex-situ resistance measurements of polypyrrole film using double-band electrode
PublikacjaMany in-situ techniques are performed in order to determine the resistance of conducting polymer film. However, the resistance measured in solution can be the combination of polymer resistance and that of other components, such as resistance of supporting electrolyte. Therefore, in this work, the influence of the solution on the resistance of polypyrrole (PPy) film has been studied. PPy film was electrchemically synthesized onto...
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Potential of novel atomic emission techniques as a tool for investigation of the possibilities of using industrial waste as additives in construction materials
PublikacjaNowadays, due to the global ecological crisis and ways to prevent a climate disaster, more and more attention is paid to green techno-logies and green Chemistry, which are part of the so-called “The Green Deal.” The main assumption is the optimization of the processes of producing necessary goods and the implementation of methods of managing postproduction waste in the least environmentally harmful manner. In the presented research,...
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Improvement of the Chimney Effect in Stack Ventilation
PublikacjaThe article is focused on the airflow in a ventilation system in a building. The work examines the methods which enhance the chimney effect. In this paper, three cases with different chimneys were analyzed for the full-scale experiment. These cases were characterized by different geometrical and material parameters, leading to differences in the intensity of the ventilation airflow. The common denominator of the cases was the room...
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Long-term comparative evaluation of an acoustic climate in selected schools before and after the acoustic treatment
PublikacjaThe results of long-term continuous noise measurements in two selected schools are presented in the paper. Noise characteristics were measured continuously there for approximately 16 months. Measurements started eight months prior to the acoustic treatment of the school corridors of both schools. An evaluation of the acoustic climates in both schools, before and after the acoustic treatment, was performed based on comparison of...
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Analysis of odour interactions in model gas mixtures using electronic nose and fuzzy logic
PublikacjaMeasurement and monitoring of air quality in terms of odour nuisance is an important problem. Although the source of these nuisances is different (e.g. wastewater treatment plants, municipal landfills), their common feature is that they are a complex mixture of odorants with different odour thresholds. An additional problem is occurrence of the odour interactions between mixture components. From a practical point of view, it would...
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FROM HARVESTING TO DISTILLATION - EFFECT OF ANALYTICAL PROCEDURES ON THE YIELD AND CHEMICAL COMPOSITION OF RHODODENDRON TOMENTOSUM (LEDUM PALUSTRE) ESSENTIAL OIL
PublikacjaRhododendron tomentosum possesses the anti-inflammatory, analgesic and antimicrobial properties, determined by the chemical composition of its essential oil. The effects of place (Miszewko, Lubichowo) and time of harvesting (June, November) as well as drying (air-drying, oven-drying, freeze-drying) and isolation (in Deryng, Clevenger and Likens-Nickerson apparatus) procedures on the yield and quality of R. tomentosum essential...
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Comprehensive stabilization of all streams of solid residues formed during sewage sludge thermal treatment – Case study
PublikacjaModern wastewater treatment plants are currently struggling with the problem of processing and ecological management of sewage sludge. Thermal utilization is a frequently used practice of excess sludge utilization especially in large wastewater treatment plants, which seems to be a quite promising concept. However, during thermal treatment, fractions of ashes and dusts are generated. Such wastes, especially the dust fraction, can...
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High precision and accuracy using low cost GNSS receivers and supporting technologies
PublikacjaThis chapter focuses on methods and techniques of positioning, based on the highly accurate and precise Global Navigation Satellite System (GNSS), which are available at a relatively low price. In this context, a comparison of different positioning methods provided by the free and open source software (FOSS) package called RTKLIB is given. Other aspects related to price reduction are also considered, including availability and...
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Sound intensity distribution around organ pipe
PublikacjaThe aim of the paper was to compare acoustic field around the open and stopped organ pipes. The wooden organ pipe was located in the anechoic chamber and activated with a constant air flow, produced by an external air-compressor. Thus, long-term steady state response was possible to obtain. Multichannel acoustic vector sensor was used to measure the sound intensity distribution of radiated acoustic energy. Measurements have been...
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Jakościowa identyfikacja pierścieni izocyjanurowych w elastomerach uretanowo-izocyjanurowych i w ich hydrolizatach.
PublikacjaStwierdzono, że metodą ATR nie można zrealizować wiarygodnej jakościowej identyfikacji pierścieni izocyjanurowych bezpośrednio w elastomerach uretanowo-izocyjanurowych (EUI). Identyfikacja taka staje się możliwa dopiero na podstawie analizy produktów hydrolizy EUI w środowisku kwaśnym. Przeprowadzono ją metodami FT-IR, C NMR i HPLC w połączeniu z UV.....
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Nitrogen dioxide gas-sensing detection with GO modified CuO thin films
PublikacjaGas sensors have been continuously developed over the last few decades for several applications including air quality monitoring, automotive industry and recently for medical use. Gas sensors are usually based on metal oxides (MOXs), such as SnO2, TiO2, ZnO, WO3, CuO. Recently, new materials such as graphene oxide and heterostructures of graphene oxide and metal oxides are utilized for gassensing applications.
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Group 11 complexes with a phosphanylphosphaalkene ligand: preparation and stability study
PublikacjaThe reactivities of two selected phosphanylphosphaalkenes, Ph2C=P-PtBu2 (1a) and (p-MeO-Ph)2C=P-PtBu2 (1b), toward CuCl, AgCl and (tht)AuCl (tht = tetrahydrothiophene) were investigated. As a result, new phosphanylphosphaalkene dimeric and monomeric complexes were formed (Cu and Ag dimeric and Au monomeric). All obtained products were air and moisture stable and light insensitive.
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Pollutant deposition via dew in urban and rural environment, Cracow, Poland
PublikacjaThis study is a comparative analysis of dew in rural and urban environment. Dew samples were collected between May and October, 2009 in two reference stations in southern Poland: Cracow and Gaik-Brzezowa. The investigation included comparison of volume and chemistry of the collected samples. Due to its formation mechanisms, dew is a good indicator of air pollution. Following parameters were analyzed in 159 collected samples: pH,...
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Natural convection in symmetrically heated vertical channels
PublikacjaThe study describes natural convection through a vertical channel, open on four sides and bound by two isothermal walls. Both balancing and infrared experimental investigations were performed in air (Pr = 0.71) to estimate the impact of channel width s and wall-to-ambient temperature difference (tw - t∞) on natural convective heat transfer, the formation of air flow patterns and the rate of flow pattern formation. The study was...
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Oczekiwania stron konfliktu i mediatorów wobec e-mediacji. Czy e-mediacja ma przyszłość?
PublikacjaArtykuł prezentuje możliwości prowadzenia mediacji – skutecznej i korzystnej, ale rzadko wykorzystywanej w Polsce metody pozasądowego rozstrzygania sporów - z wykorzystaniem profesjonalnej platformy internetowej. Na podstawie badań przeprowadzonych na grupie mediatorów oraz stron konfliktów określono oczekiwania dotyczące prowadzenia e-mediacji i wyzwania, jakie stawia przed mediatorami mediacja on-line.