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Search results for: gc-ms technique
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Rain Gardens GC_MS analysis dataset
Open Research DataThis dataset contains the results of samples analysis (no-target analysis: scan mode) using gas chromatography coupled with mass spectrometry GC–MS (GC-2030 NEXIS MS, Shimadzu, Japan or Thermo Scientific, Waltham, USA).
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Multi-directional analysis of the maintenance of rainwater harvesting systems
Open Research DataPresented data are the result of research activity entitled „Multi-directional analysis of the maintenance of rainwater harvesting systems” conducted as a part of MINIATURA 7 competition. The research consisted of a comprehensive assessment of the quality of rainwater collected and stored in a rooftop harvesting system and then purified using inline...
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Investigation of the C-1311 glucuronidation: an electrochemical approach
Open Research DataThis study was undertaken to investigate the glucuronidation of the compound C-1311 (5-diethylaminoethylamino-8-hydroxyimidazoacridinone – the model anticancer acridine derivative) using electrochemistry/mass spectrometry (EC/MS) as a complementary technique to in vitro (liver microsomes) and in silico approaches.
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Rain Gardens LC_MS/MS analysis dataset
Open Research DataThis dataset contains the results of samples analysis (target analysis with certified reference materials) using ultra-high performance liquid chromatography tandem mass spectrometry (UHPLC-MS/MS, Shimadzu, Japan).
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The profiles and spectrum of aqua solution of tannic acid by HPLC-DAD-MS analysis.
Open Research DataThe profiling of tannic acid is determined by examining the content and proportion / ratio of gallotannins [Aras et al. 2016, Clifford et al. 2007, Gauri et al. 2012, Nishizawa et al. 1982]. In order to check the ion mass distribution (TIC) in an aqueous solution of commercial tannic acid, a direct sample injection (TA) was performed into the mass spectrometer....
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GC Chromatograms for isomerization of alpha-pinene
Open Research DataData contain results of the catalytic tests for the isomerization of alpha-pinene for the Ti3C2Tx MXenes produced via acidic etching aluminum from MAX Phase (Ti3C2-Al-Ti3C2-Al-Ti3C2) using different etching agents, HF/HCl and HF/H2SO4 with different weight ratios (1:3, 1:4, and 1:5). The samples were labeled as MXene HF/HCl X:Y and MXene HF/H2SO4 X:Y,...
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A novel method for drop in drop edible oils encapsulation with chitosan using a coaxial technique
Open Research DataThe dataset present a novel one step method for oil encapsulation. In this coaxial system the oil constitutes the core of the capsule, while the chitosan solution is the polymer shell surrounding the core to provide separation of the core from the external environment. In comparison to other encapsulation methods, the presented technique is much simpler...
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The topography of Bi2VO5.5 ceramics prepared by melt-quenching technique was measured with confocal microscope
Open Research DataThe topography of Bi2VO5.5 ceramics prepared by melt-quenching technique was measured by confocal microscope.
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Integrated circuit structure surface images obtained with contact capacitive imaging technique
Open Research DataThe measurements were done using NTEGRA Prima (NT-MDT) device. CSG 10Pt probe.
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Linear impedance of Bi2VO5.5 ceramic prepared by traditional melt quenching technique measured with impedance spectroscopy method at low temperature region
Open Research DataThe linear electrical properties of Bi2VO5.5 ceramic prepared by traditional melt quenching technique was measured by impedance spectroscopy method.
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Nonlinear impedance of Bi2VO5.5 ceramic prepared by traditional melt quenching technique was measured with impedance spectroscopy method at low temperature region
Open Research DataThe nonlinear electrical properties of Bi2VO5.5 ceramic prepared by traditional melt quenching technique was measured by impedance spectroscopy method.
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Nonlinear impedance of Bi2VO5.5 ceramic prepared by traditional melt quenching technique was measured with impedance spectroscopy method at high temperature region
Open Research DataThe nonlinear electrical properties of Bi2VO5.5 ceramic prepared by traditional melt quenching technique was measured by impedance spectroscopy method.
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Two-phase water-air flow measurement using gamma-ray absorption technique – plug flow
Open Research DataThe attached datasets contains the measurement results of the air-water flow in a horizontal pipeline. Flow type: plug flow. The data shows the pulse counts of the two radiometric sets. Each of these kits consisted of a QSA Global Am-241 gamma ray source and a Tesla SKG-1 type NaI(Tl) scintillation probe. The pulses were recorded using a dedicated EC...
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Two-phase water-air flow measurement using gamma-ray absorption technique – slug flow
Open Research DataThe attached datasets contains the measurement results of the air-water flow in a horizontal pipeline. Flow type: slug flow. The data shows the pulse counts of the two radiometric sets. Each of these kits consisted of a QSA Global Am-241 gamma ray source and a Tesla SKG-1 type NaI(Tl) scintillation probe. The pulses were recorded using a dedicated EC...
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Two-phase water-air flow measurement using gamma-ray absorption technique –bubble flow
Open Research DataThe attached datasets contains the measurement results of the air-water flow in a horizontal pipeline. Flow type: bubble flow. The data shows the pulse counts of the two radiometric sets. Each of these kits consisted of a QSA Global Am-241 gamma ray source and a Tesla SKG-1 type NaI(Tl) scintillation probe. The pulses were recorded using a dedicated...
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Two-phase water-air flow measurement using gamma-ray absorption technique – transitional plug – bubble flow
Open Research DataThe attached datasets contains the measurement results of the air-water flow in a horizontal pipeline. Flow type: transitional plug – bubble flow. The data shows the pulse counts of the two radiometric sets. Each of these kits consisted of a QSA Global Am-241 gamma ray source and a Tesla SKG-1 type NaI(Tl) scintillation probe. The pulses were recorded...
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Determination of sex hormone concentration in wastewater samples.
Open Research DataConcentration levels of five selected steroid hormones in influent and effluent waters from wastewater treatment plant were determined using SPE(C18)-HPLC-ESI/MS/MS method. Sex hormones like: estradiol, estriol, estrone, 17-α-ethynyloestradiol, progesterone were present in all influent wastwater samples.
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Analytical data on molecular umbrella: cispentacin and molecular umbrella: fluorescent probe conjugates
Open Research DataAnalytical data (NMR, MS, FTIR) for nine conjugates of molecular umbrella with cispentacin, Lys(Mca) or Nap-NH2. The conjugates have been rationally designed as potential antifungal agents. 1H NMR and 13C NMR spectra were obtained at 500 MHz Varian Unity Plus spectrometer and the deuterated solvents were used as internal locks. High-resolution mass...
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Ethylene decomposition on TiO2 under UV
Open Research DataData contain chromatograms recorded during decomposition of ethylene over TiO2 in a flow reactor under UV irradiation. Semilac UV lamp with total power of 72 W was used as a source of UV light. Chromatograms were recorded in Trace GC Ultra chromatograph equipped in FID detector. Sampling was realised via the dosing sample loop. TiO2 was coated on the...
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Ethylene decomposition on TiO2 - UV and Fluorescence lamp
Open Research DataData contain chromatograms recorded during decomposition of ethylene flowing over TiO2 through the quartz tubular shape reactor. TiO2 was coated onto glass plates with dimension of 2cmx2cm, in total 3 plates were used and placed inside reactor. Reactor was irradiated by UV (Special 'TL'E, Philips) or fluorescent (Lumilux, OSRAM) 3 ring-shaped lamps,...
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Simulation of the weight averaging of pulse frequency modulated sensor output signal
Open Research DataThe aim of the research is investigation of the efficiency of weight averaging of pulse frequency modulated signal. It was shown that from the point of view of the reduction of the sampling error the best are polynomial weighing functions, for which the maximum of this component error decreases proportionally to the appropriate power of the number of...
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Assay of Cystathionine-γ-synthase (CaStr2p) activity determination.
Open Research DataThe study aimed to obtain conditions optimal for the activity of Candida albicans cystathionine-γ-synthase (CaStr2p) determination. The selection of appropriate reaction conditions included the identification of the reaction buffer and its pH, substrate, and enzyme concentrations. The activity of Str2p was measured by the detection of decrease of the...
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Activity assay of O-Acetyl-L-homoserine sulfhydrylase (CaMet15p).
Open Research DataThe study aimed to obtain conditions optimal for the activity of O-acetyl-L-homoserine sulfhydrylase (CaMet15p) and a method suitable for its measurement. The selection of appropriate reaction conditions included the identification of the reaction buffer and its pH, substrate and enzyme concentrations. The activity of CaMet15p was measured by the detection...
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The results of the nitrogen adsorption/desorption measurements of CPMD and CPMH
Open Research DataThe results of the nitrogen adsorption/desorption measurements of CPMD and CPMH. The adsorption/desorption isothermswere carried out at 77 K using a Quantachrome Autosorb-1C-MS instrument. Sample abbreviations (CPMD, CPMH) are in agreement with the markings used in the linked publication.
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Experimental investigation of the weight averaging of pulse frequency modulated sensor output signal
Open Research DataThe research aims to practically verify the results of theoretical analysis and simulations of the efficiency of weight averaging of pulse frequency modulated signal. For this purpose, a suitable test stand was built, and the control software in the LabVIEW environment was prepared. Then, a series of experiments were carried out to process and analyze...
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The photocatalytic activity of MoS2 electrodes under sunlight illumination
Open Research DataThis dataset contains the results of the photocatalytic activities of the MoS2 and MoS2 modified by SnO2 were assessed through the photocatalytic reduction of Cr6+ under the sunlight illumination. In the experiment, 20 mg of the catalyst was distributed in the K2Cr2O7 aqueous solution (50 mL, 100 mg•L-1). The mixed solution was stirred for 30 min to...
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Auditory Brainstem Responses recorded employing Audio ABR device
Open Research DataThe dataset consists of ABR measurements employing click, burst and speech stimuli. Parameters of the particular stimuli were as follows:
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Total electrical conductivity data of (Cr,Fe,Mn,Co,Ni)3O4 High-entropy spinel oxide thin films deposited on amorphous SiO2 substrate by spray pyrolysis techniqe
Open Research DataThis dataset includes electrical conductivity measurements results measured by van der pauw technique up to 900oC.
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Non-enzymatic glutathione-mediated conjugation of unsymmetrical bisacridine C-2028 with anticancer activity
Open Research DataThe presented data complement the studies on the interplay between C-2028 (anticancer-active unsymmetrical bisacridine) and the glutathione S-transferase/glutathione (GST/GSH) system.
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Topographic AFM imaging of the leaf surface with magnification of details of its morphological structure
Open Research DataTopographic imaging of the leaf surface with magnification of details of its morphological structure. Measurements in semi-contact mode. NTEGRA Prima (NT-MDT) device. NSG 01 probe.
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XRD data of (Cr,Fe,Mn,Co,Ni)3O4 High-entropy spinel oxide thin films deposited on amorphous SiO2 substrate by spray pyrolysis techniqe, annealed in a range from 400 to 900oC
Open Research DataDataset include collected XRD data of (Cr,Fe,Mn,Co,Ni)3O4 high-entropy spinel oxide thin films deposited by spray pyrolysis technique on amorphous SiO2 substrates and annealed from 400 to 900oC. Samples were prepared in the form of a ~ 500 nm thin film utilising a facile spray pyrolysis technique. The structural and electrical properties of the layers...
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A Fortran-95 algorithm to solve the three-dimensional Higgs boson equation in the de Sitter space-time
Open Research DataA numerically efficient finite-difference technique for the solution of a fractional extension of the Higgs boson equation in the de Sitter space-time is designed. The model under investigation is a multidimensional equation with Riesz fractional derivatives of orders in (0,1)U(1,2], which considers a generalized potential and a time-dependent diffusion...
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The morphology of vanadate glass-ceramics containing BaTiO3 measured with the use of AFM
Open Research DataThe structure of vanadate glass-ceramics doped with BaTiO3 was measured by AFM technique. Samples of the composition of x[BaO,TiO2]–(80 − x)V2O5–20Bi2O3 where x = 5, 10 and 15 in mol% were prepared by a conventional melt quenching technique. The melting was performed in alumina crucibles at the temperature of 1273 K–1373 K. The melts were poured on...
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Analysis of the electrical parameters of the LTO thin films
Open Research DataLithium titanate thin films were derived by sol-gel technique. Films with thickness ca. 800 nm were annealed for various time, in a range of 10h-80h at 550 deg. Electrical conductivity in a wide range of temperature was measured.
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Glutathione conjugation of the antitumor-active 1-nitroacridine derivatives compounds C-857 and C-1748 – the major role of glutathione S-transferase M1-1
Open Research DataObjectives: C-857 and C-1748 are antitumor-active agents, monomers of unsymmetrical bisacridine derivatives. The aim of this study was to analyze their glutathione (GSH) conjugation in vitro in the presence of glutathione S-transferase (GST) M1-1.
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Dataset for systematic literature review about phosphorus magnetic resonance spectroscopy (31 P MRS).
Open Research DataThe file contains the publications retrived for systematic literature review from sleceted databases: Web of Science Core Collection, Scopus, Chochrane Library, and Pubmed. Records were identified by using nesting technique. Our search log stated as follow: "phosphorus" AND ("mri spectroscopy" OR "31P MRS").
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Pore size distribution of PC-X (porous carbon materials obtained at various temperatures)
Open Research DataThese data contain pore size distribution of PC-700 (porous carbon materials obtained at 700°C), PC-800 (porous carbon materials obtained at 800°C) and PC-900 (porous carbon materials obtained at 900°C) analyzed by the nitrogen adsorption/desorption technique.
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Depth XPS profile of vanadium pentoxide
Open Research DataVanadium pentoxide sample was manufactured by sol-gel method and deposited on a substrate by spin coating technique. To determine depth profile of chemical composition of thin film, etching by Argon ion gun was used. Thin film was etched three times. Chemical composition was measured by XPS method.
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Impedance spectroscopy of the lithium titanate doped by copper thin films
Open Research DataLithium titanate doped by copper thin films were derived by sol-gel method. Prepared gel was deposited by spin-coating technique. Samples with various content of Cu were measured by impedance spectroscopy method in a wide range of temperature, from -120 up to 150 deg.
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The Scanning Electron Microscopy images of three arthropods
Open Research DataThe dataset contains micrographs of various arthropods made with the Scanning Electron Microscopy (SEM) technique. The images were done during the laboratory with students from the Faculty of Chemistry. Among the studied species, there is a fruit fly (lat.Drosophila melanogaster), a spider (most likely Sibianor aurocinctus), and a weevil insect (Curculionoidea).
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SEM/EDX data of (Cr,Fe,Mn,Co,Ni)3O4 High-entropy spinel oxide thin films deposited on amorphous SiO2 substrate by spray pyrolysis techniqe
Open Research DataThis Data set include SEM and EDX results of (Mn,Co,Fe,Ni,Cr)3O4 high-entropy spinel oxide prepared in the form of a ~ 500 nm thin film utilising a facile spray pyrolysis technique. The structural and electrical properties of the layers were characterised after exposure to temperatures in the range of 400–900 ◦C. The as-deposited layers were amorphous,...
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TEM data of (Cr,Fe,Mn,Co,Ni)3O4 High-entropy spinel oxide thin films deposited on amorphous SiO2 substrate by spray pyrolysis techniqe
Open Research DataThis Dataset include presentation of summarized TEM investigation of (Mn,Co,Fe,Ni,Cr)3O4 high-entropy spinel oxide prepared in the form of a ~ 500 nm thin film utilising a facile spray pyrolysis technique. The structural and electrical properties of the layers were characterised after exposure to temperatures in the range of 400–900 ◦C. The as-deposited...
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Thermal behaviour of vanadium xerogel powder under oxidizing atmosphere
Open Research DataThe DataSet contains the results of the thermal behavior of the vanadium xerogel powder. The information about xerogel powder synthesis is described in the Journal of Nanomaterials.
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Thermal behaviour of vanadium xerogel powder under argon atmosphere
Open Research DataThe DataSet contains the results of the thermal behavior of the vanadium xerogel powder. The information about xerogel powder synthesis is described in the Journal of Nanomaterials.
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Thermal behavior of (NH4)V4O10xH2O
Open Research DataThe DataSet contains the results of the thermal behavior of the (NH4)V4O10xH2O obtained by the hydrothermal method using different precursors: microstructured (commercially available) or nanostructured. The information about samples synthesis is described in the Materials.
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Mechanical lithography in a polymer substrate using AFM in contact mode
Open Research DataMechanical lithography in a polymer substrate. Contact mode. NTEGRA Prima (NT-MDT) device. NSG 01 probe.
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Structural and luminescence properties of B2O3-Bi2O3+10AlF3 glasses doped with Eu3+/Dy3+ ions
Open Research DataThe attached data contains the results of measurements of B2O3-Bi2O3 and B2O3-Bi2O3+10AlF3 glasses doped with Eu3+ and Dy3+ ions in different molar ratios. Glasses were synthesized by the melt quenching technique. On their basis, the structural, optical, and luminescence properties of synthesized samples were characterized. The dataset includes XRD,...
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The structure of vanadate glasses containing BaTiO3.
Open Research DataThe structure of vanadate glasses doped with BaTiO3 was measured by SEM technique. Samples of the composition of x[BaO,TiO2]–(80 − x)V2O5–20Bi2O3 where x = 5, 10 and 15 in mol% were prepared by a conventional melt quenching technique. The melting was performed in alumina crucibles at the temperature of 1273 K–1373 K. The melts were poured on a preheated...
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XPS analysis of TBBO glass
Open Research DataGlasses and glass-ceramics with nominal composition 73 TeO2– 4BaO– 3Bi2O3–18SrF2-2RE2O3 (where RE = Eu, Dy) have been synthesized by conventional melt-quenching technique and subsequent heat treatment at 370 °C for 24 h in air atmosphere. Various Eu3+ to Dy3+ molar ratio have been applied to investigate luminescence properties in both glass and glass-ceramic...
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Mercury intrusion porosimetry (MIP) results of cement pastes containing Bi2O3/Gd2O3 and silica-coated Bi2O3/Gd2O3 structures
Open Research DataMercury intrusion porosimetry (MIP) data - curves of cement pastes containing Bi2O3/Gd2O3 and silica-coated Bi2O3/Gd2O3 structures