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Search results for: BASIC LABORATORY STUDIES
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A strong preference for the TA/TA dinucleotide step discovered for an acridine-based, potent antitumor dsDNA intercalator, C-1305: NMR-driven structural and sequence-specificity studies
PublicationTriazoloacridinone C-1305, a potent antitumor agent recommended for Phase I clinical trials, exhibits high activity towards a wide range of experimental colon carcinomas, in many cases associated with complete tumor regression. C-1305 is a well-established dsDNA intercalator, yet no information on its mode of binding into DNA is available to date. Herein, we present the NMR-driven and MD-refined reconstruction of the 3D structures...
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Adsorption behavior and corrosion inhibitive characteristics of newly synthesized cyano-benzylidene xanthenes on copper/sodium hydroxide interface: Electrochemical, X-ray photoelectron spectroscopy and theoretical studies
PublicationElegant process for synthesis of 3-(7H-dibenzo[c,h]xanthen-7-yl)benzaldehyde (3), as new starting material to create a set of novel xanthene analogues, 2-(3-(7H-dibenzo[c,h]xanthen-7-yl)benzylidene)malononitrile (4), 3-(3-(7H-dibenzo[c,h]xanthen-7-yl)phenyl)-2-cyanoacrylic acid (5), and Ethyl-3-(3-(7H-dibenzo[c,h]xanthen-7-yl)phenyl)-2-cyanoacrylate (6), was achieved starting with available materials under mild conditions. Various...
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π-Indenyl substituted zirconium compounds containing terminal bondedphosphanylphosphido ligands [Ind2Zr(Cl){(Me3Si)P-PR2-jP1}]. Synthesis,X-ray analysis and NMR studies
PublicationPraca prezentuję reakcję kompleksów indenylowych cyrkonu z solami litowymi difosfanów o ogólnym wzorze R2P-P(SiMe3)Li, gdzie R = tBu, Et2N, iPr2N. W wyniku tych reakcji otrzymano 3 nowe kompleksy fosfanylofosfidowe.Otrzymane nowe kompleksy zbadano przy pomocy technik rentgenowskiej analizy strukturalnej i NMR.Dichloro-bis(indenyl)zirconium(IV) reacts with lithium derivatives of diphosphanes R2P-P(SiMe3)Li (R = tBu, Et2N, iPr2N)...
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Application of IR UWB Spectrum Shaping to IEEE 802.15.4a Standard
PublicationCoexistence of existing narrowband systems and new ultra wideband devices in the same frequency range requires using some interference mitigation techniques, for example based on spectrum shaping. This paper presents efficiency of impulse radio spectrum shaping methods, applied to IEEE 802.15.4a UWB alternate physical layer signals. Basic parameters of 802.15.4a signal structure and outline of proposed spectrum shaping methods...
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Modelling of heat and mass transfer through wooden buildings
PublicationThe aim of this review paper is to examine the most recent available studies dealing with theoretical, numerical and experimental aspects related to modelling of heat and mass transfer through wooden buildings. The main thermophysical, mechanical and hygrometric properties of wood are firstly discussed. Then, the basic governing equations of heat and mass transfer phenomena are presented. A detailed description of the physical...
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Case study 1.2C: Road infrastructure cost in Poland, Annex to Deliverable D3, Marginal cost case studies for road and rail transport. GRACE. Funded by Sixth Framework Programme.
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Conformational Studies of [11è12(CN4)]ScyII and [15è16(CN4)]ScyII? Two Scyliorhinin II Analogues by means of 2D NMR Spectroscopy and Theoretical Methods
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π-Indenyl substituted zirconium compounds containing terminal bonded phosphanylphosphido ligands [Ind2Zr(Cl){(Me3Si)P–PR2-κP1}]. Synthesis, X-ray analysis and NMR studies
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Lower rim substituted p-tert-Butylcalix[4]arenes: Part XI. New ester derivatives of calix[4]arene, their ionophoric properties and x-ray structure studies
PublicationPrzedstawiono syntezę 6-ciu nowych estrowych pochodnych kaliks[4]arenuw konformacji stożkowej. Pierwsze badania kompleksowania jonów metali przeprowadzone w membranach elektrod jonoselektywnych (ISE) potwierdziły kompleksowanie jonów sodu w sposób selektywny. Zaprezentowano strukturę rentgenowską monokryształów związku 6.
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New “one‐pot” Pd(II) and Zn(II) complexes of Schiff bases, derivatives of 1‐amino‐1‐deoxy‐d‐sorbitol: Spectroscopic studies and biological and catalytic activities
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Comparative genomics, pangenomics, and phenomic studies of Pectobacterium betavasculorum strains isolated from sugar beet, potato, sunflower, and artichoke: insights into pathogenicity, virulence determinants, and adaptation to the host plant
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Characteristics of the grey seal (Halichoerus grypus) diet in the Vistula River mouth (Mewia Łacha Nature Reserve, southern Baltic Sea), based on the osteological and molecular studies of scat samples
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Lower rim substituted tert-Butylcalix[4]arenes. Part 13. Interaction of calix-hydroxamates with Fe(III) and Pb(II); studies in ion-selective membrane electrodes (ISE)
PublicationPrzedmiotem pracy są badania oddziaływań pomiędzy trzema wybranymi hydroksamowymi pochodnymi t-butylo-kaliks[4]arenu i jonami metali z wykorzystaniem membranowych elektrod jonoselektywnych (ISE). Elektrody zawierające jako materiał aktywny wymienione związki jonoforowe charakteryzują się nernstowskim nachyleniem i szerokim zakresem liniowości na jony Pb(II), a także dobrą selektywnością na jony Pb(II)w stosunku do jonów UO2(II),...
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OSC - domain oriented ontology creation system
PublicationOntologies are, as part of semantic web, a basic component to enrich content available in the Internet with a meaning understandable for computers. In this publication an architecture and functionality of a domain oriented web portal for collaborative creation and storage of ontologies is presented. The system is being created by Gdańsk University of Technology Electronics, Telecommunications and Informatics faculty's Department...
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Chemical analysis of low carbon content coals and their applications as dye adsorbent
PublicationCoal is primarily a fuel material but lately it has been utilized as an adsorbent for removing toxic metal ions. However, its usage for removing organic pollutants is not well studied. We report here a systematic study on the use of coal samples of varying carbon contents as adsorbents for removing Basic Blue 41 as a model cationic dye. The coal samples were collected from coal mines and were thoroughly characterized. The concentrations...
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A comparative analysis of the effectiveness of corporate bankruptcy prediction models based on financial ratios: Evidence from Colombia, 2008 to 2015
PublicationLogit and discriminant analyses have been used for corporate bankruptcy prediction in several studies since the last century. In recent years there have been dozens of studies comparing the several models available, including the ones mentioned above and also probit, artificial neural networks, support vector machines, among others. For the first time for Colombia, this paper presents a comparative analysis of the effectiveness...
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Analysing selection of low-temperature medium for cogeneration micro power plant
PublicationThe article analyses the ORC system working with dry and wet low-boiling media which are most frequently used in installations of this type. Two types of cycles were examined, which were the cycle with heat regeneration for dry media: fc72, hfe7100, R227ea, R245fa, R423a and R600a, and the cycle without heat regeneration for wet media: R11, R12, R134a, R718 and 507a. The calculations were performed for the assumed required thermal...
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Enhanced method of DS-CDMA low level singnals detection
PublicationThe following article comprises three main parts. The first one generally describes two methods of low level signals detection which are in the interest of this study. The signal spectrum averaging technique is shown as well as the method exploiting averaged spectrum of the signal raised to the power of 2n (nN). Additionally, this section briefly presents proposed enhancements and modifications of these two solutions, which allow...
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Tests of bond between concrete and steel bars – literature background and program of own research
PublicationThis article deals with the issue of the bond between concrete and reinforcement. The bond is crucial for reinforced concrete elements because it is possible to transfer forces (stresses) from concrete to the reinforcement. Basic information related to the cooperation of concrete and rebars was recalled in the article. Selected issues concerning theoretical and numerical analysis as well as experiments of the bond phenomenon were...
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Effect of GIS parameters on modelling runoff from river basin. The case study of catchment in the Puck District
PublicationThe study was preceded to check the impact of the adopted digital elevation model resolution on the determination of catchment parameters and the further influence of the received information on calculations related to the hydrograph at the closing point of the basin after a synthetic 100-year precipitation episode. The study area are river basins located in the Puck commune convoying water directly to the Puck Bay. These studies...
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The silver layers in fiber-optic sensors
PublicationIn this paper a method of application of the silver layers on the surface of an optical fiber was proposed. The optical properties and surface quality of the silver layer was examined by optical microscopy. The reflection and transmission of the sample were investigated. To evaluate the silver mirror it was placed in a fiber optic Fabry-Perot interferometer and the quality of the spectra was analyzed. The commercial mirror was...
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Selected problems of sensitivity and reliability of a jack-up platform
PublicationThe paper deals with sensitivity and reliability applications to numerical studies of an off-shore platform model. Structural parameters and sea conditions are referred to the Baltic jack-up drilling platform. The study aims at the influence of particular basic variables on static and dynamic response as well as the probability of failure due to water waves and wind loads. The paper presents the sensitivity approach to a generalized...
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USE OF LANGMUIR PROBE IN DIESEL ENGINE DIAGNOSTIC RESEARCH Part I MEASUREMENT TECHNOLOGY. - Part 1 : MEASUREMENT TECHNOLOGY
PublicationIn the paper, the basic assumptions of diesel engine cylinder system's diagnosing method, based on observation of emerging and moving electric charges of ionized gas in the combustion workspaces, using Langmuir's probe. In the first part of the paper, only the technology of the measurement and results of the preliminary diagnostic tests of laboratory engine Farymann Diesel D10 were presented. The primary purpose of the research...
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3D scanning system for railway current collector contact strips
PublicationUndisturbed collection of current from a contact wire of the catenary constitutes one of the basic elements in reliable operation of electrified rail transport, particularly when vehicles move at high speed. Quality of current collection is influenced by the construction of catenary and current collectors, as well as by the technical condition and regulation of these two elements. Total contact force of a current collector head...
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2015. Motion analysis of a kitesurfer employing a vision-based measurement system
PublicationAbstract. Kitesurfing is a relatively new phenomenon with rising popularity worldwide – a recently developed extreme watersport considered a high-risk injury sport. It combines elements of several other sports, in particular, sailing, surfing, windsurfing, wakeboarding, and snowboarding. The main purpose of authors’ research in the present paper is to use a vision-based system for measuring a kitesurfer’s body movements in order...
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Rosyjskie piśmiennictwo naukowe z zakresu przekładoznawstwa. Rzecz o monografii bibliograficznej Ewy Konefał pt. Przekładoznawstwo rosyjskie. Tom 1: Autoreferaty dysertacji 1937–2015 (Wydawnictwo Uniwersytetu Gdańskiego, Gdańsk 2016) [Russian academic literature in the field of translation studies. About Eva Konefał’s bibliographic monograph Russian translation studies. Volume 1: Abstracts of dissertations 1937-2015 (Publishing house of Gdansk University, Gdansk 2016)]
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Method of selective fading as a educational tool to study the behaviour of prestressed concrete elements under excess loading
PublicationPrestressed structures are a key to realization of the boldest architectural ideas, characteristic feature of prestressed structure is better use of concrete material properties by insertion of internal forces. Learning about pre-stressed reinforced concrete structures is an integral part of Graduate Studies Program in construction engineering. Know-how of geometry change patterns in prestressed concrete elements under certain...
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Effect of wet Hydrogen Sulfide on Carbon Steels Degradation in Refinery Based on Case Study
PublicationMaterial degradation caused by wet hydrogen sulfide (Wet H2S) is one of the major issues in refineries. Carbon steel is the main construction material used in refineries and is subjected not only to thickness loss but the hydrogen is the major concern. H2S leads to high atomic hydrogen penetration in steel which causes degradation in the form of blistering and/or cracking (HIC/SOHIC) and stress cracking in the area of welds and...
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Comparative analysis of three‐phase dual active bridge converter with different transformer topology and modern universal control for DC microgrids
PublicationThe presented work discusses issues related to the use of modern multiphase topologies of Dual Active Bridge (DAB)-type converters. Converters of this type are widely used in most DC microgrid applications. The introduction emphasizes a comparative analysis between single-phase and multi-phase DAB topologies within high-power DC microgrids, delving into their respective advantages, drawbacks, design procedures, and considerations...
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Rapid development of custom web application with ruby on rails framework on the example of group project system
PublicationTechnology industry labor market requires engineers with a good preparation for work with project's tasks and team cooperation skills. One of the way for achieve that abilities during technical university education are students group projects. Running of group projects at university brings new challenges, from recruitment of students with required skills for par-ticular project, to lack of industrial procedures and ready to use...
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Influence of a lipid bilayer on the conformational behavior of amphotericin B derivatives - A molecular dynamics study.
PublicationAmphotericin B (AmB) is an effective but very toxic antifungal antibiotic. In our laboratory a series of AmB derivatives of improved selectivity of action was synthesized and tested. To understand molecular basis of this improvement, comparative conformational studies of amphotericin B and its two more selectivederivatives were carried out in an aqueous solution and in a lipid membrane. These molecular simulation studies revealed...
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Laser stimulated third harmonic generation studies in ZnO–Ta 2 O 5 –B 2 O 3 glass ceramics entrenched with Zn 3 Ta 2 O 8 crystal phases
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Marta Rusnak, Marta Szmigiel, Malwina Geniusz, Zofia Koszewicz, Monika Magdziak-Tokłowicz, Exploring the impact of cultural context on eye-tracking studies of architectural monuments in selected European cities: Sustainable heritage management.
PublicationSustainable management of architectural heritage requires conducting an inclusive diagnosis of users' opinions, considering both residents and tourists as the recipients of urban space. Given the cultural diversity within these groups, proposing the use of eye-trackers (ET) as an alternative to traditional public consultation prompts the need to assess the method's advantages and disadvantages. It remains uncertain whether individuals...
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Studies on the treatment of lipid-rich wastewater and on the influence of soluble microbial products on activity of microorganisms.Studia nad obróbką ścieków bogatych w tłuszcze(lipidy) i oddziaływanie ubocznych produktów mikroorganizmów na ich aktywność.
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In search of a new relationship between nature and society
PublicationWe live in an era of breakthrough- not only in the literal sense of the word, but the breakthrough of the century or the millennium. New discoveries and the crisis present in the economy, society, religion and ecology forces a review of all universally accepted theories. Nature, ecology and environment are the key words used in every area of human activity. It has led to the development of a new scientific field- the philosophy...
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Hybrid stepless distribution transformer with four-quadrant AC/DC/AC converter at low voltage side - simulation tests
PublicationThe article presents the work of the stepless hybrid distribution transformer (HT), as an alternative to the so far applied Automatic Voltage Regulator (AVR) solutions, used to control the voltage in the power system in terms of the fundamental harmonic. The HT is a combination of a conventional distribution transformer and an AC/DC/AC converter connected in series with the transformers secondary winding. In the work the basic...
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Effect of underwater wet welding conditions on the diffusible hydrogen content in deposited metal
PublicationIn the study mercury displacement method was used for determination of diffusible hydrogen amount in deposited metal obtained during underwater wet welding with covered electrodes in laboratory conditions according to a two-level full factorial design for three factors. The factors and their levels were chosen among conditions and parameters of welding in accordance with the results of own preliminary studies. A statistical analysis...
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Compatibility of Crude Oil Blends─Processing Issues Related to Asphaltene Precipitation, Methods of Instability Prediction─A Review
PublicationProcessing crude oil of variable composition, especially due to the need to process crude oil blends obtained from various sources, presents a tremendous process challenge. This is mainly due to the destabilization of the colloidal system manifested mostly by the precipitation of the asphaltene fraction. The precipitation of asphaltenes from crude oil is a serious problem during extraction, transport, and processing. In the latter...
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Standard Compliance Framework for effective requirements communication
PublicationStandard Compliance Framework (SCF) is a framework, which supports application of standards at the stages of achieving, assessing and maintaining the compliance. It uses Trust Case language to develop argument structures demonstrating compliance with standards. The paper presents how SCF is applied to increase effectiveness of requirements communication. Relevant mechanisms of the framework are thoroughly described referring to...
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Studies on solid phase microextraction-gas chromatographic determination of volatile chloroorganic pollutants in soil. badanie lotnych związków chloroorganicznych w glebie przy użyciu techniki mikroekstrakcji do fazy stacjonarnej i chromatografii gazowej.
PublicationLotne związki chloroorganiczne (VOXs) mogą być obecne w powietrzu, wodzie i glebie. Związki te mają właściwości kancerogenne, dlatego też ich ilość w środowisku powinna być monitorowana. W pracy przedstawiono badania nad możliwością zastosowania techniki izolacji i wzbogacania jaką jest mikroekstrakcja do fazy stacjonarnej, jej przydatność w analizie lotnych węglowodorów chloroorganicznych w różnych typach gleb z wykorzystaniem...
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Soil and groundwater contamination as a result of sewage sludge land application
PublicationThe leaching of chemical compounds (N-NO3, N-NH4, Norg, P-PO4, Ptot) and trace elements (Cd, Cu, Cr, Ni, Zn, and Pb) from sewage sludge and their migration through the soil profile was the subject of the study. The column experiments were carried out under atmospheric conditions corresponding to naturally occurring storm events - sewage sludge amended soil was irrigated with high rates of water. The column filter media used in...
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Adhesion of organic coatings to hot-dip galvanized steel
PublicationDuplex systems provide long-time corrosion protection, much longer than the sum of the lifetimes of zinc and paint used individually. However loss of adhesion between coating and zinc substrate is often found in practice. Different methods of zinc surface preparations are used in the fi eld. The aim of this study was to examine and compare coating protection when the old zinc surface, stored during long-time period (15 years) in...
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Design analysis of combined gas-vapour micro power plant with 30 kW air turbine
PublicationThe article presents basic results of the design analysis of a combined gas-vapour micro power plant with a waste-heat boiler without exhaust reheat, working in the vapour section in the Organic Rankine Cycle (ORC) system. The analysis concerned working media most frequently used in those types of power plants and planned to be used in future. The object of the analysis was a micro power plant with a 30 kW gas (air) turbine for...
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Light pollution from illuminated bridges as a potential barrier for migrating fish–Linking measurements with a proposal for a conceptual model
PublicationIlluminated bridges have become important assets to navigable aquatic systems. However, if artificial light at night (ALAN) from illuminated bridges reaches aquatic habitats, such as rivers, it can threaten the river's natural heterogeneity and alter the behavioural responses of migratory fish. Here, via a pilot study, we quantified levels of ALAN at illuminated bridges that cross a river and, propose a conceptual model to estimate...
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Identification of sustainable trypsin active‐site inhibitors from Nigrospora sphaerica strain AVA‐1
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Extraction and optimization of Penicillium sclerotiorum strain AK‐1 pigment for fabric dyeing
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The concept of a new two-stage fuse for high power pulse forming
PublicationThis manuscript introduces the concept, physical operating principle and studies on a new and unique two stage forming fuse (TSFF) with interstage spark gap commutation and presents its application for forming high power pulses of extreme parameters. The paper classifies TSFF performance and compares it with conventional single-stage forming fuses. The conclusions are supported by analytical and experimental studies in laboratory...
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Prototype of an opto-capacitive probe for non-invasive sensing cerebrospinal fluid circulation
PublicationIn brain studies, the function of the cerebrospinal fluid (CSF) awakes growing interest, particularly related to studies of the glymphatic system in the brain, which is connected with the complex system of lymphatic vessels responsible for cleaning the tissues. The CSF is a clear, colourless liquid including water (H2O) approximately with a concentration of 99 %. In addition, it contains electrolytes, amino acids, glucose, and...
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Signals Features Extraction in Radioisotope Liquid-Gas Flow Measurements using Autocorrelation Function
PublicationKnowledge of the two-phase flow structure is essential for the proper conduct of industrial processes. Description of liquid-gas flow regimes is possible by using of data analysis in time, frequency, or state-space domain. In this research studies, the autocorrelation function is applied for analysis of signals obtained for liquid-gas flow by use gamma-ray absorption. The experiments were carried out on the laboratory hydraulic...
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Interrelated shape memory and Payne effect in polyurethane/graphene oxide nanocomposites
PublicationWe report the fabrication of graphene oxide (GO) based polyurethane (PU) nanocomposites by a simple method of mixing and their shape memory properties at different temperatures. Both the polymer and the filler were synthesized in the laboratory by simple and easy methods – PU by pre-polymer method and GO by improved graphene oxide synthesis method. High molecular level dispersion of GO platelets within the PU matrix and thus good...