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Search results for: LIQUID CRYSTAL THERMOGRAPHY
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Modeling of Passive and Forced Convection Heat Transfer in Channels with Rib Turbulators
PublicationThe main goal of the research presented in this paper was the experimental and numerical analysis of heat enhancement and aerodynamic phenomena during air flow in a channel equipped with flow turbulators in the form of properly configured ribs. The use of ribs intensifies the heat transfer and at the same time increases not only the flow resistance but also the energy costs. Therefore, designing modern heat exchangers with optimal...
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10-Methyl- and 9,10-dimethyl acridinium methyl sulfate
PublicationThe title compounds, C(14)H(12)N(+).CH(3)O(4)S(-), (I), and C(15)H(14)N(+).CH(3)O(4)S(-), (II), respectively, crystallize with the planar 10-methylacridinium or 9,10-dimethylacridinium cations arranged in layers, parallel to the twofold axis in (I) and perpendicular to the 2(1) axis in (II). Adjacent cations in both compounds are packed in a 'head-to-tail' manner. The methyl sulfate anion only exhibits planar symmetry in (II)....
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The luminescence study of Ga2–x(Al0.68In0.32)xO3:Cr3+ coumpounds.
Open Research DataNear-infrared (NIR) phosphor-converted light-emitting diodes (pc-LEDs) are a highly efficient perspective NIR light source, with application hindered by a narrow emission band. In this work, we broaden the emission of a new series of NIR phosphors by controlling crystal structure disorder through cation cosubstitution. By substituting Ga3+ with (Al0.68In0.32)3+,...
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A new diagnostic IR-thermal imaging method for evaluation of cardiosurgery procedures
PublicationTwo methods for monitoring the state of the myocardium during cardiosurgical interventions based on thermal IR imaging are presented below. These methods, called static thermography and active dynamic thermography (ADT), use information about the distribution of temperature on the surface, and an external excitation source to induce thermal transient processes in a tested object. Recording the time series of thermograms allows...
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IR-THERMAL IMAGING IN CARDIOSURGERY
PublicationA method for monitoring the state of the myocardium during cardiosurgical interventions based on thermal IR imaging is presented. These methods called Static Thermography and Active Dynamic Thermography (ADT) uses information about distribution of temperature on the surface and an external excitation source to induce thermal transient processes in a tested object. Recording time series of thermograms allows to calculate parametric...
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Diagnostics of thermal processes in antenna systems of broadcast stations
PublicationDiagnostics is an important element associated with the operation of a radio antenna systems, allowing earlier detection of potential damage. Thermography is one of the diagnostic tools, which allows for non-invasive assessment of technical condition. It brings together both financial savings associated with the removal of the damage and the potential effects caused by it. The article presents an example of using a thermal imaging...
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Nutrient recovery from deammonification effluent in a pilot study using two-step reject water treatment technology
PublicationThe aim of this study was to assess the possibility of phosphorus and nitrogen recovery from the liquid fraction of digestates (reject water) pilot study using a two-step technology, where the precipitation of biogenic compounds in the form of magnesium ammonium phosphate (struvite) will be preceded by a deammonification process. The tests confirmed the possibility of nutrient recovery from deammonification effluent. A removal...
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Photoluminescence spectra of TiO2
Open Research DataThese data contain photoluminescence spectra of TiO2 measured at the temperature of liquid nitrogen. There is a comparison of the photoluminescence spectra of TiO2 heat treated at 400-600oC in the ambient (Ar) and reduced (H2) atmospheres. These emission spectra were recorded after TiO2 excitation with a wavelength of 290 nm
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In-situ generation of Ag, Cd, Hg, In, Pb, Tl and Zn volatile species by flowing liquid anode atmospheric pressure glow discharge operated in gaseous jet mode – Evaluation of excitation processes and analytical performance
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Dariusz Mikielewicz prof. dr hab. inż.
PeopleProfessor Dariusz Mikielewicz – born on February 6, 1967. in Gdansk. Here in 1974 he enrolled first to the Elementary School No. 17, and then in the Grammar School No. 5, named after Stefan Żeromski in Gdansk-Oliwa. After graduating from the Secondary School, with honors, in 1985 he successfully passed the entrance exams to the Faculty of Mechanical Engineering of Technical University of Gdansk, where he graduated with a very good...
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Kinetics of hexane and cyclohexane biodegradation using Candida subhashii in mineral salt medium in the presence of DES solution
Open Research DataDataset presents results of investigations on kinetics of biodegradation of hexane and cyclohexane in Candida subhashii.
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Structure redetermination, transport and thermal properties of the YNi3Al9 compound
PublicationSingle crystals of completely ordered variant of the YNi3Al9 compound were grown by self-flux method with excess of aluminum. The crystal structure of the title compound was redetermined from single crystal X-ray diffraction data. The structure adopts ErNi3Al9 type, space group R32, parameters of the unit cell a = 7.2838(2) Å, c = 27.4004(8) Å. The growth of relatively large single crystals of the YNi3Al9 compound, having completely...
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Interactions of selected mono- and disaccharides with precipitated calcium carbonate particles
PublicationCalcium carbonate is a widespread compound in nature and it can be produced by living organisms in the biomineralization process. Calcite, aragonite and vaterite are anhydrous polymorphic forms of calcium carbonate, wherein the calcite is the most thermodynamically stable. Vaterite is the metastable crystalline phase, which can be a precursor of calcite and aragonite, because it can easily transformed by dissolution and re crystallization...
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Hydrogen and chalcogen bonds in crystals of chalcogenadiazolecarboxylic acids – competition or cooperation?
PublicationThis article presents crystal structures of chalcogenadiazolecarboxylic acids bearing both a hydrogen and a chalcogen bond donor. The selected molecules varied in the size of the aromatic unit, the chalcogen atom and/or the position of the carboxyl group in the core structure. The most common synthons in their lattice are "R" _"2" ^"2" (8) self-complementary acid dimers or four-membered [Ch···N]2 rings. Supramolecular synthons...
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Analysis of explosion hazard on propane-butane liquid gas distribution stations during self tankage of vehicles Analiza zagrożeń wystąpienia wybuchu dla stacji dystrybucji gazu płynnego propan-butan podczas samodzielnego napełniania pojazdów
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On the Mechanism of Electrochemical Oscilations in Three-Phase System Containing Nitrobenzene with Picric Acid as Liquid Membrane.O mechaniźmie oscylacji róznicy potencjału elektorchemicznego w trójfazowych układach zawierających nitrobenzen z kwasem pikrynowym jako membraną ciekłą.
PublicationPodano składowe różnicy potencjału elektrochemicznego między fazami wodnymi oscylatora z nitrobenzynową membraną ciekłą. Na tej podstawie oraz zmian stężeń składników układu w trakcie procesu zaproponowano mechanizm powstawania oscylacji w którym najważniejszą rolę odgrywają procesy adsorpcji/desorpcji surfaktantu na granicach faz.
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Active IR-Thermal Imaging in Medicine
PublicationIn this paper we summarize results of several research projects devoted to development of new diagnostic methods and procedures based on quantitative infrared thermography in medical applications. First, basics of active dynamic thermography are presented. Described are both, instrumentation and software comprising measurement procedures including collection of series of IR-images after external excitation, data treatment with...
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Tensile test of 1.4307 / X2CrNi18-9 / AISI 304L grade austenitic steel
Open Research DataShip structures and their components are build mainly of steel. Hull steel is used to build the hull structure. Some structural elements, such as RSW (Refrigerated See Water) tanks, or LNG (Liquid Natural Gas) tanks - gas transported at temperatures below -162° C, are build from austenitic steels. Austenitic steels have a different microstructure and...
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Tensile test of 1.4541 / X6CrNi18-10 / AISI 321 grade austenitic steel
Open Research DataShip structures and their components are build mainly of steel. Hull steel is used to build the hull structure. Some structural elements, such as RSW (Refrigerated See Water) tanks, or LNG (Liquid Natural Gas) tanks - gas transported at temperatures below -162° C, are build from austenitic steels. Austenitic steels have a different microstructure and...
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Effect of different crystalline structures on W/O and O/W/O wax emulsion stability
PublicationtThe possibility of emulsion stabilization using mineral and vegetable wax particles only (without sur-factant) was investigated. Mineral waxes, paraffin wax and ceresin, and a vegetable wax, carnauba wax,were used. The content of the wax particles and the water to oil proportion were found crucial for thestability of all emulsions. Some emulsions were also produced with a liquid wax (i.e. jojoba oil). Themultiple light scattering...
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Influence of pH and low-molecular weight organic compounds in solution on selected spectroscopic and analytical parameters of flowing liquid anode atmospheric pressure glow discharge (FLA-APGD) for the optical emission spectrometric (OES) determination of Ag, Cd, and Pb
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Opracowanie optymalnych warunków rozdzielania i identyfikacji metabolitów ro lin z rodzaju droseraceae, z zastosowaniem wysokosprawnej kolumnowej chromatografii cieczowej= A research on the composition of eluent for separation of plant metabolites by column reversed phase liquid chromatography
PublicationOd kilku lat na świecie trwają badania składników roślin owadożernych wykazujących atrakcyjne właściwości biologicznie czynne, tj. działanie przeciwbakteryjne, przeciwgrzybowe, antyoksydacyjne, a być może, także, przeciwnowotworowe. Pozyskiwanie substancji biologicznieaktywnych z materiału naturalnego, na drodze hodowli in vitro a następnie ekstrakcji i rozdzielania jest bardziej korzystne pod względem ekonomicznym, niż ich wytwarzanie...
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Metal ion directed template synthesis using 2-acetyl-1,3-indandione and ethylenediamine: steric and electronic restrictions
PublicationA template synthesis using 2-acetyl-1,3-indandione and ethylenediamine results in formation of octahedral Ni complex, whose crystal structure has been resolved using single crystal X-ray diffraction. The structure indicates that only exocyclic enolic oxygen atom of the triketone takes part in the condensation with ethylenediamine.
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Tensile test of 1.4571 / X6CrNiMoTi17-12-2 / AISI 316Ti grade austenitic steel
Open Research DataShip structures and their components are build mainly of steel. Hull steel is used to build the hull structure. Some structural elements, such as RSW (Refrigerated See Water) tanks, or LNG (Liquid Natural Gas) tanks - gas transported at temperatures below -162° C, are build from austenitic steels. Austenitic steels have a different microstructure and...
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Rain Gardens SW quality dataset
Open Research DataThis dataset contains the results of parameters of storm water runoff and storm water quality in rain garden units. Samples were collected from 4 different rain gardens in Gdansk, Poland.
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Study of the optical rotatory of potassium titanyl phosphate using the advanced dual-wavelength polarimetric method
PublicationA dual-wavelength high-accuracy universal polarimeter was applied to the circular birefringence and optical activity measurement in potassium titanyl phosphate (KTP) nonlinear crystal. The experimental setup used two single-mode He-Ne lasers with close wavelengths of 594 and 633 nm as light sources. Measurement has been carried out for two crystal settings in directions of a 45-degree relative angle to the [100] and [010] crystallographic...
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Pt-rich intermetallic APt8P2 (A = Ca and La)
PublicationThe combination of experimental and theoretical investigation of two new Pt-rich intermetallic compounds: APt8P2 (A = Ca and La) is presented, including solid-state synthesis, crystal structure determination, physical properties characterization and chemical bonding analysis. APt8P2 was obtained through the high-temperature pellet synthesis. According to both single crystal and powder X-ray diffraction results, APt8P2 crystallize...
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The crystal structures of (<i>O</i>-silyl)thiobenzoates (<sup><i>t</i></sup>BuO)<sub>3</sub>SiOC(S)Ph, Ph<sub>3</sub>SiOC(S)Ph, (2,6-XyO)<sub>3</sub>SiOC(S)Ph, and PhC(O)SSSC(O)Ph
PublicationChlorek benzylu reaguje z silanotiolanami sodu R3SiSNa dając wyłącznie pochodne sililowe kwasu monotiobenzoesowego R3SiOC(S)Ph, R=t-Bu, Ph lub 2,6-XyO w postaci pomarańczowych kryształów. Wymienione produkty zostały poddane rentgenowskiej analizie strukturalnej. Badania NMR roztworów tych substancji wskazują, że te same izomery są obecne w roztworze i w ciele stałym.
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SEM micrographs of NH4VO3 crystals
Open Research DataThe DataSet contains the scanning electron microscopy (SEM) micrographs of NH4VO3 crystals obtained by the LPE-IonEx method. The SEM images clearly show that the morphology of the end product can be nicely tuned by changing the type of ammonium salt and the solvent. It can be concluded that the used solvent affected crystal shapes and their size was...
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Porównanie mocy strat energetycznych w pompie wyporowej o zmiennej wydajności określonych bez uwzględnienia bądź z uwzględnieniem mocy ściskania oleju hydraulicznego
PublicationPorównano moce strat energetycznych w pompie wyporowej o zmiennej wydajności, określone bez uwzględnienia bądź z uwzględnieniem mocy ściskania oleju hydraulicznego. Ocena mocy ściskania cieczy w pompie stała się możliwa dzięki zastosowaniu, zaproponowanej przez autora, metody określenia stopnia zapowietrzenia cieczy w pompie. W metodzie określenia stopnia zapowietrzenia cieczy w pompie oraz w ocenie mocy strat objętościowych ściskania...
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Zdzisław Kowalczuk prof. dr hab. inż.
PeopleZdzislaw Kowalczuk received his M.Sc. degree in 1978 and Ph.D. degree in 1986, both in Automatic Control from Technical University of Gdańsk (TUG), Gdańsk, Poland. In 1993 he received his D.Sc. degree (Dr Habilitus) in Automatic Control from Silesian Technical University, Gliwice, Poland, and the title of Professor from the President of Poland in 2003. Since 1978 he has been with Faculty of Electronics, Telecommunications and Informatics...
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Analiza oddziaływań w kryształach związków zawierających w strukturze pierścień pirydynowy
PublicationMożliwość tworzenia się wiązań wodorowych jest kluczowym parametrem z punktu widzenia inżynierii kryształu, ponieważ wiązania wodorowe mają bezpośredni wpływ na strukturę oraz trwałość sieci krystalicznej. Głównym celem niniejszej rozprawy doktorskiej była analiza porównawcza wiązań wodorowych występujących w układach, zawierających w strukturze pierścień pirydynowy. Badane układy podzielono na: (1) układy ze związkami krzemosiarkowymi...
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Thermodynamic Characteristics of Phenacetin in Solid State and Saturated Solutions in Several Neat and Binary Solvents
PublicationThe thermodynamic properties of phenacetin in solid state and in saturated conditions in neat and binary solvents were characterized based on differential scanning calorimetry and spectroscopic solubility measurements. The temperature-related heat capacity values measured for both the solid and melt states were provided and used for precise determination of the values for ideal solubility, fusion thermodynamic functions, and...
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Face detection in image sequences using a portable thermal camera
PublicationFace detection is often a first step in quantitative analysis of face images. It is an important research area for visible images and recently also for thermography. Due to technological developments thermal cameras may be embedded into wearable devices to provide remote healthcare. In this paper, we compared three algorithms for face detection in thermal images by testing execution time, accuracy, symmetry ratio and false-positives....
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Thermal sequences database of the skin flaps in breast reconstruction and burns
PublicationThis paper presents a database of Active Dynamic Thermography (ADT) thermal sequences gathered throughout 6 year study on ADT application in skin flap blood perfusion monitoring and burn wounds diagnosis. For skin flap monitoring the database comprises of data collected during three different breast reconstruction procedures. The patients were monitored pre, intra and post surgically within 90 days period. The sequences were used...
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Thermal sequences database of the skin flaps in breast reconstruction and burns
PublicationThis paper presents a database of Active Dynamic Thermography (ADT) thermal sequences gathered throughout 6 year study on ADT application in skin flap blood perfusion monitoring and burn wounds diagnosis. For skin flap monitoring the database comprises of data collected during three different breast reconstruction procedures. The patients were monitored pre, intra and post surgically within 90 days period. The sequences were used...
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High-accuracy polarimetric studies on lead germanate single crystals
PublicationA high-accuracy polarimetric technique has been used for the characterization of a lead germanate ferroelectric single crystal. The measurement results of the linear and circular birefringence in the [010] direction at a wavelength of 633 nm under the influence of an electric field are presented. Gyration–electric field hysteresis loops at alternative crystal positions in the polarization system have been used to determine the...
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Concentration levels of selected analytes in the gas phase of an e-cigarette aerosol
PublicationThe aerosols generated from e-cigarettes are composed of liquid and gas phases resulting from vapourized e-liquid. The apportioning of substances from e-liquid into the liquid and gas phases during e-cigarette use has not been extensively studied. Partitioning of e-liquid components between the gas and the liquid phase of the aerosol influences the substances inhaled and exhaled by the users, leading to second-hand exposure. It...
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Rain Gardens LC_MS/MS analysis dataset
Open Research DataThis dataset contains the results of samples analysis (target analysis with certified reference materials) using ultra-high performance liquid chromatography tandem mass spectrometry (UHPLC-MS/MS, Shimadzu, Japan).
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LattE- first-principles lattice energy calculations
PublicationCrystal engineering is currently attracting much interest. Its aim is to create materials of predefined properties fulfilling the requirements imposed by the applications. There are several parameters describing crystal structures, but the most important one is probably the energy of a crystal lattice. It is the energy released by the system when crystalline solid is formed out of molecules or ions in gaseous phase. Approximate...
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Comparison of the powers of energy losses in a variable capacity displacement pump determined without or with taking into account the power of hydraulic oil compression
PublicationPowers of energy losses in a variable capacity displacement pump are compared with or without taking into account the power of hydraulic oil compression. Evaluation of power of liquid compression in the pump was made possible by the use of method, proposed by the Author, of determining the degree of liquid aeration in the pump. In the method of determining the liquid aeration in the pump and of powers of volumetric losses of liquid...
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SEM images of dewetted gold films
Open Research DataGold nanostructures were prepared on silicon - Si(111) as a substrate. as a result of dewetting process. Thin golds films were deposited using a table-top dc magnetron sputtering coater under pure Ar plasma conditions . The Au target had 99.99% purity, the rate of Au layer deposition was about 0.4 nm·s−1 and the incident power was 32 W. The thickness...
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Oxidation of silver nanostructures
Open Research DataSilver nanostructures were prepared on Si substrate. Thin Ag films (2 and 6 nm thickness) were deposited using a tabletop dc magnetron sputtering coater (EM SCD 500, Leica) in pure Ar plasma. The Ag target was of 99.99% purity, the rate of layer deposition was about 0.4 nm·s−1 , and the incident power was in the range of 30–40 W. The layer thickness...
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Structural investigations of the LTO:Cu thin films
Open Research DataLithium titanate (Li1+xTi2-xO4) doped with Cu2+ ions was synthesized by sol-gel processing method. The structure was characterized by X-ray Diffraction (XRD). All samples revealed presence of LTO spinel phase. X-ray pattern of undoped LTO was free of any impurities and other crystal phases. Similarly, samples with low amount of copper dopant (x = 0.05...
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The scanning tunnelling micrographs of highly oriented pyrolytic graphite
Open Research DataThe dataset contains the results imaging of a sample of highly oriented pyrolytic graphite obtained using scanning tunneling microscopy. The above variant of scanning probe microscopy is one of the most convenient research techniques at atomic scales. The file contains images corresponding to increasing magnifications from the 1 um scale to a few nanometers....
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Comparison of XPS spectra of Ag3d for silver nanostructures and bulk material
Open Research DataAg nanostructures were prepared on borosilicate glass (Corning 1737F) and Si substrates. In both cases, the substrateswere cleaned with acetylacetone and then rinsed in ethanol. Thin Ag films (2 and 6 nm thickness) were deposited using a tabletop dc magnetron sputtering coater (EM SCD 500, Leica) in pure Ar plasma (argon, Air Products 99.999%). The...
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The Impact of Sloshing Liquids on Ship Stability for Various Dimensions of Partly Filled Tanks
PublicationLiquid sloshing phenomenon taking place in partly filled ships' tanks directly affects the stability of a vessel. However, only static calculations are carried out onboard ships nowadays and static transfer of liquid weight is taken into account in the course of routine stability calculation. The paper is focused on a dynamic heeling moment due to liquid sloshing in tanks onboard ships. A number of numerical simulations of liquid...
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Analysis of the influence of external conditions on temperature readings in thermograms and adaptive adjustment of the measured temperature value
PublicationMeasuring human temperature is a crucial step in preventing the spread of diseases such as COVID-19. For the proper operation of an automatic body temperature measurement system throughout the year, it is necessary to consider outdoor conditions. In this paper, the effect of atmospheric factors on facial temperature readings using infrared thermography is investigated. A thorough analysis of the variation of facial temperature...
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Inverse determination of sliding surface temperature based on measurements by thermocouples with account of their thermal inertia
PublicationThis study developed an inverse heat conduction algorithm to determine temperature at a sliding surface taking account of thermocouple thermal inertia. The direct heat conduction problem was solved analytically based on the Laplace integral transform approach. The inverse algorithm was applied to the problem of friction of a brake material against a steel. The experiments were conducted on a pin-on-disc tribometer for three short-time...
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Dual-wavelength laser polarimeter and its performance capabilities
PublicationA dual-wavelength optical polarimetric approach has been proposed as a means of elimination of the systematic errors and estimation of the optical anisotropy parameters for a single DKDP crystal. Our HAUP-related polarimeter uses two semiconductor lasers with the neighbouring wavelengths of 635 nm and 650 nm. Based on the temperature dependence analysis of small characteristic azimuths of light polarization with respect to the...