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Application of gas chromatography to the analysis of spirit-based alcoholic beverages
PublicationSpirit-based beverages are alcoholic drinks, which production processes are dependent on the type and origin of raw materials. The composition of this complex matrix is difficult to analyze and scientists commonly choose a gas chromatography techniques for this reason. With a wide selection of extraction methods and detectors it is possible to provide qualitative and quantitative analysis for many chemical compounds with a various...
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Devices for the production of reference gas mixtures
PublicationFor many years there has been growing demand for gaseous reference materials, which is connected with development in many fields of science and technology. As a result, new methodological and instrumental solutions appear that can be used for this purpose. Appropriate quality assurance/quality control (QA/QC) must be used to make sure that measurement data are a reliable source of information. Reference materials are a significant...
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Environmentally Oriented Models and Methods for the Evaluation of Drug x Drug Interaction Effects
PublicationThis detailed review compares known and widely used methods for drug interaction estimation, some of which now have historical significance. Pharmaceutical application has been noted as far back as several thousand years ago. Relatively late in the 20th century, however, researchers became aware that their fate and metabolism, which still remain a great challenge for environmental analysts and risk assessors. For the patient’s...
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Revision of Biological Methods for Determination of EDC Presence and Their Endocrine Potential
PublicationEndocrine-disrupting compounds (EDC) are chemicals responsible for disturbances in the hormonal balance of organisms. This group of chemicals includes both egzogenic and endogenic substances or their mixtures that impact functioning of natural hormones in organisms. In the available literature one can find information on the application of chromatographic and related techniques in the analysis of environmental samples for detection,...
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The Current State-of-the-Art in the Determination of Pharmaceutical Residues in Environmental Matrices Using Hyphenated Techniques
PublicationSeveral thousand tons of pharmaceuticals and their transformation products (metabolites and degradation products) are introduced into the environment each year. They affect both human health and the environment, therefore, analytical procedures enabling the determination of a wide range of pharmaceuticals at trace levelswithminimal effort, time, and energy are required. Nowadays, hyphenated techniques are commonly applied in pharmaceutical...
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Mobile Systems (Portable, Handheld, Transportable) for Monitoring Air Pollution
PublicationThe monitoring and analysis of atmospheric air pollutants is a rapidly developing branch of analytical chemistry. The in situ analysis of atmospheric air quality using mobile instrumentation is becoming routine. The article provides information on devices used in various kinds of mobile laboratories. It reviews the portable gas chromatographs and handheld devices used for detecting and determining specific harmful substances in...
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Analysis of MArkers of Exposure to Constituents of Environmental Tobacco Smoke (ETS)
PublicationTobacco smoke is a complex mixture of more than 4000 chemical compounds, many of which are harmful to human health. These compounds belong to various chemical classes, including amides, imides, lactams, carboxylic acids, aldehydes, ketones, alcohols, phenols, amines, hydrocarbons, ethers, and inorganic compounds. There are three types of tobacco smoke streams: the mainstream, the sidestream, and environmental tobacco smoke (ETS)....
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Comparison of different techniques for extracting Polychlorinated Biphenyls from bottom sediment samples using Isotope Dilution Mass Spectrometry
PublicationIn this work, problems that may occur during determination of trace levels of polychlorinated biphenyls in sediment samples are described. The main error sources are connected with extraction of analytes prior to final determination. During model studies, polychlorinated biphenyls have been extracted from sediment reference material (METRANAL 2) with the use of different solvents (dichloromethane, hexane, and toluene); the process...
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Analysis of arsenic species in environmental samples
PublicationMany analytical methods for determining arsenic in various forms in environmental samples have been developed in recent years. The main objective of this review article is the presentation and comparison of the three principal techniques for the determination arsenic compounds, namely: hydride generation (HG), voltammetry and chromatography (liquid chromatography including high-performance liquid chromatography (HPLC), and gas...
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New Polymeric Materials for Solid Phase Extraction
PublicationSolid phase extraction (SPE) is a popular sample preparation technique, which can be applied directly in gas–solid phase and liquid–solid phase, or indirectly to solid samples by using, e.g., thermodesorption with subsequent chromatographic analysis. Although SPE can be described as a physical extraction process involving a liquid phase and a solid phase, the increased use of packed sorbent formats seems to have led to a bias toward...
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Direct Analysis of Samples of Various Origin and Composition Using Specific Types of Mass Spectrometry
PublicationOne of the major sources of error that occur during chemical analysis utilizing the more conventional and established analytical techniques is the possibility of losing part of the analytes during the sample preparation stage. Unfortunately, this sample preparation stage is required to improve analytical sensitivity and precision. Direct techniques have helped to shorten or even bypass the sample preparation stage; and in this...
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The Use of Sensory Analysis Techniques to Assess the Quality of Indoor Air
PublicationThe quality of indoor air is one of the significant elements that influences people's well-being and health inside buildings. Emissions of pollutants, which may cause odor nuisance, are the main reason for people's complaints regarding the quality of indoor air. As a result, it is necessary to perform tests aimed at identifying the sources of odors inside buildings. The article contains basic information on the characteristics...
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Miniaturized Passive Emission Chambers for In Situ Measurement of Emissions of Volatile Organic Compounds
PublicationThe results of many different studies have demonstrated unequivocally that the quality of indoor air is often much worse than that of atmospheric air. The presence of dangerous chemical compounds in indoor air can have an adverse impact on human health and cause numerous diseases of the respiratory and circulatory systems. Such harmful chemicals get into indoor air as a result of their emission from building and indoor materials....
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Trace analysis - challenges and problems
PublicationW pracy przedstawiono podstawowe problemy związane z oznaczaniem składników śladowych i ultraśladowych w próbkach o złożonym składzie matrycy. W oparciu o dane literaturowe omówiono sposoby zapobiegania błędom jakimi mogą być obarczone wyniki oznaczeń końcowych.
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Denudation - a convenient method of isolation and enrichment of analytes
PublicationW pracy przedstawiono: podstawy teoretyczne techniki denudacyjnej; rozwiązania konstrukcyjne podstawowych typów urządzeń denudacyjnych; obszar praktycznego wykorzystania technik denudacyjnych.
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Sample preparation and chromatographic analysis of acidic herbicides in soils and sediments
PublicationW pracy przedstawiono różne techniki przygotowania próbek i oznaczania herbicydów z grupy pochodnych fenoli i pochodnych kwasów karboksylowych w próbkach gleby. Opisano wybrane metody wzbogacania i izolacji analitów, m. in.: ekstrakcję za pomocą wodnych roztworów zasad i rozpuszczalników organicznych płynem w stanie nadkrytycznym, wodą w stanie podkrytycznym, cieczą pod zwiększonym ciśnieniem, cieczą wspomaganą mikrofalami. Niski...
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Modern techniques of extraction of organic analytes from environmental matrices.
PublicationW pracy przedstawiono usystematyzowane informacje dotyczące dostępnych jak i nowych technik izolacji i wzbogacania analitów organicznych przed etapem oznaczeń końcowych.
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Preparation of gaseous standard mixtures: methods for controlling the amount of components generated in the process of thermal decomposition of immobilized compounds.
PublicationGazowe mieszaniny wzorcowe odgrywają ważną rolę w ocenie metod analitycznych i urządzeń pomiarowych. W tym przypadku gazowe mieszaniny wzorcowe mogą być traktowane jako specjalny rodzaj materiału odniesienia.Proces walidacji wymaga użycia tzw. matrycowych materiałów odniesienia. Wybór techniki umożliwiającej uzyskanie gazowej mieszaniny wzorcowej o żądanych parametrach użytkowych zależy od natury składników mierzonych i gazu...
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Fate and analysis of pharmaceutical residues in the aquatic environment.
PublicationObecność pozostałości farmaceutyków w poszczególnych elementach środowiska stanowi nowe wyzwanie zarówno z punktu widzenia technologii oczyszczania wód i ścieków, jak i dla analityków, których zadaniem jest opracowanie nowych metodyk analitycznych. Wiele stosowanych leków nie jest w organizmie całkowicie rozkładanych. Często są one wydalane po nieznacznym przekształceniu,lub nawet w niezmienionej postaci. Opisano drogi...
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Analytical procedures for PAH and PCB determination in water samples - error sources
PublicationW pracy przedstawiono poszczególne etapy procedury analitycznej wykorzystywanej do oznaczania analitów z grupy WWA i PCB w próbkach wody. Pokazano jakie problemy występują podczas oznaczania wyżej wymienionych analitów i jaki mogą mieć wpływ na końcowy wynik analizy.
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RUSSIANS ON THE POLISH LABOUR MARKET
PublicationThe article looks into the employment of Russian citizens in Poland in 2004– 2018. It presents the legal basis for Russians’ entering Poland and taking up work without having to seek a work permit, and specifies who must apply for such a permit. Russian citizens can obtain refugee status under the Geneva Convention, which grants them the right to move freely, choose their place of residence and undertake paid employment, while...
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Stochastic intervals for the family of quadratic maps
Open Research DataNumerical analysis of chaotic dynamics is a challenging task. The one-parameter families of logistic maps and closely related quadratic maps f_a(x)=a-x^2 are well-known examples of such dynamical systems. Determining parameter values that yield stochastic-like dynamics is especially difficult, because although this set has positive Lebesgue measure,...
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Local buckling of composite channel columns
PublicationThe investigation concerns local buckling of compressed flanges of axially compressed composite channel columns. Cooperation of the member flange and web is taken into account here. The buckling mode of the member flange is defined by rotation angle a flange about the line of its connection with the web. The channel column under investigation is made of unidirectional fibre-reinforced laminate. Two approaches to member orthotropic...
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Crossover from charge density wave stabilized antiferromagnetism to superconductivity in Nd1−xLaxNiC2 compounds
PublicationThe path from the charge density wave antiferromagnet NdNiC2 to the noncentrosymmetric superconductor LaNiC2 is studied by gradual replacement of Nd by La ions. The evolution of physical properties is explored by structural, magnetic, transport, magnetoresistance, and specific heat measurements. With the substitution of La for Nd, the Peierls temperature is gradually suppressed, which falls within the BCS mean-field relation for...
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VOCs absorption from gas streams using deep eutectic solvents – A review
PublicationVolatile organic compounds (VOCs) are one of the most severe atmospheric pollutants. They are mainly emitted into the atmosphere from anthropogenic sources such as automobile exhaust, incomplete fuel combustion, and various industrial processes. VOCs not only cause hazards to human health or the environment but also adversely affect industrial installation components due to their specific properties, i.e., corrosive and reactivity....
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Analysis of the Possibility of Using New Types of Protective Coatings and Abrasion-Resistant Linings under the Operating Conditions of the Spiral Classifier at KGHM Polska Miedź S.A. Ore Concentration Plant
PublicationA study was carried out to select the appropriate coatings for corrosion protection of the spiral classifier working at KGHM Polska Miedź S.A. Ore Concentration Plant. The abrasion resistance of selected protective coatings and wear-resistant linings was investigated using a DT-523 rotary abrasion tester with Taber CS-10 rubber abrasive discs. The average weight loss of the coatings after a cycle of 2000 revolutions was determined....
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Managing safety of industrial hazardous installations with emphasis on the control systems, interfaces and human factors
PublicationIn the paper a procedure for the layer of protection analysis (LOPA) as a tool to evaluate the risk of accident scenarios occurrence in hazardous installations is outlined. In such installations several protection layers exist. Human operator performance in each layer is unavoidable, but the role and tasks are different and depend on the context of situation. Based on suggestions form literature (EEMUA, CREAM) and own proposals...
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Herbarium of Division of Marine Biology and Ecology University of Gdańsk (DMBE)
Open Research DataHerbarium of Division of Marine Biology and Ecology University of Gdańsk (DMBE) is a research herbarium encompassing specimens of vascular plants and algae hosted by the Laboratory of Marine Plant Ecology at University of Gdańsk, Poland. The aim of Herbarium is to preserve marine plant and algae collections mostly from the Gulf of Gdańsk, but the herbarium...
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Generation of random fields to reflect material and geometric imperfections of plates and shells
PublicationThe paper covers two patterns of random field generation: conditional acceptance – rejection method and Karhunen – Loève expansion. The generation of two-dimensional random fields is essential in plates and shells analysis, allowing for a relevant limit and critical state assessment of geometrically and ma-terially imperfect structures. The features of both generation methods dedicate them to selected problems.
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Selective jamming of OFDM transmission in NB-IoT radio interface
PublicationThe paper presents the concept of smart jamming, which involves selective interference aimed at critical components of the OFDM signal. Research verifying the feasibility of this type of electronic attack are described. A realized testbed for jamming real NB-IoT signals in a downlink is presented. The test results demonstrate the feasibility of realizing selective jamming and its greater effectiveness compared to barrage interference.
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Pozwolić odejść, czyli... Granice interwencji
PublicationCelem tekstu jest zwrócenie uwagi na problem ostatecznej granicy interwencji konserwatorskich wobec zabytków architektury w kontekście holistycznej koncepcji ochrony dziedzictwa. Tekst adresowany jest do polskich czytelników ze względu na szczególne odniesienia do sytuacji polskiego systemu ochrony dziedzictwa. Choć architektura należy do sfery sztuk użytkowych, większość budynków nie powstawała...
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Wstępna analiza zagrożenia podtopieniami w zlewni Potoku Strzyża w Gdańsku.
PublicationCharakterystyka sieci hydrograficznej Potoku Strzyża. Analiza zagrożenia podtopie - niami z wykorzystaniem hydraulicznego modelu potoku. Przedstawienie oraz analiza wyników obliczeń. Wstępne określenie odcinków newralgicznych z punktu widze - nia zagrożenia powodziowego. Wstępna analiza możliwych przyczyn występowania podtopień na terenie zlewni Potoku Strzyża.
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Full scale measurements of pressure field induced on the quay wall by bow thrusters – indirect method for seabed velocities monitoring
PublicationThe paper presents the results of full-scale experimental investigation of loads generated on the quay wall by bow thrusters during unberthing of a self-manoeuvring vessel. The presented research allowed for the comparison of the measurements results with generally accepted empirical prediction methods and confirmed the utility of the developed measuring setup for the on-line monitoring of jet induced loads. The conclusions from the...
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2022_Elective Design II_S_Hudnik_K_Zyczkowska_There is no Planet B
e-Learning CoursesThere is no Planet B The studio will use practical interventions to explore how climate change is affecting transformations in urban / non-urban space in Gdansk. Through the identification of problems and the importance of reading the consequences in space and architecture, students will learn about the method of opening a critical public debate. Through a variety of topics and actions – micro interventions, they will record their...
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The E-Cohomological Conley Index, Cup-Lengths and the Arnold Conjecture on T 2n
PublicationWe show that the E-cohomological Conley index, that was introduced by the first author recently, has a natural module structure. This yields a new cup-length and a lower bound for the number of critical points of functionals on Hilbert spaces. When applied to the setting of the Arnold conjecture, this paves the way to a short proof on tori, where it was first shown by C. Conley and E. Zehnder in 1983.
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Kerogen to bitumen transformation with respect to host rock environment
PublicationResearch focuses on analyzing the role of rock constituents in kerogen transformation. It includes mineral and organic matter characterization, kerogen and bitumen isolation, quantification, and determination of the critical factors of transformation ratio concerning generating mobile versus less mobile hydrocarbons. The results indicate that the ratio mainly depends on the distribution and type of kerogen in the basin, and secondly...
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Elastic distortional buckling of thin-walled bars of closed quadratic cross-section
PublicationIn this study a tin-walled bar with closed quadratic cross-section is considered. The elastic stability of axially compressed bar related to the cross-section distortion is investigated. The governing differential equatio is derived with aid of the principle of stationary potential energy. The critical load for simply supported bar is found in an analytical form and it is copared with the FEM solution. Sufficient accuracy of the...
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Elastic distortional buckling of thin-walled bars of closed quadratic cross-section
PublicationIn this study a thin-walled bar with closed quadratic cross-section is considered. The elastic stability of axially compressed bar related to the cross-section distortion is investigated. The governing differential equation is derived with aid of the principle of stationary total potential energy. The critical load for the simply supported bar is found in analytical form and it is compared with the FEM solution. Sufficient accuracy...
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Analiza numeryczna i badania doświadczalne wpływu usytuowania stężeń na nośność wyboczeniową modelu kratownicy
PublicationIn the present research the results of experimental test and numerical analyses of a model of a typical truss are presented. The truss linear buckling analysis and non linear static analyses with respect to material and geometrical nonlinearity are conducted. For different stiffnesses and location of braces, the critical load and limit load for the truss are calculated and the threshold bracing stiffness is found. The results of...
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Re-use of historic wooden verandas in Sopot, Poland
PublicationSopot is the best-known seaside resort in Poland. The city is unique with regard not only to its location and natural values, but also its interesting architecture, which dates back to the end of the 19th and the beginning of the 20th century. Wooden verandas are one of the characteristic features of Sopot architecture. Their origin is associated with the Swiss style, which was fashionable at the turn of the 20th century and quite...
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Study of the formation of calcareous deposits on cathodically protected steel in Baltic sea water
PublicationPurpose – The purpose of this paper is to investigate whether the sedimentation of calcareous deposits occurs on cathodically protected steel in Baltic sea water. Design/methodology/approach – Steel electrodes were cathodically polarized in natural Baltic sea water at potential þ0.150 V vs Zn electrode in potentiostatic mode. During exposure chronoamperometric measurements were carried out. After the exposure, the electrode’s surface...
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Respiratory Rate Estimation Based on Detected Mask Area in Thermal Images
PublicationThe popularity of non-contact methods of measuring vital signs, particularly respiratory rate, has increased during the SARS-COV-2 pandemic. Breathing parameters can be estimated by analysis of temperature changes observed in thermal images of nostrils or mouth regions. However, wearing virus-protection face masks prevents direct detection of such face regions. In this work, we propose to use an automatic mask detection approach...
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de mininis state aid for entrepreneurs in EU law
Open Research DataThis dataset will provide basic information on the legislation regarding the de minimis state aid under EU law, and some literature explaining the nature and effects of the de minimis state aid for entrepreneurs in some EU Member States in the budgetary period 2014-2020. As this kind of state aid admissible under the GBER, the individual decisions of...
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The impact of shipping 4.0 on controlling shipping accidents: A systematic literature review
PublicationMaritime shipping, with a significant role in global trade, confronts various accidents leading to loss of lives, properties, and the environment. Shipping 4.0 technologies are scaling up to address this problem by employing real-time data-driven technologies, including cyber-physical systems, advanced tracking and tracing, intelligent systems, and big data analytics. Despite growing attention, there is a general lack of clarity...
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Stability analysis of nanobeams in hygrothermal environment based on a nonlocal strain gradient Timoshenko beam model under nonlinear thermal field
PublicationThis article is dedicated to analyzing the buckling behavior of nanobeam subjected to hygrothermal environments based on the principle of the Timoshenko beam theory. The hygroscopic environment has been considered as a linear stress field model, while the thermal environment is assumed to be a nonlinear stress field based on the Murnaghan model. The size-dependent effect of the nanobeam is captured by the nonlocal strain gradient...
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On local buckling of cold-formed channel members
PublicationThe paper deals with local buckling of the compressed flanges of cold-formed thin-walled channel beams subjected to pure bending or axially compressed columns. Arbitrarily shaped flanges of open cross-sections and the web-flange interactions are taken into account. Buckling deformation of a beam flange is described by displacement related to torsion of the flange about the line of its connection with the web. Total potential energy...
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Heterogeneity of national accounting systems, world-class universities and financial resources: What are the links?
PublicationThis study investigates the relationship between university financial resources, applied accounting systems, and the place of a university in the Shanghai Ranking. We find a strong relationship between the financial resources under the control of a world-class university and the position of that university in the highest tier of the global ranking. We propose a model (available online) to predict a university’s tier in the ranking...
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Superconductivity in CaBi2
PublicationSuperconductivity is observed with critical temperature Tc = 2.0 K in self-flux-grown single crystals of CaBi2. This material adopts the ZrSi2 structure type with lattice parameters a = 4.696(1) Å, b = 17.081(2) Å and c = 4.611(1) Å. The crystals of CaBi2 were studied by means of magnetic susceptibility, specific heat and electrical resistivity measurements. The heat capacity jump at Tc is DC/gTc = 1.41, confirming bulk superconductivity;...
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Application of electrochemical sensors and sensor matrixes for measurement of odorous chemical compounds
PublicationIn this paper describes the principle of operation of the electrochemical sensors and the sensor matrixes comprised of electrochemical sensors intended for measurement of odorous compounds. Critical comparison of these sensors’ advantages and disadvantages has been made. The fields of economy contributing to release of odours and the potential sources of their emission have been identified. Commercially available electrochemical...
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The Point Estimate Method in a Reticulated Shell Reliability Analysis
PublicationThe objective of this paper is to present an application of the point estimate method (PEM) to determine the probabilistic moments for engineering structures. Reliability analysis is illustrated by two examples: an estimation of the critical force in linear elastic buckling analysis and a reticulated shell limit load determinations. Calculations were also made using Monte Carlo method. It has been shown the practical usefulness...