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Search results for: CYCLOADDITION · NON-ISOCYANATE POLYURETHANE · THERMAL DECOMPOSITION · CARBON CAPTURE · BIS(CYCLIC CARBONATE) · THERMAL DEGRADATION KINETICS
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Photocatalytic decomposition of ethylene on the TiO2-polystyrene spheres
Open Research DataData contain results from the measurements of the photocatalytic decomposition of ethylene under UV irradiation with using TiO2 coating on the expanded polystyrene spheres (EPS). EPS-SiO2-TiO2 and EPS-TiO2 were used as the photocatalytic beds in the fluidized bed reactor. Both, stationary and fluidized beds were tested. The comparison of ethylene decomposition...
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Insightful studies of AuCu nanostructures deposited on Ti platform: Effect of rapid thermal annealing on photoelectrochemical activity supported by synchrotron radiation studies
PublicationIn this work, we present the influence of annealing atmospheres during rapid thermal annealing (40◦C/s) on nanostructured Ti platforms modified by 10 nm layer of AuCu alloy obtained via magnetron sputtering. The AuCu/Ti platform annealed under hydrogen atmosphere exhibits the best photoelectrochemical activity under visible light, i.e. 27 times higher photocurrent than for pure Ti dimpled platform, and the lowest reflectance with minimum...
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Strain-dependent behaviour of cold recycled material mixtures in cyclic compression tests
PublicationThe purpose of the study is to evaluate strain-dependent behaviour of Cold Recycled Material (CRM) mixtures using three frameworks typically applied for Hot Mix Asphalt (HMA): linear viscoelastic (LVE) limits; non-linearity directions; changes in rheological model parameters. To this aim, the complex modulus of three CRM mixtures with different bitumen-to-cement ratio (0.2, 0.6 and 1.8) was measured in cyclic compression mode,...
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An approach for estimation of water wall degradation within pulverized-coal boilers
PublicationThe main aim of this paper is to estimate the lifetime of water walls of pulverized-coal boilers at nominal conditions as well as after degradation of water tubes. An approach for a pulverized-coal chamber degradation process has been formulated based on operational and experimental data. This model was formulated using on-line state monitoring of a pulverized coal burner with aim of preventing the fireplace screens from high degradation...
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The Impact of Hybrid Flame Retardant Compositions on the Performance of Foamed Flexible Polyurethane/Ground Tire Rubber Composites
PublicationCurrent sustainability-oriented trends affect polyurethane (PU) materials and stimulate the incorporation of recycled or waste-based materials as fillers. Ground tire rubber (GTR) poses as an auspicious candidate due to the excellent performance of car tires. Despite the benefits related to the mechanical performance, it contributes to the increasing flammability of the resulting composites. Herein, presented work assessed the...
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Forced Degradation Studies of Ivabradine and In Silico Toxicology Predictions for Its New Designated Impurities
PublicationAll activities should aim to eliminate genotoxic impurities and/or protect the API against degradation. There is a necessity to monitor impurities from all classification groups, hence ivabradine forced degradation studies were performed. Ivabradine was proved to be quite durable active substance, but still new and with insufficient stability data. Increased temperature, acid, base, oxidation reagents and light were found to cause...
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Separate synthesis and evaluation of glucitol bis-phosphate and mannitol bis-phosphate, as competitive inhibitors of fructose bis-phosphate aldolases
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Factors causing degradation of sulfadimetoxine
PublicationSulfadimetoxine is a representative of sulfonamide drugs which presence inhibits growth of activated sludge bacteria, rhat is necessary for the effective mineralization of organic and inorganic contaminants. Therefore factors which con prevent this situation are searched. Aim of this study is selection of conditions causing efficien degradation of the drug- sulfadimetoxine. The impact of such aspects as : the type of oxidizing...
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Termooksydacyjna i fotooksydacyjna degradacja pianek poliuretanowych
PublicationPrzeprowadzono ocenę efektywności działania wybranych środków przeciwstarzeniowych w sztywnych piankach poliuretanowych, otrzymywanych na drodze syntezy jednoetapowej. Ocenę tę oparto na pomia-rach zmian barwy oraz wytrzymałości mechanicznej zsyntezowanych materiałów. Na podstawie analizy uzyskanych wyników stwierdzono, iż dodatek 3% mieszaniny I rzędowego antyutleniacza fenolowego oraz benzotriazolowego absorbera UV znacząco zmniejsza...
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Degradation mechanisms and protective coatings for ferritic stainless-steel interconnects of solid oxide fuel cells: A review
PublicationFerritic stainless steels (FSSs) are promising interconnect materials for solid oxide fuel cells (SOFCs). However, FSSs undergo fast thermal-oxidation during SOFC operation, generating poorly-conductive oxide scales and volatile chromium-oxides detrimental to cathodes. Developing protective coatings is crucial for inhibiting degradation of FSS-interconnects. This article starts with a brief discussion of the oxidation behavior...
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2,4-Bis[bis(diisopropylamino)phosphanyl]-1,2,3,4-tetraphosphabicyclo[1.1.0]butane
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Non-disjoint Decomposition Using r-admissibility and Graph Coloring and Its Application in Index Generation Functions Minimization
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Preparation and characterization of Pt–N/TiO2 photocatalysts and their efficiency in degradation of recalcitrant chemicals
PublicationSeries of Pt–N/TiO2 photocatalysts were synthesized using the sol–gel method. The photocatalysts’ characteristics by X-ray diffractometry (XRD), scanning transmission electron microscopy (STEM), diffuse reflectance spectroscopy (DRS), X-ray photoelectron spectroscopy (XPS) showed that sample with the molar ratio Ti:N equal 1:4 and platinum nanoparticles size of about 3 nm had anatase structure, about 94 m2/g specific surface area...
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Tailoring diamondised nanocarbon-loaded poly(lactic acid) composites for highly electroactive surfaces: extrusion and characterisation of filaments for improved 3D-printed surfaces
PublicationA new 3D-printable composite has been developed dedicated to electroanalytical applications. Two types of diamondised nanocarbons - detonation nanodiamonds (DNDs) and boron-doped carbon nanowalls (BCNWs) - were added as fillers in poly(lactic acid) (PLA)-based composites to extrude 3D filaments. Carbon black served as a primary filler to reach high composite conductivity at low diamondised nanocarbon concentrations (0.01 to 0.2...
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Studies on Aminoanthraquinone-Modified Glassy Carbon Electrode: Synthesis and Electrochemical Performance toward Oxygen Reduction
PublicationIn this paper, 9,10-anthraquinone (AQ) derivative-modified glassy carbon (GC) electrodes were studied towards the electrochemical reduction of oxygen in aqueous and non-aqueous solutions. The reaction of 1-chloro-9,10-anthraquinone with aliphatic diamines was applied for the synthesis of amino-9,10-anthraquinone derivatives. The obtained AQ derivatives were grafted onto the surface of glassy carbon electrodes by electropolymerisation...
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Mechanical Properties of Twisted Carbon Nanotube Bundles with Carbon Linkers from Molecular Dynamics Simulations
PublicationThe manufacturing of high-modulus, high-strength fibers is of paramount importance for real-world, high-end applications. In this respect, carbon nanotubes represent the ideal candidates for realizing such fibers. However, their remarkable mechanical performance is difficult to bring up to the macroscale, due to the low load transfer within the fiber. A strategy to increase such load transfer is the introduction of chemical linkers...
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Effect of bio-polyol molecular weight on the structure and properties of polyurethane-polyisocyanurate (PUR-PIR) foams
PublicationThe increasing interest in polyurethane materials has raised the question of the environmental impact of these materials. For this reason, the scientists aim to find an extremely difficult balance between new material technologies and sustainable development. This work attempts to validate the possibility of replacing petrochemical polyols with previously synthesized bio-polyols and their impact on the structure and properties...
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The electrochemical studies for chitosan hydrogel membranes on glassy carbon substrates
Open Research DataThis dataset contains various electrochemical studies carried out to investigate the preconcentration of [Fe(CN)6]3- ions by chitosan hydrogel membranes coating the glassy carbon electrodes. The glassy carbon electrode (GCE, 3.0 mm diameter) was first polished with Al2O3 powder (0.3 mm) using a polishing kit from Buehler, rinsed with deionized...
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Singlet oxygen-dominated peroxymonosulfate activation by layered crednerite for organic pollutants degradation in high salinity wastewater
PublicationAdvanced oxidation processes have been widely studied for organic pollutants treatment in water, but the degradation performance of radical-dominated pathway was severely inhibited by the side reactions between the anions and radicals, especially in high salinity conditions. Here, a singlet oxygen (1O2)-dominated non-radical process was developed for organic pollutants degradation in high salinity wastewater, with layered crednerite...
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Forced degradation studies of ivabradine and in silico toxicology predictions for its new designated impurities
PublicationAll activities should aim to eliminate genotoxic impurities and/or protect the API againstdegradation. There is a necessity to monitor impurities from all classification groups,hence ivabradine forced degradation studies were performed. Ivabradine was provedto be quite durable active substance, but still new and with insufficient stability data.Increased temperature, acid, base, oxidation reagents and...
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Contribution of non-carbonate inorganic and organic alkalinity to total measured alkalinity in pore waters in marine sediments (Gulf of Gdansk, S-E Baltic Sea)
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Stiffness change of abdominal prosthesis Optomesh™ under cyclic loading
PublicationAbdominal prostheses are used in humans for abdominal wall strengthening or reconstruction. From the mechanical point of view they are membranes, so their basic mechanical property is tensile stiffness. This property is experimentally identified for a selected implant, OptomeshTM. The obtained results are described herein. Uni-axial simple and cyclic tension tests are a basis for the analysis. Both kinds of tests allowed to distinguish...
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Graph Decomposition for Memoryless Periodic Exploration
PublicationWe consider a general framework in which a memoryless robot periodically explores all the nodes of a connected anonymous graph by following local information available at each vertex. For each vertex v, the endpoints of all edges adjacent to v are assigned unique labels within the range 1 to deg (v) (the degree of v). The generic exploration strategy is implemented using a right-hand-rule transition function: after entering vertex...
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Studies on Aminoanthraquinone-Modified Glassy Carbon Electrode: Synthesis and Electrochemical Performance toward Oxygen Reduction
PublicationIn this paper, 9,10-anthraquinone (AQ) derivative-modified glassy carbon (GC) electrodes werestudied towards the electrochemical reduction of oxygen in aqueous and non-aqueous solutions. The reaction of 1-chloro-9,10-anthraquinone with aliphatic diamines was applied for the synthesis of amino-9,10-anthraquinone derivatives. The obtained AQ derivatives were grafted onto the surface of glassy carbon electrodes by electropolymerisation...
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Primary degradation of antidiabetic drugs
PublicationType 2 diabetes is a chronic disease affecting a large portion of the world population and is treated by orally administered drugs. Since these drugs are often taken in high doses and are excreted unchanged or partially metabolised many of them are nowadays detected in surface waters or wastewater treatment plants effluents. Unmetabolised antidiabetics or some of their transformation products retain their pharmacological activity,...
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New bis(azobenzocrown)s with dodecylmethylmalonyl linkers as ionophores for sodium selective potentiometric sensors
PublicationNovel biscrowns 1 and 2 were synthesized from 13-membered azobenzocrown ethers containing bromoalkylenoxy chains in para position relative to the azo group. The synthesized diester molecules are dodecylmethylmalonic acid derivatives differing by the linker length. The synthesized compounds have the potential of being used as sodium ionophores in ion-selective electrodes. They were characterized and used as ionophores in classic...
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In-situ FTIR study of reaction mechanism and chemical kinetics of a Xundian lignite during non-isothermal low temperature pyrolysis
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The motion influence on respiration rate estimation from low-resolution thermal sequences during attention focusing tasks
PublicationGlobal aging has led to a growing expectancy for creating home-based platforms for indoor monitoring of elderly people. A motivation is to provide a non-intrusive technique, which does not require special activities of a patient but allows for remote monitoring of elderly people while assisting them with their daily activities. The goal of our study was to evaluate motion performed by a person focused on a specific task and check...
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Adsorption Kinetics of Acid Dye Acid Red 88 onto Magnetic Multi‐Walled Carbon Nanotubes‐Fe3C Nanocomposite
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ISI Bilimi ve Teknigi Dergisi-Journal of Thermal Science and Technology
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Polyurethane-wood composites (PU-WC) as a method of wood waste management
PublicationIn recent years, due to the progressive environmental degradation and increase of environmental awareness, the sustainability of production systems in wood processing, the wood industry, and wood waste management is a crucial issue for European industry and society. Consequently, the problem of generating wood-like waste and the associated risks has become an increasingly noticeable challenge for science. Although various methods...
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N,N' -Bis(2-pirydyl)benzene-1,2-diamine.
PublicationN,N' -Bis(2-pirydylo)benzeno-1,2-diamina na skutek zahamowania swobodnej rotacji wokół częściowo podwójnego wiązania C-N pomiędzy resztami aminową oraz pirydynową może przyjąć dwie konformacje. Konformacja E jest stabilizowana przez cykliczne wiązanie wodorowe pomiędzy protonem grupy aminowej i atomem azotu pirydyny (N-H...N); tworzy się centrosymetryczny motyw typu pierścienia ośmioczłonowego. Druga konformacja Z charakteryzuje...
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Reaction Kinetics Mechanisms and Catalysis
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Database of speech and facial expressions recorded with optimized face motion capture settings
PublicationThe broad objective of the present research is the analysis of spoken English employing a multiplicity of modalities. An important stage of this process, discussed in the paper, is creating a database of speech accompanied with facial expressions. Recordings of speakers were made using an advanced system for capturing facial muscle motion. A brief historical outline, current applications, limitations and the ways of capturing face...
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Evaluation of reformer tubes degradation after long term operation
PublicationPurpose of this paper is to show the effect of long-term service at elevated temperatures on microstructural changes of cast steel reformer tubes made of the alloy IN-519 (24%Cr, 24%Ni, Nb). The relationship between mechanical properties and microstructure degradation is discussed. Investigations were performed on five tubes taken from ammonia reformer furnace. Tubes worked at temperature of 880C and 3,2 MPa pressure. The operation...
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Numerical solution of fractional neutron point kinetics in nuclear reactor
PublicationThis paper presents results concerning solutions of the fractional neutron point kinetics model for a nuclear reactor. Proposed model consists of a bilinear system of fractional and ordinary differential equations. Three methods to solve the model are presented and compared. The first one entails application of discrete Grünwald-Letnikov definition of the fractional derivative in the model. Second involves building an analog scheme...
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Spectroscopic, thermal and equilibrium characterization of U(VI) ions sorption on inulin in the presence of phosphates
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The effect of lithium fluoride on the thermal stability and thermoluminescence properties of borosilicate glass and glass-ceramics
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Influence of modes of thermal hardening and the subsequent cryogenic processing on structure and properties of steel 38Ni3CrMoV
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Influence of mechanochemical treatment on thermal and structural properties of silica–collagen and hydroxyapatite–collagen composites
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Sensitivity of personalized ventilation air terminal device geometry with regard to a human thermal sensation
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Burn depths evaluation based on active dynamic IR thermal imaging - A preliminary study
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Thermal Barrier Coatings for High-Temperature Performance of Nickel-Based Superalloys: A Synthetic Review
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Thermal analysis of manganese(II) complexes of general formula(Et4N)2[MnBrnCl4−n]
PublicationBadano termiczną dekompozycję związków zawierających aniony [MnBrnCl4−n]2− (n = 0-4) i kation tetraetylammonium. Wykorzystywano metody DSC i TG. Badania prowadzono w atmosferze argonu w temperaturze 173-500K (DSC)i 300-1073K (TG). Produkty dekompozycji określono za pomocą MS, FTIR, Far-FTIR i dyfraktometrii rentgenowskiej.
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Analysis of transient thermal processes for improved visualization of breast cancer using IR imaging.
PublicationPrzedstawiono analizę możliwości i ograniczeń metod termograficznych w diagnostyce nowotworów piersi. Przeanalizowane termiczne modele numeryczne piersi z nowotworem pokazują, iż zastosowanie nowej metody aktywnej termografii dynamicznej z termicznym wymuszeniem zewnętrznym, może znacząco poprawić skuteczność wykrywania nowotworów piersi we wczesnym stadium ich rozwoju . Pokazano również wyniki badania klinicznego pacjentki...
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Compensation of thermal deformations as a method of improving performance of large tiling pad thrust bearings.
PublicationTermiczne odkształcenia klocków łożyskowych wywierają niekorzystny wpływ na właściwości łozysk o dużych średnicach. W pracy przedstawiono przegląd znanych z techniki sposobów ograniczania odkształceń termicznych.Na podstawie wyników własnych badań szczegółowo omówiono efekty kompensacji odkształceń w dwóch przykładowych rozwiązaniach konstrukcyjnych: łożysku z klockami podpartymi na sprężynach śrubowych i z klockami podpartymi...
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The Influence of Laser Surface Alloying on the Thermal Fatigue Resistance of Hot Work Tool Steels
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Evaluation of Influence of the Addition Nanofillers on the Mechanical and Thermal Properties Terpolymers Ester-Ether-Amide
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Multivariate analysis of seasonal variation in the composition and thermal properties of butterfat with an emphasis on authenticity assessment
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Stability of oil‐in‐water emulsions as influenced by thermal treatment of whey protein dispersions or emulsions
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