Search results for: impedance spectroscopy
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Miniaturized impedance analyzer using AD5933
PublicationThe paper presents the analyzer allowing to measure impedance in a range of 10 ohms <|Zx|<10 Gohms in a wide frequency range from 10 mHz up to 100 kHz. The device specific features are: miniaturization, low power consumptions and the use of impedance measurement method based on DSP. These features were possible thanks to the use of newest generation of large scale integration chips: e.g. „system on a chip” microsystems (AD5933)...
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Miniaturized impedance analyzer using AD5933
PublicationThe paper presents the analyzer allowing to measure impedance in a range of 10 ohms <|Zx|<10 Gohms in a wide frequency range from 10 mHz up to 100 kHz. The device specific features are: miniaturization, low power consumptions and the use of impedance measurement method based on DSP. These features were possible thanks to the use of newest generation of large scale integration chips: e.g. „system on a chip” microsystems (AD5933)...
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Programmable dynamically changing RC model for evaluation of Dynamic EIS methods and instrumentation
PublicationThe paper concerns the RC equivalent circuit of electrochemical cell with the impedance changed during the experiment. The model was constructed using the digital potentiometers controlled by the microcontroller. This solution allows to control the model impedance by the software means. By creating adequate changes of the impedance spectrum as a time function, the different impedance measurement method can be tested to find out...
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Using A Particular Sampling Method for Impedance Measurement
PublicationThe paper presents an impedance measurement method using a particular sampling method which is an alternative to DFT calculation. The method uses a sine excitation signal and sampling response signals proportional to current flowing through and voltage across the measured impedance. The object impedance is calculated without using Fourier transform. The method was first evaluated in MATLAB by means of simulation. The method was...
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Enhanced Spectroscopic Insight into Acceptor-Modified Barium Strontium Titanate Thin Films Deposited via the Sol–Gel Method
PublicationIn the present paper, composite thin films of barium strontium titanate (BaxSr1−xTiO3) with an acceptor modifier (magnesium oxide—MgO) were deposited on metal substrates (stainless steel type) using the sol–gel method. The composite thin films feature BaxSr1−xTiO3 ferroelectric solid solution as the matrix and MgO linear dielectric as the reinforcement, with MgO concentrations ranging from 1 to 5 mol%. Following thermal treatment...
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Modelling of dielectric properties of BiNbO4-based microwave ceramics
PublicationIn the present paper results of the studies devoted to computer simulations of dielectric response of electroceramics in a frequency domain as well as analysis of the experimental data are given. As an object of investigations BiNbO4-based microwave ceramics was taken. Simulations of the hypothetical impedance response of the ceramic system were performed under assumption of the brick-layer model. A strategy for analysis and modelling...
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Analysis of the Possibility of Using New Types of Protective Coatings and Abrasion-Resistant Linings under the Operating Conditions of the Spiral Classifier at KGHM Polska Miedź S.A. Ore Concentration Plant
PublicationA study was carried out to select the appropriate coatings for corrosion protection of the spiral classifier working at KGHM Polska Miedź S.A. Ore Concentration Plant. The abrasion resistance of selected protective coatings and wear-resistant linings was investigated using a DT-523 rotary abrasion tester with Taber CS-10 rubber abrasive discs. The average weight loss of the coatings after a cycle of 2000 revolutions was determined....
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Recycled rubber wastes-based polymer composites with flame retardancy and electrical conductivity: Rational design, modeling and optimization
PublicationPolymer recycling techniques experience a maturity period of design and application. Rubbers comprise a high proportion of polymer wastes, highly flammable and impossible to re-melt. Polymer composites based on ground tire rubber (GTR) and ethylene-vinyl acetate copolymer (EVA) containing carbon black (CB) (1–50 phr), with variable EVA/GTR weight composition (10/90, 25/75, 50/50, 75/25 and 90/10), and processing temperature (Low:...
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A complete impedance analysis of electrochemical cells used as energy sources
PublicationA comprehensive description of impedance ofelectrochemical systems has been presented, along withthe assumptions of the method used. In this method, amultisinusoidal current excitation signal is used. Thechanges of potential of both the electrodes and thepotential difference between these electrodes are allregistered simultaneously as a function of time. Theproposed method offers the possibility of separatelydetermining the instantaneous...
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Platform Supporting the Esophageal Impedance Analysis
PublicationThe esophageal pH-impedance examination is one of the most popular diagnostic methods for identifying the upper gastrointestinal tract’s diseases. Inconclusive test evaluation criteria makes it difficult to state the definite diagnosis. In this paper, the computer platform supporting the research and teaching process in the area of pH-impedance analysis is presented. Users, having a variety of mathematical and statistical methods...
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Uncertainty estimation of loop impedance measurement determined by the vector method
PublicationThis article presents a detailed analysis of uncertainty estimation of loop impedance measurement determined by the vector method. The analysis includes the following estimates: resistance variance, voltage variance and time measurement variance. This paper presents a methodology for estimating the combined standard uncertainty of loop impedance by the vector method. The vector method allows to determine loop impedance based on...
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Ellipse-fitting algorithm implementation in the impedance measurement system based on DAQ card with FPGA
PublicationThe paper presents an implementation of the ellipse-fitting algorithm in the impedance measurement system based on DAQ card equipped with FPGA chip. The method implementation was tested by simulation means as well as experimentally in the designed and presented measurement system. Finally, the limit values of sampling parameters which assures satisfying accuracy were given.
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Zaawansowane Metody Pomiarowe i Diagnostyczne 2022/2023
e-Learning Courses{mlang en} 1. Introduction/Guide for the use of the International System of Units2. Rules and style conventions for expressing values of quantities.3. The role of measurement uncertainty in conformity assessment. 4. Probabilistic model for measurement processes, estimation theory5. Analog-digital conversion methods6. Selected structures of classical analog-digital converters7. New techniques of analog-digital conversion: sigma-delta...
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Zaawansowane Metody Pomiarowe i Diagnostyczne 2023/2024
e-Learning Courses{mlang en} 1. Introduction/Guide for the use of the International System of Units2. Rules and style conventions for expressing values of quantities.3. The role of measurement uncertainty in conformity assessment. 4. Probabilistic model for measurement processes, estimation theory5. Analog-digital conversion methods6. Selected structures of classical analog-digital converters7. New techniques of analog-digital conversion: sigma-delta...
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Assessment of organic coating degradation via local impedance imaging
PublicationThe paper presents a new approach to organic coating condition evaluation at micrometer scale using localized impedance measurements. It is based on atomic force microscopy (AFM) in contact mode. Impedance is measured between conductive AFM tip and metal substrate covered with organic coating. A single-frequency voltage perturbation signal is applied between the electrodes and current response signal is registered. As the tip is...
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A method of measuring RLC components for microcontroller systems
PublicationA new method of measuring RLC components for microcontroller systems dedicated to compact smart impedance sensors based on a direct sensor-microcontroller interface is presented. In the method this direct interface composed of a reference resistor connected in series with the tested sensor impedance is stimulated by a square wave generated by the microcontroller, and then its voltage response is sampled by an internal ADC of the...
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A family of new generation miniaturized impedance analyzers for technical object diagnostics
PublicationThe paper presents the family of three analyzers allowing to measure impedance in range of 10 ohm<|Zx|<10 Gohm in a wide frequency range from 10 mHz up to 100 kHz. The most important features of the analyzers family are: miniaturization, low power consumption, low production cost, telemetric controlling and the use of impedance measurement method based on digital signal processing DSP. The miniaturization and other above mentioned...
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Determination of time dependence of coated metal electrical and electrochemical parameters during exposure using principal component analysis
PublicationThe use of the principal component analysis (PCA) permits the complex and quantitative analysis of the time dependence of electrical and electrochemical parameters of coated metal obtained by fitting impedance data. So far, changes in electrical and electrochemical parameters during exposure were analyzed independently. In this way, some of the information contained in the relationship between changes in parameters over time are...
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Electrical Propterties of Solution Mixtures for Bath Supervision in Ambient Assisted Living
PublicationImpedance properties of bath solution are compared. Any ingredient such as soap, shampoo or bathing salt changes bath-solution’s electrical properties eg. impedance. We have measured and analysed influence of typical bathing ingredients on electrical properties of the solution. We investigate impedance changes over frequency range from 100Hz tu 100kHz as it is most applicable for person detection. Electrical properties of bath...
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Selected problems of earth fault loop impedance testing in circuits fed from UPS
PublicationIn the paper a principle of earth fault loop impedance testing in low voltage systems has been presented. Selected factors, influencing accuracy of the testing, are indicated. A structure of UPS of VFI-type and the problem of impedance testing in circuits with such type of UPS are discussed.
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Influence of vacuum sublimation deposited metal layer thickness on metrological parameters of the amperometric gas sensor with Nafion membrane
PublicationThe paper presents the results of investigation on an influence of vacuum sublimation deposited platinum layer thickness on the signal, sensitivity and response time of a prototype of sulphur dioxide sensor with Nafion membrane. The working electrode was made by vacuum sublimation deposition of platinum on a surface of Nafion membrane. Pt layers deposited changed an initial structure of Nafion membrane and that phenomenon was utilized...
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Fault Loop Impedance Measurement in Circuits Fed by UPS and Principle of Safety Protection
PublicationThis paper indicates a significant problem of uncertainty of fault loop impedance (FLI) measurement in circuits powered from uninterruptible power supply (UPS) (double-conversion AC-DC-AC). The correctly determined value of this impedance, related to the short-circuit current disconnection time and to the reference value, is one of the most important elements that determines the approval of an electrical installation and its receivers...
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Nonlinear Impedance as Possible Result of Ion-Polaron Interaction in Cu2O-Al2O3-SiO2 Glass
PublicationNonlinear a.c. impedance measurements were performed in Cu2O-Al2O3-SiO2 glass in wide frequency range. The obtained results shows that a large nonlinearity in the impedance signal is observed at moderate electric fields of an order 1V/mm. The contents of the third harmonics reaches about 10% and strongly depends on temperature and frequency. The investigated glass exhibits mixed electronic-ionic conductivity. Electronic conduction...
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Nonlinear impedance in oxide glasses containing single and mixed alkali ions
PublicationThe aim of the present was to find more clues on the nonlinearities in impedance of oxide glasses. The first family of researched glasses has a composition of FeO-P2O5-Na2O. Oxide glasses containing iron and alkali are well known for a very low alkali ion mobility and may be considered purely polaron conducting. These glasses show no detectable nonlinearities in the impedance spectra. The second was a family of ionic conducting...
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Investigation on accelerated impedance spectrum measurement method with multisine signal stimulation
PublicationThe paper presents an investigation on the accelerated impedance spectrum measurement method, oriented at parameter identification of technical objects modelled by a linear equivalent circuit, e.g. anticorrosion coatings.The method is based on multisine signal stimulation of an object and response analysis by triangle window filterbanks.It has several advantages, as compared with conventional point-by-point spectrum measurement....
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Adaptive estimation of the transformer stray capacitances for DC–DC converter modelling
PublicationNew low cost and accurate estimation method of transformer stray capacitances for wide band DC–DC converter modelling and design is proposed. The Wiener filter (WF) method is applied to estimate the transformer impedance – referred to the selected transformer winding configurations. Laboratory tests are used to adapt the filter, that is to find optimal impedance which minimises mean square error between measured, noise perturbed...
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Electronic conductivity in the SiO2-PbO-Fe2O3 glass containing magnetic nanostructures
PublicationThe linear impedance spectra of iron–silicate–lead glass samples were measured in the frequency range from 1 MHz to 1 MHz and in the temperature range from 153 K to 423 K. The structure was investigated by means of XRD and atomic force microscopy. Local electrical and magnetic properties of the samples were tested with the aid of electrostatic force microscopy (EFM) and magnetic force microscopy (MFM). The obtained results show...
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Optimal configuration of an electrode array for measuring ventricles' contraction
PublicationAn influence of an electrode-array configuration on an impedance signal composition for a fixed spatial distribution of its sources is examined in the paper. The Finite Element Method and Geselowitz relationship were used for examining three different electrode-arrays. A sensitivity approach was used to evaluate each configuration assuming that localization of the signal source is known. A conductivity change, thus the source of...
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Monitoring of CRT by means of impedance multiple measurements - simulation studies
PublicationCardiac resynchronization therapy (CRT) is a very promising treatment for patients with congestive heart failure. An Impedance Cardiography (ICG) is used for evaluation of heart mechanical activity. A simulation study with the use of a FEM model was performed. The developed realistic model of the thorax, based on CT data obtained from examination of a 68-year-old man, consisted of 212 000 tetrahedral elements. Different configurations...
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Analysis of thoracic regional impedance changes using PCA approach
PublicationA multichannel impedance and one lead electrocardiographic recording system has been developed. The impedance measurement unit is built using a four-electrode technique. It consists of a sinusoidal, 40 kHz, current source and five measurement channels. Circumferential current electrodes have been located at a neck and an abdomen. Voltagemeasurement disk electrodes formed five two-electrode measurement ports. The impedance change...
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Optimization of the Relative Humidity of Reactant Gases in Hydrogen Fuel Cells Using Dynamic Impedance Measurements
PublicationWater management is a key factor affecting the efficiency of proton exchange membrane fuel cells (PEMFCs). The currently used monitoring methods of PEMFCs provide limited information about which processes or components that humidity has a significant impact upon. Herein, we propose the use of a novel approach of impedance measurements using a multi-sinusoidal perturbation signal, which enables impedance measurements under dynamic...
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Implementation and Validation of Multisinusoidal, Fast Impedance Measurements in Atomic Force Microscope Contact Mode.
PublicationThis study presents a novel approach to impedance measurements. The methodology discussed is limited to contact in the sample-probe system under ambient conditions without the presence of electrolyte. Comparison with results of direct and alternating current measurements for well-defined metallic surfaces are made. In spite of idealization related to the type of contact examined, the proposed technique provides an improvement of...
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Impulse Impedance Measurements of Lightning Protection Earthings
PublicationLightning protection earthing systems should be tested at currents with time parameters similar to those of lightnings. A method and definition of a measured value of impulse impedance are introduced. The impulse impedance was determined by a quotient of voltage drop on the tested earthing to a value of current in measure circuit. The usefulness of the impulse method for lightning protection evaluation is tested on radio base stations...
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Multifrequency Nanoscale Impedance Microscopy (m-NIM): A novel approach towards detection of selective and subtle modifications on the surface of polycrystalline boron-doped diamond electrodes
PublicationIn this paper, we describe the modification of Nanoscale Impedance Microscopy (NIM), namely, a combination of contact-mode atomic force microscopy with local impedance measurements. The postulated approach is based on the application of multifrequency voltage perturbation instead of standard frequency-by-frequency analysis, which among others offers more time-efficient and accurate determination of the resultant impedance spectra...
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Evaluation of applicability of classic methods of a fault loop impedance measurement to circuits with residual current devices
PublicationMeasurement of fault loop impedance in low voltage grids and systems is in most cases performed to verify the effectiveness of protection against electric shock by automatic disconnection of supply. For the sake of measurement accuracy, it is advisable to perform it using large current. Unfortunately, in circuits with residual current devices which are very widely used nowadays, a large measurement current may trigger those devices...
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Impedance monitoring of fuel cell stacks
PublicationThis paper presents an innovative, electrochemical impedance method for monitoring of electrochemical behaviour of a multi-cell, direct methanol fuel cell (DMFC) device. This method not only provides classical voltage changes at successive cells but also allows their detailed impedance behaviour to be presented. Impedance characteristics of individual cells within a fuel cell stack (depending on actual operating conditions) are...
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Scalable Measurement System for Multiple Impedance Gas Sensors
PublicationAuthor proposes scalable architecture of the measurement system for gas sensor with impedance dependance of the gas concentration. The main part of the system is a single-board impedance analyser. The number of analysers working in parallel can be configured according to specific application. The system is controlled by a single computer which organises the measurement cycle and store the acquired measurement data. The system is...
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A telemedical and an outpatient thoracic impedance measurements - a validation algorithm of the electrodes placement
PublicationThis paper presents the algorithm for validation of electrodes locations for the thoracic impedance measurements. In particular the presented algorithm was designed to perform the telemetric sleep apnea monitoring. One of the problems, during the clinical tests of a developed device, was to preserve the repeatability of measurements. It strongly depended on the appropriate electrodes placement on the examined person’s thorax. It...
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Application of different modes of nanoscale impedance microscopy in materials research
PublicationIn recent years, there is noticeable interest in application of various types of scanning probe microscopy in material science research. One of them is contact atomic force microscopy combined with local impedance measurements, known as nanoscale impedance microscopy. Literature references present its application in investigations of new materials, microelectronics diagnostics, or research of protective coatings performance. In...
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EM-Driven Multi-Objective Design of Impedance Transformers By Pareto Ranking Bisection Algorithm
PublicationIn the paper, the problem of fast multi-objective optimization of compact impedance matching transformers is addressed by utilizing a novel Pareto ranking bisection algorithm. It approximates the Pareto front by dividing line segments connecting the designs found in the previous iterations, and refining the obtained candidate solutions by means of poll-type search involving Pareto ranking. The final Pareto set is obtained using...
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Impedance monitoring of corrosion degradation of plasma electrolytic oxidation coatings (PEO) on magnesium alloy
PublicationImpedance technique based on continuous multisinusoidal current perturbation was used to explain degradation process of plasma electrolytic oxidation coatings (PEO) on magnesium alloy. An obtained impedance spectrum was fitted by electrical equivalent circuit to describe properties of conversion layer on magnesium alloy. Additionally, galvanostatic mode maintained during experiment, with DC current equal to zero, allowed to achieve...
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Comparison of Impedance-Source Networks for Two and Multilevel Buck–Boost Inverter Applications
Publicationmpedance-source networks are an increasingly popular solution in power converter applications, especially in single-stage buck-boost power conversion to avoid additional front-end dc-dc power converters. In the survey papers published, no analytical comparisons of different topologies have been described, which makes it difficult to choose the best option. Thus, the aim of this paper is to present a comprehensive analytical comparison...
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Design optimization of novel compact circular polarization antenna
PublicationThe paper describes a structure and a design optimization procedure of a miniaturized circular polarization antenna with elliptical ground plane slots and feed line with stepped-impedance stubs. Constrained optimization of all antenna parameters is executed in order to explicitly reduce the antenna size while maintaining required impedance axial ratio bandwidth of 5 GHz to 7 GHz at the same time. The size of the optimized antenna...
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Hybrid Method Analysis of Unshielded Guiding Structures
PublicationA combination of mode matching, finite element methods and generalized impedance matrix is presented in a context of propagation problems for open guiding structures. The computational domain is divided into two regions: the first one is a circular cylinder containing whole guiding structure and the second one surrounds this artificial cylinder. The impedance matrix is calculated with the use of finite element method in the first...
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An Application Supporting Gastroesophageal Multichannel Intraluminal Impedance-pH Analysis
PublicationDue to a significant rise in the number of patients diagnosed with diseases of the upper gastrointestinal tract and the high cost of treatment, there is a need to further research on one of the most popular diagnostic tests used in this case – esophageal Multichannel Intraluminal Impedance and pH measurement. This may lead to finding new diagnostically relevant information, used to quicken and improve the diagnostic procedure....
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Electromagnetic plane wave scattering from a cylindrical object with an arbitrary cross section using a hybrid technique
PublicationA hybrid technique combining finite-element and mode-matching methods for the analysis of scattering problems in open and closed areas is presented. The main idea of the analysis is based on the utilization of the finite-element method to calculate the post impedance matrix and combine it with external excitation. The discrete analysis, which is the most time- and memory-consuming, is limited here only to the close proximity of...
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Excitation of Circularly Polarized Wave via Single-Feed Metasurface-Integrated Compact Antenna for Internet of Things
PublicationA compact circularly polarized (CP) quasi-omnidirectional antenna is introduced for internet of things (IoT). The structure consists of two components implemented on FR-4 substrates, and sep-arated by an air gap: one printed with a rectangular patch fed through a matching network, and another with a metasurface and a ground plane. Two different methods for impedance matching are employed. An equivalent circuit model of the antenna...
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A Wearable System Developed to Monitor People Suffering from Vasovagal Syncope
PublicationA wearable system for monitoring non-invasively signals invaluable when examining person suffering from vasovagal syncope is presented in the paper. Following signals are continuously recorded: electrocardiogram, photopletysmogram, impedance cardiogram and electrodermal resistance.
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Design and optimization of a novel compact broadband linearly/circularly polarized wide-slot antenna for WLAN and Wi-MAX applications
PublicationA novel topologically modified structure of a compact low profile wide-slot antenna for broadband applications is presented. The antenna comprises a modified E-shaped slot with unequal arm lengths in the ground plane, and a parasitic quasi-rectangular loop placed coplanar with the feedline. For exciting orthogonal modes with equal amplitude, a single-point feeding technique with an asymmetrical geometry of the coplanar waveguide...
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Non-isolated resonant quasi-Z-source network DC–DC converter
PublicationA novel non-isolated resonant quasi-impedance (quasi-Z)-source network DC–DC converter is proposed. The resonant impedance source network is derived from the quasi-Z-source network by including the autotransformer-based resonant cell instead of the second inductor of the quasi-Z-network. The leakage inductance of the autotransformer and two resonant capacitors connected in series with the autotransformer windings constitute a high-frequency...