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Search results for: TEM
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High-temperature kinetics study of 430L steel powder oxidized in air at 600–850 °C
PublicationThe 430L stainless steel powder with a mean particle size of 95 μm was studied to determine its high-temperature oxidation properties. Continuous thermogravimetric measurements were carried out for 100 h in air at temperatures in the range of 600–850 °C. Even though a considerable amount of Cr (up to ˜5 wt.% Cr) inside the grains was depleted – especially inside small grains – no breakaway oxidation was observed. This indicates...
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High temperature oxidation behavior of SUS430 SOFC interconnects with Mn-Co spinel coating in air
PublicationIn this study, SUS430 alloy is evaluated for its high temperature corrosion properties as a possible material for interconnects of solid oxide fuel cells (SOFCs). Samples are coated with Mn-Co by commercial physical vapor deposition (PVD) process and oxidized in air for 1250 h at 800 °C. A dense cubic Mn-Co-Fe spinel layer is formed on the surface, showing great effect on corrosion reduction compared with the samples without coating....
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Deposition and Electrical and Structural Properties of La0.6Sr0.4CoO3 Thin Films for Application in High-Temperature Electrochemical Cells
PublicationLow-temperature deposition of electroceramic thin films allows the construction of new devices and their integration with existing large-scale fabrication methods. Developing a suitable low-cost deposition method is important to further advance the development of microdevices. In this work, we deposited a 1-lm-thick La0.6Sr0.4CoO3d (LSC) perovskite with high electrical conductivity on sapphire substrates at 400C and analyzed its...
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Identification of damages in the inlet air duct of a diesel engine based on exhaust gas temperature measurements
PublicationThe temperature of the exhaust gas of a diesel piston engine, measured in the characteristic control sections of its thermo-flow system, can be a valuable source of diagnostic information about the technical condition of the elements limiting the working spaces thus separated, including the turbocharging system, but also its fuel supply system and replacement of the medium. In standard marine engine measurement systems equipped...
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High Temperature Corrosion Evaluation of Porous Hastelloy X Alloy in Air and Humidified Hydrogen Atmospheres
PublicationIn this work a commercially available porous Hastelloy X alloy is characterized in terms of high temperature corrosion resistance. The alloy was oxidized in the temperature range from 500C to 900C in air and humidified hydrogen for 100 hours. Corrosion rates and porosity changes were measured. Microstructural characterization was performed using X-ray diffractometry and scanning electron microscopy. Results show that porous alloys...
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Low temperature growth of diamond films on optical fibers using Linear Antenna CVD system
PublicationIt is not trivial to achieve a good quality diamond-coated fibre interface due to a large difference in the properties and composition of the diamond films (or use coating even) and the optical fibre material, i.e. fused silica. One of the biggest problems is the high temperature during the deposition which influences the optical fibre or optical fibre sensor structure (e.g. long-period gratings (LPG)). The greatest advantage of...
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Influence of High Temperature Oxidation on Hydrogen Absorption and Degradation of Zircaloy-2 and Zr 700 Alloys
PublicationThe present research was aimed at determining the effects of the oxide layers on hydrogen absorption, microstructure and mechanical properties of the Zircaloy- 2 and Zr 702 alloys. The oxidation was made at 350 °C, 700 °C and 900 °C for 10 to 30 min in laboratory air, followed by hydrogen cathodic charging for 72 h and annealing at 400 °C for 4 h. The slow strain rate tests were carried out on oxidized, charged and annealed specimens. The...
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Study of pH and temperature effect on lipophilicity of catechol-containing antioxidants by reversed phase liquid chromatography
PublicationLipophilicity of selected antioxidant phytochemicals, including flavonoids, phenolic acids and xanthonoids, was determined by reversed phase high performance liquid chromatography with UV detection (RP-HPLC-UV). The analyses run at different temperature and pH conditions in isocratic mode suggested that lipophilicity as distribution coefficient (logD) between aqueous and organic phase decreases with increasing temperature. For...
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High-Temperature Oxidation of Heavy Boron-Doped Diamond Electrodes: Microstructural and Electrochemical Performance Modification
PublicationIn this work, we reveal in detail the effects of high-temperature treatment in air at 600 °C on the microstructure as well as the physico-chemical and electrochemical properties of boron-doped diamond (BDD) electrodes. The thermal treatment of freshly grown BDD electrodes was applied, resulting in permanent structural modifications of surface depending on the exposure time. High temperature affects material corrosion, inducing...
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Influence of CeO2 and TiO2 Particles on Physicochemical Properties of Composite Nickel Coatings Electrodeposited at Ambient Temperature
PublicationThe Ni-TiO2 and Ni-CeO2 composite coatings with varying hydrophilic/hydrophobic characteristics were fabricated by the electrodeposition method from a tartrate electrolyte at ambient temperature. To meet the requirements of tight regulation by the European Chemicals Agency classifying H3BO3 as a substance of very high concern, Rochelle salt was utilized as a buffer solution instead. The novelty of this study was to implement a...
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Influence of wall temperature on heat transfer coefficient during R 22 boiling in microfin tube
PublicationPrzedstawiono wyniki badań współczynnika przejmowania ciepła i spadku ciśnienia podczas wrzenia czynnika R 22 w rurze nisko żebrowanej. Opisano stanowisko i procedurę badawczą. Zaobserwowano spadek współczynnika przejmowania. Opisano stanowisko i procedurę badawczą. Zaobserwowano spadek współczynnika przejmowania ciepła wraz ze wzrostem temperatury ścianki rury.
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Surface morphology of PrBa2Cu3O7-ë single crystals after the long lasting high temperature reduction. .
PublicationZaprezentowano wyniki szczegółowej analizy powierzchni kryształów poddanych długotrwałej redukcji wysokotemperaturowej. Badania za pomocą skaningowej mikroskopii (SEM) wykazały obecność niestabilnych strukturalnie krystalitów powstałych w wyniku rozpadu powierzchni kryształów. Zanikanie zaindukowanego przy pomocy obróbki wysokotemperaturowej nadprzewodnictwa może być spowodowane migracją defektów podsieci Pr-Ba z wnętrza...
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Experimental study of the fuel jet combustion in high temperature and low oxygen content exhaust gases
PublicationPrzeprowadzono badania eksperymentalne spalania pojedynczego strumienia paliwa gazowego. Paliwo podawano współosiowo do generowanych przez konwencjonalny palnik gazowy spalin o wysokiej temperaturze i niskiej zawartości tlenu. Badano wpływ zawartości tlenu w utleniaczu na widzialność płomienia i skład produktów spalania.
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Effect of the Cooling Time in Annealing at 350°C on the Phase Transformation Temperatures of a Ni<sub>5</sub><sub>5</sub>Ti<sub>4</sub><sub>5</sub> wt. Alloy
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ZASTOSOWANIE STATYSTYKI F ROZKŁADU FISHERA-SNEDECORA DO OCENY ISTOTNOŚCI WPŁYWU ZMIAN STOPNIA KOMPRESJI SILNIKA O ZS NA ŚREDNIĄ WARTOŚĆ MIĘDZYSZCZYTOWĄ TEMPERATURY SPALIN WYLOTOWYCH
PublicationW artykule omówiono wpływ zmian stopnia kompresji na parametry pracy silnika o ZS, m.in. na temperaturę spalin wylotowych. Przedstawiono budowę stanowiska laboratoryjnego, na którym przeprowadzono badania eksperymentalne. Scharakteryzowano, w jaki sposób w istniejącym silniku wprowadzano faktyczne zmiany stopnia kompresji. Zaprezentowano program badań eksperymentalnych uwzględniający dostępne stanowisko badawcze i jego możliwości...
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Testing an evaporator operation with a bifurcation manifold, condenser temperature 20 and evaporator temperature 85
Open Research DataThe experiment was conducted to test the evaporator operation. The heat exchanger was equipped with minigeometry (set of 50 parallel minichannels or single minigap). The studies were conducted for various mass flow rate of the working fluid and for various temperatures at the inlet of the evaporator. Accurate information about the test rig, the parameters...
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Testing an evaporator operation with a trapezoidal manifold, condenser temperature 90 and evaporator temperature 90
Open Research DataThe experiment was conducted to test the evaporator operation. The heat exchanger was equipped with minigeometry (set of 50 parallel minichannels or single minigap). The studies were conducted for various mass flow rate of the working fluid and for various temperatures at the inlet of the evaporator. Accurate information about the test rig, the parameters...
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Testing an evaporator operation with a bifurcation manifold, condenser temperature 20 and evaporator temperature 70
Open Research DataThe experiment was conducted to test the evaporator operation. The heat exchanger was equipped with minigeometry (set of 50 parallel minichannels or single minigap). The studies were conducted for various mass flow rate of the working fluid and for various temperatures at the inlet of the evaporator. Accurate information about the test rig, the parameters...
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Testing an evaporator operation with a rectangular manifold, condenser temperature 30 and evaporator temperature 90
Open Research DataThe experiment was conducted to test the evaporator operation. The heat exchanger was equipped with minigeometry (set of 50 parallel minichannels or single minigap). The studies were conducted for various mass flow rate of the working fluid and for various temperatures at the inlet of the evaporator. Accurate information about the test rig, the parameters...
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Testing an evaporator operation with a trapezoidal manifold, condenser temperature 70 and evaporator temperature 60
Open Research DataThe experiment was conducted to test the evaporator operation. The heat exchanger was equipped with minigeometry (set of 50 parallel minichannels or single minigap). The studies were conducted for various mass flow rate of the working fluid and for various temperatures at the inlet of the evaporator. Accurate information about the test rig, the parameters...
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Testing an evaporator operation with a bifurcation manifold, condenser temperature 20 and evaporator temperature 95
Open Research DataThe experiment was conducted to test the evaporator operation. The heat exchanger was equipped with minigeometry (set of 50 parallel minichannels or single minigap). The studies were conducted for various mass flow rate of the working fluid and for various temperatures at the inlet of the evaporator. Accurate information about the test rig, the parameters...
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Testing an evaporator operation with a bifurcation manifold, condenser temperature 20 and evaporator temperature 90
Open Research DataThe experiment was conducted to test the evaporator operation. The heat exchanger was equipped with minigeometry (set of 50 parallel minichannels or single minigap). The studies were conducted for various mass flow rate of the working fluid and for various temperatures at the inlet of the evaporator. Accurate information about the test rig, the parameters...
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Application of fiber optic sensors using Machine Learning algorithms for temperature measurement of lithium-ion batteries
PublicationOptical fiber sensorsusing low-coherence interferometry require processing ofthe output spectrum or interferogramto quickly and accurately determine the instantaneous value of the measured quantity, such as temperature.Methods based on machine learning are a good candidate for this application. The application of four such methods in an optical fiber temperature sensoris demonstrated.Using aZnO-coated...
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Biochemical assays of intensified methane content in biogas from low-temperature processing of waste activated sludge
PublicationAnaerobic digestion (AD) is implemented as an important ‘waste to energy’ approach for converting organic-rich byproducts such as sewage sludge into biogas and nutrient-rich digestate. Sewage sludge consists of primary sludge and waste activated sludge (WAS), and low biodegradability of WAS limits methane production. This study presents the influence of the low-temperature pretreatment (LT-PT) of WAS on the efficiency of AD. Different...
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High-Temperature Tensile Behaviour of GTAW Joints of P92 Steel and Alloy 617 for Two Different Fillers
PublicationThis study explores the high-temperature (HT) tensile rupture characteristics of a dissimilar gas-tungsten-arc-welded (GTAW) joint between P92 steel and Alloy 617, fabricated using ER62SB9 and ERNiCrCoMo-1 fillers. The high-temperature tensile tests were performed at elevated temperatures of 550 ◦C and 650 ◦C. An optical microscope (OM) and a field emission scanning electron microscope (FESEM) were utilized to characterize the...
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Effects of La0.8Sr0.2MnO3 and Ag electrodes on bismuth-oxide-based low-temperature solid electrolyte oxygen generators
PublicationIn this study, La0.8Sr0.2MnO3 (LSM) was used as the ceramic electrode in a (Bi1.50Y0.50)0.98Zr0.04O3+δ (BYO)-based solid electrolyte oxygen generator (SEOG) and its performance was compared with that of a previously studied high-fire Ag electrode. Among La0.6Sr0.4Co0.2Fe0.8O3, LaNi0.6Fe0.4O3, Cu1.4Mn1.6O4, and LSM materials, only LSM materials did not trigger any chemical reaction or interdiffusion with BYO at temperatures up to...
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Prediction of cast-in-place concrete strength of the extradosed bridge deck based on temperature monitoring and numerical simulations
PublicationThe work is devoted to the implementation of a monitoring system for high performance concrete embedded in the span of an extradosed bridge deck using a modified maturity method augmented by numerical simulations conducted by the authors’ FEM code. The paper presents all research stages of bridge construction and considers the conclusions drawn from the results of laboratory tests, field measurements, and numerical calculations....
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Investigation of the 0.4C-35Cr-45Ni-Nb Alloy after Service in High-Temperature Steam and Hydrocarbons Environment
PublicationThe paper presents the results of investigation of the 0.4C-35Cr-45Ni-Nb alloy, which operated in the cracked hydrocarbon feeds and dilution steam at 1125 C. The material originated from the pyrolytic furnace coil tubes, of which internal walls were in contact with the aforementioned medium, whereas the external walls were in contact with the flue gases. The examination included metallographic and mechanical tests on the material...
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Low temperature growth of carbon nanotubes from methane catalytic decomposition over nickel supported on a zeolite
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NICKEL-BASED LAYERED PEROVSKITE CATHODE MATERIALS FOR APPLICATION IN INTERMEDIATE-TEMPERATURE SOLID OXIDE FUEL CELLS
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<title>Correction of fiber optic ion sensor readings using a fiber optic temperature sensor</title>
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Analysis of the selection of low temperature medium for a turbine power plant using ocean thermal energy (OTEC)
PublicationThe paper presents the results and conclusions of numerical calculations modelled in the EES program of a closed OTEC cycle. The following mediums were analysed: ammonia, R32, R41, R404a, R407c, R410a, R423a, R500, R502, R507a and R114, R152a, R234fa, R600, R1234yf, R1234ze. Analogous assumptions were adopted as in the ORC cycle with heat regeneration for dry refrigerants without regeneration for wet refrigerants. Each of them...
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Influence of low-temperature physical hardening on stiffness and tensile strength of asphalt concrete and stone mastic asphalt
PublicationThis paper presents laboratory testing of stiffness modulus and indirect tensile strength of three asphalt concrete (AC) and three stone mastic asphalt (SMA) mixes after isothermal storage at temperature of -20oC, at different time intervals up to 16 days. The tests under repeated dynamic loading showed physical hardening of all tested mixes which was manifested by an evident increase of their stiffness moduli after isothermal...
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Automatic Adjustment of Integration Time in the NIR Camera for Calibrated Temperature Measurement during Inductive Heating Processes
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New devices to capture the temperature effect under dynamic compression and impact perforation of polymers, application to PMMA
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The Impact of Experimental Temperature and Water Level Manipulation on Carbon Dioxide Release in a Poor Fen in Northern Poland
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Mechanical response of 6061-T6 aluminium alloy subjected to dynamic testing at low temperature: Experiment and modelling
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Effect of high temperature exposure on the fatigue damage development of X10CrMoVNb9-1 steel for power plant pipes
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Effect of plasma nitriding process on the fatigue and high temperature corrosion resistance of Inconel 740H nickel alloy
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A Novel Method for High Temperature Fatigue Testing of Nickel Superalloy Turbine Blades with Additional NDT Diagnostics
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MITOGEN-ACTIVATED PROTEIN KINASE 4 impacts leaf development, temperature, and stomatal movement in hybrid aspen
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Effect of temperature and ionic strength on volumetric and acoustic properties of solutions of urea alkil derivatives in aqueous NaCl
PublicationThe present work was undertaken to study volumetric and acoustic properties for diluted solutions of tetramethylurea in pure water and for urea, n-propylurea, n-butylurea and tetramethylurea in 0.5 or 1 moldm3 aqueous solutions of sodium chloride. This paper presents measured values of densities and sound velocities at T = (288.15, 298.15 and 308.15) K. From these data the apparent molar volumes, , adiabatic compressibilities,...
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On the tendency of temperature and electric field dependences of interface recombination in P3HT:PCBM organic bulk heterojunction solar cells
PublicationWe demonstrate theoretical explanation of the temperature and electric field dependences of recombination coefficients in an organic P3HT:PCBM bulk heterojunction solar cell. Based onthe model of interface recombination, two analytical formulas describing the relative ratio of the interface (γI ) to the Langevin (γL) recombination coefficients have been derived. Our analysis indicates that the sign of parameters φT and φF determines...
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Short-term changes in thickness and temperature of the active layer in summer in the Kaffiøyra region, NW Spitsbergen, Svalbard
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Experiments and Numerical Simulations of the Annealing Temperature Influence on the Residual Stresses Level in S700MC Steel Welded Elements
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Application possibilities of the low-temperature repairs on creep-resistance turbine components from material GX23CrMoV12-1
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Temperature-Based Prediction of Joint Hardness in TIG Welding of Inconel 600, 625 and 718 Nickel Superalloys
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Time window based features extraction from temperature modulated gas sensors for prediction of ammonia concentration
PublicationElectronic gas recognition systems, in literature commonly referred as electronic noses, enable the recognition of a type and a concentration of various volatile compounds. Typical electronic gas-analyzing device consists of four main elements, namely, gas delivery subsystem, an array of gas sensors, data acquisition and power supply circuits and data analysis software. The commercially available metal-oxide TGS sensors are widely...
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DETERMINING THE TIME CONSTANT USING TWO METHODS AND DEFINING THE THERMOCOUPLE RESPONSE TO SINE EXCITATION OF GAS TEMPERATURE
PublicationThis paper describes the two methods of determining the time constant of type K thermocouple, for two construction solutions: the exposed weld and the mantle fillet weld. This is an important parameter indicating the response time of the thermocouple on the recorded signal. The first method consists of determining the value of τ in the way of numerical simulation of heat exchange between the thermocouple and the current of gas...
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Characterizing surface and air temperature in the Baltic Sea coastal area using remote sensing techniques and GIS
PublicationEstimation of surface temperature using multispectral imagery retrieved from satellite sensors constitutes several problems in terms of accuracy, accessibility, quality and evaluation. In order to obtain accurate results, currently utilized methods rely on removing atmospheric fluctuations in separate spectral windows, applying atmospheric corrections or utilizing additional information related to atmosphere or surface characteristics...