Filters
total: 466
filtered: 406
Search results for: Compliance with Restrictions
-
Acylic congener of cucurbituril: synthesis and recognition properties.
PublicationZaprezentowano syntezę analogów acyklicznych cucurbiturilu oraz ich zdolności do kompleksowania wybranych 16 amin, dioli, kwasów dikarboksylowych, pochodnych guanidyny oraz pirydyny. Obserwowane tworzenie kompleksów przebiegało około 180 razy słabiej niż dla cucurbiturilu. Wyniki te świadczą o potencjalnych możliwościach zbliżonych do analogów cyklicznych pod względem tworzenia kompleksów i rozpoznawania wyżej wymienionych...
-
Diastereoselective formation of glucoluril dimers: isomerization mechanismand implications for cucurbit[n]uril synthesis
PublicationZaprezentowano syntezę pochodnych glikolurylu tworzących ściśle sprecyzowane dimeryczne struktury w roztworze wodnym. Opisano diastereoselektywną syntezę pochodnych o strukturze amfifilowej. Przedstawiono mechanizm reakcji oraz struktury krystalograficzne wybranych związków.
-
Enantiomeric self-recognition of a facial amphiphile triggered by [{Pd(ONO2)(en)}2]
PublicationOpisano syntezę pochodnych glikolurylu tworzących dimeryczne struktury w roztworze wodnym prowadzące do samorozpoznania enancjomerycznego. Struktury te uzyskano dzięki koordynacji do [{Pd(ONO2)(en)}2].
-
Methylene bridged glycoluril dimers: synthetic methods
PublicationZaprezentowano syntezę pochodnych glikolurylu tworzących ściśle sprecyzowane dimeryczne struktury w roztworze wodnym. Opisano diastereoselektywną syntezę pochodnych o strukturze amfifilowej.
-
A new and convenient method for the preparation of functionalized phosphorothioates
PublicationA new and efficient method for the synthesis of alkyl and aryl phosphorothioates in high yields via the reaction of (5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorin-2-yl)disulfanyl derivatives with trimethyl phosphite was developed.
-
Nowa metoda syntezy niesymetrycznych trisulfidów
PublicationUgrupowanie trisulfidowe często odpowiada za aktywność biologiczną związków, w którch występuje [1]. Najbardziej znanymi przedstawicielami związków zawierających to ugrupowanie są kalicheamycyna [2] i esperamycyna [3].Wyzwaniem w syntezie organicznej jest niesymetrycznie podstawione ugrupowanie trisulfidowe. Istniejące metody syntezy [4] tego ugrupowania cechują się niską wydajnością oraz znaczną ilością produktów ubocznych.W ramach...
-
Evaluation of solid phase extraction for downstream separation of propane-1,3-diol and butan-1-ol from fermentation broth
PublicationGlycerol is mainly a by-product of fat splitting and biodiesel production. This study examined the use of chemically modified silica gels for downstream separation of propane-1,3-diol and butan-1-ol from fermentation broths obtained through the glycerol fermentation process. The developed method was found to be simple and efficient for the isolation and purification of butan-1-ol from the other components in the fermentation mixture....
-
Scheduling of identical jobs with bipartite incompatibility graphs on uniform machines. Computational experiments
PublicationWe consider the problem of scheduling unit-length jobs on three or four uniform parallel machines to minimize the schedule length or total completion time. We assume that the jobs are subject to some types of mutual exclusion constraints, modeled by a bipartite graph of a bounded degree. The edges of the graph correspond to the pairs of jobs that cannot be processed on the same machine. Although the problem is generally NP-hard,...
-
CMOS implementation of an analogue median filter for image processing in real time
PublicationAn analogue median filter, realised in a 0.35 μm CMOS technology, is presented in this paper. The key advantages of the filter are: high speed of image processing (50 frames per second), low-power operation (below 1.25 mW under 3.3 V supply) and relatively high accuracy of signal processing. The presented filter is a part of an integrated circuit for image processing (a vision chip), containing: a photo-sensor matrix, a set of...
-
Standards Conformity Framework in comparison with contemporary methods supporting standards application
PublicationAchieving and assessing conformity with standards and compliance with various sets of requirements generates significant costs for contemporary economies. Great deal of this is spent on fulfilment of safety and security requirements. However, standards application is not supported sufficiently by the tools available on the market. Therefore, Standards Conformity Framework (SCF) containing methods and tools which provide support...
-
Diagnostic tolerances' evaluation method of the start-up exhaust temperature of a naval gas turbine
PublicationThe conducted investigations aimed to elaborate the method of marking diagnostic tolerances of the exhaust temperature of a gas turbine observed during engine's start-up process. The diagnostic tolerances were determined by means of statistical inference by creating the hypothesis about a normal distribution of the start-up exhaust temperature's dispersion in the initial operation moment, which was subsequently verified applying...
-
A Target Information Display for Visualising Collision Avoidance Manoeuvres in Various Visibility Conditions
PublicationThe paper introduces a new approach to displaying information on targets. The proposed display visualises three types of information: targets’ motion parameters (typical for target tracking), combinations of own course and speed which collide with those targets (typical for Collision Threat Parameters Area display by Lenart (1983)) and combinations of own course and speed which are not compliant with COLREGS in this case (based...
-
The comparison of cytotoxic and genotoxic activities of glucosinolates, isothiocyanates, and indoles
PublicationChemopreventive properties of Brassica vegetables are attributed mainly to their characteristic compounds—glucosinolates (GLs) and their main hydrolysis products—isothiocyanates (ITCs) and indoles. In this study, we compared antiproliferative activity (MTT test in HT29 cells) and genotoxic effects (comet assay in HT29 cells and restriction analysis in a cell-free system) of three GLs (sinigrin (SIN), glucotropaeolin (GTL), and...
-
Effects of Basalt and Carbon Fillers on Fire Hazard, Thermal, and Mechanical Properties of EPDM Rubber Composites
PublicationDue to growing restrictions on the use of halogenated flame retardant compounds, there is great research interest in the development of fillers that do not emit toxic compounds during thermal decomposition. Polymeric composite materials with reduced flammability are increasingly in demand. Here, we demonstrate that unmodified graphene and carbon nanotubes as well as basalt fibers or flakes can act as effective flame retardants...
-
Risk Analysis by a Probabilistic Model of the Measurement Process
PublicationThe aim of the article is presentation of the testing methodology and results of examination the probabilistic model of the measurement process. The case study concerns the determination of the risk of an incorrect decision in the assessment of the compliance of products by measurement. Measurand is characterized by the generalized Rayleigh distribution. The model of the meas-urement process was tested in parallel mode by six risk...
-
Revitalization of the Narrow-Gauge Żuławy Commuter Railway and its effect on shipping conditions in the Vistula delta
PublicationThe article presents the Żuławy Access Railway and the effect of its revitalization on the change of navigational conditions in the Vistula delta. One of the problems analyzed in the article is the intersection of two different transport branches - the inland waterway and rail transport branches. A solution to the problem of their functioning is presented, without any major restrictions. Possible changes in navigational conditions...
-
Speed management on local government managed roads – research, recommendations and guidelines
PublicationCommissioned by the National Road Safety Council Secretariat, the project “Guidelines for speed management on local government managed roads” studied car driver be haviour when subjected to selected speed management measures such a local speed restrictions, surveillance, traffic calming and restricted speed areas. In addition, analyses were conducted on the impact of selected me asures...
-
INFLUENCE OF A VERTEX REMOVING ON THE CONNECTED DOMINATION NUMBER – APPLICATION TO AD-HOC WIRELESS NETWORKS
PublicationA minimum connected dominating set (MCDS) can be used as virtual backbone in ad-hoc wireless networks for efficient routing and broadcasting tasks. To find the MCDS is an NP- complete problem even in unit disk graphs. Many suboptimal algorithms are reported in the literature to find the MCDS using local information instead to use global network knowledge, achieving an important reduction in complexity. Since a wireless network...
-
Genotoxic properties of glucosinolates and isothiocyanates present in Brassica vegetables
PublicationThe bioactive phytochemicals found in Brassica vegetables, in this number glucosinolates (GLS), as well as products of their degradation such as isothiocyanates (ITC) and indoles, are regarded as the most promising chemopreventive compounds. These secondary metabolites display stron antibiological activity and constitute defence system preventing the development of agrophages attacking Brassica plants. Such properties suggest...
-
Education of Logisticians in Poland: Problems and Prospects in Students’ Opinion
PublicationLogistics is one of the key sectors of the Polish economy. Its value reflects not only its own capacity, but also the role it plays in ensuring the proper functioning of the entire economy. The rapid development of the industry and the highest demands on logistics solutions bring to the fore the problem of preparing a new generation of specialists in logistics. That is why the question of compliance to learning expectations of...
-
The Taxonomy Spatial Measure of Development in the Standard of Living Analysis
PublicationIncorporation of spatial relationships in the construction of taxonomy measure of development is gaining popularity in Polish literature. However, there is no one common idea concerning how the spatial relationship should be taken into account when creating a synthetic variable nor, indeed, where the spatial weight matrix should be placed. It seems that the inclusion of spatial relationships is more important in smaller regions’...
-
Using argument structures to create a measurement plan
PublicationWhile planning an experiment the same question always arises: What are the goals of the experiment and which measurements are needed to demonstrate that the goals have been achieved? Deciding about the extent of raw data to be collected, the metrics to be constructed on those data and the interpretation of the metrics with respect to the assumed goals is by no means a trivial task. In this paper we show how a well known Gal-Question-Metrics...
-
Instrumented End Notched Flexure - Crack propagation and process zonemonitoring. Part I: Modelling and analysis
PublicationAnalysis of the three-point bending, End Notched Flexure (ENF), test is presented for exploitation with a new experimental methodology using the backface strain monitoring technique. The model consists oftwo Timoshenko beams joined with a two parameter elastic foundation, to evaluate stress and strain fields in both adherends and the adhesive layer, together with the specimen compliance and energyrelease rate. This model is compared...
-
Evaluation of Vehicle Routing Problem Algorithms for Transport Logistics Using Dedicated GIS System
PublicationThe development and research related to optimization of fleet management is of high interest among many industrial and scientific entities related to logistics and transport. Optimal distribution of transportation resources leads to significant cost reduction. In this context, scientific research related to so called Vehicle Routing Problem (VRP) which relies on determining the shortest transport routes for a strictly limited number...
-
Applying agiile practices to the development of safety-critical software
PublicationDevelopment of safety critical software is subjected to numerous restrictions and recommendations. To meet these requirements classical software development models (e.g. V-model) are usually applied. Agile methodologies, although rapidly increasing their popularity, were generally regarded as unsuitable for such projects. However, they offer potential benefits which provide a strong incentive to incorporate them into safety-critical...
-
Zastosowanie założeń koncepcji efektuacji w organizowaniu wydarzenia kulturalnego – studium przypadku
PublicationThe paper presents how the effectuation model, which stems from the business studies, can be applied as a tool for analysing the activities undertaken as part of culture organisation. The key element of this model involves the control-based approach to the future instead of making predictions about the future. The outline of the theoretical background is followed by the results of the qualitative research, where the answers were...
-
Model of Rules for IT Organization Evolution
PublicationThe aim of this paper is to introduce the Model of Rules for IT Organization Evolution which shall be in compliance with the Generic IT Organization Evolution Model. Due to its general nature, a set of practical adjustments is proposed in order to adapt the Generic Model to the IT Service Management domain. Further, two sets of rules describing the evolution of the IT Service Management area are defined based on two types of rules...
-
Modeling, simulation, and validation of a TB41 crash test of the H2/W5/B concrete vehicle restraint system
PublicationThe paper addresses numerical simulations of a concrete vehicle restraint system. The model is described in detail. The advanced material law of the continuous surface cap model was used to analyze the damage locations in concrete barrier segments. The results were validated against the TB41 full-scale crash test. The test was conducted in compliance with European standard EN 1317, and the validation was performed in accordance...
-
Water uptake in protective organic coatings and its reflection in measured coating impedance
PublicationWater uptake in commercially available epoxy coating on mild steel using impedance spectroscopy and gravimetry was studied. The water content in the coating was determined using the Brasher-Kingsbury equation and various methods of coating capacitance calculation used in the literature. The obtained results were compared with reference gravimetric data. An overestimation of values obtained from impedance data in relation to gravimetric...
-
Born–Oppenheimer potential energy curves of NaK from the optimised atomic basis sets
PublicationThe article presents adiabatic potential energy curves of the ground and excited electronic states for the diatomic NaK molecule. The calculations were made using the ab initio computational methods to include electron correlation. The studied molecule was calculated as the effective two-electron problem, in which only the valence electrons of the molecule are explicitly taken into account. The remaining electrons with atomic nuclei...
-
ESTYMACJA WSPÓŁCZYNNIKÓW SZTYWNOŚCI ZAMOCOWANIA PODATNEGO PRZEDMIOTU OBRABIANEGO NA STOLE FREZARKI
PublicationW pracy przedstawiono metodę estymacji współczynników sztywności Elementów Sprężystych (ES) modelujących zamocowanie podatnego wielkogabarytowego przedmiotu obrabianego na stole frezarki. Proponowana metoda bazuje na algorytmie optymizacji za pomocą roju cząstek (ang. Particle Swarm Optimization), który pozwala na uzyskanie dobrej zgodności (aktualizacji) modelu Metody Elementów Skończonych (MES) z modelem pochodzącym z identyfikacji...
-
Właściwości pigmentów kadmowych po narażeniach chemicznych i naświetlaniu promieniowaniem UV
Publication -
Study on properties of oxide pigments after environmental expositions Badania w�a�ciwo�ci pigment�w tlenkowych po nara�eniach �rodowiskowych
Publication -
A novel and efficient synthesis of unsymmetrical disulfides
PublicationOpracowano metodę otrzymywania niesymetrycznych disulfidów z odpowiednich tioli w oparciu o bromek sulfenylowy.
-
A convenient method for the preparation of functionalized N-acylsulfenamides from primary amides.
PublicationWe have developed a convenient method for the synthesis of functionalized N-acylsulfenamides under mild conditions and in moderate to good yields. The designed method is based on the reaction of (5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl)-disulfanyl derivatives with nitrogen nucleophiles generated from primary amides or imides and sodium hydride. The developed method allows for the preparation of N-acylsulfenamides bearing...
-
Recent Developments in the Synthesis of Unsymmetrical Disulfanes (Disulfides). A Review
PublicationThe synthesis of unsymmetrical disulfanes is an important transformation in organic synthesis and medicinal chemistry. The current review is intended to summarize achievements in the synthesis of unsymmetrical disulfanes over the last decade (2004–2014).
-
TBAF Promoted Formation of Symmetrical Trisulfides
PublicationWe have developed a new method for the synthesis of functionalized symmetrical trisulfides based on (5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorin-2-yl)disulfanyl derivatives prepared from readily available 5,5-dimethyl-2-sul-fanyl-2-thioxo-1,3,2-dioxaphosphorinane or bis(5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl) disulfide. The symmetrical trisulfides can be obtained from aliphatic and aromatic thiols andL-cysteine derivatives...
-
Efficient Synthesis of Functionalized Unsymmetrical Dialkyl Trisulfanes
PublicationWe have developed a convenient method for the synthesis of functionalized unsymmetrical dialkyl trisulfanes under mild conditions in very good yields. The designed method is based on the reaction of (5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl)-disulfanyl derivatives with alkyl disulfanyl anions generated in situ from S-acetyl disulfanyl derivatives and sodium methoxide. The developed method allows for the preparation of...
-
Three-fast-searchable graphs
PublicationIn the edge searching problem, searchers move from vertex to vertex in a graph to capture an invisible, fast intruder that may occupy either vertices or edges. Fast searching is a monotonic internal model in which, at every move, a new edge of the graph G must be guaranteed to be free of the intruder. That is, once all searchers are placed the graph G is cleared in exactly |E(G)| moves. Such a restriction obviously necessitates...
-
EXPERIMENTAL EVALUATION OF DLC/STEEL SLIDING CONTACTS’ OPERATIONAL ENVELOPE
PublicationIn an industrial project concerning sliding bearings, a sliding pair was selected of high alloy steel vs. industrial grade DLC coated high alloy steel as a basis for an innovative design of high performance sliding bearings lubricated with a synthetic oil for use in geared transmission units. The development process required credible data on the ultimate resistance of the sliding pair to very high contact stress. An experimental...
-
Experimental research on marine oil-lubricated stern tube bearing
PublicationBearings of propeller shafts are very crucial elements of the propulsion system of each of the ships. The safety of shipping depends on their durability and reliability. The new legal restrictions mean that today we are looking for environmentally friendly solutions. That is why water-lubricated bearings are becoming more and more popular. So, will oil-lubricated shaft bearings belong to the past? The bearing with a white metal...
-
The potential of Web-GIS and geovisual analytics in the context of marine cadastre
PublicationThe importance of the marine environment to human existence makes it imperative that information models represent the multidimensional nature of reality as closely as possible in order to facilitate good governance. Information regarding jurisdiction, as well as the effects of formal law and community interests on the marine environment (e.g. nature and spatial extents as well as rights, responsibilities, restrictions etc.) would...
-
Linear Pantographic Sheets: Existence and Uniqueness of Weak Solutions
Publicationwe address the well-posedness of the planar linearized equilibrium problem for homogenized pantographic lattices. To do so: (i) we introduce a class of subsets of anisotropic Sobolev’s space as the most suitable energy space E relative to assigned boundary conditions; (ii) we prove that the considered strain energy density is coercive and positive definite in E ; (iii) we prove that the set of placements for which the strain...
-
Current trends in analytical strategies for determination of polybrominated diphenyl ethers (PBDEs) in samples with different matrix compositions – Part 1.: Screening of new developments in sample preparation
PublicationPolybrominated diphenyl ethers (PBDEs) are ubiquitous compounds in the environment. Restrictions on the use of PBDEs introduced at the beginning of the 21st century have not eliminated these highly persistent and bioaccumulative compounds from the environment. Despite many existing regulations to control and phase out, extensive research on PBDEs is still necessary to fully evaluate the hazard their create to the environment. In...
-
ISSUES OF ECONOMIC ANALYSIS OF ELECTRIC ENERGY GENERATION IN A FLOATING POWER PLANT
PublicationThis article presents basic dependences for conducting a technical and economic analysis related with investment projects. It describes a combined system of a compression ignition engine and a steam turbine, whose aim, when placed on a floating platform, is to generate electric energy in the so-called distributed generation system. Such a system involves a reciprocating internal combustion engine and a connected steam turbine system...
-
Researching Digital Society: Using Data-Mining to Identify Relevant Themes from an Open Access Journal
PublicationOpen Access scholarly literature is scientific output free from economic barriers and copyright restrictions. Using a case study approach, data mining methods and qualitative analysis, the scholarly output and the meta-data of the Open Access eJournal of e-Democracy and Open Government during the time interval 2009–2020 was analysed. Our study was able to identify the most prominent research topics (defined as thematic clusters)...
-
Researching Digital Society: Using Data-Mining to Identify Relevant Themes from an Open Access Journal
PublicationOpen Access scholarly literature is scientific output free from economic barriers and copyright restrictions. Using a case study approach, data mining methods and qualitative analysis, the scholarly output and the meta-data of the Open Access eJournal of e-Democracy and Open Government during the time interval 2009–2020 was analysed. Our study was able to identify the most prominent research topics (defined as thematic clusters)...
-
Polish tax reform "Polski Ład" – consequences of introducing changes on the example of selected flat-rate tax forms for micro and small companies
PublicationThis article describes aspects related to the introduction of the latest tax reform in Poland. The changes initiated in January 2022, under the name Polski Ład, concern a wide range of tax changes in Poland. Reform, in a broad sense, is a multidimensional government development program, which is primarily aimed at getting out of the crisis caused by the COVID-19 pandemic and a smooth transition to financing strategic goals in investment...
-
Scaled agile framework. Dealing with software process‐related challenges of a financial group with the action research approach
PublicationThis article reports on a domain-specific software development venture at Nordea. We explore organizational constraints, challenges, and corrective actions undertaken when scaling the agile development approach of their Core Banking Platform program. The fit and required customizations of the rather complex and rigid SAFe framework in a policy-heavy financial institution are audited against the organic growth of the program. In...
-
Automatic Detection and Monitoring of Cyanobacterial Blooms in the Context of the Marine Cadastre
PublicationIn the wake of the European and global spatial data infrastructures (SDI) it is important to build information systems which use and serve thematic data in compliance with the INSPIRE Directive. In the context of hydrographic data, the Directive requires EU member states to collect and share information on maritime areas divided into regions and sub-regions, as well as coastal zone management areas. These data are part of recently...