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Luminescence properties of Eu3+ and Tb3+ doped silica-based xerogels
PublicationPure SiO2 xerogels and SiO2 xerogels containing SrF2: Eu3+/: Tb3+ crystals were prepared using sol-gel method. Luminescent spectra showed excitation and emission peaks characteristic to Eu3+ and Tb3+ 4f - 4f transitions. ET Tb3+→Eu3+ has been observed. XRD pattern of SiO2 matrix confirmed lack of long range order. Patterns of SiO2-SrF2:Eu3+ and SiO2-SrF2:Tb3+ showed peaks corresponding to SrF2. SEM images have shown agglomerates...
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Binuclear Co(II), Zn(II) and Cd(II) tri-tert-butoxysilanethiolates. Synthesis, crystal structure and spectroscopic studies.
PublicationA series of Co(II), Zn(II) and Cd(II) complexes have been synthesized in reaction of respective metal tri-tert-butoxysilanethiolates with pyrazine 1 and 2 and 1,2-bis(2-pyridyl)ethylene 3–5. All compounds have been characterized by single-crystal X-ray structure determination, elemental analysis, FT-IR and thermogravimetry. Obtained complexes are bimetallic with the formula of [M{SSi(OtBu)3}2(μ-L)]2 and metal ions bridged by N,N′-spacer....
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A numerical and experimental analysis of multi-hole orifice in turbulent flow
PublicationIn this research study, the comprehensive metrological analysis is investigated for a 4-hole orifice with module m = 0.25 installed in the pipeline with an internal diameter of 50 mm. A detailed numerical simulation was performed for the turbulence models: k-ε-realizable and k-ω-BSL. The novelties of the research include model validation by comparing the results of numerical studies with the experiment conducted in the area of...
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Wykorzystanie xml do reprezentacji cyfrowych dokumentów muzycznych
PublicationW bibliotekach cyfrowych dokumentów muzycznych potrzebny jest format pozwalający na wymianę danych różnego typu związanych z dokumentem muzycznym. Otwarty format XML posiada wiele zalet, które pozwalają na zastosowanie go w tej bibliotece. W rozdziale zwrócono uwagę na możliwość wykorzystania formatów MPEG-7, MARCXML oraz MusicXML do opisania różnorodnych aspektów muzyki. Połączenie wszystkich informacji związanych z dokumentem...
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Scent emitting multimodal computer interface for learning enhancement
PublicationKomputerowy interfejs aromatyczny stanowi ważne uzupełnienie procesu stymulacji polisensorycznej. Stymulacja ta odgrywa kluczową rolę w terapii i kształceniu dzieci z zaburzeniami rozwoju (np. w przypadku autyzmu czy ADHD). Opracowany interfejs może stać się elementem wyposażenia tzw. sal doświadczania świata, ale może być także stosowany niezależnie stanowiąc znaczące wzbogacenie komputerowych programów edukacyjnych. Dzięki możliwości...
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Synthesis and properties of porous Sr 0.96 Y 0.04 Ti 1−x Nb x O 3
PublicationA series of porous, single phase Sr0.96Y0.04Ti1-xNbxO3 samples was obtained using a wet synthesis method (modified citrate sol-gel) method. Temperature-programmed reduction (TPR) and temperature-programmed oxidation (TPO) measurements have shown high stability of the obtained material in variable (oxidizing/reducing) atmospheres. All samples exhibit high conductivity in hydrogen atmosphere with the highest value (around 1S/cm)...
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Photocatalytic Decomposition of Air Pollutants using Electrodeposited Photocatalysts on Stainless Steel
PublicationThe aim of research was to develop an immobilization method for photocatalysts, which is an alternative to the sol-gel or dip coating methods and can be simply scaled up for technical applications. The investigated photocatalyst was TiO2, which was electrochemically deposited onto a cathode made of stainless steel. This deposited film was photocatalytically active. In order to enhance the photoactivity of the TiO2 film, commercially...
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E-learning - prawdziwa czy fikcyjna koncepcja edukacyjnego rozwoju uczelni
PublicationNie można zaprzeczyć, że wykorzystanie narzędzi multimedialnych oraz Internetu pozwala na dodanie istotnych, z punku widzenia dydaktyki, komponentów edukacyjnych tworzących kompetencje i umiejętności zawodowe, a także te czysto akademickie. Trzeba rozważyć, czy wszystkie strony procesu dydaktycznego na uczelni są przygotowane do e−learningu. Oczywistym wymogiem jest posiadanie odpowiedniej bazy sprzętowej i przygotowanej kadry...
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Functional Safety Analysis including Human Factors
PublicationIn this paper selected aspects of human factors are discussed that should be taken into account during the design of safety-related functions for a complex hazardous installation and its protections. The layer of protection analysis (LOPA) methodology is used for simplified risk analysis based on defined accident scenarios. To control the risk the safety instrumented functions (SIFs) are identified and their safety integrity levels...
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Cyclic voltammetry curves of the V2O5 nanorods (Na-ion batteries)
Open Research DataThe DataSet contains the next thirty cycles voltammetry curves for the V2O5 nanorods obtained by the sol-gel method. The cyclic voltammetry was measured using the AUTOLAB 302N potentiostat-galvanostat. The measurements were carried out in a voltage range of 2 V to 4 V vs. Na/Na+ at a scan rate of 1 mV/s. As an electrolyte 1M NaPF6 was applied.
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XRD patterns of V2O5 nanostructures
Open Research DataThe DataSet contains the XRD patterns of vanadium pentaoxide nanostructures obtained by the sol-gel with different annealing temperatures under synthetic air. The results show that crystallinity dependent on the annealing temperature.
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Cyclic voltammetry curves of the V2O5 nanocrystals (Na-ion batteries)
Open Research DataThe DataSet contains the next thirty cycles voltammetry curves for the V2O5 nanocrystals obtained by the sol-gel method. The cyclic voltammetry was measured using the AUTOLAB 302N potentiostat-galvanostat. The measurements were carried out in a voltage range of 2 V to 4 V vs. Na/Na+ at a scan rate of 1 mV/s. As an electrolyte 1M NaPF6 was applied.
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XRD patterns of VO2 and V2O3 nanostructures
Open Research DataThe DataSet contains the XRD patterns of VO2 and V2O3 nanostructures obtained by the sol-gel with different reaction conditions. The information about xerogel powder synthesis is described in the Journal of Nanomaterials. The xerogel powder was annealing under argon atmosphere in the temperature range 400-1000C. The results show that the morphology...
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Biowaste chicken eggshell powder as a potential cure modifier for epoxy/anhydride systems: competitiveness with terpolymer-modified calcium carbonate at low loading levels
PublicationBiowaste chicken eggshell (ES) powder was applied as a potential cure modifier in epoxy/anhydride systems. Cure behaviour and kinetics of composites filled with very low content (0.1 wt% based on epoxy resin) of ES, calcium carbonate (CaCO3), and terpolymer-modified fillers, mES and mCaCO3, were discussed comparatively. Surface analysis was performed by X-ray photoelectron spectroscopy. Cure kinetics was investigated by differential...
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n/d n/d
ProjectsProject realized in Faculty of Chemistry according to Homing Plus/2012-6/16 agreement from 2013-05-22
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WEAR OF Si OR B DOPED AMORPHOUS CARBON COATINGS
PublicationThe paper describes a complex wear research on DLC (amorphous carbon) moped with boron (B) and silicone (Si). The tests were carried out in two different sliping systems: flat–on–flat (ring contact, unidirectional sliding) and ball–on–flat (reciprocating sliding). Water and medical saline solutions were used as lubricants. A comparative analysis of the results revealed differences in the initiation and progress of wear and the...
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ZZIT SS 2022
e-Learning Courses -
Scanning electrochemical micrographs of poly(lactic acid) 3D printed electrodes ablated by femtosecond laser
Open Research DataThe dataset contains the scanning electrochemical micrographs of the femtosecond laser (FSL) ablation at the surface of commercially available carbon black-filled poly(lactic acid) 3D printed electrode. The process is used for the increase of the charge transfer of this electrode in electrochemical studies.
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Rate performance of the V2O5 nanocrystals as cathode material in Li-ion batteries
Open Research DataThe DataSet contains the galvanostatic charge/discharge curves of the V2O5 nanocrystals obtained by the sol-gel method. The battery tests of the samples were performed using the Atlas-Sollich 0961 (Atlas-Sollich, Poland) with different current densities in the voltage range between 2.0 V and 4.0 V vs. Li/Li+. Here 1C is 294 mAh g-1.
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XRD patterns of V2O3 nanostructures
Open Research DataThe DataSet contains the XRD patterns of V2O3 nanostructures obtained by the sol-gel with different reaction conditions. The xerogel powder was annealing under a reducing atmosphere (94% Ar, 6% H2) in the temperature range 350-700C. The results show that crystallinity dependent on the annealing temperature.
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Cyclic voltammetry curves of the V2O5 nanorods (Li-ion batteries)
Open Research DataThe DataSet contains the next thirty cycles voltammetry curves for the V2O5 nanocrystals obtained by the sol-gel method. The cyclic voltammetry was measured using the AUTOLAB 302N potentiostat-galvanostat. The measurements were carried out in a voltage range of 2 V to 4 V vs. Li/Li+ at a scan rate of 1 mV/s. The results show that in the subsequent cycles,...
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Cyclic voltammetry curves of the V2O5 nanocrystals (Li-ion batteries)
Open Research DataThe DataSet contains the next thirty cycles voltammetry curves for the V2O5 nanocrystals obtained by the sol-gel method. The cyclic voltammetry was measured using the AUTOLAB 302N potentiostat-galvanostat. The measurements were carried out in a voltage range of 2 V to 4 V vs. Li/Li+ at a scan rate of 1 mV/s. The results show that in the subsequent cycles,...
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Rate performance of the V2O5 nanorods as cathode material in Li-ion batteries
Open Research DataThe DataSet contains the galvanostatic charge/discharge curves of the V2O5 nanorods obtained by the sol-gel method. The battery tests of the samples were performed using the Atlas-Sollich 0961 (Atlas-Sollich, Poland) with different current densities in the voltage range between 2.0 V and 4.0 V vs. Li/Li+. Here 1C is 294 mAh g-1.
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Thermal properties of VO2 and V2O3 nanostructures
Open Research DataThe DataSet contains the DSC and TG curves of VO2 and V2O3 nanostructures obtained by the sol-gel with different reaction conditions. The information about xerogel powder synthesis is described in the Journal of Nanomaterials. The xerogel powder was annealing under argon atmosphere at the selected temperature: 500C, 600C, and 1000C.
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SEM micrographs of morphology evolution of VO2 and V2O3 nanostructures
Open Research DataThe DataSet contains the scanning electron microscopy (SEM) micrographs of VO2 and V2O3 nanostructures obtained by the sol-gel with different reaction conditions. The information about xerogel powder synthesis is described in the Journal of Nanomaterials. The xerogel powder was annealing under argon atmosphere in the temperature range 400-800C. The...
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Conversion of waste biomass to designed and tailored activated chars with valuable properties for adsorption and electrochemical applications
PublicationWaste biomass, a renewable energy source, is inexpensive material that has great potential in sorp-tion and electrochemical application. The selected waste materials (corncobs, coconut shells, wal-nuts, and pistachio husks) allow to close the production cycle and enable material recycling, which are important aspects in the hierarchy of waste management. The proposed methodology for pro-duction and activation of biochars can be...
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Programowa realizacja bramy sygnalizacyjnej między siecią PSTN/ISDN a siecią Internet
PublicationRealizacja idei społeczeństwa informacyjnego wymaga odpowiedniej infrastruktury teleinformacyjnej dla której przewidziano sieci następnej generacji (NGN) a w tym Internet następnej generacji (NGI). W pracy przedstawiono rozwiązanie jednego z problemów wynikającego z przekształcenia obecnych sieci do sieci NGN. Jest to problem sterowania połączeniem dla usługi telekomunikacyjnej nazywanej popularnie telefonia (mowa). Realizacja...
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Optical recognition elements: macrocyclic imidazole chromoionophores entrapped in silica xerogel
PublicationMaterials containing new chromoionophores consisting of crown residue and azole moiety as partsof macrocycles were encapsulated by the sol-gel procedure in silica xerogel matrices and proposed aschemical recognition elements especially for such metal ions as Li+, Cs+ and Cu2+. Action of these recognition elements is in principle based on changes of reflectance. The recognition elements containing 21-membered chromogenic...
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Ag/Pt-modified TiO2 nanoparticles for toluene photooxidation in the gas phase
PublicationAg/Pt-modified TiO2nanocomposites were synthesized using the sol–gel method. The effect of metal typeand amount as well as synthesis route on the photocatalytic activity in reaction of toluene removal, usedas a model volatile organic compound, was investigated. Toluene, at the concentration of about 200 ppm,was irradiated over modified TiO2using light-emitting diodes (LEDs, max= 415 nm). The results showedthat toluene could be...
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Transparent thin films of Cu-TiO2 with visible light photocatalytic acitivity
PublicationThin films of Cu–TiO2 with a high level of transparency were prepared by a dip-coating procedure on the glass surface. CuCl2 was used as a copper precursor added during sol – gel synthesis of TiO2. The extension of optical absorption into the visible region of as-prepared thin films was indicated by UV/Vis spectroscopy. Only the anatase phase was detected by X-ray di ffraction analysis (XRD). The presence of copper in the structure...
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KQL - język dostępu do konglomeratowych baz wiedzy
PublicationJednym z kierunków rozwoju systemów informatycznych w ostatnich latach jest ewolucja systemów opartych na danych do systemów opartych na wiedzy. W ramach tego procesu są prowadzone prace między innymi nad nowymi reprezentacjami wiedzy i językami dostępu do wiedzy. Języki dostępu do baz wiedzy są w dużej mierze uzależnione od metod reprezentacji wiedzy, ponieważ operują na jej elementach. Wraz z zaproponowaniem konglomeratowej reprezentacji...
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A method of verification diagnostics for functional safety analysis
PublicationProblemy analizy bezpieczeństwa zostały zapoczątkowane w lotnictwie i energetyce jądrowej, a obecnie wprowadzane są szeroko do różnych gałęzi przemysłu, jak przemysł chemiczny, mechaniczny, etrochemiczny, spożywczy, itp. W analizie bezpieczeństwa funkcjonalnego względem przyjętego poziomu SIL wyznacza się prawdopodobieństwa nie wypełnienia określonej funkcji na żądanie (PDF). Do tego celu stosuje się różne metody analityczne, wykorzystuje...
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Enviromental factors az the elements determingthe development of floating homes
PublicationThe popularity of Floating Homes in Western Europe and North America is noticeable. The interest in thesefacilities in Poland is also constantly growing. The popularity of Floating Homes is due to climate change, risingland prices and population density in city centers. However, environmental factors play a significant role in theirdevelopment. The publication presents the results of research on the impact of environmental factors...
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Enhanced Electrochemical Performance of MnCo1.5Fe0.5O4Spinel for Oxygen Evolution Reaction through Heat Treatment
PublicationMnCo1.5Fe0.5O4 spinel oxide was synthesized using the sol−gel technique, followed by heat treatment at various temperatures (400, 600, 800, and 1000 °C). The prepared materials were examined as anode electrocatalysts for watersplitting systems in alkaline environments. Solid-state characterization methods, such as powder X-ray diffraction and X-ray absorption spectroscopy (XAS), were used to analyze the materials’ crystallographic...
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Computer-Aided Greenery Design—Prototype Green Structure Improving Human Health in Urban Ecosystem
PublicationIncreasing population and urbanization, with climate change consequences, such as rising temperatures, influence public health and well-being. The search to improve the quality of life in cities becomes one of the priority objectives. A solution can be found in the role of greenery in an urban environment and its impact on human health. This opens a path toward experimentation on microclimate green structures that can be inserted...
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Silicon Oxycarbide-Graphite Electrodes for High-Power Energy Storage Devices
PublicationHerein we present a study on polymer-derived silicon oxycarbide (SiOC)/graphite composites for a potential application as an electrode in high power energy storage devices, such as Lithium-Ion Capacitor (LIC). The composites were processed using high power ultrasound-assisted sol-gel synthesis followed by pyrolysis. The intensive sonication enhances gelation and drying process, improving the homogenous distribution of the graphitic...
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Assessment of the devulcanization process of EPDM waste from roofing systems by combined thermomechanical/microwave procedures
PublicationEthylene-propylene-diene rubber (EPDM) is a elastomer widely used in common industrial applications. EPDM can be shaped into sheets and employed as isolating material for roofing systems. In this study, scraps of EPDM from commercial, industrial and residential roofing systems were treated by combined thermo-mechanical and microwave devulcanization processes including peroxide of benzoyl (BPO). The devulcanized EPDM (Dev-EPDM)...
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URBAN TRANSFORMATIONS
PublicationMentor&Student Research Lab is a common initiative of the members of Gdańsk University of Technology student research club, Urban Revolution Laboratory LEM-ur and International Society of City and Regional Planners ISOCARP. The aim of the event was to promote collaboration of professionals and the student in the area of research on the city and the region. During three months' Workshop five groups leaded by ISOCARP Mentors performed...
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Visual Content Learning in a Cognitive Vision Platform for Hazard Control (CVP-HC)
PublicationThis work is part of an effort for the development of a Cognitive Vision Platform for Hazard Control (CVP-HC) for applications in industrial workplaces, adaptable to a wide range of environments. The paper focuses on hazards resulted from the nonuse of personal protective equipment (PPE). Given the results of previous analysis of supervised techniques for the problem of classification of a few PPE (boots, hard hats, and gloves...
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Design, Synthesis, and Enzymatic Evaluation of Novel ZnO Quantum Dot-Based Assay for Detection of Proteinase 3 Activity
PublicationHerein, the synthesis and application of functionalized quantum dot-based protease probes is described. Such probes are composed of nontoxic ZnO nanocrystals decorated by amino groups followed by linker and labeled peptide attachment. Spherical NH2-terminated ZnO quantum dots (QDs) with the average size ranging from 4 to 8 nm and strong emission centered at 530 nm were prepared using the sol−gel method. The fluorescence of ZnO...
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Safety Integrity Verification Issues of the Control Systems for Industrial Process Plants
PublicationThe aim of this article is to identify and discuss some issues that can be encountered in designing the industrial automation and control systems (IACS) for implementing safety functions. In a functional safety standard IEC 61511 for the process industry such systems are named the basic process control systems (BPCS) and the safety instrumented systems (SIS). In a generic functional safety standard IEC 61508 they are depicted as...
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2-D constitutive equations for orthotropic Cosserat type laminated shells in finite element analysis
PublicationWe propose 2-D Cosserat type orthotropic constitutive equations for laminated shells for the purpose of initial failure estimation in a laminate layer. We use nonlinear 6-parameter shell theory with asymmetric membrane strain measures and Cosserat kinematics as the framework. This theory is specially dedicated to the analysis of irregular shells, inter alia, with orthogonal intersections, since it takes into account the drilling...
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Analiza niezawodności człowieka-operatora w kontekście bezpieczeństwa funkcjonalnego.
PublicationArtykuł przedstawia niektóre kwestie analizy warstwowego systemu zabezpieczeń instalacji podwyższonego ryzyka z uwzględnieniem analizy niezawodności człowieka HRA (human reliability analysis). Działania człowieka operatora w odniesieniu do systemu operatorskiego HSI (human system interface), w tym systemu alarmowego i potencjalnych błędów człowieka mogą mieć istotny wpływ na wyniki analiz probabilistycznych w procesie weryfikacji...
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Mentor&Student Research Lab – Urban Transformations – Introduction
PublicationMentor&Student Research Lab - "Urban Transformations" is a common initiative of the members of Gdańsk University of Technology student research club, Urban Revolution Laboratory and the International Society of City and Regional Planners ISOCARP. The aim of the event was to promote collaboration of professionals and the students in the area of research on the city and the region. During three months’ Workshop five groups leaded...
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New procedure for the examination of the degradation of volatile organonitrogen compounds during the treatment of industrial effluents
PublicationWe present a new procedure for the determination of 32 volatile organonitrogen compounds in samples of industrial effluents with a complex matrix. The procedure, based on dispersive liquid–liquid microex-traction followed by gas chromatography with nitrogen-phosphorus and mass spectrometric detection, wasoptimized and validated. Optimization of the extraction included the type of extraction and disperser sol-vent, disperser solvent...
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Zarządzanie bezpieczeństwem funkcjonalnym w przemyśle
PublicationNiniejszą pracę poświęcono aktualnym zagadnieniom zarządzania bezpieczeństwem funkcjonalnym w nawiązaniu do wymagań normy międzynarodowej IEC 61508:2010 w kontekście międzynarodowych przewodników dotyczących całościowego zarządzania bezpieczeństwem w zakładach przemysłu procesorowego. Przedstawiono zagadnienia analizy i oceny ryzyka zorientowane na określenie wymaganego poziomu nienaruszalności SIL (Safety Integrity Level) funkcji...
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Morphological and electrochemical characterization of ceramic carbon foam electrodes water treatment applications
Open Research DataThis dataset contains morphological and electrochemical characterization of ceramic carbon foam employed as an electrode (CFFE) for the oxidation of a target pollutant. The dataset includes:
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Analiza Niezawodności Człowieka w Ramach Funkcji związanych z Bezpieczeństwem w Przykładowej Instalacji
PublicationW analizie bezpieczeństwa funkcjonalnego systemów sterowania i zabezpieczeń należy określić wymagany poziom nienaruszalności bezpieczeństwa SIL w procesie analizy ryzyka, a następnie zweryfikować ten poziom stosując odpowiednie metody modelowania probabilistycznego. Działania człowieka mogą mieć istotny wpływ na realizację funkcji bezpieczeństwa. Wpływ ten ocenia się na podstawie wyników analizy niezawodności człowieka HRA. W niniejszym...
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General concept of functional safety - standarisation and sector aspects
PublicationRozdział poświęcono koncepcji bezpieczeństwa funkcjonalnego. Bezpieczeństwo funkcjonalne jest częścią bezpieczeństwa całkowitego zależną od odpowiedniej odpowiedzi systemów sterowania i/lub zabezpieczeń na sygnały wejściowe podczas wystąpienia stanów nienormalnych maszyny, instalacji lub obiektu podwyższonego ryzyka. Koncepcja bezpieczeństwa funkcjonalnego przedstawiona w normie IEC 51508 stanowi przykład dobrej praktyki inżynierskiej...
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Determination of nine high-intensity sweeteners in various foods by high-performance liquid chromatography with mass spectrometric detection
PublicationAn analytical procedure involving solid-phase extraction (SPE) and high-performance liquid chromatography-mass spectrometry has been developed for the determination of nine high-intensity sweeteners authorised in the EU; acesulfame-K (ACS-K), aspartame (ASP), alitame (ALI), cyclamate (CYC), dulcin (DUL), neohesperidin dihydrochalcone (NHDC), neotame (NEO), saccharin (SAC) and sucralose (SCL) in a variety of food samples (i.e. beverages,...