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Boron Difluoride Complexes of Carbamoyl Meldrum's Acids
Publication5-[Hydroxy(aryl/alkylamino)methylene]-2,2-dimethyl-1,3-dioxane-4,6-diones react with BF3•Et2O in mild conditions leading to the formation of boron difluoride complexes of carbamoyl Meldrum's acids. The X-ray structure has been obtained for one representative complex. The obtained new compounds are fairly stable at standard ambient conditions and easily isolable.
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Rapid design optimization of compact couplers using response features and adjoint sensitivities
PublicationA technique for rapid EM-driven design optimization of compact microwave couplers is presented. Our approach exploits response features and adjoint sensitivities and allows for low-cost design closure both in terms of performance enhancement and structure miniaturization. It is demonstrated using a compact rat-race coupler working at 1 GHz and compared to adjoint-based gradient optimization.
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UAV Survey Images - 3D Model - Jastrzebia Gora Cliff 07.2017- MP1
Open Research DataDataset description: Raw images from photogrammetric survey. Object: Cliff in Jastrzebioa GoraLocation: Jastrzebia Gora, Pomerania, PolandDrone type: DJI Mavic Pro 1Flight plan: Single Grid/Free FlightTarget Product: 3D ModelDate: 06.07.2017Direct georeferencing: yesMetadata data: yes/GPSGCP: NOGCP Quality: N/ACamera Name: DJI FC220Model type: PerspectiveImage...
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UAV Survey Images - 3D Model - Trakt Sw Wojciecha Street - Orunia
Open Research DataDataset description: Raw images from photogrammetric survey. Object: Street Trakt Sw Wojciecha - OruniaLocation: Gdansk Orunia, Pomerania, PolandDrone type: DJI Mavic Pro 1Flight plan: Double GridTarget Product: 3D ModelDate: 17.11.2018Direct georeferencing: yesMetadata data: yes/GPSGCP: NoGCP Quality: N/ACamera Name: DJI FC220Model type: PerspectiveImage...
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UAV Survey Images - 3D Model - GUT Water Tower MP1
Open Research DataDataset description: Raw images from photogrammetric survey. Object: Water Tower at Gdansk University Of Technology CampusLocation: Gdansk, Pomerania, PolandDrone type: DJI Mavic Pro 1Flight plan: CircleTarget Product: 3D ModelDate: 13.05.2019Direct georeferencing: yesMetadata data: yes/GPSGCP: NoGCP Quality: N/ACamera Name: DJI FC220Model type: PerspectiveImage...
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UAV Survey Images - DTM - Sopot Tombolo (Salient) Measurement - MP2
Open Research DataDataset description: Raw images from photogrammetric survey. Object: littoral zone in SopotLocation: Sopot, Pomerania, PolandDrone type: DJI Mavic Pro 2Flight plan: Single GridTarget Product: Digital Terrain ModelDate: 23.11.2019Direct georeferencing: yesMetadata data: yes/GPSGCP: YESGCP Quality: RTKCamera Name: Hasselblad L1D-20cModel type: PerspectiveImage...
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UAV Survey Images - 3D Model - Jastrzebia Gora Cliff 11.2017- MP1
Open Research DataDataset description: Raw images from photogrammetric survey. Object: Cliff in Jastrzebioa GoraLocation: Jastrzebia Gora, Pomerania, PolandDrone type: DJI Mavic Pro 1Flight plan: Single Grid/Free FlightTarget Product: 3D ModelDate: 05.11.2017Direct georeferencing: yesMetadata data: yes/GPSGCP: NOGCP Quality: N/ACamera Name: DJI FC220Model type: PerspectiveImage...
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UAV Survey Images - 3D Model - GUT Water Tower MP2
Open Research DataDataset description: Raw images from photogrammetric survey. Object: Water Tower at Gdansk University Of Technology CampusLocation: Gdansk, Pomerania, PolandDrone type: DJI Mavic Pro 2Flight plan: CircleTarget Product: 3D ModelDate: 08.11.2019Direct georeferencing: yesMetadata data: yes/GPSGCP: NoGCP Quality: N/ACamera Name: Hasselblad L1D-20cModel...
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XRD for molybdenum sulfide modified with nickel or platinum nanoparticles
Open Research DataThe presented data showcases the results of XRD analysis conducted on molybdenum sulfide modified with nickel or platinum nanoparticles . The MoS2 was prepared on the TiO2 nanotube substrates via a facile hydrothermal method, followed by the deposition by magnetron sputtering of Ni or Pt nanoparticles on the MoS2 surface. Structural characterization...
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XRD patterns of the V2O5 nanorods after thermal treatment under reducing atmosphere
Open Research DataThe DataSet contains the XRD patterns of V2O5 nanorods after thermal treatment under a reducing atmosphere. Samples were annealed at 450C for 2, 20, and 40h under a reducing atmosphere (94% Ar, 6% H2).
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Numerical Analysis of an Impact of Planned Location of Sewage Discharge on Natura 2000 Areas – The Dead Vistula Region Case Study
PublicationThis article presents results of an analysis of impact of a designed discharge of contaminated water into the Dead Vistula (Wisła Martwa) in the region of the Isthmus (Przesmyk) with the aim of determination of a possible effect of the pollution onto protected areas of Natura 2000 (bird habitats and sites, especially the Bird Paradise – Ptasi Raj) nature reserve. The analysis was conducted on the basis of the two-dimensional modelling...
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UAV Survey Images - 3D Model - Gdansk Church Pw. Św. Wojciecha - MP2
Open Research DataDataset description: Raw images from photogrammetric survey. Object: Kościół Rzymskokatolicki Pw. Św. WojciechaLocation: Gdansk, Pomerania, PolandDrone type: DJI Mavic Pro 2Flight plan: Circle (Point Of Interest) + Free flightTarget Product: 3D ModelDate: 02.04.2022Direct georeferencing: yesMetadata data: yes/GPSGCP: YESGCP Quality: RTKCamera Name:...
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UAV Survey Images - DTM- Gdansk Church Pw. Św. Wojciecha - MP2
Open Research DataDataset description: Raw images from photogrammetric survey. Object: Kościół Rzymskokatolicki Pw. Św. WojciechaLocation: Gdansk, Pomerania, PolandDrone type: DJI Mavic Pro 2Flight plan: Double GridTarget Product: Digital Terrain ModelDate: 02.04.2022Direct georeferencing: yesMetadata data: yes/GPSGCP: YESGCP Quality: RTKCamera Name: Hasselblad L1D-20cModel...
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The luminescence study of Sr3−xBaxP5N10Cl: Eu2+ nitridophosphate.
Open Research DataA series of zeolitic nitridophosphate phosphors Sr2.91−xBaxP5N10Cl:0.09Eu2+ was synthesized by our collaborators from National Taiwan University using a hot isostatic press. Detailed thermal properties were determined using the temperature-dependent photoluminescence intensity and decay time. This research provides a different perspective to analyze...
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TG and DTG profiles for plastics: LDPE, HDPE, PP, PD and PET
Open Research DataThe dataset includes:
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UAV Survey Images - 3D Model - Allegory of science figure - on the tower of the main building of Gdansk University of Technology - MP1
Open Research DataDataset description: Raw images from photogrammetric survey. Object: Golden figure at the top of the main bulding of Gdansk University Of TechnologyLocation: Gdansk, Pomerania, PolandDrone type: DJI Mavic Pro 1Flight plan: CircleTarget Product: 3D ModelDate: 13.10.2018Direct georeferencing: yesMetadata data: yes/GPSGCP: NoGCP Quality: N/ACamera Name:...
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UAV Survey Images - 3D Model - Allegory of science figure - on the tower of the main building of Gdansk University of Technology - MP2
Open Research DataDataset description: Raw images from photogrammetric survey. Object: Golden figure at the top of the main bulding of Gdansk University Of TechnologyLocation: Gdansk, Pomerania, PolandDrone type: DJI Mavic Pro 2Flight plan: CircleTarget Product: 3D ModelDate: 08.11.2019Direct georeferencing: yesMetadata data: yes/GPSGCP: NoGCP Quality: N/ACamera Name:...
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UAV Survey Images - orthophotomap- Gdansk University of Technology campus photogrametry test field- MP2
Open Research DataDataset description: Raw images from photogrammetric survey. Object: The photogrametry test field within Gdansk University Of Technology CampusLocation: Gdansk, Pomerania, PolandDrone type: DJI Mavic Pro 2Flight plan: Single GridTarget Product: 3D ModelDate: 17.05.2022Direct georeferencing: yesMetadata data: yes/GPSGCP: YESGCP Quality: RTKCamera Name:...
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Physicochemical and photocatalytic data of Nb-doped faceted TiO2
Open Research DataRaw numerical data, obtained from the physicochemical measurements (XRD, DR-UV/Vis, EPR) and numerical data on photocatalytic activity (phenol degradation and 4-nitrophenol reduction) extracted from the HPLC-DAD results, obtained for the TiO2 nanoparticles that expose majority of the {0 0 1}, {1 0 0} or {1 0 1} facets and were doped with the nominal...
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SEM image and EDS map of SrTi0.50Fe0.50O3-d powder aglomerate
Open Research DataThis dataset contains image of the SrTi0.50Fe0.50O3-d powder aglomerate with EDS map analysis results. Images were obtained using a PhenomXL (Thermo Fisher Scientific, the Netherlands) scanning electron microscope (SEM) with an accelerating voltage of 10 kV in a high vacuum mode. The chemical compositions of the investigated powder were determined...
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SEM image and EDS map of SrTi0.65Fe0.35O3-d powder aglomerate
Open Research DataThis dataset contains image of the SrTi0.65Fe0.35O3-d powder aglomerate with EDS map analysis results. Images were obtained using a PhenomXL (Thermo Fisher Scientific, the Netherlands) scanning electron microscope (SEM) with an accelerating voltage of 10 kV in a high vacuum mode. The chemical compositions of the investigated powder were determined...
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XRD patterns of ammonium vanadate nanocrystals
Open Research DataThe DataSet contains the XRD patterns of ammonium vanadate nanobelts obtained by the hydrothermal method with different conditions. The results show that the structure and phase compositions of samples dependent on reaction conditions.
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XRD patterns of VO2 and V6O13 nanostructures
Open Research DataThe DataSet contains the XRD patterns of VO2 and V6O13 thin films deposited on a silicon substrate. The as-prepared thin films were annealing under a reducing atmosphere (94% Ar, 6% H2) at 500, 600 and 700C for 10h.
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XRD patterns of V2O5 thin film morphology dependent on substrate types
Open Research DataThe DataSet contains the XRD patterns of the V2O5 thin film structure dependent on substrate types. The as-prepared thin films were deposited on alumina, zirconium, zirconium oxide and metallic vanadium substrate, then was annealing under an oxidizing atmosphere at 600C for 10h.
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SEM image and EDS map of SrTi0.30Fe0.70O3-d powder aglomerate
Open Research DataThis dataset contains image of the SrTi0.30Fe0.70O3-d powder aglomerate with EDS map analysis results. Images were obtained using a PhenomXL (Thermo Fisher Scientific, the Netherlands) scanning electron microscope (SEM) with an accelerating voltage of 10 kV in a high vacuum mode. The chemical compositions of the investigated powder were determined...
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XRD patterns of V2O5 nanostructures
Open Research DataThe DataSet contains the XRD patterns of vanadium pentaoxide nanostructures obtained by the sol-gel with different annealing temperatures under synthetic air. The results show that crystallinity dependent on the annealing temperature.
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XRD patterns of VO2 and V2O3 nanostructures
Open Research DataThe DataSet contains the XRD patterns of VO2 and V2O3 nanostructures obtained by the sol-gel with different reaction conditions. The information about xerogel powder synthesis is described in the Journal of Nanomaterials. The xerogel powder was annealing under argon atmosphere in the temperature range 400-1000C. The results show that the morphology...
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XRD patterns of vanadium oxide nanostructures on silicon substrate obtained by V2O5 recrystallization
Open Research DataThe DataSet contains the XRD patterns of vanadium oxide nanostructures on silicon substrates obtained by recrystallization of V2O5 thin films between 800-1200°C under synthetic air. The thin films were obtained by the sol-gel method. The information about sol synthesis is described in the Journal of Nanomaterials.
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XRD patterns of VO2 and V2O3 thin films obtained at 500°C
Open Research DataThe DataSet contains the XRD patterns of VO2 and V2O3 thin films obtained by the sol-gel method. The information about sol synthesis is described in the Journal of Nanomaterials. The thin films with different thicknesses (3-9 AsP layers) were deposited on a silicon substrate and were annealing at 500°C under an argon atmosphere.
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XRD patterns of vanadium oxide nanostructures on quartz glass substrate obtained by V2O5 recrystallization
Open Research DataThe DataSet contains the XRD patterns of vanadium oxide nanostructures on quartz glass substrates obtained by recrystallization of V2O5 thin films between 800-1200°C under synthetic air. The thin films were obtained by the sol-gel method. The information about sol synthesis is described in the Journal of Nanomaterials.
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Chemical composition of V2O5 nanorods
Open Research DataThe DataSet contains the chemical compositions of the V2O5 nanorods on a silicon substrate. The thin films were obtained by the sol-gel method. The information about sol synthesis is described in the Journal of Nanomaterials. The As-prepared thin films were annealed at 600C under a synthetic air atmosphere.
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The structure of electricity production in Poland (data as at the end of 2010)
Open Research DataThe energy market in Poland is characterized primarily by the use of only one raw material for the production of electricity. In 2010, as much as 91.4% of electricity was produced on the basis of hard coal or lignite. Therefore, the remaining sources used for the production of electricity participated in the production of electricity to a small extent....
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XRD patterns of VO2 and V2O3 thin films obtained at 700°C
Open Research DataThe DataSet contains the XRD patterns of VO2 and V2O3 thin films obtained by the sol-gel method. The information about sol synthesis is described in the Journal of Nanomaterials. The thin films with different thicknesses (5-9 AsP layers) were deposited on a silicon substrate and were annealing at 700°C under an argon atmosphere.
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Wnioski dla Polski i regionu Pomorza wynikające z organizacji Mistrzostw Europy w Piłce Nożnej przez Portugalię
PublicationAnaliza przypadku EURO 2004 w Portugalii niesie szereg interesujących wniosków dla Polski w kontekście organizacji przez nasz kraj Mistrzostw Europy w 2012 roku. W opracowaniu podjęto sie próby określenia działań zmierzających do zminimalizowania ryzyka niepowodzenia tej największej sportowej imprezy, jaka kiedykolwiek była przeprowadzana w Polsce.
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Diaminophosphinoboranes: effective reagents for phosphinoboration of CO2
PublicationThe monomeric diaminophosphinoboranes readily react with CO2 under mild conditions to cleanly form products of the general formula R2P-C(=O)-O-B(NR2)2 in the absence of a catalyst. The isolated products from the CO2-phosphinoboration were fully characterized by NMR spectroscopy, IR spectroscopy, and X-ray diffraction. The mechanism of CO2 phosphinoboration with diaminophosphinoboranes was elucidated by DFT calculations.
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Odzysk bioplastiku i celulozy z osadów ściekowych
PublicationW ramach programu Energy and Raw Materials Factory prowadzone są badania nad odzyskiem celulozy oraz biotworzyw. Produkcja biopolimerów oraz bioplastiku ujawnia bowiem niezwykły potencjał obecny w kulturach mikrobiologicznych. Zaczęto także badać odzysk celulozy ze ścieków jako nowe źródła do produkcji kwasu mlekowego, z którego powstają bioplastiki.
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Self-assembly of zinc and cobalt complexes mimicking active site of alcohol dehydrogenase
PublicationPo raz pierwszy zsyntetyzowano obojętne kompleksy cynku i kobaltu naśladujące strukturę centrum aktywnego dehydrogenazy alkoholowej z wodą jako dodatkowym ligandem. Jakość otrzymanych kryształów pozwoliła na szczegółową analizę wewnątrzcząsteczkowych wiązań wodorowych w kryształach tych związków. Wnioski potwierdzono za pomocą spektroskopii FT-IR w ciele stałym.
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Intramolecular interactions in crystals of tris(2,6-diisopropylphenoxy)silanethiol and its sodium salts
PublicationHydrolytically stable tris(2,6-diisopropylphenoxy)silanethiol has been obtained and reacted with sodium. Solid state interactions within and between the molecules of tris(2,6-diisopropylphenoxy)silanethiol including S-H---π-interactions between the S-H unit and the π-system of the arene have been analyzed. The interactions are documented by X-ray diffraction and FT-IR spectroscopy.
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Isostructural zinc and cadmium silanethiolates with bridging biimidazole co-ligands – Enhanced luminescence of zinc complex
PublicationTwo dinuclear complexes of zinc and cadmium with silanethiolate and bridging biimidazole ligands are characterized by X-ray diffraction, FT-IR, UV–Vis and emission spectroscopies. The complexes 1 (Zn) and 2 (Cd) are isostructural but exhibit different electronic structures and different character of frontier HOMO orbitals as indicated by DFT calculations. Lluminescence studies prove strong emission properties of zinc complex.
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Evaluation of cathode materials for electrochemical photocatalyst deposition
PublicationElectrochemical deposition of photocatalyst, especially TiO2, onto several cathode materials was investigated and evaluated. The deposited films were characterized by scanning electron microscopy (SEM), energy dispersive X-ray spectrometer (EDX) and electrochemical measurements. Photocatalytic activity was determined by the decomposition of cyclohexane in air by irradiation with ultraviolet light emitting diodes. It was found that...
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Halogen bonded polypseudorotaxanes based on a pillar[5]arene host
PublicationTwo crystalline supramolecular polypseudorotaxanes were obtained by combining permethylated pillar[5]arene as a macrocyclic wheel with 1,4-bis(1-imidazolyl)butane and 1,4-bis(iodoethynyl)benzene or 1,4-diiodo-1,3-butadiyne linked by C–I⋯N halogen bonds and creating a polyrotaxane axis. The resulting highly ordered supramolecular arrays were characterized by X-ray crystallography.
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Wsadowe i cykliczne szeregowanie 1- i 2-procesorowych zadań jednostkowych na maszynach dedykowanych.
PublicationW pracy autorzy zajmują się modelem szeregowania zadań 1- i 2- procesorowych. Rozważane są przy tym dwa warianty: klasyczny określany jako wsadowy i cykliczny, który występuje w przypadku wielokrotnego powtarzania raz zaprojektowanego harmonogramu. Dla obu przypadków badane są własności teoretyczne i konstruowane algorytmy przybliżone.
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Optymalne układy konstrukcyjne hal stalowych.
PublicationW referacie przedstawiono wyniki analizy wybranych układów konstrukcyjnych hal stalowych z uwagi na nminimum masy konstrukcji. Opracowano algorytm obliczeniowy umożliwiający uwzględnienie wplywu takich czynników jak: schemat statyczny, rozstaw ram i rozstaw płatwii i rodzaj pokrycia dachowego. Przeanalizowano ponad 5 tyś. kombinacji możliwych układów konstrukcyjnych.
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Heavy Metals in a High Arctic Fiord and Their Introduction with the Wastewater: A Case Study of Adventfjorden-Longyearbyen System, Svalbard
PublicationLongyearbyen is the largest settlement on Svalbard archipelago, with 2400 permanent residents and approximately 150,000 tourists visiting every year. The city annually releases approximately 285,000 m3 of untreated wastewater to the nearby Adventfjorden. To date, the environmental impact of this continuous input has been studied mainly regarding the sediments and benthic fauna in the fiord. Here, we present results from a study...
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Enhanced visible light photocatalytic activity of Pt/I-TiO2 in a slurry system and supported on glass packing
PublicationHighly photoactive I/TiO2, Pt/I-TiO2 nanocomposites were obtained using a hydrothermal and wet impregnation method. The incorporation of iodine and modification with 0.05 mol% of platinum leads to enhanced photocatalytic activity as compared to singly doped TiO2 due to the presence of impurity energy level in the structure of TiO2. X-ray diffraction, TEM microscopy, UV–Vis spectroscopy, X-ray photoelectron spectroscopy and BET...
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Exhaled breath gas sensing using pristine and functionalized WO3 nanowire sensors enhanced by UV-light irradiation
PublicationThe development of advanced metal-oxide-semiconductor sensing technologies for the detection of Volatile Organic Compounds (VOCs) present in exhaled breath is of great importance for non-invasive, cheap and fast medical diagnostics. Our experimental studies investigate the effects of operating temperature selection and UV-light irradiation on improving the response of WO3 nanowire sensors towards exhaled breath exposure. Herein,...
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Qualitative characteristics and comparison of volatile fraction of vodkas made from different botanical materials by comprehensive two-dimensional gas chromatography and the electronic nose based on the technology of ultra-fast gas chromatography
PublicationBACKGROUND Vodka is a spirit-based beverage made from ethyl alcohol of agricultural origin. At present, increasingly more vodka brands have labels that specify the botanical origin of the product. Until now, the techniques for distinguishing between vodkas of different botanical origin have been costly, time-consuming and insufficient for making a distinction between vodka produced from similar raw materials. Therefore, it is...
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The influence of nanostructures size on V2O5 electrochemical properties as cathode materials for lithium ion battery
PublicationIn this paper, V2O5 nanostructures with a size depending on the annealing temperature are successfully synthesized by a sol-gel method. The crystal structure and morphology of samples are characterized by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), transmission electron microscopy (TEM), selected area electron diffraction (SEAD) and scanning electron microscopy (SEM), respectively. Electrochemical testing such...
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Local Structure and Stability of SEI in Graphite and ZFO Electrodes Probed by As K-edge Absorption Spectroscopy
PublicationThe evolution of the solid electrolyte interphase (SEI) during the first Li uptake in advanced Li-ion electrodes is studied by X-ray absorption spectroscopy (XAS). The As atoms present in the electrolyte solution were used as a local probe for monitoring the SEI growth on different electrodes. High-quality As K-edge spectra were collected in fluorescence mode for a set of graphite and carbon-coated ZnFe2O4 electrodes. XAS measurements...
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Impact of strontium non-stoichiometry of SrxTi0.3Fe0.7O3-δ on structural, electrical, and electrochemical properties for potential oxygen electrode of intermediate temperature solid oxide cells
PublicationThis work presents the results of a comprehensive study on the impact of the A-site non-stoichiometry of SrxTi0.3Fe0.7O3-δ (x = 0.90, 0.95, 1.00, 1.05) ceramics on their physicochemical properties. The materials were fabricated by the conventional solid-state reaction method and their structure was determined by X-ray diffractometry, X-ray photoelectron spectroscopy and electron microscopy. Their sintering and thermal expansion...