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Wyniki wyszukiwania dla: FTIR spectrum of formaldehyde
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Temperature measurement of supercapacitor with the use of ZnO coated microsphere-based fiber-optic sensor - 40 Celsius degrees
Dane BadawczeApplication of a microsphere-based fiber-optic sensor with 200 nm zinc oxide (ZnO) coating, deposited by Atomic Layer Deposition (ALD) method, for temperature measurements of supercapasitor, is presented. Internal temperature of the supercapacitor is investigated in the range between 30°C and 90°C. The supercapacitor temperature was investigated using...
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Temperature measurement of supercapacitor with the use of ZnO coated microsphere-based fiber-optic sensor - 85 Celsius degrees
Dane BadawczeApplication of a microsphere-based fiber-optic sensor with 200 nm zinc oxide (ZnO) coating, deposited by Atomic Layer Deposition (ALD) method, for temperature measurements of supercapasitor, is presented. Internal temperature of the supercapacitor is investigated in the range between 30°C and 90°C. The supercapacitor temperature was investigated using...
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Temperature measurement of supercapacitor with the use of ZnO coated microsphere-based fiber-optic sensor - 55 Celsius degrees
Dane BadawczeApplication of a microsphere-based fiber-optic sensor with 200 nm zinc oxide (ZnO) coating, deposited by Atomic Layer Deposition (ALD) method, for temperature measurements of supercapasitor, is presented. Internal temperature of the supercapacitor is investigated in the range between 30°C and 90°C. The supercapacitor temperature was investigated using...
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Wpływ glikolu na przebieg glikolizy oraz właściwości, budowę i stabilność termiczną glikolizatów i otrzymanych z ich udziałem poliuretanów
PublikacjaCelem pracy było zbadanie wpływu zastosowanych glikoli na przebieg glikolizy odpadowych pianek poliuretanowych (PUR) w procesach w których stosowano masowy nadmiar odpadu poliuretanowego w stosunku do środka glikolizującego oraz budowy i odporności termicznej poliuretanów z glikolizatów. Glikolizaty otrzymywano w reakcji odpadowej pianki poliuretanowej z glikolami o 3 - 6 atomach węgla w cząsteczce. Proces glikolizy katalizowano...
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Effect of crystallinity on structural, thermal, and in vitro dissolution properties of Na2O-CaO-Nb2O5/MgO-P2O5 glass-ceramics
PublikacjaThe impact of the crystallinity on structural, thermal, and in vitro dissolution properties were examined for Na2O- CaO-Nb2O5/MgO-P2O5 glasses/glass-ceramics. Glass-ceramics were synthesized via a spontaneous crystallization process. The Nb content in the materials increased with melting temperature, furthermore, the crystallinity is proportional to the Nb content. The presence of crystalline niobates and phosphates is confirmed...
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Arbutin: Isolation, X-ray structure and computional studies
PublikacjaArbutin, an active component originated from Serratula quinquefolia for skin-whitening use and treating skin related allergic inflammation, was characterized by microanalysis, FTIR, UV-Vis, multinuclear NMR spectroscopy, and single crystal X-ray diffraction method. The geometries of the studied compound were optimized in singlet states using the density functional theory (DFT) method with B3LYP functional. Electronic spectra were...
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Spectral reflectance modeling of ZnO layers made with Atomic Layer Deposition for application in optical fiber Fabry-Perot interferometric sensors
PublikacjaSuitability of zinc oxide (ZnO) layers grown using Atomic Layer Deposition for operation in optical-fiber extrinsic Fabry-Perot sensors is investigated using a numerical model. Reflectance spectra obtained using the developed model indicate that the application of these layers in optical-fiber extrinsic Fabry-Perot sensors is difficult as it may require a source whose spectrum width is about 300 nm. A series of ZnO layers grown...
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Selection of excitation signals for high-impedance spectroscopy
PublikacjaA method of fast impedance spectroscopy of technical objects with high impedance (|Zx| > 1 GOhm) is evaluated in this paper. An object is excited with a signal generated by a digital-to-analog converter (DAC) located on the U2531A DAQ module. Response signals proportional to current flowing through and voltage across the measured object are sampled by analog-to-digital converters (ADC) in the DAQ module. The object impedance spectrum...
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An optimal form of the finite element mass matrix in the analysis of longitudinal vibrations of rods
PublikacjaIn this paper, an attempt is made to find the optimal form of the mass matrix of a rod finite element, which allows one to obtain the smallest errors in the longitudinal frequency determination of natural vibrations of any boundary conditions within the whole range of determined frequencies. It is assumed that the mass matrix can be treated as a linear combination of the consistent and diagonal matrices. Based on analytical considerations,...
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Multispectral impedance quality testing of coil-coating system using principal component analysis
PublikacjaThe task of quality checking of the coil-coated system was undertaken using impedance spectroscopy. In order to properly characterize the system the new impedance spectrum was calculated as an averaged result of 12 experimental spectra obtained from 12 different places of the sample at the same time of immersion in 3% of NaCl. The experimental spectra were recorded for a 24-h period at 1 h intervals between starting points of each...
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Analysis of the instantaneous power signal for bearing diagnostics -bearing damaged
Dane BadawczeThe attached dataset contains the measurement results of the instantaneous values of current and voltage, recorded during the diagnostics of a damaged bearing. Bearing diagnostics can be carried out based on the method, which relies on the measurement and analysis of the variability of the signal instantaneous power, defined as the product of instantaneous...
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Analysis of the instantaneous power signal for bearing diagnostics - bearing undamaged
Dane BadawczeThe attached dataset contains the measurement results of the instantaneous values of current and voltage, recorded during the diagnostics of an undamaged bearing. Bearing diagnostics can be carried out based on the method, which relies on the measurement and analysis of the variability of the signal instantaneous power, defined as the product of instantaneous...
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Instantaneous power signal measurements for bearing diagnostics
Dane BadawczeBearing diagnostics can be carried out based on the method, which relies on the measurement and analysis of the variability of the signal instantaneous power, defined as the product of instantaneous current and voltage power supplied to the engines. Bearing damage causes the appearance of deformations, which are in the form of additional harmonic components...
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Theory and application of Near-infrared spectroscopy
PublikacjaIn recent years one can observe a significant increase in the requirements on quality control in all industrial sectors. The growing number of involved analyses makes the traditional, time consuming, requiring use of large quantities of reagents, thus expansive methods inconvenient especially for industrial applications. Fortunately, there is a very fast, cheap and not invasive analytical method that is increasingly used in qualitative...
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Quantification of Compatibility Between Polymeric Excipients and Atenolol Using Principal Component Analysis and Hierarchical Cluster Analysis
PublikacjaAn important challenge to overcome in the solid dosage forms technology is the selection of the most biopharmaceutically efficient polymeric excipients. The excipients can be selected, among others, by compatibility studies since incompatibilities between ingredients of the drug formulations adversely affect their bioavailability, stability, efficacy, and safety. Therefore, new, fast, and reliable methods for detecting incompatibility...
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Metody usuwania zakłóceń podczas pomiarów polowych widm Ramana
PublikacjaW pracy zostały scharakteryzowane źródła zakłóceń występujące podczas pomiarów widm Ramana w warunkach polowych. Zaprezentowano wpływ czasu integracji na jakość rejestrowanych widm w przypadkach, gdy szumy własne spektrometru mają składową typu 1/f, dominującą w zakresie małych częstotliwości. Przedstawiono także wyniki uzyskane podczas pomiarów z detekcją synchroniczną, stosowaną w przenośnych spektrometrach Ramana, w pomiarach...
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Comparative Evaluation of Multicoil Inductive Power Transfer Approaches Based on Z-source Network
PublikacjaThis paper describes comparative evaluation between wireless power transfer topologies with utilization of Z-source network. Paper describes components calculation method. List of open-loop, close-loop simulations were conducted to compare both topologies. Spectrum of signals is also researched.
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Analiza porównawcza olejów z pirolizy opon oraz pirolizy biomasy, pod względem użyteczności jako paliwa
PublikacjaRosnąca niestabilność na tradycyjnych rynkach paliw kopalnych ożywiła zainteresowanie produkcją paliw alternatywnych z biomasy. Piroliza jest obiecującym procesem dla konwersji biomasy odpadowej w użyteczne paliwo płynne. W niniejszej pracy przedstawiono analizę porównawczą olejów z pirolizy opon oraz pirolizy biomasy, pod względem bezpośredniego wykorzystania jako paliwa. Olej z pirolizy opon został dostarczony przez zakład utylizacji...
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Analiza porównawcza olejów z pirolizy opon oraz pirolizy biomasy, pod względem użyteczności jako paliwa
PublikacjaRosnąca niestabilność na tradycyjnych rynkach paliw kopalnych ożywiła zainteresowanie produkcją paliw alternatywnych z biomasy. Piroliza jest obiecującym procesem dla konwersji biomasy odpadowej w użyteczne paliwo płynne. W niniejszej pracy przedstawiono analizę porównawczą olejów z pirolizy opon oraz pirolizy biomasy, pod względem bezpośredniego wykorzystania jako paliwa. Olej z pirolizy opon został dostarczony przez zakład utylizacji...
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Interactions between hydration spheres of two different solutes in solution: The least squares fitting with constraints as a tool to determine water properties in ternary systems
PublikacjaBiological systems are complex and the problem of their description lies in mutual interactions between their components. This paper is focused on model experiment-based studies which can reduce these difficulties. The ternary aqueous N-methylacetamide (NMA)–Na2HPO4 system has been studied by means of the FTIR spectroscopy. A novel difference spectra method aimed to extract the spectral contribution of water affected simultaneously...
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Reclaimed Rubber/Poly(ε‐caprolactone) Blends: Structure, Mechanical, and Thermal Properties
PublikacjaThe amount of elastomeric waste, especially from tires is constantly increasing on a global scale. The recycling of these residua should be considered a priority. Compounding the waste rubbers with other polymers can be an excellent alternative to reuse waste materials. This procedure requires solving the issue of the lack of compatibility between the waste rubber particles and other polymers. Simultaneously, there is a claim for...
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Effect of waviness and roughness components on transverse profiles of turned surfaces
PublikacjaThis paper presents the authors method of simultaneous analysis of roughness and waviness irregularity components, with the aim of better defining the key qualities and characteristics.Periodical surface machining traces may be analyzed spectrally, with the irregularity's peaks and troughs being used to define the wave's amplitude.In this work the standard composition for filtering waviness and roughness components of a surface...
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Detection system for optical coherence tomography: Czerny-Turner spectrometer
PublikacjaResearch methods based on spectral analysis have powerful impact on development in many field of science. Signal spectrum can be a source of useful and important data. It enables to obtain information about physical and chemical properties of tested materials. This paper has been devoted to describe optical design for high resolution spectrometer, which is significant element of optical coherence tomography (OCT) systems. Designed...
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Fiber-optic Fabry-Pérot sensors – modeling versus measurements results
PublikacjaThis paper describes how parameters of investigated substances and the fiber-optic Fabry-Pérot sensing interferometer affect the spectrum of the optical radiation at the output of the sensor. First, the modeling of the operation of the sensing interferometer was conducted. Most important parameters and effects that were taken into account are: dependences of the refractive indices of the core and the cladding, as well the mode...
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Recycling of Polyurethanes Containing Flame-Retardants and Polymer Waste Transformed into Flame-Retarded Polyurethanes
PublikacjaThe growing number of polyurethanes (PUs) produced every year has developed methods for their mechanical and chemical recycling which yield valuable products like substitutes for commercial polyols or flame-retardants. PUs can be produced in different shapes and forms (i.e., elastomers, flexible or rigid foams, coatings, etc.) using several different components (i.e., di- or polyisocyanates, ester- or ether-based polyols, low-molecular...
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The role of organic and mineral constituents on kerogen transformation ratio
PublikacjaThe main aim of this dissertation is to determine the role of mineral and organic matter constituents in kerogen transformation ratio. Practical aspects of the work include application of the results in the assessment of hydrocarbon production potential; to make process of hydrocarbon recovery more predictable consistent and efficient. The work used shale from the Vaca Muerta formation from the Nequen basin in Argentina. The formation...
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Synthesis and Investigation of Glycolysates and Obtained Polyurethane Elastomers
PublikacjaScharakteryzowano proces glikolizy poprodukcyjnych odpadów poliuretanowych przeprowadzony przy użyciu glikolu heksametylenowego. Przedstawiono niektóre właściwości fizykochemiczne otrzymanych glikolizatów. Omówiono wyniki analizy termicznej, termomechanicznej oraz budowy chemicznej metodą FTIR zsyntetyzowanych elastomerów poliuretanowych. Właściwości mechaniczne zmierzono w warunkch statycznych przy użyciu uniwersalnej maszyny...
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Demonstrator technologii C-IED
PublikacjaArtykuł przedstawia budowę i działanie opracowanego na Politechnice Gdańskiej demonstratora technologicznego systemu AEGIS, przeznaczonego do przeciwdziałania atakom z wykorzystaniem prowizorycznych urządzeń wybuchowych detonowanych drogą radiową (RCIED — Radio Controlled Improvised Explosive Devices). Przedstawiono zaimplementowaną oryginalną metodę generowania sygnału zagłuszającego o dowolnie ukształtowanym widmie częstotliwościowym,...
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Dependence of biological sensing on temperature based on investigation of SARS-CoV-2
Dane BadawczePresented dataset is the result of an investigation of the attachment of SARS-CoV-2 specific IgG in the temepratures relevant in biology. The samples were measured during a period of 15 minutes, at 5°C, 25°C and 55°C. The measurements were performed using the microspher-based fiber-optic sensor, as an interferometer. The broadband optical light source...
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The electronic excited states of dichloromethane in the 5.8-10.8 eV energy range investigated by experimental and theoretical methods
PublikacjaWe present a comprehensive experimental high-resolution vacuum ultraviolet (VUV) photoabsorption spectrum of dichloromethane, CH 2 Cl 2 , with absolute cross sections determined for the full 5.8–10.8 eV energy-range. The calculations on the vertical excitation energies and oscillator strengths were performed using the equation-of-motion coupled cluster method, restricted to the single and double excitations level (EOM-CCSD), and...
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Unusual Influence of Fluorinated Anions on the Stretching Vibrations of Liquid Water
PublikacjaInfrared (IR) spectroscopy is a commonly used and invaluable tool in the studies of solvation phenomena in aqueous solutions. Concurrently, ab initio molecular dynamics (AIMD) simulations deliver the solvation shell picture at a molecular detail level and allow for a consistent decomposition of the theoretical IR spectrum into underlying spatial correlations. Here, we demonstrate how the novel spectral decomposition techniques...
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DMSO and TMAO—Differences in Interactions in Aqueous Solutions of the K-Peptide
PublikacjaInteractions between a solvent and their co-solute molecules in solutions of peptides are crucial for their stability and structure. The K-peptide is a synthetic fragment of a larger hen egg white lysozyme protein that is believed to be able to aggregate into amyloid structures. In this study, a complex experimental and theoretical approach is applied to study systems comprising the peptide, water, and two co-solutes: trimethylamide...
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Proton transfer and hydrogen bonds in supramolecular, self-assembled structures of imidazolium silanethiolates. X-ray, spectroscopic and theoretical studies
PublikacjaThe reaction of 1-methylimidazole, 2-ethyl-4-methylimidazole and 2-ethylimidazole with tris(2,6- diisopropylphenoxy)silanethiol (TDST) leads to the formation of three new salts, which have been characterized by elemental analyses, thermogravimetric analyses, FTIR spectroscopy, and their structures were determined by single-crystal X-ray diffraction. Structural analyses indicate that in all three compounds a proton transfer has...
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MODELLING OF TOXIC COMPOUNDS EMISSION IN MARINE DIESEL ENGINE DURING TRANSIENT STATES AT VARIABLE PRESSURE OF FUEL INJECTION
PublikacjaTransient states are an important part of the spectrum of engine loads, especially the traction engines. In the case of marine diesel engines, transient states are of particular importance in reducing the analysis of motion units for special areas and maneuvering in port, the participation of transient states in the load spectrum significantly increases, also, the emission of toxic compounds from this period increases proportionally....
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Interactions of fish gelatin and chitosan in uncrosslinked and crosslinked with EDC films: FT-IR study
PublikacjaFilms based on fish gelatin, chitosan and blend of fish gelatin and chitosan before and after cross-linking with EDC have been characterized by FT-IR spectroscopy. The FT-IR spectrum of fish gelatin film showed the characteristic amide I, amide II and amide III bands, and the FT-IR spectrum of chitosan film confirmed that the polymer was only a partially deacetylated product, and included CH3-C=O and NH2 groups, the latter both...
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Investigating Feature Spaces for Isolated Word Recognition
PublikacjaThe study addresses the issues related to the appropriateness of a two-dimensional representation of speech signal for speech recognition tasks based on deep learning techniques. The approach combines Convolutional Neural Networks (CNNs) and time-frequency signal representation converted to the investigated feature spaces. In particular, waveforms and fractal dimension features of the signal were chosen for the time domain, and...
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Electronic structure and rovibrational predissociation of the 2^1Π state in KLi
PublikacjaAdiabatic potential energy curves of the 3^1Σ^+, 3^3Σ^+, 2^1Π and 2^3Π states correlating for large internuclear distance with the K(4s) + Li(2p) atomic asymptote were calculated. Very good agreement between the calculated and the experimental curve of the 2^1Π state allowed for a reliable description of the dissociation process through a small (∼20 cm−1 for J = 0) potential energy barrier. The barrier supports several rovibrational...
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Application of analytical methods for the determination of bioactive compounds in some berries
PublikacjaFluorometry, ESI-MS, FTIR, and radical scavenging assays were used for characterization of bioactive compounds and the levels of their antioxidant activities. Polyphenols, flavonoids, anthocyanins, and ascorbic acid and the level of antioxidant activity of water extracts of “Murtilla-like” [Myrteola nummularia (Poiret) Berg.], and other widely consumed berries were determined and compared. The contents of bioactive compounds and...
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The Influence of Calcium Glycerophosphate (GPCa) Modifier on Physicochemical, Mechanical, and Biological Performance of Polyurethanes Applicable as Biomaterials for Bone Tissue Scaffolds Fabrication
PublikacjaIn this paper we describe the synthesis of poly(ester ether urethane)s (PEEURs) by using selected raw materials to reach a biocompatible polyurethane (PU) for biomedical applications. PEEURs were synthesized by using aliphatic 1,6-hexamethylene diisocyanate (HDI), poly(ethylene glycol) (PEG), α,ω-dihydroxy(ethylene-butylene adipate) (Polios), 1,4-butanediol (BDO) as a chain extender and calcium glycerolphosphate salt (GPCa) as...
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Poli(uretanoepoksydy) otrzymane z opracowanych małocząsteczkowych przedłużaczy łańcuchów
PublikacjaPrzeprowadzono syntezy małocząsteczkowych przedłużaczy łańcuchów z żywicy epoksydowej Epidian 6 oraz 4-ech glikoli. Budowę produktów scharakteryzowano FTIR i 13C NMR. Zsyntezowane związki wykorzystano w reakcji z prepolimeramiuretanowymi otrzymując nowe materiały nazwane poli(uretanoepoksydami). Zbadano statyczne i dynamiczne właściwości mechaniczne oraz właściwości termiczne otrzymanych polimerów.
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Surface properties of barley straw
PublikacjaWłaściwości powierzchniowe słomy jęczmiennej (Hordeum vulgare) odgrywają kluczową rolę w zastosowaniach przemysłowych, takich jak sorpcja rozlewów olejowych oraz oczyszczenie gleby. Zbadano niejednorodność chemiczną oraz morfologiczną liści i łodyg słomy jęczmiennej poprzez pomiar kątów zwilżania wodą oraz olejem oraz z zastosowaniem techniki FTIR, SEM oraz AFM.
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Analysis of odour interactions in model gas mixtures using electronic nose and fuzzy logic
PublikacjaMeasurement and monitoring of air quality in terms of odour nuisance is an important problem. Although the source of these nuisances is different (e.g. wastewater treatment plants, municipal landfills), their common feature is that they are a complex mixture of odorants with different odour thresholds. An additional problem is occurrence of the odour interactions between mixture components. From a practical point of view, it would...
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Evaluation of Health Hazard Due to Emission of Volatile Organic Compounds from Various Processing Units of Wastewater Treatment Plant
PublikacjaThe paper describes an attempt at health risk assessment and odour concentration determination in the most important units of a wastewater treatment plant. The cancer risk (CR) and hazard index (HI) parameters in selected measurement locations were calculated based on the results of chromatographic analyses (GCxGC-TOF-MS) and the United States Environmental Protection Agency (US EPA) guidelines. No exceedance of the CR and HI acceptable...
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Narrowband Transmission Quality in Presence of Modified IEEE 802.15.4a Impulse Radio Interference
PublikacjaThis paper presents results of measurement of narrowband transmission quality in presence of impulse radio UWB interference. IEEE 802.15.4a UWB signal is being used as interferer, also with frame structure modifications which lead to change spectrum of the interference. Equations and coefficients which allow to calculate ratio between power of useful and interference signal are also presented.
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Frequency response spectra applied to assess efficiency of the training techniques
PublikacjaThe purpose of the research is to assess the increase of the muscle strength and power. Movement of the human body when the moving one impacts a stationary or moving body is taken under consideration. The waveform produced by an impact is transformed into frequency domain. The acceleration record is transformed as a complex spectrum, by the use of a Discrete Fourier Transformation. In this paper the applications of the discrete...
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Multi-mode vibronic interactions in the five lowest electronic states of the fluorobenzene radical cation
PublikacjaThe multi-mode vibronic interactions between the five lowest electronic states of the fluorobenzene radical cation are investigated theoretically, based on ab initio electronic structure data, and employing the linear vibronic coupling model. Low-energy conical intersections, and strong vibronic couplings are found to prevail within the set of X-A and B-C-D cationic states, while the interactions between these two sets of states...
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Objectivity in the non-Markovian spin-boson model
PublikacjaObjectivity constitutes one of the main features of the macroscopic classical world. An important aspect of the quantum-to-classical transition issue is to explain how such a property arises from the microscopic quantum theory. Recently, within the framework of open quantum systems, there has been proposed such a mechanism in terms of the so-called spectrum broadcast structures. These are multipartite quantum states of the system...
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Impedance spectra of ZnO varistor type 280 model O M ver. 89
Dane BadawczeThe impedance spectrum of high-voltage ZnO varistor obtained using FRA EIS impedance spectrosocpy measurement method. The 1V sinusoidal excitation was used. The frequency range was chosen from 10 kHz down to 100 uHz. The object under test and the measuring instrument were placed in a Faraday cage due to high impedance of the object. The data was acquired...
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Ewa Kamieńska-Piotrowicz dr hab. inż.
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Tellurite based glass doped by Eu3+ ions - XPS measurements
Dane BadawczeEu3+ doped tellurite glass ceramics containing SrF2 nanocrystals were prepared using melt quenching technique and subsequent heat treatment of glass in 370 °C for different time periods. Thermal properties of glass matrix have been determined based on DSC measurements. XRD and XPS results confirmed formation of SrF2 nanocrystals in glass matrices after...