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Search results for: bio-based 1,3-propanediol
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Pharmaceuticals and other contaminants of emerging concern in Admiralty Bay as a result of untreated wastewater discharge: Status and possible environmental consequences
PublicationConsidering how the impact of human activity in Antarctica is growing, the aim of this study was to conduct the first assessment of pharmaceuticals and personal care products (PPCPs), other emerging contaminants (ECs), and antibiotic resistance genes present in the western shore of the Admiralty Bay region of King George Island. In total, more than 170 substances were evaluated to assess the potential environmental risks they pose...
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SEI Growth and Depth Profiling on ZFO Electrodes by Soft X-Ray Absorption Spectroscopy
PublicationZnFe2O4 (ZFO) Li-ion batteries (LIBs) represent a reliable, affordable, and safe energy storage technology for use in portable application. However, current LIB active materials (graphite, lithium/transition metal spinel or layered oxides, olivine structures) can store only limited energy since they rely on insertion storage based on solid-state host-guest interactions. Moreover, performances and durability of the cells are strongly...
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Physicochemical Properties and Application of Silica-Doped Biochar Composites as Efficient Sorbents of Copper from Tap Water
PublicationThis article concerns research on new sorption materials based on silica-doped activated carbon. A two-stage synthesis involved pyrolysis of plant material impregnated in a water glass solution , followed by hydrothermal activation of the pyrolysate in KOH solution. The resulting composite can be used as a sorbent in drinking water filters. The proposed method of synthesis enables the design of materials with a surface area...
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Cathodically activated Au/TiO2 nanocomposite synthesized by a new facile solvothermal method: An efficient electrocatalyst with Pt-like activity for hydrogen generation
PublicationWe report here a facile, template-free and one-step solvothermal approach for the synthesis of high-temperature stable gold/titania nanocomposite (NCs), providing a new, simple, quick and inexpensive wet-chemical route. Our approach is based on the assembly of gold salt and titanium butoxide in dimethyl sulfoxide (DMSO). Also, we present here, for the first time, a cathodically activated Au/TiO2 catalyst with Pt/C activity for...
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A la recherche d’une coherence perdue – Possible Arguments for the Non-application of EU Law in Member States
PublicationThe European Union (EU) is an international organization which has a broad scope of competences that have been transferred to it by its Member States in the founding Treaties. The object of the article is to identify arguments raised, or that potentially might be raised, by national Constitutional Courts (and in the future possibly by other actors as well) to exclude in certain instances the application of EU law or EU jurisprudence...
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Multibeam Sonar Characterisation of Seafloor in the Context of Visualisation and Dissemination of Marine Data
PublicationThe paper presents the seafloor characterisation method based on multibeam sonar data. it relies on using three types of multibeam seafloor sensing data: 1) the grey-level sonar images (echograms) of seabed, 2) the 3D model of the seabed surface which consists of high resolution bathymetric data, 3) the set of time domain bottom echo envelopes received in the consecutive sonar beams. The classification is performed by utilisation...
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Comparative field test for measurement of PM10 dust in atmospheric air using gravimetric (reference) method and b-absorption method (Eberline FH 62-1)
PublicationThe paper presents the results of a field test carried out in Gdansk region between 01-01-2010 and 31-12-2010 in order to demonstrate equivalence of the Eberline FH 62-1 sampler to the reference gravimetric method of suspended PM10 dust measurement. The differences in PM10 dust concentration provided by both methods have been discussed for different seasons of the year. A method of estimation of the correction factors/correction...
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Transport properties of aqueous ionic liquid microemulsions: influence of the anion type and presence of the cosurfactant
PublicationTransport properties, viz. specific conductivity, dynamic viscosity and apparent diffusion coefficients, were measured as a function of water content in aqueous ionic liquid microemulsions containing 1-butyl-3- methylimidazolium hexafluorophosphate, [BMIM][PF6] and bis(trifluoromethanesulphonyl)imide, [BMIM][Tf2N], stabilized by the nonionic surfactant TX-100, or its mixture with a cosurfactant, i.e. butanol. The investigation covered...
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The Usefulness of Cyclic Diamidines with Different Core-substituents as Antitumor Agents
PublicationA series of related polycationic compds. has been screened for potential antitumor activity by the NCI's in vitro testing (one dose primary anticancer assay and the NCI-60 full panel screening). The GI50 values of triazines 3 and 4 are on av. 1.9 μM and 2.4 μM, resp. Furan 8 deserves mention too (1.9 μM). The biol. test results showed that carbazole 10 possessed cytotoxic activity in the nanomolar range, much better than...
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Magnetic deep eutectic solvents as efficient media for extraction of furfural and 5-hydroxymethylfurfural from aqueous samples
PublicationThe extraction of furfural (FF) and 5-hydroxymethylfurfural (HMF) from hydrolysates is currently one of the main challenges in bio-refinery. In this work, the separation of FF and HMF from the aqueous phase was carried out using a new type of green solvents – Magnetic Deep Eutectic Solvents (MDES). A conductor-like screening model for realistic solvents (COSMO-RS) was used for the preselection of 400 MDES. MDES which exhibit the...
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Synthesis of compounds with C-P-P and C=P-P bond systems based on the phospha-Wittig reaction
PublicationA reactivity study of a β-diketiminate titanium(III) phosphanylphosphido complex [MeNacNacTi(Cl){η2-P(SiMe3)-PtBu2}] (1) towards ketones such as benzophenone, 9-fluorenone, acetophenone, cyclopentanone, cyclohexanone and cycloheptanone is reported. The reactions of 1 with aromatic ketones (without α-protons) directly lead to the Ti(III) complex [MeNacNacTi(μ2-Cl)(OSiMe3)] (5) as well as Ti(IV) complexes with the pinacol condensation...
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Potential applications of crude glycerol in polymer technology–Current state and perspectives
PublicationThe increasing use of bio-based fuels and fuel additives, among them biodiesel, causes significant surplus of crude glycerol on the market which creates new challenges in terms of its sustainable utilization. A lot of ways for the incorporation of this by-product into different branches of industry requires purification by expensive and complicated processes. Therefore, researchers are seeking for applications of untreated crude...
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Perspectives on the replacement of harmful organic solvents in analytical methodologies: a framework toward the implementation of a generation of eco-friendly alternatives
PublicationVolatile organic solvents derived from non-renewable fossil feedstocks are commonplace in analytical laboratories. In spite of their convenient performance in countless unit operations, their environmental, health and safety issues represent a major area of concern. The progressive replacement of organic solvents obtained from fossil resources by eco-friendly alternatives would involve remarkable advances within the framework of...
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A nine-input 1.25 mW, 34 ns CMOS analog median filter for image processing in real time
PublicationIn this paper an analog voltage-mode median filter, which operates on a 3 × 3 kernel is presented. The filter is implemented in a 0.35 μm CMOS technology. The proposed solution is based on voltage comparators and a bubble sort configuration. As a result, a fast (34 ns) time response with low power consumption (1.25 mW for 3.3 V) is achieved. The key advantage of the configuration is relatively high accuracy of signal processing,...
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Estimation of platinum in environmental water samples with solid phase extraction technique using inductively coupled plasma mass spectrometry
PublicationZoptymalizowano metodykę oznaczania śladowych poziomów stężeń platyny (IV) w oparciu o technikę ekstrakcji do fazy stałej w połączeniu ze spektrometrią mas z plazmą wzbudzoną indukcyjnie. Na etapie wzbogacania platyny wykorzystano żel krzemionkowy modyfikowany grupami aminopropylowymi. Ilościowy odzysk platyny uzyskano poprzez wykorzystanie 1.0 mol L-1 roztworu tiomocznika jako eluenta. Odchylenie standardowe wyników (RSD) było...
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The electrochemical determination of isatin at nanocrystalline boron-doped diamond electrodes: stress monitoring of animals
PublicationUltra-thin nanocrystalline boron-doped diamond electrodes (B:NCD) were used for the electrochemical determination of isatin in dog urine samples using cyclic voltammetry and square wave voltammetry in a phosphate buffer saline, pH = 7.2. No additional modification or pretreatment of the electrode surface was required in this approach, being of high importance for the facile detection procedure. The increase of the peak current...
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Kant i kantyzmy.O okresach i sposobach obecności Kanta w filozofii
PublicationArtykuł opisuje pięć okresów obecności Kanta:1. Wczesny kantyzm, ktory nie miał do czynienia z zamkniętym obrazem Kanta, 2.Idealizm niemiecki, gdzie Kant staje się częścią rozwoju idealizmu niemieckiego' 3.Neokantyzm redukujący filozofię do teorii poznania i wartości,4.Okres powrotu do realizmu i do ontologicznej oraz metafizycznej interpretacji Kanta,5.Okres współczesny.
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Wpływ stoczni na środowisko naturalne
PublicationW referacie, w sposób przeglądowy, opisano podstawowe problemy związane z wpływem stoczni na środowisko naturalne. Podpunkty 1 i 2 odnoszą się do sytuacji przeszłej i obecnej. Podpunkty 3 i 4 odnoszą się do sytuacji nowej, która wynika ze wstąpienia Polski do UE. Pociąga to za sobą konieczność wprowadzenia zmian dostosowawczych przez każdą ze stoczni.
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Continuous and discontinuous modeling of cracks in concrete elements
PublicationW artykule przedstawiono różne sposoby modelowania rys w elementach betonowych w warunkach mieszanego sposobu obciążenia przy zastosowaniu modeli ciągłych i nieciągłych. Symulacje wykonano przy zastosowaniu 3 różnych modeli ciągłych: modelu sprężysto-plastycznego, modelu w ramach mechaniki zniszczeniowej i modelu rys rozmytych z rysami obracającymi się oraz 1 modelu nieciągłego przy zastosowaniu stref kontaktu..
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Photoconduction and magnetic field effect on photoconduction in hole-transporting star-burst amine (m-MTDATA) films
PublicationPhotoconduction and magnetic field effect on photoconduction have been investigated as a function of electric field strength, excitation light intensity and wavelength in vacuum evaporated films of m-MTDATA (4,4′,4″-tris(N-(3-methylphenyl)-N-phenylylamino) triphenylamine), the starburst amine commonly used as hole-transporting material in organic light-emitting diodes. The photocurrent is found to be generated by the singlet exciton...
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Electrochemical activity and characterization of hybrid material consisted of poly(3,4- ethylenedioxythiophene) and silver hexacyanocobaltate
PublicationPrac przedstawiono charakterystykę elektrochemiczną oraz powierzchniową materiału hybrydowego składającego się z polimeru przewodzącego, poli(3,4-etylenodioksytiofenu) oraz nieorganicznej sieci typu redoks, heksacyjanokobaltanu srebra. Materiał scharakteryzowano technikami jak AFM, SEM. Skład materiału oznaczono za pomocą mikroanalizy rentgenowskiej EDX. Analiza potwierdziła obecność sieci nieorganicznej w materiale. Proporcja...
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Optimisation of conditions for precipitation of collagen from solution using kappa-carrageenan. Studies on collagen from the skin of Baltic cod (Gadus morhua)
PublicationZbadano wpływ stężenia kolagenu (0,012-3%) wyekstrahowanego ze skór dorsza bałtyckiego (Gadus morhua) i stężenia kappa-karagenu w obecności NaCl (0-5%) na wydajność strącania włókien kolagenowych z roztworu przy pH 2,2-8. Stwierdzono, że wydajność strącania włókien jest wprost proporcjonalna do masowego stosunku kappa-karagen : kolagen w zakresie niższym od 0,4. Kolagen rozpuszczony w kwasie cytrynowym jest całkowicie strącony,...
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Effect of glycosoaminoglycans on reconstitution of collagen fibrils
PublicationCelem pracy było sprawdzenie efektywności rekonstytucji fibryli i włókien z roztworu kwasu solnego kolagenu skór bydlęcych pod wpływem glikozaminoglikanów (GAGs), wydzielonych z tchawic bydlęcych, w układach o sile jonowej w zakresie 0-0,7 oraz pH 3-8. Stwierdzono, że dodatek GAGs do roztworu kolagenu powoduje natychmiastowe powstawanie włókien, których ilość wzrasta wraz z ilością dodanych glikozaminoglikanów i stężeniem kolagenu....
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Development of an Analytical Protocol for Determination of Cyanide in Human Biological Samples Based on Application of Ion Chromatography with Pulsed Amperometric Detection
PublicationA simple and accurate ion chromatography (IC) method with pulsed amperometric detection (PAD) was proposed for the determination of cyanide ion in urine, sweat, and saliva samples. The sample pretreatment relies on alkaline digestion and application of Dionex OnGuard II H cartridge. Under the optimized conditions, the method showed good linearity in the range of 1–100 μg/L for urine, 5–100 μg/L for saliva, and 3–100 μg/L for sweat...
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Application of theory of semi-Markov processes to determining distribution of probabilistic process of marine accidents resulting from colission of ships
PublicationIn this paper is presented possible application of the theory of semi-Markov processes to elaborating an eight-state model of the process of occurrence of serviceability state and unserviceability states of sea-going ships making critical manoeuvres during their entering and leaving the ports. In the analysis it was taken into account that sea-going ships are in service for a very long time t (t → ∞). The model was elaborated to...
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Use of pyridinium and pyrrolidinium ionic liquids for removal of toluene from gas streams
PublicationSeparation of toluene from a toluene/N2 gas mixture using supported liquid membranes based on a series of pyridinium (1-butylpyridinium- bis(trifluoromethylsulfonyl)imide - [C4Py][Tf2N], 1-hexylpyridinium trifluoromethanesulfone [C6Py][Tf2N]) and pyrrolidinium (1-butyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl)imide - [C4Pyrr][Tf2N], 1-hexyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl)imide - [C6Pyrr][Tf2N], 1-butyl-1-methylpyrrolidinium...
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Towards sustainable catalyst-free biomass-based polyurethane-wood composites (PU-WC): From valorization and liquefaction to future generation of biocomposites
PublicationA substantial aspect of materials engineering lies in the responsible process of designing polymer-based materials. Due to environmental pollution, excessive consumption of natural resources, and increasing environmental awareness of society, there is a massive need for polyurethane (PU) materials with reduced environmental impact. To date, research on catalyst-free polyurethane-wood composites (PU-WC) has demonstrated a huge potential...
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New σ-phases in the Nb–X–Ga and Nb–X–Al systems (X = Ru, Rh, Pd, Ir, Pt, and Au)
PublicationPreviously unreported σ-phases in the ternary niobium-based systems Nb–X–Ga for X = Ru, Rh, Pd, Ir, Pt, Au, and Nb–X–Al for X = Ir, and Pt are presented, prepared by arc-melting followed by annealing at 1000 °C for 1 week. The phases are primitive tetragonal (P42/mnm, no. 136) with lattice parameters of a = 9.8336(2)–9.9432(1) Å and c = 5.1098(1)–5.1718(1) Å. Refinements of the single crystal X-ray diffraction data for the Ru and...
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Heptaene macrolides biosynthesis by Streptomyces species
PublicationPolyene macrolides are one of the groups of secondary metabolites, generated by microorganisms belonging to the Streptomyces genus. These compounds, containing 3 - 7 conjugated double bonds systems in their molecules exhibit high antifungal activity against a broad spectrum of fungal pathogens with heptaenes demonstrating the highest antifungal potential. At the large extent, efficiency of biosynthesis of these natural products...
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Homoisocitrate dehydrogenase from Candida albicans: properties, inhibition, and targeting by an antifungal pro-drug
PublicationThe LYS12 gene from Candida albicans, coding for homoisocitrate dehydrogenase was cloned and expressed as a His-tagged protein in Escherichia coli. The purified gene product catalyzes the Mg2+- and K+-dependent oxidative decarboxylation of homoisocitrate to alpha-ketoadipate. The recombinant enzyme demonstrates strict specificity for homoisocitrate. SDS-PAGE of CaHIcDH revealed its molecular mass of 42.6±1 kDa, while in size-exclusion...
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A comprehensive review of open data platforms, prevalent technologies, and functionalities
PublicationOpen data can play a crucial role in different sectors of the world,such as government, science, research, technology, culture, andfinance. There are several necessary measures that every organiza-tion needs to consider before opening data. There are three majorsteps to opening the data: (1) Preparation stage, and (2) launchingthe open data initiative (3) In this case, the feedback mechanismstudy such as expand and sustain stage,...
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Low energy elastic scattering of electrons from hexafluoropropene (C3F6)
PublicationWe present cross sections from a joint experimental and theoretical study on elastic electron scattering from hexafluoropropene (C3F6) in the gas phase. The experimental results, using low energy electron spectroscopy, were obtained at incident electron energies of 0.5, 1, 1.5, 2, 3, 4, 5, 6, 10, 12, 15 and 20 eV, for scattering angles ranging from 10°to 130°. The theoretical method used in the computation of the integral, momentum...
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Independent Domination Subdivision in Graphs
PublicationA set $S$ of vertices in a graph $G$ is a dominating set if every vertex not in $S$ is adjacent to a vertex in~$S$. If, in addition, $S$ is an independent set, then $S$ is an independent dominating set. The independent domination number $i(G)$ of $G$ is the minimum cardinality of an independent dominating set in $G$. The independent domination subdivision number $\sdi(G)$ is the minimum number of edges that must be subdivided (each...
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Droga ekspresowa S7 Koszwały - Kazimierzowo Ocena rozwiązań konstrukcyjnych elementów posadowienia obiektów inżynierskich w ciągu drogi ekspresowej S7 na odcinku Koszwały – Kazimierzowo.
PublicationPrzedmiotem opracowania jest ocena rozwiązań posadowienia obiektów inżynierskich w ciągu drogi ekspresowej S7 na odcinku Koszwały – Kazimierzowo, przedstawionych przez Transprojekt Gdański Sp. z o.o., ul. Partyzantów 72A, 80-254 Gdańsk. Weryfikacja obejmuje: 1. MA-01 – Most autostradowy 2. MA-19 – Most autostradowy 3. WA-16 – Wiadukt 4. WD-18 – Wiadukt 5. WD-24 – Wiadukt
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Modele biomechaniczne układów mięśniowo-szkieletowych
PublicationZakres niniejszej pracy obejmuje: 1) przedstawienie podstawowych cech fizjologicznych będących podstawą do zamodelowania zachowania pojedynczego mięśnia szkieletowego (biomechanika mięśnia szkieletowego) oraz zespołu mięśni (biomechanika zespołu mięśni szkieletowych); 2) zaprezentowanie sposobu modelowania zachowania mięśnia szkieletowego obłego (wrzecionowatego) i pierzastego oraz układu mięśni jednostawowych i dwustawowych;...
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Specification of private art galleries used in the central part of old town Belgrade
PublicationIn Belgrade, since the late 1990s, private art galleries have appeared that indirectly create the image of the city through the propagation of art, take part in the education process of the residents and undertake criticism of local and global events. The article is an answer to the following questions: [1] why and how do the bottom-up art oriented places appear in Belgrade, [2] how do they function, and (3) what is their architectural...
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Ti3C2 MXenes-based catalysts for the process of α-pinene isomerization
PublicationIn this study, the catalytic performance of Ti3C2 MXene materials in the reaction of α-pinene isomerization was demonstrated. The influence of etching agents (HF, HF/H2SO4, and HF/HCl; weight ratios of mixed acids: 1 : 3, 1 : 4, and 1 : 5) on removing Al atoms from MAX phase, creation of an accordion-like structure typical...
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Sense of safety and opinions about COVID-19 vaccinations in Polish school teachers: The role of conspiracy theories belief and fear of COVID-19
PublicationThe co-occurrence of COVID-19 conspiracy theories (CCT) and fear of the coronavirus (FCV) can be linked to how safe people feel and how much they endorse vaccinations. School teachers were one of the vaccination priority groups in Poland. We conducted three cross-sectional studies (N1 = 1006; N2 = 1689; N3 = 627) to find out the potential interactive effects of CCT belief and FCV in predicting sense of safety (SoS; Studies 1-3),...
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Wybrane metody diagnostyki łożysk silników indukcyjnych oparte o pomiar prądu
PublicationW artykule zawarto przegląd wybranych metod diagnostyki łożysk silnika indukcyjnego, bazujących na pomiarach prądu zasilającego. Jedno z nowych rozwiązań przetwarzania sygnałów zostało zaadaptowane przez autorów do stosowanego przez nich systemu diagnostycznego. Wyniki wstępnych badań symulacyjnych zweryfikowanych badaniami na rzeczywistym obiekcie wskazują, że rozwiązanie to ułatwia diagnozowanie. Autorzy zamierzają prowadzić...
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New bis(azobenzocrown)s with dodecylmethylmalonyl linkers as ionophores for sodium selective potentiometric sensors
PublicationNovel biscrowns 1 and 2 were synthesized from 13-membered azobenzocrown ethers containing bromoalkylenoxy chains in para position relative to the azo group. The synthesized diester molecules are dodecylmethylmalonic acid derivatives differing by the linker length. The synthesized compounds have the potential of being used as sodium ionophores in ion-selective electrodes. They were characterized and used as ionophores in classic...
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A dual-control strategy based on electrode material and electrolyte optimization to construct an asymmetric supercapacitor with high energy density
PublicationMetal-organic frames (MOFs) are regarded as excellent candidates for supercapacitors that have attracted much attention because of their diversity, adjustability and porosity. However, both poor structural stability in aqueous alkaline electrolytes and the low electrical conductivity of MOF materials constrain their practical implementation in supercapacitors. In this study, bimetallic CoNi-MOF were synthesized to enhance the electrical...
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A Canonical Switched Capacitor DC-DC Converter. A look at how the historical SC synthesis problem is getting solved
PublicationWe reconsider a solution to the historical problem in switched capacitor (SC) DC-DC converter synthesis. Specifically, we retackle the problem of constructing an SC twophase network realizing arbitrary voltage conversion ratio within rational bounds defined. Theoretical foundations are available in our earlier research [3] where a nonconstructive proof of existence was given. We briefly review and comment on known circuit solutions...
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How can the work environment be redesigned to enhance the well-being of individuals with autism?
PublicationPurpose – This article examines the opportunities to create optimal conditions for individuals with autism, to work successfully within the contemporary workplace and improve their well-being. These opportunities arise from digital technology (DT) development, enabling the work environment to be remodeled by providing new possibilities and ways of working. The author discusses both technology-based as well as non-technological accommodations...
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Detection of propofol concentrations in blood by Raman spectroscopy
PublicationIn this paper we present a proof-of-concept of a Raman spectroscopy-based approach for measuring the content of propofol, a common anesthesia drug, in whole human blood, and plasma, which is intended for use during clinical procedures. This method utilizes the Raman spectroscopy as a chemically–sensitive method for qualitative detection of the presence of a drug and a quantitative determination of its concentration. A number of...
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Enhanced interfacial and mechanical performance of styrene-butadiene rubber/silica composites compatibilized by soybean oil derived silanized plasticization
PublicationSilanized plasticizer (SP) was chemically derived and synthesized from soybean oil (SBO) co-vulcanized with bis-(3-(triethoxysilyl)-propyl) tetrasulfide (TESPT) by using the sulfur-accelerated curing system. SP extended styrene-butadiene rubber (SBR)/silica composites have been studied for their improved filler dispersion through coupling interaction at the SBR/silica interface. The effect of SP on cross-link density, thermal,...
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Tuning of photocatalytic activity by creating a tridentate coordination sphere for palladium
PublicationThe synthesis and characterisation of an asymmetric potential bridging ligand bmptpphz (bmptpphz = 2,17-bis(4-methoxyphenyl)tetrapyrido[3,2-a:2’,3’-c:3’’,2’’-h:2’’’,3’’’-j] phenazine) is presented. This ligand contains a 1,10-phenanthroline (phen) and a 2,9-disubstituted phen sphere and possesses a strong absorbance in the visible. Facile coordination of the phen sphere to a Ru(tbbpy)2 core leads to Ru(bmptpphz) ([(tbbpy)2Ru(bmptpphz)](PF6)2;...
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Całkowite przekroje czynne na rozpraszanie elektronów na drobinach wieloatomowych
PublicationGłównym celem rozprawy doktorskiej było zmierzenie absolutnych całkowitych przekrojów czynnych (TCS) na rozpraszanie elektronów w szerokim zakresie energii (~1-400 eV) dla wybranych drobin: BCl3, B(CD3)3, NF3, N(CH3)3, P(CH3), SO2Cl2, SO2ClF, SF4, c-C2H4O oraz c-C3H6O (dla ośmiu drobin otrzymano całkowite przekroje czynne po raz pierwszy, natomiast dla dwóch pozostałych został znacznie rozszerzony zakres energii dostępnych danych)....
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The dynamics of the total output of the Japanese fisheries sector: An analysis using input-output approach
PublicationThe purpose of this study is to investigate the dynamics of the total output of the fisheries industry when the changes of the final demand occur. This study focuses on the case of Japan. This study employs a demand-pull Input-Output (IO) quantity model, one of the calculation instruments in the IO analysis, as an analysis tool. Two conditions are included in calculation and analysis parts, namely (1) “whole sector change”, and...
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Structural factors affecting affinity of cytotoxic oxathiole-fused chalcones toward tubulin
PublicationSynthesis, in vitro cytotoxic activity, and interaction with tubulin of (E)-1-(6-alkoxybenzo[d][1,3]oxathiol- 5-yl)-3-phenylprop-2-en-1-one derivatives (2) are described. Some of the compounds demonstrated cytotoxic activity at submicromolar concentrations, and the activity could be related to interaction with tubulin at the colchicine binding site. Interaction of selected derivatives with tubulinwas evaluated using molecular modeling,...
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Reactions of lithiated diphosphanes R2P-P(SiMe3)LiTHF (R = tBu, iPr) with [(PNP)TiCl2]. Two different coordination types of phosphanylphosphido ligand to the metal center.
Publication[(PNP)TiCl2] (PNP = N[2-PiPr2-4-methylphenyl]2) reacts with one equivalent of lithium derivative of diphosphane R2P-P(SiMe3)LinTHF (R = tBu, iPr) in toluene and forms the first complex with g1-coordination [(PNP)Ti(Cl){g1-P(SiMe3)-PtBu2}] (1) and complex with g2-coordination [(PNP)Ti(Cl){g2-P(SiMe3)-PiPr2}] (2) of phosphanylphosphido ligands to the titanium center. The similar reaction with two equivalents of tBu2P-P(SiMe3)LinTHF...