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Search results for: KARTA PŁATNICZA
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Ion Chromatography in Environmental Analysis of Selected Organic Acids
PublicationLow molecular mass carboxylic acids (LCAs) occur in many environmental compartments dueto natural processes and human activity. When volatile and nonvolatile acids are to be monitored then liquidchromatography, including ion chromatography seems a method of choice. At high pH the acids are inionized form and can be separated as carboxylats by means of anion exchange chromatography. LCAs canalso be separated at low pH by ion exclusion...
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Soxhlet Extraction and New Developments Such as Soxtec in: Comprehansive Sampling and Sample Preparation
PublicationSoxhlet extraction is one of the most popular techniques for extraction of analytes from solid materials. Since its discovery in 1879, the standard Soxhlet technique has been routinely applied in almost every analytical laboratory. Up to this day, Soxhlet extraction technique remains a standard technique to which the performance of modern extraction techniques is compared.Over the years, an intensive research on different modifications...
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Determination of Selected Organic Acids in Animal Farm Water Samples by Ion Chromatography
PublicationLow molecular mass carboxylic acids (LCAs) occur in many environmental compartments due to natural processes and human activity. They are an important group of organic pollutants of waste water that mainly includes, volatile fatty acids, and also dicarboxylic, aromatic, hydroxy- and ketoacids. LCAs are present in the environment at concentrations between 1 to 5000 ppm and different methods have been reported for their determination...
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Environmental fate of BTEX compounds in ambient air
PublicationAs a result of the industrialization and urbanization in the world, human pressure on the environment is intensifying, leading to detrimental changes in both biotic and abiotic compartments. One of the many consequences of this state of affairs is the increasing rate of emission into the atmosphere of volatile organic compounds, including the so-called BTEX (benzene, ethylbenzene, toluene, xylenes) compounds. The article reviews...
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Sposoby zagospodarowania ciepła odpadowego z silników jednostek pływających Cześć 2. Wykorzystanie ciepła do ogrzewania
PublicationW pierwszej części artykułu (COW 2/2017) omówiono możliwości wykorzystania nieużytkowej energii chemicznej paliwa do chłodzenia jednostek pływających. W drugiej części autorzy opisali systemy pozwalające wykorzystać tę energię do ogrzewania. Oprócz opisania budowy układów pozwalających na wykorzystanie ciepła odpadowego do ogrzewania, porównano je pod względem wydajności. Podjęto także próbę wskazania rozwiązania o najwyższej efektywności...
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Sposoby zagospodarowania ciepła odpadowego z silników napędowych jednostek pływających Cześć 1. Wykorzystanie ciepła do napędu urządzeń chłodniczych
PublicationEnergia chemiczna paliwa jest w wielu przypadkach zaledwie w połowie wykorzystana jako energia napędowa silnika. Pozostała część jako ciepło odpadowe przekazywana jest do otoczenia. Dzięki odpowiednim układom przetwarzania ciepło ze spalin można wykorzystać do wytwarzania chłodu lub jako ciepło użytkowe, w systemach HVAC (ang. heating, ventilation, air conditioning – ogrzewanie, wentylacja, klimatyzacja). Tym samym koszty pracy...
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Manganese(III) Promoted Cyclization of N-alkenyl-N-(2-hydroxyethyl) amides to Iso-Oxacepham Potent β-Lactamase Inhibitors
PublicationBackground: β-Lactams are still a subject of interest of organic chemists. The main reason for this interest is due to their application as a chemotherapeutic. β-Lactam antibiotics are still the most commonly used drugs in bacterial infections. Method: Methods using 4-exo-trig radical cyclization leading to β-lactams are an alternative to classical Staudinger`s β-Lactams formation. We prepared N-alkenyl-N-(2-hydroxyethyl)amides...
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Modyfikacje polimeraz DNA jako rozwiązania problemów w reakcjach PCR
PublicationReakcja PCR już od wielu lat jest podstawowym narzędziem stosowanym w biotechnologii molekularnej. Nadal napotykamy jednak liczne problemy podczas jej przeprowadzania związane z trudnymi matrycami, obecnością inhibitorów itp. Optymalizacja reakcji PCR jest więc niezbędna w celu poprawy wyników. Jednym z rozwiązań tych problemów może być modyfikowanie polimeraz DNA. W powyższym artykule opisano problemy i rozwiązania zależne polimerazy...
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Swoboda przepływu osób w krajach Unii Europejskiej - szanse i zagrożenia
PublicationCelem niniejszego opracowania jest zbadanie, w jaki sposób swoboda przepływu osób wpłynęła na kształtowanie się salda populacji ludności i migracji w poszczególnych krajach UE. Autorzy mając na uwadze zachodzące przeobrażenia demograficzne zadali sobie pytanie w jaki sposób będą te zmiany wpływały na funkcjonowanie gospodarek oraz czy swoboda przepływu osób i migracje mogą rekompensować niedobory zasobów pracy wynikające ze zmian...
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Badania oczyszczania ścieków pożarniczych metodą osadu czynnego
PublicationZbadano efektywność biologicznego oczyszczania ścieków pożarniczych, uwzględniając nitryfikację, w laboratoryjnym reaktorze z osadem czynnym. Przebadano ścieki surowe rozcieńczone, ścieki poddane koagulacji związkami glinu oraz ścieki po koagulacji i utlenianiu z zastosowaniem reakcji Fentona. Efektywność oczyszczania mierzono stopniem redukcji ChZT. Badano aktywność dehydrogenaz mikroorganozmów osadu czynnego, stężenie azotu amonowego...
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Charakterystyka i ocena możliwości oczyszczania zaolejonych ścieków pożarniczych
PublicationPrzedstawiono wyniki badań ścieków powstałych podczas gaszenia pożaru 20000m3 zbiornika z benzyną. Większą część zanieczyszczeń w ściekach stanowiły zawiesiny trudno opadające i koloidalne - odpowiednio 40% i 30% ładunku ChZT. Pozostałe po koagulacji zanieczyszczenia rozpuszczone poddano utlenieniu z wykorzystaniem reakcji Fentona uzyskując dalszą redukcję ChZT do 95%.
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Możliwości i ograniczenia metod oznaczania lotnych i średniolotnych związków organicznych w wodach
PublicationW pracy przedstawiono i omówiono krytycznie metodyki analityczne wykorzystywane do oznaczania szerokiego spektrum analitów (z grupy lotnych i średniolotnych związków organicznych) w próbkach wody. Szczególną uwagę zwrócono na operacje związane z takimi etapami odpowiednich procedur analitycznych jak: pobieranie próbek, izolacja i/lub wzbogacanie analitów przed etapem oznaczeń końcowych.
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Determination and pathways of nitrogen during wastewater treatment.
PublicationŚcieki rafineryjne, farmaceutyczne oraz z przemysłu spożywczego charakteryzują się wysoką zawartością azotu amonowego. Biologiczne oczyszczanie ścieków przemysłowych zazwyczaj stwarza poważne problemy technologiczne. Azot zawarty w tego typu ściekach jest zawarty w aminach, amidach, czyli związkach, które wymagają wstępnego oczyszczania w celu zmniejszenia ich stężenia do wartości nie inhibujących reakcji biochemicznych oraz nitryfikacji....
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Ocena cyklu życia - wieloaspektowa analiza oddziaływania produktu na środowisko
PublicationPrzedstawiono zasady oceny wpływu na środowisko techniką LCA zgodnie z normami Międzynarodowej Organizacji Standaryzacji. Technika LCA jest ekologicznym wskaźnikiem stanowiącym podstawę dokonania wyboru w kwestiach środowiskowych towarzyszących procesom produkcyjnym i usługowym, lub innej działalności człowieka. Zaletą tej techniki jest porównywanie wielkości oddziaływania na środowisko przez dwa lub większą liczbę produktów, różne...
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Investigation of biological and photochemical treatment of municipal landfill leachates
PublicationW pracy przedstawiono rezultaty badań charakterystyki oraz efektywności foto- oraz biodegradacji odcieków z dwóch składowisk komunalnych w północnej Polsce. Celem pracy było zbadanie efektywności oczyszczania w systemie UV, UV/H2O2 oraz możliwości biologicznego oczyszczania odcieków metodą osadu czynnego. Stosowanie metody kombinowanej (UV/H2O2/osad czynny) pozwoliło na uzyskanie lepszej efektywności oczyszczania (98% spadek wartości...
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Towards Robust Identification of Nonstationary Systems
PublicationThe article proposes a fast, two-stage method for the identification of nonstationary systems. The method uses iterative reweighting to robustify the identification process against the outliers in the measurement noise and against the numerical errors that may occur at the first stage of identification. We also propose an adaptive algorithm to optimize the values of the hyperparameters that are crucial for this new method.
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Application of fiber optic sensors using Machine Learning algorithms for temperature measurement of lithium-ion batteries
PublicationOptical fiber sensorsusing low-coherence interferometry require processing ofthe output spectrum or interferogramto quickly and accurately determine the instantaneous value of the measured quantity, such as temperature.Methods based on machine learning are a good candidate for this application. The application of four such methods in an optical fiber temperature sensoris demonstrated.Using aZnO-coated...
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Use of the AHP Method for Preference Determination in Yacht Design
PublicationA sailing yacht is a human-centred product, the design of which revolves primarily around the wants and desires of the future owner. In most cases, these preferences are not measurable, such as a personal aesthetic feeling, or a need for comfort, speed, safety etc. The aims of this paper are to demonstrate that these preferences can be classified and represented numerically, and to show that they are correlated with the type of...
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Do clusters help companies to "go green"? Experience of Polish National Key Clusters
PublicationThis study aims to explore cluster activity in the field of green transformation, taking into account the green, low-carbon and circular economy. Our intention was to identify the main green practices used by cluster organizations, which we showed through the lens of the attributes of both the cluster and the cluster organization. Through our study, we sought to answer the question: what is the role of cluster organizations in...
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Modelling of Ship’s Heeling and Rolling for the Purpose of Gantry Control Improvement in the Course of Cargo Handling Operations in Sea Ports
PublicationThe paper presents two proposals of models of interaction between a ship and cargo being loaded or discharged by a gantry in port, in terms of heeling and rolling of the vessel. The main purpose of such modelling is the need for improvement of gantry control with regard to faster operations thanks to more accurate estimation of level and moment of cargo release from a gantry hook or spreader. The study may be the contribution to...
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Investigating trip and parking characteristics of hospitals: A case study from Tri-City, Poland
PublicationThis research aims to investigate public hospitals’ trip and parking characteristics based on the study conducted in Poland in September 2021 on the example of the Tri-City agglomeration. The main objective of the research was to build models of the relationship between the number of trips during peak transport hours and the number of beds. The second research element was the analysis of transport behavior in these areas. The research...
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Mixed, quantum-classical description of electron density transfer in the collision process
PublicationIn this work, we investigate an ion-atom model describing the time-dependent evolution of electron density during the collision. For a S3+- H system, numerical simulations are based on classical trajectory calculations, and the electron density behaviour is described with the time-dependent Schrödinger equation. We apply the finite difference method to obtain quantitative insights into the charge transfer dynamics, providing detailed...
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Usuwanie ze ścieków chlorowanych węglowodorów przez osad czynny
PublicationW laboratorium modelu biologicznej oczyszczalni ścieków zbadano możliwość biodegradacji chlorowanych węglowodorów, mogących występować w ściekach przemysłowych. Stosowano osad czynny z oczyszczalni komunalnej oraz z zakładów syntezy organicznej. Po tygodniowej adaptacji stwierdzono niemal całkowity zanik niektórych chlorowanych węglowodorów.
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Determination of aminoglycoside antibiotics: current status and future trends
PublicationThe use of aminoglycoside antibiotics is prevalent in medicine and agriculture. Their overuse increases their mobility in the environment, resulting in a need for reliable methods for their determination in a variety of matrices. However, the properties of aminoglycosides, in particular their high polarity, make the development of such methods a non-trivial task, inciting researchers to tackle this complex issue from different...
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Limited selectivity of amperometric gas sensors operating in multicomponent gas mixtures and methods of selectivity improvement
PublicationIn recent years, smog and poor air quality have became a growing environmental problem. There is a need to continuously monitor the quality of the air. The lack of selectivity is one of the most important problems limiting the use of gas sensors for this purpose. In this study, the selectivity of six amperometric gas sensors is investigated. First, the sensors were calibrated in order to find a correlation between the concentration...
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Determination of percolation threshold in cement composites with expanded graphite by impedance spectroscopy
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Konsekwencje ekonomiczne inwazji pasożytniczych u zwierząt gospodarskich
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Solid Phase Micro-Extraction, a Versatile and Handy Tool in Environmental Trace Organic Analysis, Gets a New Class of Coatings, Polymeric Ionic Liquids
PublicationSolid phase microextraction (SPME) fundamentals, characteristics and application are described. The special stress is put on characteristics of sorbents used as SPME fiber coatings. Description of commercially available fibers and the present-day trends in development of new sorbents for SPME are given. Discussion is focused on possibility of application of ionic liquids (IL) and polymeric ionic liquids (PIL) as SPME fiber coatings....
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A framework estimating the minimum sample size and margin of error for maritime quantitative risk analysis
PublicationThe average accident frequency is essential for quantitative risk analysis and is conventionally estimated from accident statistics. This paper has systematically synthesised the knowledge on statistical errors and offered the missing instructions, a framework, for determining the minimum sample size and the margin of error (MOE) when calculating the average accident frequency from an accident database at hand. We have applied...
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Standard of living in Poland at regional level - classification with Kohonen self-organizing maps
PublicationThe standard of living is spatially diversified and its analyzes enable shaping regional policy. Therefore, it is crucial to assess the standard of living and to classify regions due to their standard of living, based on a wide set of determinants. The most common research methods are those based on composite indicators, however, they are not ideal. Among the current critiques moved to the use of composite...
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Experimental investigations on heat transfer enhancement in shell coil heat exchanger with VARIABLE Baffles GEOMETRY
PublicationThe paper presents the possibility of using passive intensification of heat transfer in the form of baffles to increase the energy efficiency of the shell and coil heat exchanger. The experiment was carried out by using a modular coil heat exchanger in the form of an electric heater. Water was used as a working fluid with constant thermal-flow parameters at the inlet of the module. It should be noted that experiments were made...
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Correlation between charge density waves and antiferromagnetism in Nd1−xGdxNiC2 solid solutions
PublicationWe report a study on the evolution of a charge density wave and antiferromagnetism in the series of the polycrystalline solid solution Nd1−xGdxNiC2 (0 _ x _ 1) by means of magnetic and transport properties measurements. The experimental results reveal the violation of the de Gennes law and a strong correlation between the Peierls, Néel, and Curie-Weiss temperatures, which strongly suggests a cooperative interaction between the...
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Ship domain applied to determining distances for collision avoidance manoeuvres in give-way situations
PublicationShip domain is often used in marine navigation and marine traffic engineering as a safety condition. The basic idea behind those applications is that an encounter of two or more ships can be considered safe if neither of ship domains is intruded by other ships. Research utilising this approach has been documented in numerous works, including publications on optimising collision avoidance manoeuvres performed to fulfil domain-based...
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Evaluation of the Commercial Electrochemical Gas Sensors for the Monitoring of CO in Ambient Air
PublicationAir pollution is a growing concern of civilized world, which has a significant impact on human health and the environment. Recent studies highlight that the exposure to polluted air can increase the incidence of diseases and deteriorate the quality of life. Hence, it is necessary to develop tools for real-time air quality monitoring. For air pollution monitoring a wide range of stationary gas and particulate analysers can be used....
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A Ship Domain-Based Method of Determining Action Distances for Evasive Manoeuvres in Stand-On Situations
PublicationA ship encounter can be considered safe if neither of ships’ domains (defined areas around ships) is intruded by other ships. Published research on this includes optimising collision avoidancemanoeuvres fulfilling domain-based safety conditions.However, until recently there was no method, using ship’s domain to determine exact moment when a particular collision avoidance manoeuvre can still be successfully performed. The authors...
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Prace rozwojowe nad pierwszą polską ładowarką teleskopową
PublicationW artykule dokonano przeglądu prac wykonanych przez członków Zespołu Hydrauliki i Pneumatyki Wydziału Mechanicznego Politechniki Gdańskiej w ramach programu „Bon na innowacje” dla firmy „Hydro-Metal Adam Gordziejczyk”. Obiektem prac była ładowarka teleskopowa z napędem hydraulicznym o udźwigu 1,5 T. Pierwsza część prac polegała na obliczeniach MES i poprawie sztywności konstrukcji ramy i wysięgnika. Druga część prac polegała na...
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Kurs na energię
PublicationJednym z nadrzędnych celów, jakie stawia przed sobą Unia Europejska, jest realizacja tzw. polityki zrównoważonego rozwoju. Ma ona polegać na implikacji sprzyjających warunków dla powstania konkurencyjnej gospodarki niskoemisyjnej.
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Multi-objective weather routing of sailboats considering wave resistance
PublicationThe article presents a method to determine the route of a sailing vessel with the aid of deterministic algorithms. The method assumes that the area in which the route is to be determined is limited and the basic input data comprise the wind vector and the speed characteristic of the vessel. Compared to previous works of the authors, the present article additionally takes into account the effect of sea waves with the resultant resistance...
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Diethyl carbonate as a green extraction solvent for chlorophenol determination with dispersive liquid–liquid microextraction
PublicationThe principles of green analytical chemistry indicate that the search for greener organic solvents for extraction applications is crucial. In this study diethyl carbonate (DEC) is proved to be a green solvent, as it is relatively nontoxic, obtainable from renewable resources and biodegradable. Here it is applied as an extraction solvent for chlorophenol determination in water samples with dispersive liquid–liquid microextraction....
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Charge density wave and large nonsaturating magnetoresistance in YNiC2 and LuNiC2
PublicationWe report a study of physical properties of two quasi-low-dimensional metals YNiC2 and LuNiC2 including the investigation of transport, magnetotransport, galvanomagnetic, and specific heat properties. In YNiC2 we reveal two subsequent transitions associated with the formation of weakly coupled charge density wave at TCDW=318K and its locking in with the lattice at T1=275K. These characteristic temperatures follow the previously...
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Wpływ intensywności prędkości uderzenia na niszczenie cząstkami stałymi w środowisku wodnym stali X10CrAlSi18
PublicationErozja cząstkami stałymi w środowisku wodnym jest złożonym zjawiskiem ze względu na jednoczesne oddziaływanie wielu czynników, takich jak prędkość i kąt uderzenia, koncentracja cząstek, własności materiału i cząstek stałych, prowadząc do efektu synergicznego. Zmiana jakiegokolwiek parametru procesu erozyjnego prowadzi do zmiany szybkości erozji. Z tego względu istotne jest badanie wpływu poszczególnych czynników na proces niszczenia....
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Porównanie wybranych typów elektrowni jądrowych z reaktorem HTGR
PublicationWśród interesujących rozwiązań elektrowni jądrowych USA, Rosja i Chiny proponują zastosowanie tzw. pływających morskich elektrowni nuklearnych. Wchodzi w rachubę wyposażenie ich w reaktor wysokotemperaturowy typu HTGR, chłodzony gazem. Przeprowadzono rozważania i obliczenia sprawności dla bloków 560 MW parowej elektrowni jądrowej i elektrowni z turbiną gazową. Wyższa sprawność turbin parowych nie dyskredytuje możliwości zastosowania...
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Comparative Greenness Evaluation
PublicationGreenness of analytical procedure is multivariable aspect as many greenness criteria should be taken into consideration. On the other hand, modern analytical chemistry offers dozens of analytical procedures, based on different sample preparation and final determination techniques that are used for the determination of a given analyte in a given matrix. For such complex decision-making processes, multi-criteria decision analysis...
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Selectivity of amperometric gas sensors in multicomponent gas mixtures
PublicationIn recent years smog and poor air quality became a growing environmental problem. There is a need to continuously monitor the quality of air. The lack of selectivity is one of the most important problems limiting the use of gas sensors for this purpose. In this study, a selectivity of the six amperometric gas sensors is being investigated. Calibration of sensors has been performed in order to find a correlation between concentration...
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Things You Might Not Know about the k-Nearest Neighbors Algorithm
PublicationRecommender Systems aim at suggesting potentially interesting items to a user. The most common kind of Recommender Systems is Collaborative Filtering which follows an intuition that users who liked the same things in the past, are more likely to be interested in the same things in the future. One of Collaborative Filtering methods is the k Nearest Neighbors algorithm which finds k users who are the most similar to an active user...
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Charge Transfer, Complexes Formation and Furan Fragmentation Induced by Collisions with Low-Energy Helium Cations
PublicationThe present work focuses on unraveling the collisional processes leading to the fragmentation of the gas-phase furan molecules under the He+ and He2+ cations impact in the energy range 5–2000 eV. The presence of different mechanisms was identified by the analysis of the optical fragmentation spectra measured using the collision-induced emission spectroscopy (CIES) in conjunction with the ab initio calculations. The measurements of...
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Ranking of Heterogeneous Catalysts Metals by Their Greenness
PublicationCatalysis is very important process in industry and laboratory practice, especially from the point of green chemistry principles. However, eco-friendly character of heterogeneous catalysts, containing transition metal components has not been evaluated, yet. Therefore, we perform a comprehensive assessment of 18 heterogeneous metal catalysts (Pd, Pt, V, Co, Ni, Mo, Ru, Mn, Au, Cu, Cd, Zr, Fe, Rh, Ir, Sn, Zn, Ag) using multicriteria...
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Preliminary Results of a System-theoretic Assessment of Maritime Autonomous Surface Ships' Safety
PublicationWhile a system‐theoretic approach to the safety analysis of innovative socio‐technical systems gains a growing acceptance among academia, safety issues of Maritime Autonomous Surface Ships (MASS) remain largely unexplored. Therefore, we applied a System‐Theoretic Process Analysis to develop and analyze a preliminary model of the unmanned shipping system in order to elaborate safety recommendations for...
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Modeling of Accidental Bunker Oil Spills as a Result of Ship's Bunker Tanks Rupture - a Case Study
PublicationAIS (Automatic Identification System) data analysis is used to define ship domain for grounding scenarios. The domain has been divided into two areas as inner and outer domains. Inner domain has clear border, which is based on ship dynamic characteristics. Violation of inner domain makes the grounding accident unavoidable. Outer domain area is defined with AIS data analyzing. Outer domain shows the situation of own ship in compare...
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Chemometrics approaches to green analytical chemistry procedure development
PublicationChemometric tools are widely used in analytical chemistry for the reduction of data dimensionality, grouping of variables and processing of analytical signals. They have also the potential to be applied in analytical procedure development with the aim of minimizing the procedure’s environmental impact. The design of experiment gives the possibility to obtain much better information on the system response than in case of “changing...