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Search results for: gis morski
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Impedance investigations of amperometric gas sensor containing aprotic solvent
PublicationSkonstruowany został amperometryczny czujnik gazowy w układzie trójelektrodowym ze złotą elektrodą roboczą bezpośrednio napyloną na membranę Nafionową. W publikacji przedstawiono wyniki badań charakterystyk czujnika do oznaczania ditlenku siarki wypełnionego elektrolitem zawierającym różne względne zawartości DMSO/H2O. Wyniki badań impedancyjnych zostały przeanalizowane w oparciu o zaproponowany elektryczny układ zastępczy.
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UV/VIS light-enhanced photocatalysis for water treatment and protection
PublicationPraca zawiera wyniki badań nad zaawansowanymi metodami fotokatalitycznymi w aspekcie degradacji zanieczyszczeń w fazie ciekłej. Fenol i chlorowane pestycydy zostały zastosowane jako związki modelowe. Równocześnie prowadzono badania dotyczące ścieków pestycydowych. Rozważane układy: UV/TiO2 w zawiesinie lub osadzony na szklanych mikrosferach oraz UV/H2O2/powietrze. Poprzez modyfikację tlenku tytanu(IV) pierwiastkami niemetalicznymi...
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Electrooxidation of dissolved dsDNA backed by in situ UV-Vis spectroscopy
PublicationPrzeprowadzono badania elektrochemicznego utleniania dsDNA stosując metody cyklowoltametryczne na elektrodzie weglowej, platynowej, platynowej w formie siatki oraz z siatki platynowej osadzonej na węglu. Otrzymane wyniki analizy spektroelektrochemicznej wykazały, że wraz ze wzrostem potencjału i piku prądowego absorpcja roztworu dsDNA wzrasta w sposób zależny od typu elektrody. Jednak położenie maksimum absorpcji nie zmieniało...
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Gas turbine as ship prime mover - specific problems and prospects.
PublicationPrzedstawiono ewentualne możliwości zastosowania turbin gazowych w okrętownictwie. Analizowano aspekty ekologiczne, ekonomiczne i techniczne.
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Resistance Noise Higher-Order Spectrums in Nanoparticle Gas Sensors.
PublicationPrzedstawiono badania fluktuacji rezystancji sensora gazu wykonanego z nanocząstek WO3. Stwierdzono występowanie składowych o rozkładzie prawdopodobieństwa różnym od rozkładu Gaussa. W celu zwiększenia czułości i selektywności wykrywanych gazów zastosowan do analizy obserwowanych fluktuacji spektra wyższych rzędów.
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N,N' -Bis(2-pirydyl)benzene-1,2-diamine.
PublicationN,N' -Bis(2-pirydylo)benzeno-1,2-diamina na skutek zahamowania swobodnej rotacji wokół częściowo podwójnego wiązania C-N pomiędzy resztami aminową oraz pirydynową może przyjąć dwie konformacje. Konformacja E jest stabilizowana przez cykliczne wiązanie wodorowe pomiędzy protonem grupy aminowej i atomem azotu pirydyny (N-H...N); tworzy się centrosymetryczny motyw typu pierścienia ośmioczłonowego. Druga konformacja Z charakteryzuje...
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Application of the dynamic EIS to investigation of transport within organic coatings
PublicationW pracy przedstawiono wyniki badań nad gwałtownym niszczeniem organicznych powłok ochronnych. Zastosowano technikę Dynamicznej Elektrochemicznej Spektroskopii Impedancyjnej (DEIS). Przez 60 sekund powłoka poliwinylowa poddawana była działaniu chlorku metylenu. W tym czasie rejestrowano chwilowe widma impedancyjne, co pozwoliło na prześledzenie dynamiki procesu degradacji powłoki. Potwierdzono przydatność techniki DEIS w badaniu...
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Gas sensing by thermoelectric voltage fluctuations in SnO2 nanoparticle films
PublicationPrzedstawiono eksperymentalne wyniki wykrywania gazów za pomocą badania fluktuacji napięcia termoelektrycznego w warstwie SnO2 przygotowanej z jednorodnych ziaren o średnicy 20 nm. Obserwowano fluktuacje napięcia bez zewnętrznej polaryzacji warstwy SnO2. Intensywność obserwowanych fluktuacji przekraczała 1000-krotnie intensywność szumów termicznych. Obserwowane zjawisko może byc wykorzystane do zwiększenia czułości wykrywania...
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Selected concentration techniques for gas chromatographic analysis of environmental samples
PublicationThe paper describes the role and tasks of environmental analysis and monitoring. It emphasises the leading role played by gas chromatography, especially when coupled with suitable sample preparation. This is demonstrated by some literature evidence and mainly by the author's original work on the design of sample preparation apparatus and development of GC-based methods of determination of a wide variety of organic pollutants in...
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(3,5-Dimethylpyridine)bis(tri-tert-butoxysilanethiolato)zinc(II)
PublicationMetodą rentgenowskiej analizy strukturalnej oznaczono strukturę kompleksu 3,5-dimetylopirydyny z Bis(tri-tert-butoksysilanotiolanem)cynku. Atom cynku wykazuje koordynację zniekształconej bipiramidy trygonalnej. Sieć krystaliczna jest stabilizwana tylko poprzez oddziaływania van der Waalsa.
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Bis(tetra-n-butylammonium) tetrabromocadmate(II) toluene disolvate
PublicationW pracy opisano strukturę tetrabromokadmianu tetrabutyloamoniowego będącego solwatem toluenowym. W kompleksowym anionie tego związku atom kadmu jest koordynowany przez cztery jony bromkowe tak, że cały układ przyjmuje kształt tetraedru z wszystkimi kątami Br-Cd-Br równymi 109.8o. Długość wiązania Cd-Br wynosząca 2.591Å jest typowa dla układów zawierających jako anion [CdBr4]2-.
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Toward Safe and Efficient Recovery of Gas Munitions Dumped at Sea
PublicationThe proposal of a system for the safe recovery of unexploded ordnance (UXO), chemical weapons (CW) and chemicalwarfare agents (CWA) dumped at sea mainly after WWI and WWII is described in this work. The proposed solutionaddresses the tasks required to neutralise thousands of tons of dumped material and the currently available solutionsand proposed ideas. Requirements concerning the features of a recovery system are defined and...
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Pluralist View on Inequality from Luxemburg Income Study (LIS)
PublicationThe authors start by reviewing the history of the Luxembourg Income Study (LIS), originating from an interdisciplinary project involving economists, sociologists, and political scientists, centered on the cross-country perspective in inequality analysis. They then conduct a meta-analysis of the papers produced by scholars who have taken advantage of the data availability, showing how the theme of income/wealth inequality has been...
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Harmonization and Quality Assurance of Income and Wealth Data: The Case of LIS.
PublicationComparability of concepts in survey data harmonization is essential for scientific analyses. LIS – also known as the Luxembourg Income Study or LIS Cross-National Data Center in Luxembourg – acquires and harmonizes income and wealth microdata to provide the scientific community with a comparable database that is unique in the world in its growing temporal and geographic breadth. Over many decades, scholars worldwide have used the...
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Ionospheric scintillations computation using real-time GPS observations
PublicationThe following paper presents the results of quasi-real-time determination of the values of phase scintillations indices at the period of ionospheric disturbances that occurred as a consequence of the Sun flares observed on March 7 and 9, 2012. Double-frequency observations with 1-second measurement interval from the EPN (EUREF Permanent Network) network sites located at high latitudes were used for the analysis. To determine the phase...
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GPS-derived height changes in diurnal and sub-diurnal timescales
PublicationThis paper describes the research concerning precise short-time GPS solutions conducted in the Centre of Applied Geomatics, Military University of Technology, Warsaw, Poland. The data from ASG-EUPOS (Polish Active Geodetic Network) was processed using Bernese 5.0 software and EPN (EUREF Permanent Network) standards and models. In this study, the adapted 3-hour observation window is shifted every hour for obtaining hourly geocentric...
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Nonlinear phenomena of small-scale sound in a gas with exponential stratification
PublicationThe nonlinear dynamics of perturbations, quickly varying in space, with comparatively large characteristic wavenumbers k: k>1/H, is considered. H is the scale of density and pressure reduction in unperturbed gas, as the coordinate (H is the so-called height of the uniform equilibrium gas). Coupling nonlinear equations which govern the sound and the entropy mode in a weakly nonlinear flow are derived. They describe the dynamics...
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Techniques of acquiring additional features of the responses of individual gas sensors
PublicationGas sensors usually exhibit lack of selectivity, require fre quent calibration, exhibit drift of the response and a lot of factors, such as humidity or ambient temperature, influen ce their performance. Different approaches can be used to overcome this shortcomings. Building arrays of different sensors and usage of pattern recognition methods to analyze responses of elements...
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Meat freshness classification using ultra-fast gas chromatography
PublicationMeat constitutes an important component of human diet. In order to ensure that it is safe to consume, it is important to be able to determine whether a particular sample is fresh. To this end, an analysis of the headspace of pork, beef, and poultrywas performed over a period of seven days using ultra-fast gas chromatography. Compounds that may possibly be used as indicators of spoilage were identified. Based on the obtained results...
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Gas turbines – technological development and potential use in CAES systems
PublicationThis article briefly describes Compressed Air Energy Storage (CAES), focusing on the technological development of one of the key elements of such systems – the gas turbines. It presents the basic parameters and features of gas turbines, as well as turbine classes with example models. Main tendencies in the structural and technological development are discussed. Changes and trends on electric energy markets are becoming more and...
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IMPEDANCE MEASUREMENT MODULE FOR GAS SENSORS WITH TEMPERATURE CONDITIONING FEATURE
PublicationThe paper presents an impedance measurement module which is aimed for gas sensor. Sensor’s heater temperature conditioning and modulation feature is available in order to allow implementation of different techniques improving selectivity and sensitivity of gas sensors. The measurement module uses three-parameter sine-fitting technique for impedance measurement. To monitor sensor temperature, the resistance of the sensor’s heater...
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LOW COST MEASUREMENT MODULE FOR MATRIX OF AMPEROMETRIC GAS SENSOR
PublicationThis paper describes an amperometric sensor module for gas concentration measurement. A module can be used for many types of electrochemical gas sensors without major hardware changes. Device is based on AVR ATmega8 microcontroller. As signal processing circuit a specialized integrated circuit LMP9l000 configurable via I2C interface is used. The concept of a measuring system composed of several modules dedicated for a gas sensors...
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Efficiency of gas detection algorithms using fluctuation enhanced sensing
PublicationEfficiency of various gas detection algorithms by applying fluctuation enhanced sensing method was discussed. We have analyzed resistance noise observed in resistive WO3- nanowires gas sensing layers. Power spectral densities of the recorded noise were used as the input data vectors for two algorithms: the principal component analysis (PCA) and the support vector machine (SVM). The data were used to determine gas concentration...
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Spinning Fluids Reactor: A new design of a gas – liquid contactor
PublicationCurrent trends in chemical reactor design are based on adapting these to the requirements of a particular chemical process. Processes involving reactions between the gas and liquid phase in particular require precise adjustment of all parameters. The common denominator for most modern design solutions is enhancement of the mass transfer area and the overall volumetric mass transfer coefficient. Gas – liquid contactors evolved from...
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Occurrence and Determination of Volatile Fatty Acids in Landfill Leachate and Gas
PublicationIn landfills containing biological matter volatile fatty acids (VFAs) are generated at high rate at the early stage of waste disposal and their content in leachate is high as compared to the leachate from old parts of landfill since they are converted to methane gas. Monitoring of the leachate for the content of VFAs can help determine the processes occurring in waste and possible effect of the leachate on the environment in the...
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Clean gas technologies - towards zero-emission repowering of Pomerania.
PublicationThe main aim this work is to show the different thermodynamic cycles which improve efficiency and/or decrease emission like: Cheng cycle, Szewalski cycle, LOTHECO cycle, hybrid pSOFC/GT cycle, inverse Brayton cycle, low-emission cycle and zero-emission cycle. For that purpose, cycles and results of analysis are first studied and, secondly, new concept is presented. The role of coupled analysis 0D and 3D in cycle’s devices is also...
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Occurrence and Determination of Volatile Fatty Acids in Landfill Leachate and Gas
PublicationIn landfills containing biological matter volatile fatty acids (VFAs) are generated at high rate at the early stage of waste disposal and their content in leachate is high as compared to the leachate from old parts of landfill since they are converted to methane gas. Monitoring of the leachate for the content of VFAs can help determine the processes occurring in waste and possible effect of the leachate on the environment in the...
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Domestic ORC micro-CHP combined with a commercial gas boiler
PublicationThe chapter presents the results of experimental studies conducted during the launch of the first in Poland demonstration prototype of the micro ORC coupled to a domestic gas boiler. The accomplished studies indicated the possibility for the ORC module to work with such boiler (autonomous source of heat) with a prototype single-stage axial micro turbine as the expansion machine. Confirmation of that fact has been delineated in...
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Technika ochrony odbiorników GPS przed atakami typu spoofing
PublicationArtykuł został poświęcony problemowi tzw. spoofingu w systemach nawigacji satelitarnej GNSS. Mianem spoofingu GNSS określa się niepowołaną transmisję sygnałów GNSS, imitujących sygnały nadawcze z satelitów nawigacyjnych. Celem takiego działania jest doprowadzenie do wskazania przez odbiornik GNSS nieprawidłowych informacji o położeniu, prędkości i czasie. Przeprowadzenie takiego ataku jest możliwe wskutek braku odpowiedniej ochrony...
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A calibration model for gas sensor array in varying environmental conditions
PublicationAbstract: Gas-analyzing systems based on gas sensors, commonly referred to as electronic noses, are the systems which enable the recognition of volatile compounds in their working environment and provide the on-line results of analysis. The most commonly used type of sensors in such systems is semiconductor gas sensors. They are considered to be the most reliable in the long-term applications (more than 1 year), however,...
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Detection and Mitigation of GPS Spoofing Based on Antenna Array Processing
PublicationIn this article authors present an application of spatial processing methods for GPS spoofing detection and mitigation. In the first part of this article, a spoofing detection method, based on phase delay measurements, is proposed. Accuracy and precision of phase delay estimation is assessed for various qualities of received signal. Spoofing detection thresholds are determined. Efficiency of this method is evaluated in terms of...
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Low cost electrochemical sensor module for measurement of gas concentration
PublicationThis paper describes a low cost electrochemical sensor module for gas concentration measurement. A module is universal and can be used for many types of electrochemical gas sensors. Device is based on AVR ATmega8 microcontroller. As signal processing circuit a specialized integrated circuit LMP9l000 is used. The proposed equipment will be used as a component of electronic nose system employed for classifying and distinguishing...
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Sensitivity to nitrogen dioxide of electrocatalytic gas sensor based on NASICON
PublicationW pracy przedstawiono wyniki badań czujnika elektrokatalitycznego na bazie NASICONu.
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Chiral gas chromatography as a tool for investigation into illicitly manufactured methamphetamine
PublicationW pracy przedstawiono zastosowanie gazowej chromatografii chiralnej do rozdzielania związków ubocznych powstających w trakcie syntezy metylamfetaminy. Opisano rozdzielanie enancjomerów efedryny, pseudoefedryny, chlorowanych związków posrednich i metylamfetaminy stosując do derywatyzacji bezwodniki fluorowanych kwasów. Jako fazę chiralną zastosowano CHIRALDEX B-DM. Do rozdzielenia enancjomerów pseudoefedryny oraz chlorowanych produktów...
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Efektywność filtracji przestrzennej sygnałów w przeciwdziałaniu spoofingowi GPS
PublicationPrzedstawiono metodę przeciwdziałania spoofingowi GPS poprzez formowanie minimum charakterystyki kierunkowej układu antenowego. Opisano metodykę i wyniki badań tłumienia sygnałów niepożądanych w obecności szumu. Zaprezentowano rezultaty statystycznej analizy wpływu filtracji przestrzennej na tłumienie prawdziwych sygnałów GPS. W podsumowaniu wykazano korzyści wynikające z użycia przyjętej metody, w...
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Low-energy positron scattering from gas-phase uracil
PublicationQuantum scattering calculations are presented for the interaction of low energy positrons with the uracil molecule, an important component of biological systems. The rotational elastic and inelastic cross sections and vibrational inelastic cross sections are reported and compared with existing experiments, indicating a general trend of the cross sections different from the experimental findings and in line with what should be expected...
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A calibration model for gas sensor array in varying environmental conditions
PublicationAbstract: Gas-analyzing systems based on gas sensors, commonly referred to as electronic noses, are the systems which enable the recognition of volatile compounds in their working environment and provide the on-line results of analysis. The most commonly used type of sensors in such systems is semiconductor gas sensors. They are considered to be the most reliable in the long-term applications (more than 1 year), however,...
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Application of gas chromatography to the analysis of spirit-based alcoholic beverages
PublicationSpirit-based beverages are alcoholic drinks, which production processes are dependent on the type and origin of raw materials. The composition of this complex matrix is difficult to analyze and scientists commonly choose a gas chromatography techniques for this reason. With a wide selection of extraction methods and detectors it is possible to provide qualitative and quantitative analysis for many chemical compounds with a various...
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Possibilities of Increasing the Overall Efficiency of Gas-steam CHP Microplant
PublicationThe paper presents ways to increase the efficiency of a gas-steam micro power plant by modifying the cycle combination. The modification consists in partial release of the fluid downstream of the gas turbine and using it for ORC fluid overheating and evaporation. Advantages of this solution over the simplest gas and steam cycles’ combination are demonstrated.
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Analysis and interpretation of radiometric signals in a liquid-gas bubble flow
PublicationThe article presents the analysis of signals from a radiometric system consisting of two scintillation probes and two gamma radiation sealed sources. Calculations and interpretation were carried out for the bubble flow of the water-air mixture in the horizontal pipeline. The analysis of the obtained signals was done in time and frequency domain. In the frequency domain, a range of usable frequencies was identified, which were associated...
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Investigation of the temperature modulation parameters on semiconductor gas sensor response
PublicationIn this work we present the results of the investigation of the sensing properties of semiconductor gas sensors with a sinusoidally modulated temperature in the presence of synthetic air (SA) and three volatile air pollutants, i.e. NH3, NO2 and SO2. The measurements were performed for different average sensor heater temperatures and the amplitude of the modulation signal. In addition, the extraction of features from the sensor...
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Wetting of supports by ionic liquids used in gas separation processes
PublicationCiecze jonowe są stosowane w procesach separacji gazów jako selektywne rozpuszczalniki. Są szeroko stosowane w technologii immobilizowanych membran ciekłych, głównie w procesach oczyszczania strumieni gazowych. Praca ta charakteryzuje komercyjnie dostępne membrany porowate używane we wspomnianych procesach. Określenie właściwości nośników i fazy membranowej ma na celu wyznaczenie czynników mających wpływ na stabilności takich układów...
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Fluctuation-enhanced scent sensing using a single gas sensor
PublicationScent or aroma sensing during aromatherapy can be carried out by applying only a single resistance gas sensor (TGS - Taguchi Gas Sensors). This paper considers the efficiency of detection of essential oils by DC resistance and its fluctuations observed in TGS sensors. A detailed study has been conducted for scents emitted by five popular essential oils using three sensor types (TGS 2600, TGS 2602, TGS 823). The research was focused...
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Experimental investigation of domestic gas boiler fitted with ORC module
PublicationIn the paper the prototype of innovative domestic cogenerative ORC system, consisting of a conventional gas boiler and a small size axial vapour microturbines (in-house designed for ORC and the commercially available for Rankine cycle (RC)), evaporator and condenser were scrutinised. In the course of study the fluid working temperatures, rates of heat, electricity generation and efficiency of the whole system were obtained. The...
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Electron interactions with Bis(pentamethylcyclopentadienyl) titanium(IV) dichloride and difluoride
PublicationWe present a combined experimental and theoretical study of the interaction of electrons with Bis(pentamethylcyclopentadienyl)titanium(IV) dichloride (Cp∗2TiCl2) and difluoride (Cp∗2TiF2). We report the experimental measurements of partial cross sections for the dissociative electron attachment (DEA) and the electron ionization (EI) mass spectra of isolated molecules. Estimates of the absolute cross sections are done on the basis...
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Wavelet Transform Analysis of Temperature Modulated Gas Sensor Response
PublicationThe aim of the study was to evaluate whether it is possible to extract the information about the gas concentration despite the influence of humidity. Commercial semiconductor sensor response was examined under the application of a periodic temperature change. The data was collected using measurement protocol for different concentrations of ammonia at specified levels of relative humidity. In this work we focused on the evaluation...
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Two-dimensional gas chromatography – principles and application in fruits analysis
PublicationTwo-dimensional gas chromatography is a rapidly developing analytical technique. One of the major uses of this technique is its use for food analysis. The paper presents the principle of operation and history of this analytical technique. The specification of the two-dimensional gas chromatography technique has been discussed. The principles of separation of ingredients and application of the method, particularly in the analysis...
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Monitorowanie regionalnych zmian jonosfery z godzinnych obserwacji GPS
PublicationW nowoczesnych metodach przestrzennego wyznaczania pozycji główną rolę odgrywają globalne systemy satelitarne, pozwalające na wyznaczenie pozycji obiektu niezależnie od czasu i położenia, w najbliższym sąsiedztwie Ziemi. Obecnie znanych jest kilka satelitarnych systemów pozycjonowania o zasięgu globalnym. Wśród nich wymienić należy: GPS, GLONASS, DORIS, PRARE, w niedalekiej przyszłości - GALILEO. Wykorzystanie poszczególnych systemów,...
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Activities of the Astro-geodetic Observatory in Jozefoslaw in the frame of IGS and EUREF
PublicationThe Astrogeodetic Observatory of the Institute of Geodesy and Geodetic Astronomy of the Warsaw University of Technology (WUT) in Jozefoslaw was incorporated in 1957. In 1991 it joined the International GPS Service (IGS) and started to operate as a permanent in 1993. Since then the following permanent services have been maintained: GPS observations using Trimble and Turbo Rogue receivers, tidal gravimetric observations with LaCoste&Romberg...
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Low-energy positron scattering from gas-phase benzene
PublicationIn this paper we are presenting calculations of the elastic cross section of positrons with gas-phase benzene for the energy range from 0.25 eV to 9.0 eV. The calculations are done with the molecular R-matrix method for positron-scattering from poly-atomic molecules using a scaling factor to scale the electron-positron interaction. The scaling factor influences the position of the poles of the R-matrix. We adjust the scaling factor...