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Wyniki wyszukiwania dla: unconventional gas resources
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Application of gas chromatography–tandem mass spectrometry for the determination of amphetamine-type stimulants in blood and urine
PublikacjaAmphetamine, methamphetamine, phentermine, 3,4-methylenedioxyamphetamine (MDA), 3,4-methylenedioxymethamphetamine (MDMA), and 3,4-methylenedioxy-N-ethylamphetamine (MDEA) are the most popular amphetamine-type stimulants. The use of these substances is a serious societal problem worldwide. In this study, a method based on gas chromatography-tandem mass spectrometry (GC-MS/MS) with simple and rapid liquid-liquid extraction (LLE)...
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Authenticity Assessment of the "Onisiówka" Nalewka Liqueurs Using Two-Dimensional Gas Chromatography and Sensory Evaluation
PublikacjaThe “Onisiówka” nalewka liqueur is a regional Polish alcoholic beverage, which is inscribed on the list of regional and traditional products of the Ministry of Agriculture and Rural Development in Poland. It is produced from multiflower honey, black elderberry flower syrup, and spirit. Due to fact that the “Onisiówka” nalewka liqueur has never been investigated, these studies are the foundation for further work on this regional...
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Gas chromatography-olfactometry (GC-O), electronic noses (e-noses) and electronic tongues (e-tongues) for in vivo food flavour measurement
PublikacjaThe capter revies two types of artificial olfaction instrumentation, i.e. gas-chromatography-olfactometry (GC-O) and chemical sensor technologies (electronic nose and tongue), combined with multivariate data processing methods as promising approaches for rapid analysis of food. The chapter also includes examples of specific applications for the detection of food flavour and volatile components.
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Evaluation of Linkers’ Influence on Peptide-Based Piezoelectric Biosensors’ Sensitivity to Aldehydes in the Gas Phase
PublikacjaRecent findings qualified aldehydes as potential biomarkers for disease diagnosis. One of the possibilities is to use electrochemical biosensors in point-of-care (PoC), but these need further development to overcome some limitations. Currently, the primary goal is to enhance their metrological parameters in terms of sensitivity and selectivity. Previous findings indicate that peptide OBPP4 (KLLFDSLTDLKKKMSEC-NH2) is a promising...
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Deposition and characterization of organic polymer thin films using a dielectric barrier discharge with different C2Hm/N2 (m = 2, 4, 6) gas mixtures
PublikacjaOrganic polymer thin films have been deposited on Si(100) and aluminum coated glass substrates by a dielectric barrier discharge (DBD) operated at medium pressure using different C2Hm/N2 (m = 2, 4, 6) gas mixtures. The deposited films were characterized by various spectroscopic techniques. Fourier transform infrared reflection absorption spectroscopy (FT-IRRAS) revealed the chemical functional groups present in the films. The surface...
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β-cyclodextrin-containing polymer based on renewable cellulose resources for effective removal of ionic and non-ionic toxic organic pollutants from water
PublikacjaA novel, bio-derived cyclodextrin-based trifunctional adsorbent has been successfully synthesized for efficient, rapid and simultaneous removal of a broad-spectrum of toxic ionic (anionic and cationic dyes) and non-ionic organic pollutants from water. The composition, morphology and the presence of functional groups in the obtained sorption material were characterized by elemental analysis, XRD, SEM, and FTIR spectroscopy. The...
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A Comparison of Ammonia Emission Factors from Light-Duty Vehicles Operating on Gasoline, Liquefied Petroleum Gas (LPG) and Compressed Natural Gas (CNG)
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Computational analysis of substituent effects on proton affinity and gas-phase basicity of TEMPO derivatives and their hydrogen bonding interactions with water molecules
PublikacjaThe study investigates the molecular structure of 2,2,6,6-tetramethylpiperidine-1-oxyl (TEMPO) and its derivatives in the gas phase using B3LYP and M06-2X functional methods. Intermolecular interactions are analyzed using natural bond orbital (NBO) and atoms in molecules (AIM) techniques. NO2-substituted TEMPO displays high reactivity, less stability, and softer properties. The study reveals that the stability of TEMPO derivatives...
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Nitrogen oxides removal from hydrogen flue gas using corona discharge in marine boilers: Application perspective
PublikacjaThis paper focuses on the combustion of hydrogen in boilers, as it appears to be a more effective method than using fuel cells for heating purposes due to higher boiler efficiency. One of the main disadvantages of hydrogen combustion in air is NOx formation. Therefore, the authors decided to introduce corona discharge as an inno- vative technique to clean hydrogen flue gas by effectively reducing NOx levels. The method involves...
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Impacts of Using Exhaust Gas Recirculation and Various Amount of Dimethyl Ether Premixed Ratios on Combustion and Emissions on a Dual-Fuel Compression Ignition Engine
PublikacjaIn the presented research, the authors dealt with the specific properties of the combustion process of dimethyl ether (DME) in a combustion car (Volkswagen Golf IV) engine AJM 1.9 TDI PDE made by Volkswagen factory. Dimethyl ether is an alternative fuel produced most often from natural gas, which can be used in compression ignition engines as a single fuel or co-burned with diesel oil. This work describes the impacts of using exhaust...
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Direct solid phase microextraction combined with gas chromatography – Mass spectrometry for the determination of biogenic amines in wine
PublikacjaA direct method based on immersion solid phase microextraction (DI-SPME) gas chromatography mass-spectrometry (GC-MS) was optimized and validated for the determination of 16 biogenic amines in Polish wines. In the analysis two internal standards were used: 1,7-diaminoheptane and bis-3-aminopropylamine. The method allows for simultaneous extraction and derivatization, providing a simple and fast mode of extraction and enrichment....
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The Influence of Gas Mixture in the Glow-Discharge Nitriding Process of Austenitic Stainless Steel on Characteristic of Nitrided Cases
PublikacjaAustenitic stainless steels characterize with excellent corrosion resistance, although low mechanical properties. In many cases that limits their exploitation in industrial applications. Moreover, austenitic stainless steel is susceptible to local corrosion in the presence of halide ions. In present works, it was emphasized that the nitriding of austenitic stainless steels gives some potential abilities to obtain beneficial effect...
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Application of normal-phase high-performance liquid chromatography followed by gas chromatography for analytics of diesel fuel additives
PublikacjaThe paper presents the results of investigations on new procedures of determination of selected cleaning additives in diesel fuel. Two procedures: one-step analysis using gas chromatography with flame ionization detection (GC-FID) or mass spectrometry (GC-MS) and a two-step procedure in which normal-phase high-performance liquid chromatography (NP-HPLC) was used for preliminary separation of the additives, were compared. The additive...
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Evaluation of flavour profiles in e-cigarette refill solutions using gas chromatography–tandem mass spectrometry
PublikacjaMany flavour compounds that are present in e-liquids for e-cigarettes are responsible for specific tastes and smoking sensations for users. Data concerning content and specific types of flavours is often limited and unknown to users. The aim of the research was to define and compare flavour profiles of e-liquids with the same group taste from different manufacturers. Gas chromatography coupled with tandem mass spectrometry (GC–MS/MS)...
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Removal of cyclohexane vapors from air in biotrickling filters: Effects of gas mixture composition and circular economy approach
PublikacjaThis work presents results of investigations on biotrickling filtration of air polluted with cyclohexane co-treated in binary, ternary and quaternary volatile organic compounds (VOCs) mixtures, including vapors of hexane, toluene and ethanol. The removal of cyclohexane from a gas mixture depends on the physicochemical properties of the co-treated VOCs and the lower the hydrophobicity of the VOC, the higher the removal efficiency...
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Diagnostic Analysis of Exhaust Gas with A Quick-Changing Temperature from a Marine Diesel Engine Part II / Two Factor Analysis
PublikacjaThe article presents a continuation of research carried out to determine the effect of input parameters (changes in engine structure parameters) on selected output parameters (diagnostic measures), based on quickly changing exhaust gas temperature. A method of determining the simultaneous influence of two input factors (the structure parameter and the engine load) on one output factor was presented, as well as an evaluation...
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Fungal co-culture improves the biodegradation of hydrophobic VOCs gas mixtures in conventional biofilters and biotrickling filters
PublikacjaThe present study systematically evaluated the potential of Candida subhashii, Fusarium solani and their consortium for the abatement of n-hexane, trichloroethylene (TCE), toluene and α-pinene in biofilters (BFs) and biotrickling filters (BTFs). Three 3.2 L BFs packed with polyurethane foam and operated at a gas residence time of 77 s with an air mixture of hydrophobic volatile organic compounds (VOCs) were inoculated with C. subhashii,...
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Assessment of Failure Occurrence Rate for Concrete Machine Foundations Used in Gas and Oil Industry by Machine Learning
PublikacjaConcrete machine foundations are structures that transfer loads from machines in operation to the ground. The design of such foundations requires a careful analysis of the static and dynamic effects caused by machine exploitation. There are also other substantial differences between ordinary concrete foundations and machine foundations, of which the main one is that machine foundations are separated from the building structure....
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Inspection of rubber linings operating in flue gas desulphurisation units
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Methods of preparation and performance of sealed gas photomultipliers for visible light
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Modeling of a Combined Cycle Gas Turbine Integrated with an Adsorption Chiller
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Charge Loss in Gas-Phase Multiply Negatively Charged Oligonucleotides
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Impedance investigations of amperometric gas sensor containing aprotic solvent
PublikacjaSkonstruowany został amperometryczny czujnik gazowy w układzie trójelektrodowym ze złotą elektrodą roboczą bezpośrednio napyloną na membranę Nafionową. W publikacji przedstawiono wyniki badań charakterystyk czujnika do oznaczania ditlenku siarki wypełnionego elektrolitem zawierającym różne względne zawartości DMSO/H2O. Wyniki badań impedancyjnych zostały przeanalizowane w oparciu o zaproponowany elektryczny układ zastępczy.
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Chemometric analysis for optimizing derivatization in gas chromatography-based procedures
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Low-energy positron scattering from gas-phase uracil
PublikacjaQuantum scattering calculations are presented for the interaction of low energy positrons with the uracil molecule, an important component of biological systems. The rotational elastic and inelastic cross sections and vibrational inelastic cross sections are reported and compared with existing experiments, indicating a general trend of the cross sections different from the experimental findings and in line with what should be expected...
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Clean gas technologies - towards zero-emission repowering of Pomerania.
PublikacjaThe main aim this work is to show the different thermodynamic cycles which improve efficiency and/or decrease emission like: Cheng cycle, Szewalski cycle, LOTHECO cycle, hybrid pSOFC/GT cycle, inverse Brayton cycle, low-emission cycle and zero-emission cycle. For that purpose, cycles and results of analysis are first studied and, secondly, new concept is presented. The role of coupled analysis 0D and 3D in cycle’s devices is also...
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Chemiresistive gas sensors based on carbon nanotubes - fabrication and application
PublikacjaOpisano przygotowanie i możliwości zastosowania chemirezystancyjnych czujników gazów wykonanych z nanorurek węglowych.
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Amperometric gas sensors with elektrodes chemically deposited on Nafion membrane
PublikacjaW pracy przedstawiono opis metod otrzymywania elektrod pracujących w czujnikach amperometrycznych gazów z elektrolitem ciekłym. Zaprezentowano metody chemiczne takie jak: metoda impregnacji-redukcji i metoda Takenaka-Torikai. Przedstawiono przegląd konstrukcji czujnikowych gazowych z elektrodami tego typu.
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Shale gas: insight into Baltic Basin and some technical aspects
PublikacjaWybrane zagadnienia w poszukiwaniu i produkcji gazu z łupków na bazie własnych doświadczeń na obszarach basenu Morza Bałtyckiego, Pomorza i Połnocnej Polski.
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Sensitivity to nitrogen dioxide of electrocatalytic gas sensor based on NASICON
PublikacjaW pracy przedstawiono wyniki badań czujnika elektrokatalitycznego na bazie NASICONu.
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Chiral gas chromatography as a tool for investigation into illicitly manufactured methamphetamine
PublikacjaW pracy przedstawiono zastosowanie gazowej chromatografii chiralnej do rozdzielania związków ubocznych powstających w trakcie syntezy metylamfetaminy. Opisano rozdzielanie enancjomerów efedryny, pseudoefedryny, chlorowanych związków posrednich i metylamfetaminy stosując do derywatyzacji bezwodniki fluorowanych kwasów. Jako fazę chiralną zastosowano CHIRALDEX B-DM. Do rozdzielenia enancjomerów pseudoefedryny oraz chlorowanych produktów...
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The Application of Open Capillary Modules for Sweeping Gas Membrane Distillation
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Gas turbine as ship prime mover - specific problems and prospects.
PublikacjaPrzedstawiono ewentualne możliwości zastosowania turbin gazowych w okrętownictwie. Analizowano aspekty ekologiczne, ekonomiczne i techniczne.
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Gas sensing by thermoelectric voltage fluctuations in SnO2 nanoparticle films
PublikacjaPrzedstawiono eksperymentalne wyniki wykrywania gazów za pomocą badania fluktuacji napięcia termoelektrycznego w warstwie SnO2 przygotowanej z jednorodnych ziaren o średnicy 20 nm. Obserwowano fluktuacje napięcia bez zewnętrznej polaryzacji warstwy SnO2. Intensywność obserwowanych fluktuacji przekraczała 1000-krotnie intensywność szumów termicznych. Obserwowane zjawisko może byc wykorzystane do zwiększenia czułości wykrywania...
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Resistance Noise Higher-Order Spectrums in Nanoparticle Gas Sensors.
PublikacjaPrzedstawiono badania fluktuacji rezystancji sensora gazu wykonanego z nanocząstek WO3. Stwierdzono występowanie składowych o rozkładzie prawdopodobieństwa różnym od rozkładu Gaussa. W celu zwiększenia czułości i selektywności wykrywanych gazów zastosowan do analizy obserwowanych fluktuacji spektra wyższych rzędów.
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Toward Safe and Efficient Recovery of Gas Munitions Dumped at Sea
PublikacjaThe proposal of a system for the safe recovery of unexploded ordnance (UXO), chemical weapons (CW) and chemicalwarfare agents (CWA) dumped at sea mainly after WWI and WWII is described in this work. The proposed solutionaddresses the tasks required to neutralise thousands of tons of dumped material and the currently available solutionsand proposed ideas. Requirements concerning the features of a recovery system are defined and...
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The influence of electrocatalytic toxic gas sensor construction on its performance
PublikacjaW pracy przedstawiono porównanie właściwości elektrokatalitycznych czujników gazów przygotowanych na bazie różnych elektrolitów stałych oraz wykonanych w różnych technologiach.
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Fluctuation-enhanced scent sensing using a single gas sensor
PublikacjaWykrywanie zapachów podczas aromaterapii może być przeprowadzone za pomocą pojedynczego sensora gazów. W pracy rozważono efektywność detekcji zapachów olejków eterycznych za pomocą rezystancji DC oraz zjawisk fluktuacyjnych w tych sensorach, typu TGS2600,TGS2602,TGS823. Badania koncentrowały się na praktycznym zastosowaniu w aromaterapii do określania intensywności emitowanego zapachu. Opisano szczegółowo system do emisji zapachów.
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Sorption properties of asphaltene stationary phases for gas chromatography separations
PublikacjaW pracy przedstawiono wyniki badań nad możliwością wykorzystania faz stacjonarnych na bazie frakcji asfaltenowych do rozdzielania mieszanin związków chemicznych z wykorzystaniem chromatografii gazowej oraz porównano selektywność faz przygotowanych z frakcji asfaltenowych wyizolowanych z różnych surowców. Na podstawie uzyskanych wyników obliczono wartości liniowych indeksów retencji oraz stałych Rohrschneidera McReynoldsa, za pomocą...
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OPTIMALIZATION OF SORBENT FEEDING IN THE DRY METHOD OF FLUE GAS DESULFURIZATION
PublikacjaThe swiftly developing sea transport contributes to a considerable increase of fuel usage in the international shipping, which results in the escalation of toxic compounds emitted into the atmosphere. It is followed by the constantly heightened requirements limiting those emissions. In the case of sulfur oxide emission, inside of SECA (Sulfur Emission Control Area), the maximum content of sulfur in the shipping fuels used on the...
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Wetting of supports by ionic liquids used in gas separation processes
PublikacjaCiecze jonowe są stosowane w procesach separacji gazów jako selektywne rozpuszczalniki. Są szeroko stosowane w technologii immobilizowanych membran ciekłych, głównie w procesach oczyszczania strumieni gazowych. Praca ta charakteryzuje komercyjnie dostępne membrany porowate używane we wspomnianych procesach. Określenie właściwości nośników i fazy membranowej ma na celu wyznaczenie czynników mających wpływ na stabilności takich układów...
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Simulations of behaviour of granular bodies using a lattice-gas automaton.
PublikacjaW artykule przedstawiono wyniki numerycznej analizy przepływu materiałów granulowanych podczas 3 różnych problemów: przepływu silosowego, przepływu kanałowego i tworzenia się nasypu. W modelu zaczerpniętym z teorii gazów przyjęto kolizje cząsteczek i dysypację energii. Wyniki porównano z doświadczeniami.
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Technical State Assessment of Charge Exchange System of Self-Ignition Engine, Based On the Exhaust Gas Composition Testing
PublikacjaThis paper presents possible use of results of exhaust gas composition testing of self - ignition engine for technical state assessment of its charge exchange system under assumption that there is strong correlation between considered structure parameters and output signals in the form of concentration of toxic compounds (ZT) as well as unambiguous character of their changes. Concentration of the analyzed ZT may be hence considered...
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Integrated plant-wide modelling for evaluation of the energy balance and greenhouse gas footprint in large wastewater treatment plants
PublikacjaModern wastewater treatment plants (WWTPs) should maintain a balance between three combined sustainability criteria, including effluent quality, energy performance and greenhouse gas (GHG) emissions. All of these criteria were considered in the integrated plant-wide model developed in this study. The proposed model incorporates new features, including: (i) the addition of associated facilities to the overall energy balance and...
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Determination of antifreeze substances in the airport runoff waters by solid-phase microextraction and gas chromatography–mass spectrometry method
PublikacjaA new method has been developed for the determination of antifreeze agents such as ethylene glycol (EG), propylene glycol (PG), and diethylene glycol (DEG) in the samples of airport runoff water. The method is based on headspace solid–phase microextraction (HS–SPME) of target analytes, which is coupled with gas chromatography–mass spectrometry (GC–MS). Until now, there was a lack of appropriate methodology for collecting reliable...
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Monolithic capsule phase microextraction prior to gas chromatography-mass spectrometry for the determination of organochlorine pesticides in environmental water samples
PublikacjaIn this study, a capsule phase microextraction (CPME) protocol followed by gas chromatography-mass spectrometry is proposed for the accurate and sensitive monitoring of organochlorine pesticides (OCPs) in environmental water samples. Different monolithic sol–gel encapsulated sorbents were compared and monolithic sol–gel poly(ethylene glycol)-based sorbent incorporated into porous microextraction capsules resulted in the highest...
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Experimental investigation of performance and emission characteristics of a miniature gas turbine supplied by blends of kerosene and waste tyre pyrolysis oil
PublikacjaFossil fuels are non-renewable sources of energy that could be depleted in the near future, giving rise to amajor energy crisis. Scientists from all over the world are working on new technologies to produce fuelnot only from renewable sources but also from waste. This article is concerned with: (i) waste tyremanagement by means of the pyrolysis process, (ii) investigation of physico-chemical parameters ofwaste tyre pyrolysis oil...
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A geophysical, geochemical and microbiological study of a newly discovered pockmark with active gas seepage and submarine groundwater discharge (MET1-BH, central Gulf of Gdańsk, southern Baltic Sea)
PublikacjaHigh-resolution bathymetric data were collected with a multi-beam echosounder in the southern part of the Baltic Sea (region MET1, Gulf of Gdańsk) revealing the presence of a 10 m deep and 50 m in diameter pockmark (MET1-BH) on the sea bottom (78.7 m). To date, no such structures have been observed to reach this size in the Baltic Sea. The salinity of the near-bottom water in the pockmark was about 2 PSU (about 31.22 mmol/l...
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Evaluation of the significance of the effect of the active cross-sectional area of the inlet air channel on the specific enthalpy of the exhaust gas of a diesel engine using statistics F of the Fisher-Snedecor distribution
PublikacjaThis paper presents the application of Fisher-Snedecor distribution F statistics to assess the significance of the influence of changes in the active cross-sectional area of the inlet air channel (Adol) flow in a diesel engine on the observed diagnostic parameter determined on the basis of measurements of the quick changing exhaust gas temperature in the outlet channel, which is the specific enthalpy of the exhaust gas stream within...
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Market Price Prediction of Property Rights from Gas Fired Plants or Plants with Total Installed CHP Source Capacity Below 1 MW until 2025
PublikacjaThe resolution on the Polish Energy Policy until 2030 (PEP-30) was adopted by the Council of Ministers on 10 November 2009. The document specifies the combined electricity and heat generation as a direction of pursuing the goals of energy efficiency, fuel and energy supply security, competitive fuel and energy markets development, and reduction of the energy sector’s environmental impact. PEP-30 assumes that electricity generation...