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Search results for: ELECTROCHEMICAL DEPOSITION METHOD
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Detection of stress corrosion cracking dynamics by dynamic electrochemical impedance spectroscopy.
PublicationKlasyczne badania korozji naprężeniowej nie dają precyzyjnych informacji o dynamice takiego procesu korozyjnego. Nowa technika dynamicznej elektrochemicznej spektroskopii impedanyjnej, która została opracowana w Katedrze Elektrochemii, Korozji i Inżynierii Materiałowej stwarza takie możliwości. Fakt ten związany z zastosowaną metodologią analizy umożliwiającą selektywną analizą czasowo-częstotliwościową danych pomiarowych.Praca...
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Investigations of the passive layer cracking by means of Dynamic Electrochemical Impedance Spectroscopy
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Electrochemical investigations of stainless steels used in flue‐gas desulphurization units
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Detection of stress corrosion cracking dynamics by dynamic electrochemical impedance spectroscopy
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Synthesis and electrochemical characterization of poly(3,4-ethylenedioxythiophene) modified by iron hexacyanocobaltate
PublicationPraca dotyczy sposobu syntezy oraz elektrochemicznej charakterystyki materiału kompozytowego złożonego z poli(3,4-etylenodioksytiofenu) i heksacyjanokobaltanu(III) żelaza(II). Wybrany materiał badany był przy użyciu spektroskopii impedancyjnej, chronopotencjometrii oraz woltamperometrii cyklicznej w kontakcie z elektrolitem wodnym (KCl) oraz aprotycznym (LiPF6 w mieszaninie węglanu etylenu i węglanu propylenu). Materiał charakteryzuje...
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Synthesis, characterization, and electrochemical testing of carbon nanotubes derivatized with azobenzene and anthraquinone.
PublicationWielościenne i jednościenne nanorurki węglowe modyfikowano na ścianach bocznych związkami elektrochemicznie aktywnymi, takimi jak azobenzen i antrachinon. Funkcjonalizowane nanorurki badano technikami spektroskopowymi i elektrochemicznymi oraz wykorzystując mikroskopię elektronową. Wyniki tych badań potwierdziły chemiczną modyfikację.
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Metal heksacyanoferrate network synthesized inside polymer matrix for electrochemical capacitors
PublicationPrzedmiotem publikacji jest charakterystyka elektrochemiczna polimeru przewodzącego (poli(3,4-etylenodioksytiofenu)) modyfikowanego błękitem pruskim oraz jego pochodnymi, pochodną kobaltową oraz pochodną niklową. Materiały są stabilne elektrochemicznie, a uzyskane wartości pojemności elektrycznej pozwalają na wykorzystanie ich przy konstrukcji kondensatorów elektrochemicznych.
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An electrochemical interface for direct analysis of amlodipine in tablets and human blood samples
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Electrochemical and catalytic assessment of peripheral bromoaryl-substituted manganese and iron porphyrazines
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Amine-Based Ionic Liquid for CO2 Capture and Electrochemical or Thermal Regeneration
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Palladium nanoparticles deposited on graphene and its electrochemical performance for glucose sensing
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Microwave-assisted hydrothermal synthesis and electrochemical studies of α- and h-MoO3
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Electrochemical oxidation of ionic liquids at highly boron doped diamond electrodes
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Double Bias of Mistakes: Essence, Consequences, and Measurement Method
PublicationThere is no learning without mistakes. However, there is a clash between‘positive attitudes and beliefs’regarding learning processes and the ‘negative attitudes and beliefs’towardthese being accompanied bymistakes. Thisclash exposesa cognitive bias towardmistakesthat might block personal and organizational learning. This study presents an advanced measurement method to assess thebias of mistakes. The essence of it is the...
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The Method of Finding the Optimal Spindle Speed When Milling Flexible Details
PublicationThe paper presents a new method of vibration reduction during milling of flexible details. The method consists in selecting the optimal spindle speed, based on the natural frequency of the workpiece. For this purpose, an original method was created, which is based on minimizing the work of cutting forces in the direction of the depth of cutting. The effectiveness of the method has been proved by comparing the RMS values of vibration...
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Facile synthesis and characterization of graphene and N-doped graphene by CVD method from liquid precursors for promising electrode materials
PublicationIn this study, high-quality and few-layered graphene was synthesized using the chemical vapor deposition (CVD) method from liquid sources. Two different liquid carbon sources, pyridine, and benzene, were used and deposited on nickel foam under heat conditions using a bubbler in a quartz tube. X-ray diffraction (XRD) and Raman analysis confirmed the crystalline properties of graphene and N-doped graphene, demonstrating the high...
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Application of the LifeRoSE method in funcionality evaluation of road safety equipment
PublicationThe article presents a mathematical model of the life cycle estimation method of road safety equipment. Then the model was adjusted to estimate the life cycle costs of the chosen horizontal road marking. Using the LCC method, the functionality of the horizontal marking was evaluated in terms of efficiency, durability and economic effectiveness. The article also presents the impact of selected factors on the life cycle costs of...
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Sensor Position Estimation Method for IoT Using Mobile Reference Node
PublicationThe paper proposes an innovative method of locating objects for the Internet of Things (IoT). The proposed method allows the position of a fixed measuring sensor (MS) to be estimated using one mobile base station with a known position moving around the MS. The mathematical analysis of the method, and three algorithms — Newton’s (NA), gradient descent (GD) and genetic (GA) — for solving the system of non-linear positional equations...
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A New Method for Automatic Generation of Animated Motion
PublicationA new method for generation of animation with a quality comparable to a natural motion is presented. Proposed algorithm is based on fuzzy description of motion parameters and subjective features. It is assumed that such processing increases naturalness and quality of motion, which is verified by subjective evaluation tests. First, reference motion data are gathered utilizing a motion capture system, then these data are reduced...
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An extension of the method of quasilinearization
PublicationMetodę kwazilinearyzacji zastosowano do problemów początkowych gdy prawą stronę zagadnienia można przedstawić za pomocą nieliniowej funkcji "rozszerzenia", zakładając o niej pewną regularność. Pokazano, że odpowiednio skonstruowane ciągi monotoniczne są zbieżne kwadratowo do rozwiązania problemu. Praca uogólnia odpowiednie wyniki, gdy prawa strona jest sumą funkcji wklęsłych i wypukłych ze względu na ostatni argument.
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Characteristics of the Hydrophytes Method
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A standard analytical method as the common good and pollution abatement measure
PublicationA standard method can be considered as a common-good “resource,” and the solution to “the commons” problems usually lies in societal self-organization. The multi-criteria decision analysis (MCDA) was applied to model complex phenomena, such as the standard selection for imidacloprid determination. In this process, the standard was self-selected by the analytical chemistry society. The results show that analytical chemistry is a...
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Evolutionary Sets of Safe Ship Trajectories: development of the method
PublicationThe Evolutionary Sets of Safe Ship Trajectories is a method solving ship encounter situations. The method combines evolutionary approach to planning ship trajectory with some of the assumption of game theory. For given positions and motion parameters the method finds a near optimal set of safe trajectories of all ships involved in an encounter. The version presented here is an updated one and its authors have tested extensively...
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Variational Method of Finding Streamlines in Ring Cascades for Creeping Flows
PublicationThis paper presents a new, analytical method of finding streamlinesfor creeping flows inside a ring cascade which is composed of an infinite number of infinitely thin blades. An analytical solution has been obtained through minimisation of a dissipation functional by means of variational calculus method. The necessary condition for optimum of a functional gives the Stokes equation if some additional assumptions are introduced....
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Application of the Optimum Dataset Method in Archeological Studies on Barrows
PublicationLight Detection and Ranging (LiDAR) became one of the technologies used in archaeological research. It allows for relatively easy detection of archaeological sites that have their own field form, e.g.: barrows, fortresses, tracts, ancient fields [1]. As a result of the scanning, the so-called point cloud is obtained, often consisting of millions of points. Such large measurement datasets are very time-consuming and labor-intensive...
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Trust Management Method for Wireless Sensor Networks
PublicationA Wireless Sensor Network (WSN) is a network of spatially distributed autonomous sensors to monitor physical or environmental conditions, such as temperature, sound, pressure, etc. and to cooperatively pass their data to the main location. The first wireless network that bore any real resemblance to a modern WSN is the Sound Surveillance System (SOSUS), developed by the United States Military in the 1950s to detect and track Soviet...
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Determining the leakage current resistive component by the orthogonal vector method
PublicationThe measurement of the metal – oxide surge arresters (MOSA) leakage current and the analysis of its components is a key diagnostic criterion according to technical standards. During on site MOSA condition assessment, the easy way is based on the measurement only leakage current, without the inconvenient live working measurements of supply voltage. Orthogonal vectors method of determination the resistive leakage current is presented....
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Method for universal detection of two-photon polarization entanglement
PublicationDetecting and quantifying quantum entanglement of a given unknown state poses problems that are fundamentally important for quantum information processing. Surprisingly, no direct (i.e., without quantum tomography) universal experimental implementation of a necessary and sufficient test of entanglement has been designed even for a general two-qubit state. Here we propose an experimental method for detecting a collective universal...
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Very high altitude micro air vehicle deployment method
PublicationThe paper presents the original work and method for high altitude micro air vehicle deployment. The method is based on the scientific ballooning, and adapted for stratospheric flight of commercial off-the-shelf micro air vehicle in flying wing configuration. The High Altitude Micro Air Vehicle, built for this research, was deployed during a test experiment at the lower level of the stratosphere. The results of the experiment and...
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Comparative field test for measurement of PM10 dust in atmospheric air using gravimetric (reference) method and b-absorption method (Eberline FH 62-1)
PublicationThe paper presents the results of a field test carried out in Gdansk region between 01-01-2010 and 31-12-2010 in order to demonstrate equivalence of the Eberline FH 62-1 sampler to the reference gravimetric method of suspended PM10 dust measurement. The differences in PM10 dust concentration provided by both methods have been discussed for different seasons of the year. A method of estimation of the correction factors/correction...
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Adsorption behavior and corrosion inhibitive characteristics of newly synthesized cyano-benzylidene xanthenes on copper/sodium hydroxide interface: Electrochemical, X-ray photoelectron spectroscopy and theoretical studies
PublicationElegant process for synthesis of 3-(7H-dibenzo[c,h]xanthen-7-yl)benzaldehyde (3), as new starting material to create a set of novel xanthene analogues, 2-(3-(7H-dibenzo[c,h]xanthen-7-yl)benzylidene)malononitrile (4), 3-(3-(7H-dibenzo[c,h]xanthen-7-yl)phenyl)-2-cyanoacrylic acid (5), and Ethyl-3-(3-(7H-dibenzo[c,h]xanthen-7-yl)phenyl)-2-cyanoacrylate (6), was achieved starting with available materials under mild conditions. Various...
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Ship Evolutionary Trajectory Planning Method with Application of Polynomial Interpolation
PublicationPaper presents the application of evolutionary algorithms and polynomial interpolation in ship evolutionary trajectory planning method. Evolutionary algorithms allows to find a coIlision free trajectory in real time, while polynomial interpolation allows to model smooth trajectory which keeps continuity of velocity and acceleration values along path. Combination of this two methods allows to find trajectory, which under some assumptions,...
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Efficacious Alkaline Copper Corrosion Inhibition by a Mixed Ligand Copper(II) Complex of 2,2′-Bipyridine and Glycine: Electrochemical and Theoretical Studies
PublicationA mixed ligand copper(II) complex, namely, [Cu(BPy)(Gly)Cl]⋅2H2O (CuC) (BPy=2,2′-bipyridine and Gly=glycine), was synthesized and characterized. The synthesized CuC complex was tested as inhibitor to effectively mitigate the corrosion of copper in alkaline solutions using the linear sweep voltammetry (LSV) and linear polarization resistance (LPR) techniques. For the sake of comparison, such two D.C. electrochemical techniques were...
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New method for personalization of avatar animation
PublicationThe paper presents a method for creating a personalized animation of avatar utilizing fuzzy inference. First the user designs a prototype version of animation, with keyframes only for important poses, roughly describing the action. Then animation is enriched with new motion phases calculated by the fuzzy inference system using descriptors given by the user. Various degrees of motion fluency and naturalness are possible to achieve....
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Atypical application of the parametric method for track infrastructure inventory
PublicationFor many years, satellite systems have seen widespread use in a variety of technical applications, as well as in operations related to setting-out and the exploitation of track infrastructure. Their main applications include an inventory of the trackage course and detecting changes in its position. In both of these tasks, the most important element that determines the quality of an analyses is the high accuracy of the determinations...
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Polymodal Method of Improving the Quality of Photogrammetric Images and Models
PublicationPhotogrammetry using unmanned aerial vehicles has become very popular and is already commonly used. The most frequent photogrammetry products are an orthoimage, digital terrain model and a 3D object model. When executing measurement flights, it may happen that there are unsuitable lighting conditions, and the flight itself is fast and not very stable. As a result, noise and blur appear on the images, and the images themselves can...
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A convenient method for the preparation of functionalized N-acylsulfenamides from primary amides.
PublicationWe have developed a convenient method for the synthesis of functionalized N-acylsulfenamides under mild conditions and in moderate to good yields. The designed method is based on the reaction of (5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl)-disulfanyl derivatives with nitrogen nucleophiles generated from primary amides or imides and sodium hydride. The developed method allows for the preparation of N-acylsulfenamides bearing...
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Fast High-Impedance Spectroscopy Method Using SINC Signal Excitation
PublicationIn this paper the method of fast impedance spectroscopy of technical objects with high impedance (|Zx| > 1 Gohm) is evaluated by means of simulation and practical experiment. The method is based on excitation of an object with a sinc signal and sampling response signals proportional to current flowing through and voltage across the measured impedance. The object impedance spectrum is obtained with use of continuous Fourier transform...
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The method of location and identification of weak electric field source in seawater
PublicationThe paper presents the method and measurement system that allows to lacate the detected object and to identify parameters of its simplified model in form of a current dipole.
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Simple Measurement Method for Resistive Sensors Based on ADCs of Microcontrollers
PublicationA new, complete measurement method for resistance measurement of resistive sensors for systems based on microcontrollers equipped with analog-to-digital converters (ADCs) is proposed. The interface circuit consists of only four resistors, including a resistive sensor and a reference resistor, connected directly to the microcontroller pins. It is activated only during measurements, which significantly reduces power consumption....
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A Rapid and Simple Method for Screening Microorganisms with a Potential for Catechol Biodegradation
PublicationCatechol is a highly toxic compound that is also a key intermediate in biodegradation pathways of various aromatic compounds. In this paper, a new screening method for isolation of microorganisms with the potential for catechol biodegradation is reported. The method described is based on the ability of catechol to form a color complex with Fe3+ ions. For this purpose, basal medium that is widely used for classification of microorganisms...
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Biomolecular influenza virus detection based on the electrochemical impedance spectroscopy using the nanocrystalline boron-doped diamond electrodes with covalently bound antibodies
PublicationNew rapid pathogen detection methods with improved cost-effectiveness and efficiency are currently in the focus of the scientists from all over the world. Based on the experiences from the rapid spread of the influenza virus pandemic in 2009 it is clear that the development of the system for early diagnosis of this infection is essential. The crucial stage of the treatment is the detection of the viral infection during its initial...
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Structure and electrical properties of Y, Fe-based perovskite mixed conducting composites fabricated by a modified polymer precursor method
PublicationIn this work, samples of Y0.07Sr0.93Ti1-xFexO3-d with 20, 40, 60 and 80 mol% of iron amount were prepared by a low-temperature polymer precursor method. The SEM-EDS analysis proved that analyzed Y0.07Sr0.93Ti1-xFexO3-d samples were composites of two Ti- and Fe-rich perovskite samples. This kind of composite consists of two phases in which one has a good ionic and the other electronic conductivity, which makes such a composite a...
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Parallel implementation of the DGF-FDTD method on GPU Using the CUDA technology
PublicationThe discrete Green's function (DGF) formulation of the finite-difference time-domain method (FDTD) is accelerated on a graphics processing unit (GPU) by means of the Compute Unified Device Architecture (CUDA) technology. In the developed implementation of the DGF-FDTD method, a new analytic expression for dyadic DGF derived based on scalar DGF is employed in computations. The DGF-FDTD method on GPU returns solutions that are compatible...
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Smart Cities System Design Method Based on Case Based Reasoning
PublicationThe objective of this paper is to present the results of research carried out to develop a design method for Smart Cities systems. The method is based on the analysis of design cases of Smart Cities systems in cities, the selection of the city appropriate to the requirements for implementation and application. The Case Based Reasoning method was used to develop the proposed design methodology, along with mechanisms of the conversion...
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Investigation on accelerated impedance spectrum measurement method with multisine signal stimulation
PublicationThe paper presents an investigation on the accelerated impedance spectrum measurement method, oriented at parameter identification of technical objects modelled by a linear equivalent circuit, e.g. anticorrosion coatings.The method is based on multisine signal stimulation of an object and response analysis by triangle window filterbanks.It has several advantages, as compared with conventional point-by-point spectrum measurement....
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New Method for Determination of Adjustment Corrections for Crane Rail Axes
PublicationElectronic tacheometers are currently a standard instrument used in geodetic work, including also geodetic engineering measurements. One of the many applications of tacheometers in engineering geodesy are 3D control measurements of crane rail axes. This paper proposes a new method of computing adjustment corrections for crane rail axes based on 3D polar measurements performed with an electronic tacheometer. The intermediary method...
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THE SYNCHROSQUEEZING METHOD IN BEARING ESTIMATION OF STATIONARY SIGNALS FOR PASSIVE SONAR WITH TOWED ARRAY
PublicationIn this paper, a novel method of bearing estimation in a passive sonar system with a towed array is introduced. The classical approach of bearing estimation based on the spatial spectrum [1] is extended by using the synchrosqeezing method that is a part of the reassignment method introduced by Kodera et al. [2]. Using this method leads to a precise bearing estimation. The proposed method requires a relatively small amount of computation,...
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Preliminary designing method of external pressure vessels for sea subsurface aplications
PublicationThis paper describes a unique engineering method intended for the preliminary designing of marine subsurface buoy mooring systems. The solved designing problem consists in determining geometrical parameters and selecting structural materials for a vessel of a buoyancy necessary to contain measuring instruments of a given mass, as well as its maximum dimensions and operational submersion depth. The assumed variability range of...
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Nipagin-Functionalized Porphyrazine and Phthalocyanine—Synthesis, Physicochemical Characterization and Toxicity Study after Deposition on Titanium Dioxide Nanoparticles P25
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