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Search results for: sample preparation techniques
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Determination of Selected Metals in Fruit Wines by Spectroscopic Techniques
PublicationThe determination of metals in different types of food and beverages samples has drawn significant attention due to several reasons with the most important one being the nutritional and toxic effects of these elements or their compounds. The knowledge of certain elements content in wines/fruit wines is of special interest due to their toxicity in case of excessive intake and also the effect they seem to have on the organoleptic...
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Methods of Assessing Degradation of Supercapacitors by Using Various Measurement Techniques
PublicationThis article presents the qualitative analyses of the construction of supercapacitor samples. The analyses are based on the suggested thermographic measurements as well as the technique of testing the inherent noise of the investigated element. The indicated assessment methods have been referred to the currently used parameters for the qualitative evaluation of supercapacitors. The approach described in this paper, which introduces...
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PTR-MS and GC-MS as complementary techniques for analysis of volatiles: A tutorial review
PublicationThis tutorial review is a critical commentary on the combined use of two instrumental analytical techniques, namely GC-MS and PTR-MS. The first mention of such an analytical approach likely appeared after the year 2000 and despite many advantages, it has not been applied very often. Therefore, the aim of this article is to elaborate on the concept of their combined use and to provide a curse tutorial for those considering taking...
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Accelerometer-based Human Activity Recognition and the Impact of the Sample Size
PublicationThe presented study focused on the recognition of eight user activities (e.g. walking, lying, climbing stairs) basing on the measurements from an accelerometer embedded in a mobile device. It is assumed that the device is carried in a specific location of the user’s clothing. Three types of classifiers were tested on different sizes of the samples. The influence of the time window (the duration of a single trial) on selected activities...
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Thermally stimulated carrier transport due to stepwise sample heating.
PublicationPodano przybliżone rozwiązania równań nieizotermicznego transportu nośników w izolującym ciele stałym ze stanami pułapkowymi, dla przypadku krokowego ogrzewania próbki. Otrzymane wyniki zweryfikowano za pomocą symulacji Monte Carlo dla gaussowskiego rozkładu pułapek.
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Development and validation of the attitude towards Surrogacy Scale in a polish sample
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Adaptation of the Four Forms of Employee Silence Scale in a Polish sample
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The influence of the substrate temperature on the preparation of DNA films for studies under vacuum conditions
PublicationExperiments were carried out to determine the dependence of the physical form of supercoiled DNA films on the initial temperature of the substrate. Such films are often used in irradiation experiments involving low energy particles, like electrons or photons. In order to obtain absolute values for cross sections for such experiments, the spatial distribution of the sample in the film has to be well estimated. These investigations...
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Talents, Competencies and Techniques of Business Analyst: A Balanced Professional Development Program
PublicationThis paper presents preliminary results of action research in which we search for fundamentals of an universal theory of balanced approaches to software process. It is developed on the basis of balanced approach for professional development program for business analysts which integrates approaches oriented on talents, competencies and techniques. This paper includes the description of key concepts in background approaches, components...
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Practical issues for the implementation of survivability and recovery techniques in optical networks
PublicationFailures in optical networks are inevitable. They may occur during work being done for the maintenance of other infrastructures, or on a larger scale as the result of an attack or large-scale disaster. As a result, service availability, an important aspect of Quality of Service (QoS), is often degraded. Appropriate fault recovery techniques are thus crucial to meet the requirements set by the Service Level Agreements (SLAs) between...
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The Current State-of-the-Art in the Determination of Pharmaceutical Residues in Environmental Matrices Using Hyphenated Techniques
PublicationSeveral thousand tons of pharmaceuticals and their transformation products (metabolites and degradation products) are introduced into the environment each year. They affect both human health and the environment, therefore, analytical procedures enabling the determination of a wide range of pharmaceuticals at trace levelswithminimal effort, time, and energy are required. Nowadays, hyphenated techniques are commonly applied in pharmaceutical...
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Selected aspects of two-phase flow studies using different visualization techniques in minichannels
PublicationThe subject of the study is to present the possibility of the use of visualization techniques in the researches on two-phase flows, carried out by the authors for many years. These works included as follows: heat transfer during the flow boiling, boiling crises and condensation in flow. The issue of the heat transfer intensification during the flow boiling through the channels of small diameters was analyzed. All this work focused...
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Minimization of vibrations during milling of flexible structures using mechatronic design techniques
PublicationThe paper presents an innovative effective method of minimizing vibrations during milling of flexible structures, using a new vibration suppression method based on a workpiece holder with adjustable support stiffness. The proposed method is rooted in mechatronic design techniques, which can become a standard procedure for optimizing the milling process.
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Preparation of exfoliated graphite by microwave irradiation
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Studies on the Preparation and Characterisation of Carbon Nanostructures
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Fatal intoxication with hydrocarbons in deltamethrin preparation
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Preparation of Descriptive Geometry Course in English
PublicationW artykule przedstawiono wybrane różnice stosowane w zapisie konstrukcji geometrycznych w podręcznikach do geometrii wykreślnej w różnych krajach.
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Nanoparticles Preparation Using Microemulsion Systems
PublicationW rozdziale opisano otrzymywanie nanocząstek za pomocą metody mikroemulsyjnej oraz wpływ parametrów reakcji na powstawanie nanocząstek. Omówiono różne rodzaje struktur bimetalicznych - rdzeń-otoczka i stopowe.
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Proton Conducting Ceramic Powder Synthesis by a Low Temperature Method
PublicationMolten salt synthesis (MSS) is a simple method for the preparation of ceramic powders with specific morphology. The main role of the molten salts is to increase the reaction rate and lower the reaction temperature. It occurs because of much higher mobility of reactants in the liquid medium than in the solid state. In this work the molten salt synthesis was applied to produce ceramic powders of La0995Ca0005NbO4 and BaCe09−xZrxY01O3....
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Development of potential candidate reference materials for drugs in bottom sediment, cod and herring tissues
PublicationRegular use of a reference material and participation in a proficiency testing program can improve the reliability of analytical data. This paper presents the preparation of candidate reference materials for the drugs metoprolol, propranolol, carbamazepine, naproxen, and acenocoumarol in freshwater bottom sediment and cod and herring tissues. These reference materials are not available commercially. Drugs (between 7 ng/g and 32...
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Organic semiconductor rubrene thin films deposited by pulsed laser evaporation of solidified solutions
PublicationOrganic semiconductor rubrene (C42H28) belongs to most preferred spintronic materials because of the high charge carrier mobility up to 40 cm2(V·s)-1. However, the fabrication of a defect-free, polycrystalline rubrene for spintronic applications represents a difficult task. We report preparation and properties of rubrene thin films deposited by pulsed laser evaporation of solidified solutions. Samples of rubrene dissolved in aromatic...
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Hydrogen production from biomass using dark fermentation
PublicationHydrogen applicability in the power, chemical and petrochemical industries is constantly growing. Efficientmethods of hydrogen generation from renewable sources, including waste products, are currently being de-veloped, even though hydrogen is mainly produced through steam reforming or thermal cracking of natural gasor petroleum fractions. In paper alternative methods of hydrogen production with a particular emphasis on darkfermentation...
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Properties of ordered titanium templates covered with Au thin films for SERS applications
PublicationtCurrently, roughened metal nanostructures are widely studied as highly sensitive Raman scattering sub-strates that show application potential in biochemistry, food safety or medical diagnostic. In this workthe structural properties and the enhancement effect due to surface enhanced Raman scattering (SERS) ofhighly ordered nano-patterned titanium templates covered with thin (5–20 nm) gold films are reported.The templates are formed...
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Cannabinoids: Challenges, opportunities and current techniques towards its extraction and purification for edibles
PublicationDue to the multiple health benefits associated with the consumption of cannabinoids, there is a current trend on continuing to explore their biological properties. Cannabidiol (CBD) is likely to be the most investigated endocannabinoid from the cannabis plant. Unfortunately, the purification of CBD from its natural source and psychotropic analogue (tetrahydrocannabinol, THC) is timely challenging for the research community based...
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Using wavelet techniques for multibeam sonar bathymetry data compression
PublicationMultibeam sonars are widely used in applications like high resolution bathymetry measurements or underwater object imaging. One of the significant problems in multibeam sensing of the marine environment is large amount of data which must be transmitted from the sonar processing unit to an operator station using a limited bit rate channel. For instance, such a situation would be in the case when the multibeam sonar was mounted on...
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Quantifying the effective mobilized RAP content during hot in-place recycling techniques
PublicationThe utilization of in-place recycling techniques is capable of consuming 100% reclaimed asphalt pavement (RAP). Hot in-place recycling (HIR) is one of the promising techniques to rehabilitate the pavements suffering from minor cracking issues through heat scarification, additive injecting, mechanical mixing, and compacting. However, the main concern of using 100% RAP in HIR remains as how much RAP can be activated and mobilized...
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EMI mitigation of GaN power inverter leg by local shielding techniques
PublicationThis paper presents local shielding techniques applied to a half-bridge inverter leg with the aim to reduce the common mode (CM) current noise at converter’s DC input. The research study is conducted for 650V Enhancement mode Gallium Nitride (GaN) power transistor switches. Main contributors of parasitic capacitances referred to the inverter-leg middle point node are identified. Then, shielding solutions are proposed to reduce...
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Fractional delayor application in self-tuning sub-sample delay estimator
PublicationW artykule przedstawiono nowe rozwiązanie samonastrajalnego estymatora opóźnienia sygnału sinusoidalnego. Estymator działa w czasie dyskretnym. Proponowane rozwiązanie wykorzystuje kaskadowe połączenie cyfrowego filtru ułamkowo opóźniającego służącego do synchronizacji próbkowania i liniowo-fazowego cyfrowego filtru Hilberta. Oryginalność polega na zastosowaniu tu filtrów cyfrowych o bardzo małej złożoności numerycznej. Jest ona...
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Comparison of Compact Reduced Basis Method with Different Model Order Reduction Techniques
PublicationDifferent strategies suitable to compare the performance of different model order reduction techniques for fast frequency sweep in finite element analysis in Electromagnetics are proposed and studied in this work. A Frobenius norm error measure is used to describe how good job a reduced-order model is doing with respect to the true system response. In addition, the transfer function correct behavior is monitored by studying the...
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Measurement techniques of tailored optical fibers
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DSP techniques for determining ''Wow'' distortions
PublicationArtykuł przedstawia opis algorytmów do wyznaczania charakterystyki zniekształceń kołysania dźwięku. Są to algorytmy: śledzenia przydźwięku sieciowego, śledzenia pozostałości magnetycznej prądu podkładu wielkich częstotliwości, adaptacyjnej analizy środka ciężkości widma dla wybranej części zniekształconego sygnału. Przedstawione algorytmy pozwalają na implementację programową i sprzętową.
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Music information analysis and retrieval techniques
PublicationCelem artykułu jest przedstawienie kluczowych zagadnień gwałtownie rozwijającej się gałęzi multimediów, reprezentowanej przez systemy automatycznego wyszukiwania informacji muzycznej MIR - Music Information Retrieval, która urasta do samodzielnej dziedziny zastosowań w obrębie informatyki muzycznej. W artykule przedstawiono wybrane systemy wyszukiwania informacji muzycznej oraz przedstawiono przykład takiego systemu, zrealizowanego...
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Applications of soft modelling and intelligent techniques
PublicationW edytorialu omówiono szeroko obecne praktyczne zastosowania modelowania miękkiego oraz technik inteligentnych, rozumianych jako takie techniki, które potrafią wspomagać podejmowanie decyzji w zmiennych warunkach otoczenia.
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DSP techniques in wow defect evaluation
PublicationReferat przedstawia dwie metody określania przebiegu pasożytniczego drżenia dźwięku. Obie wykorzystują analizę pasożytniczych artefaktów. Wybrane artefakty to: przydźwięk sieciowy i wysokoczęstotliwościowy prąd podkładu. Precyzyjny przebieg zniekształcenia kołysania oblicza się wykorzystując informacje zawarte w widmie sygnałów, a uzyskane poprzez STFT lub modelowanie AR. Referat zawiera opis eksperymentów i uzyskane wyniki.
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Integration of speech enhancement and coding techniques
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Application of ionic liquids in chromatographic techniques
PublicationCiecze jonowe (ang. Ionic Liquids, ILs) z uwagi na swoje unikalne właściwości fizyko – chemiczne oraz możliwość prostej modyfikacji budowy, w znacznym stopniu przyczyniły się do rozwoju technik rozdzielania. W chromatografii gazowej fazy stacjonarne w postaci cieczy jonowych stanowią istotne uzupełnienie istniejących faz stacjonarnych na bazie polisiloksanów i glikolu polietylenowego. Ze względu na wysoką stabilność termiczną...
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Test Execution Logging and Visualization Techniques
PublicationTraditionally, log traces of test cases ex ecution are stored in textual format and their analysis is done in a post- execution phase. Our approach bases on the concept of gr aphical presentation of te st execution which enables better analysis of log traces and also gives the opportunity to consider them on-line. In particular, we discuss the graphical symbols we chose, we pres ent the logging interface we defined a nd describe...
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Detection of gaseous compounds with different techniques
PublicationSensing technology has been developed for detection of gases in some environmental, industrial, medical, and scientific applications. The main tasks of these works is to enhance performance of gas sensors taking into account their different applicability and scenarios of operation. This paper presents the descriptions, comparison and recent progress in some existing gas sensing technologies. Detailed introduction to optical sensing...
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Fast Design Optimization of Waveguide Filters Applying Shape Deformation Techniques
PublicationThis paper presents an efficient design of microwave filters by means of geometry optimization using shape deformation techniques. This design procedure allows for modelling complex 3D geometries which can be fabricated by additive manufacturing (AM). Shape deforming operations are based on radial basis function (RBF) interpolation and are integrated into an electromagnetic field simulator based on the 3D finiteelement method (FEM)....
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Identification of aromatic compounds in odours mixture by gas chromatography and field olfactometry techniques
PublicationThis paper shows the results of investigation on identification aromatic compounds present in odorous mixture in atmospheric air samples collected in a vicinity of the oil refinery LOTOS S.A., located in Gdansk, during March and April period have be presented. The studies were conducted by the use of comprehensive two-dimensional gas chromatograph equipped with a cryogenic modulator and coupled with a time-of-flight mass spectrometer,...
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Ionic liquids in extraction techniques: Determination of pesticides in food and environmental samples
PublicationThe intensive use of pesticides in agricultural practices has promoted the appearance of environmentaland public health problems. Due to that, scientists face challenges with developing simple, fast, sensitive,selective, and low-cost methods dedicated to determining pesticide residues in food and environmentalsamples. Following thefifth principle of Green Analytical Chemistry, chemists are searching for greeneralternatives for...
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Engineering Au nanoparticle arrays on SiO2 glass by pulsed UV laser irradiation
PublicationWe study semi-regular arrays of Au nanoparticles (NP) obtained via UV laser irradiation of thin Au films on glass substrate. The NP structures are prepared from films of a thickness up to 60 nm produced by discharge sputtering or pulsed laser deposition, and annealed by nanosecond laser pulses at 266 or 308 nm, respectively, at fluencies in the range of 60-410 mJ/cm2. For the rare- and close-packed NP structures, consistent description...
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Biosynthetic and synthetic access to amino sugars.
PublicationAmino sugars are important constituents of a number of biomacromolecules and products of mi crobial secondary metabolism, including antibiotics. For most of them, the amino group is located at the positions C1, C2 or C3 of the hexose or pentose ring. In biological systems, amino sugars are formed due to the catalytic activity of specific aminotransferases or amidotransferases by introducing an amino functionality derived from L-glutamate...
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Bio-based semi-aromatic polyesters for coating applications
PublicationLinear and branched bio-based semi-aromatic (co)polyesters were evaluated as resins for solvent-basedand powder coatings. Dimethyl-2,5-furandicarboxylate (DMF), 2,3-butanediol and various multifunc-tional comonomers were used to synthesize amorphous hydroxyl-end-capped (co)polyesters. The resinswere cross-linked using the -caprolactam blocked trimer of isophorone diisocyanate. Both the solvent-based and powder coatings proved to...
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Magnetic superhydrophobic melamine sponges for crude oil removal from water
PublicationThis paper proposes the preparation of a new sorbent material based on melamine sponges (MS) with superhydrophobic, superoleophilic, and magnetic properties. This study involved impregnating the surface of commercially available MS with eco-friendly deep eutectic solvents (DES) and Fe3O4 nanoparticles. The DES selection was based on the screening of 105 eutectic mixtures using COSMO-RS modeling. Other parameters affecting the efficiency...
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Progress, Challenge, and Perspective of Bimetallic TiO2-Based Photocatalysts
PublicationBimetallic TiO2-based photocatalysts have attracted considerable attention in recent years as a class of highly active catalysts and photocatalysts under both UV and Vis light irradiation. Bimetallic noble metal structures deposited on TiO2 possess the ability to absorb visible light, in a wide wavelength range (broad LSPR peak), and therefore reveal the highest level of activity as a result of utilization of a large amount of...
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Steroid Sulfatase Inhibitors Based on Phosphate and Thiophosphate Flavone Analogs
PublicationA series of phosphate and thiophosphate flavone derivatives were synthesized and biologically evaluated in vitro for inhibition of steroid sulfatase (STS) activity. The described synthesis includes the straightforward preparation of 7-hydroxy-2-phenyl-4H-chromen-4-one 3a, 2-(4-fluorophenyl)-7-hydroxy-4H-chromen-4-one 3b, 7-hydroxy-2-(4-(trifluoromethyl)phenyl)-4H-chromen-4-one 3c, 7-hydroxy-2-(p-tolyl)-4H-chromen-4-one 3d modified...
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Temperature influence on tire/road noise evaluated by the drum method
PublicationAmbient air and road surface temperatures substantially affect the road vehicle noise emission. The temperature influence on tire/road noise depends mainly on tire-road combination. It is different for dense and porous pavements, for bituminous and cement ones. It differs also depending on tires. The correction procedures for temperature effect are still under consideration and preparation. Laboratory experiment was prepared to...
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Effect of modified soybeen oil amount on rheological characteriza-tion of polyurethane pre-polymers
PublicationPolyurethanes (Pu’s) are the polymeric materials which have got urethane groups in the structure. The properties of Pu’s depend both on the method of preparation and monomers used. Polyurethanes are produced by two methods known as one step or two step method called as “pre-polymers method”, especially for the case of segmented polyurethanes (SPU’s). These materials are thermoplastic block copolymers of the (AB)n type consisting...
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Regeneration of marine engine valves using laser surfacing
PublicationThis article presents an analysis of the applicability of laser surfacing of the exhaust valve face of a marine diesel engine using cobalt-based powder. After preparation by machining, the selected valves were subjected to laser surfacing using a high-power ROFIN DL020 laser. The EuTroLoy 16012 powder was used in the surfacing process. One of the valves was cut and subjected to metallographic examination and hardness measurements,...