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Search results for: SPME/GC
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Social media for e-learning of citizens in smart city
PublicationThe rapid development of social media can be applied for citizens’ e-learning in a smart city. Big cities have to cope with several open issues like a growing population or a traffic congestion. Especially, a home and public space is supposed to be used in more efficient way. Sustainable homes and buildings can be planned with using some modern techniques. Even currently, there is a huge problem with a lack of key resources like...
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Karolina Sobieraj mgr inż.
PeopleMSc. Karolina Sobieraj graduated in 2018 in the field of Renewable Energy Sources and Waste Management in the specialization of Waste Management, with a scholarship from the Minister of Science and Higher Education for students for outstanding scientific achievements in the 2017/2018 academic year. From October 2019, she started studies at the UPWr Doctoral School in the discipline of environmental engineering, mining and energy....
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Decentralized energy systems. Social aspects of energy production and use (10h, 2 ECTS credits)
e-Learning CoursesThe main aim of the course is to introduce students to the socio-political aspects of the decentralization of energy systems. The motivation behind these changes is not only due to technological developments or economic issues. The main driving force are wider social and political trends. Many energy supply projects that are being developed and implemented today assume an active role for consumers in energy production, who become...
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Polyethylene glycol-coated solid-phase microextraction fibres for the extraction of polar analytes-A review
PublicationThe article discusses the merits and limitations of commercially available solid-phase microextraction (SPME) fibres and compares them with the new type of extraction coatings, in particular those containing polyethylene glycol as sorbent, as well as the methods of the preparation of the latter. It also analyses their possible application for the extraction of a broad spectrum of analytes, with particular emphasis on the sampling...
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Sequences of internal transcribed spacer 1, 5.8S ribosomal RNA gene and internal transcribed spacer 2 of psychrotolerant pigment-producing yeast-like fungi
Open Research DataDNA encoding ITS1-5.8S-ITS2 fragments of psychrotolerant pigment-producing yeast-like fungi named Red, Pink and Black were PCR amplified using ITS1 5' TCCGTAGGTGAACCTGCGG 3' and ITS4 5’ TCCTCCGCTTATTGATATGC 3’ primers and sequenced by Sanger method using the same primers.
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Successive Iterative Method for Higher-Order Fractional Differential Equations Involving Stieltjes Integral Boundary Conditions
PublicationIn this paper, the existence of positive solutions to fractional differential equations with delayed arguments and Stieltjes integral boundary conditions is discussed. The convergence of successive iterative method of solving such problems is investigated. This allows us to improve some recent works. Some numerical examples illustrate the results.
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Comparing some convolution-based methods for creation of surround sound. W: [CD-ROM] Collected papers. First Pan-American/Iberian Meeting on Acoustics. 144 Meeting of the Acoustical Society of America. III Iberoamerican Cong- ress of Acoustics. 9o Mexican Congress of Acoustics. Cancun, Q. R. Mxico, 2-6 Dec. 2002. [B.m.:ASA]**2002 paper 2pPP22, 7 s. 8 rys. 1 tab. bibliogr. 12 poz. system nagrań dźwięku dookólnego z wykorzystaniem splotu odpowiedzi impul- sowej sali.
PublicationW referacie przedstawiono eksperymenty związane z symulacją dźwięku dookól-nego w sali koncertowej. W tym celu wykorzystano splot odpowiedzi impulsowejz danego wnętrza (wielokanałowe nagrania odpowiedzi impulsowej) z nagraniamiz komory bezechowej. Uzyskany w ten sposób sygnał został następnie przypisa-ny do odpowiednich kanałów w systemie dookólnym. Uzyskane w ten sposób nag-rania były następnie porównywane w testach subiektywnych...
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Multidisciplinary Open System Transferring Knowledge for R2B Development
PublicationDespite many efforts, there is still a serious problem in transferring knowledge from research to business. The problem is especially visible in Poland – the cooperation of R2B is ineffective. We are trying to solve this problem using some IT support. The manuscript presents some solutions developed at the Gdańsk University of Technology. In particular, the platform called “MOST Knowledge” is deeply described. Its layer architecture,...
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Ischaemic cardiomyopathy - Female, 60 - Tissue image [10080730015784761]
Open Research DataThis is the histopathological image of HEART, MEDIASTINUM, AND PLEURA tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Ischaemic cardiomyopathy - Female, 60 - Tissue image [10080730015781351]
Open Research DataThis is the histopathological image of HEART, MEDIASTINUM, AND PLEURA tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Ischaemic cardiomyopathy - Female, 60 - Tissue image [3300730069468871]
Open Research DataThis is the histopathological image of HEART, MEDIASTINUM, AND PLEURA tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Ischaemic cardiomyopathy - Female, 60 - Tissue image [10080730015783421]
Open Research DataThis is the histopathological image of HEART, MEDIASTINUM, AND PLEURA tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Ischaemic cardiomyopathy - Female, 60 - Tissue image [10080730015785291]
Open Research DataThis is the histopathological image of HEART, MEDIASTINUM, AND PLEURA tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Orthogonality relations for the associated Legendre functions of imaginary order
PublicationOrthogonality relations for the associated Legendre functions of imaginary order are derived. They are expressed in terms of the Dirac delta function. The method is based on some known properties of the associated Legendre functions and the Dirac delta distribution. A special case of one of the relations has appeared in some recent applications.
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Demographic Changes in Poland – The Regional Dimension
PublicationThe article notes that the ageing process does not occur uniformly across all Polish regions, i.e. at the same pace and with the same intensity. The results of studies indicating the regions being most vulnerable to the ageing of the regional community and the negative consequences of this process in the next two decades are presented.
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Architects and urban planners in the face of energy transition - smart cities energy aspects in shaping building structures and cities
PublicationContemporary architects and urban planners are facing steadily increasing challenges. The growing problems around environmental issues, shrinking natural resources and climate action are just some of them. Currently, planning should also include balancing with all the aspects of sustainable development such as not only the environmental issues, but also social and economic ones. How to meet them in the era of energy transition...
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Economic situation perception and the growth plans of microenterprises, case of Poland
PublicationNumerous scientific studies provide information on the impact of the environment on the launch, operation and growth of businesses. Reflections on the environment can result from two perspectives: the objective and the subjective one. The first relates to the economic analysis and/or sociological research, whereas the second relies on the perception of the environment by the interested parties themselves. While analysing companies...
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Multi agent grid systems
PublicationThis chapter presents an idea of merging grid and volunteer systemswith multi agent systems. It gives some basics concerning multi agentsystem and the most followed standard. Some deliberations concerningsuch an existing systems were made in order to finally present possibilities of introducing agents into the Comcute system.
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Analysis of volatile oxidation products in rapeseed oil
PublicationCelem pracy było opracowanie metody umożliwiającej określenie stabilności oksydatywnej oleju rzepakowego na podstawie analizy lotnych produktów utleniania lipidów. Na etapie opracowywania metody dobrano optymalne parametry ekstrakcji lotnych analitów techniką SPME. Przeprowadzono również elementy walidacji tej procedury. Zaproponowano też substancje markerowe mogące posłużyć za wyróżniki procesu utleniania lipidów.
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Modeling of performance of an AUV stealth vehicle. Design for operation.
PublicationIn the paper some results of research connected with modelling of performance and risk assessment of an AUV stealth vehicle are presented. A general approach to design of the stealth AUV autonomous underwater vehicle under consideration is introduced. The basic stealth characteristics of the AUV stealth vehicle are briefly described. The method of research is introduced. The AUV stealth vehicle concept is presented including the...
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Modelling of performance of an AUV stealth vehicle. Design for operation.
PublicationIn the paper some results of research connected with modelling of performance and risk assessment of an AUV stealth vehicle are presented. A general approach to design of the stealth AUV autonomous underwater vehicle under consideration is introduced. The basic stealth characteristics of the AUV stealth vehicle are briefly described. The method of research is introduced. The AUV stealth vehicle concept is presented including the...
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High-performance activation of ozone by sonocavitation for BTEX degradation in water
PublicationThis work presents a novel advanced oxidation process (AOP) for degradation of emerging organic pollutants – benzene, toluene, ethylbenzene and xylenes (BTEXs) in water. A comparative study was performed for sonocavitation assisted ozonation under 40–120 kHz and 80–200 kHz dual frequency ultrasounds (DFUS). Based on the obtained results, the combination of 40–120 kHz i.e., low-frequency US (LFDUS) with O3 exhibited excellent oxidation...
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Studies on the formation of formaldehyde during 2-ethylhexyl 4-(dimethylamino)benzoate demethylation in the presence of reactive oxygen and chlorine species
PublicationIn order to protect the skin from UV radiation, personal care products (PCPS) often contain chemical UV-filters. These compounds can enter the environment causing serious consequences on the water ecosystems. The aim of this study was to examine, the effect of different factors, such as UV light, the presence of NaOCl and H2O2 on the formaldehyde formation during popular UV filter, 2-ethylhexyl 4-(dimethylamino)benzoate (ODPABA)...
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Volatile organohalogen compounds in human urine: the effect of environmental exposure
PublicationW pracy przedstawiono wyniki oznaczania lotnych związków chlorowcoorganicznych w próbkach moczu pochodzących m.in. od dawcow narazonych na kancerogeny w miejscu pracy i dawcow spozywajacych wode poddana procesowi uzdatniania przez chlorowanie. Do izolacji i wzbogacania analitów z moczu, posiadającego skomplikowaną matrycę, wykorzystano technikę analizy fazy nadpowierzchniowej nad cienką warstwą cieczy z samoczynną generacją ciekłego...
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Opracowanie metodyki oznaczania pestycydów chloroorganicznych oraz polichlorowanych bifenyli w próbkach żywności pochodzenia morskiego
PublicationW pracy przedstawiono wyniki badań dotyczących możliwości wykorzystania różnych technik ekstrakcji związków chloroorganicznych z próbek żywności. Zaprezentowano podstawy badanych technik, oceniono ich przydatność do izolacji wybranych analitów z grupy pestycydów i polichlorowanych bifenyli z próbek żywności i wytypowano najkorzystniejszą technikę. Przedstawiony został wpływ różnych parametrów ekstrakcji na odzyski analitów. Wyłoniono...
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Mocz ludzki jako źródło informacji na temat narażenia człowieka na różnorodne czynniki chemiczne
PublicationMocz - jest to wydzielina wytwarzana przez nerki w ilości ok. 1500 ml na dobę; płyn zawierający oprócz wody (95%) szkodliwe i zbędne produkty przemiany materii. Mocz jest materiałem biologicznym niezwykle bogatym w niezbędne informacje na temat funkcjonowania organizmu człowieka i efektów narażenia na szkodliwe substancje pochodzące z otaczającego środowiska. Ze względu na swoje właściwości, prosty sposób pobierania próbki, który...
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Effect of alcohol consumption on the levels of volatile organohalogen compounds in blood and urine = Wpływ spożywania alkoholu na poziom lotnych związków chlorowcoorganicznych w krwi i moczu ludzkim
PublicationW pracy przedstawiono wyniki oznaczania lotnych związków chlorowcoorganicznych w próbkach moczu i krwi pochodzących od dawców w różny sposób narażonych na ekspozycje lotnych związków chlorowcoorgnicznych (styl życia: palenie papierosów, picie alkoholu, przyjmowanie lekarstw czy rodzaj wykonywanej pracy). Do izolacji i wzbogacania analitów z próbek moczu i krwi, wykorzystano technikę analizy fazy nadpowierzchniowej nad cienką warstwą...
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On new concepts in computer control of auxiliary gas chromatographic equipment = Nowe koncepcje dotyczące komputerowego sterowania wyposażeniem pomocniczym w chromatografii gazowej
PublicationChromatografia gazowa była pierwszą techniką analityczną poddaną kontroli komputera, jeszcze przed pojawieniem się komputerów osobistych. W związku z niewystarczającą granicą oznaczalności i rozdzielczością, nawet najbardziej najlepszych systemów, technika ta często wiązana jest z etapem wstępnego przygotowania próbki (izolacji i wzbogacania analitów), realizowanych w odrębnych urządzeniach pomocniczych. Bywają one dość złożone...
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The estimation of total volatile organic compounds emissions generated from peroxide cured natural rubber/polycaprolactone blends
PublicationNatural rubber (NR)/polycaprolactone (PCL) blends at the ratio of 90/10% wt. (NR/PCL90/10) and 70/30% wt. (NR/PCL70/30), with a constant amount of dicumyl peroxide, were prepared by compounding in an internal mixer. Obtained NR/PCL bio-based blends were cured at three different temperatures (150 °C, 160 °C and 170 °C). The total content of volatile organic compounds (TVOC) as a function of the NR/PCL blends ratio, and their curing...
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Determination of fuel combustion product in airport runoff water samples using liquid–liquid extraction with gas chromatography–spectrometry
PublicationDetermination of xenobiotics in samples of airport runoff water is both a complex and indispensable task due to an increasing threat resulting from the activities of numerous airports. The aim of this study was to develop, optimize, and validate a procedure based on liquid–liquid extraction (LLE) coupled with gas chromatography–mass spectrometry (GC–MS) for the determination of polycyclic aromatic hydrocarbons (PAHs). So far, no...
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Elicitation strategies for the improvement of essential oil content in Rhododendron tomentosum (Ledum palustre) bioreactor-grown microshoots
PublicationRhododendron tomentosum Harmaja, previously Ledum palustre L., is a fragrant plant growing in swampy areas, which is characterized by well-known repellent properties and the anti-arthritic potential. In the present study, R. tomentosum microshoots cultivated in RITA® bioreactor, providing the alternative, environment-independent source of the valuable essential oil, were treated for 7 days with copper and nickel salts, methyl jasmonate,...
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Dispersive liquid-liquid microextraction combined with gas chromatography–mass spectrometry for in situ determination of biogenic amines in meat: Estimation of meat's freshness
PublicationA dispersive liquid-liquid microextraction (DLLME) gas chromatography–mass spectrometry (GC–MS) technique was developed for the determination of selected biogenic amines (BAs) in samples of poultry, pork and beef. Prior to the extraction process, an appropriate volume of sodium hydroxide solution was added to each of the portioned samples. Next, samples were homogenized, centrifuged and finally sonicated at an increased temperature....
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Feasibility study of a Raman spectroscopic route to drug detection
PublicationWe present an surface-enhanced Raman spectroscopy (SERS) approach for detection of drugs of abuse in whole human blood. We utilize a near infrared laser with 830 nm excitation wavelength in order to reduce the influence of fluorescence on the spectra of blood. However, regular plasmon resonance peak of plasmonic nanoparticles, such as silver or gold fall in a much lower wavelength regime about 400 nm. Therefore, we have shifted...
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Divulging the anti-acetylcholinesterase activity of Colletotrichum lentis strain KU1 extract as sustainable AChE active site inhibitors
PublicationAlzheimer’s disease (AD), also called senile dementia is a neurodegenerative disease seen commonly in the elderly and is characterised by the formation of β-amyloid plaques and neurofbrillary tangles (NFT). Though a complete understanding of the disease is lacking, recent studies showed the role of the enzyme acetylcholinesterase (AChE) in pathogenesis. Finding new lead compounds from natural sources has always been a quest for...
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Capillary gas chromatography using a -cyclodextrin forenantiomeric separation of methylamphetamine, its precursors andchloro intermediates after optimization of the derivatization reaction
PublicationtThe enantiomeric ratio of methylamphetamine (MAMP) is closely related to the optical activity of precur-sors and reagents used for the synthesis and this knowledge can provide useful information concerningthe origins and synthetic methods used for illicit manufacture. The information can be utilized for reg-ulation of the precursors and investigation of the manufacturing sources but this requires analyticalprocedures to determine...
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Investigation of stability of aqueous solutions containing trace amounts of volatile organic analytes
PublicationOznaczając lotne związki chlorowcoorganiczne w matrycy wodnej należy uwzględnić specyficzne właściwości, którymi charakteryzują się te związki, a mianowicie:- niska temperatura wrzenia; - wysoka prężność pary nad roztworem; - stosunkowo niska rozpuszczalność w wodzie.Właściwości te należy uwzględnić w trakcie przygotowania wodnych roztworów wzorcowych wykorzystywanych na etapie kalibracji i badań modelowych. Ze względu na istotność...
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Inteligentne systemy agentowe w systemach zdalnego nauczania
PublicationW pracy omówiono inteligentne systemy agentowe w systemach zdalnego nauczania. Po krótkim przedstawieniu ewolucji systemów zdalnego nauczania i ich wybranych zastosowań, scharakteryzowano inteligentne agenty edukacyjne. Omówiono wykorzystanie programowania genetycznego oraz algorytmów neuro-ewolucyjnych do implementacji oprogramowania tej klasy. Ponadto, nawiązano do modelu Map-Reduce, który efektywnie wspiera architekturę nowoczesnego...
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Sequences of large subunit ribosomal RNA gene, partial sequence encoding D1/D2 domain of psychrotolerant pigment-producing yeast-like fungi
Open Research DataDNA fragments encoding D1/D2 domain of large subunit ribosomal RNA of psychrotolerant pigment-producing yeast-like fungi named Red, Pink and Black were PCR amplified using NL1 5’ GCATATCAATAAGCGGAGGAAAAG 3’ and NL4 5’ GGTCCGTGTTTCAAGACGG 3’ primers and sequenced by Sanger method using the same primers.
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Gas chromatographic determination of volatile aliphatic and selected aromatic amines, without derivatization: solid phase microextraction
PublicationW pracy opisano wykorzystanie techniki chromatografii gazowej do oznaczania śladowych stężeń lotnych amin alifatycznych i wybranych amin aromatycznych w próbkach o różnym składzie matrycy. W tym przypadku aminy nie podlegają procesowi derywatyzacji przed etapem końcowym a na etapie pobierania próbek analitów jest wykorzystana technika mikroekstrakcji do fazy stacjonarnej (SPME).
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Volunteer Computing System Comcute with Smart Scheduler
PublicationIn this paper, a volunteer grid called Comcute is studied. Moreover, the harmony search scheduler is proposed. This scheduler has been designed for efficient using some resources of volunteer grid. The harmony search scheduler optimizes both a workload of a bottleneck computer and the cost of grid. Finally, some experiment outcomes have been discussed.
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A study on of music features derived from audio recordings examples – a quantitative analysis
PublicationThe paper presents a comparative study of music features derived from audio recordings, i.e. the same music pieces but representing different music genres, excerpts performed by different musicians, and songs performed by a musician, whose style evolved over time. Firstly, the origin and the background of the division of music genres were shortly presented. Then, several objective parameters of an audio signal were recalled that...
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Tyre/road noise measurements on ISO tracks according to the UNECE Regulation 117
PublicationWithin the Polish-Norwegian research project ELANORE, a limited Round Robin Test has been performed on 3 ISO tracks in Northern Europe. The basic objective of the project is to improve the EU directive on labelling of tyres for noise and rolling resistance, and this directive is based on the measurement procedures defined in the UN ECE Reg.117. The same test car, test tyres and measurement equipment as well as personnel were used...
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Urban scene semantic segmentation using the U-Net model
PublicationVision-based semantic segmentation of complex urban street scenes is a very important function during autonomous driving (AD), which will become an important technology in industrialized countries in the near future. Today, advanced driver assistance systems (ADAS) improve traffic safety thanks to the application of solutions that enable detecting objects, recognising road signs, segmenting the road, etc. The basis for these functionalities...
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Sample preparation techniques for determination of pesticide residues in food samples
PublicationPesticides are very important in increasing the efficiency and quality of agricultural production. They are applied in many spheres of life, not only in agriculture, and their applications are expanding. Despite their numerous merits, pesticides are some of the most toxic substances contaminating our environment and have a negative impact on the human health. Properties of pesticides such as stability, ability to bioaccumulation...
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Collaborative Delivery by Energy-Sharing Low-Power Mobile Robots
PublicationWe study two variants of delivery problems for mobile robots sharing energy. Each mobile robot can store at any given moment at most two units of energy, and whenever two robots are at the same location, they can transfer energy between each other, respecting the maximum capacity. The robots operate in a simple graph and initially each robot has two units of energy. A single edge traversal by an robot reduces its energy by one...
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Computationally-efficient design optimisation of antennas by accelerated gradient search with sensitivity and design change monitoring
PublicationElectromagnetic (EM) simulation tools are of primary importance in the design of contemporary antennas. The necessity of accurate performance evaluation of complex structures is a reason why the final tuning of antenna dimensions, aimed at improvement of electrical and field characteristics, needs to be based on EM analysis. Design automation is highly desirable and can be achieved by coupling EM solvers with numerical optimisation...
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Non-invasive follicular thyroid neoplasm with papillary-like nuclear features (NIFTP) - Female, 67 - Tissue image [11010630088563951]
Open Research DataThis is the histopathological image of THYROID GLAND tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Non-invasive follicular thyroid neoplasm with papillary-like nuclear features (NIFTP) - Female, 67 - Tissue image [11010630088569751]
Open Research DataThis is the histopathological image of THYROID GLAND tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Non-invasive follicular thyroid neoplasm with papillary-like nuclear features (NIFTP) - Female, 67 - Tissue image [11010630088562471]
Open Research DataThis is the histopathological image of THYROID GLAND tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Non-invasive follicular thyroid neoplasm with papillary-like nuclear features (NIFTP) - Female, 67 - Tissue image [11010630088562991]
Open Research DataThis is the histopathological image of THYROID GLAND tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.