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Wyniki wyszukiwania dla: speech%20synthesis
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Chemical modifications of natural oils and examples of their usage for polyurethane synthesis
PublikacjaNatural oils have been used in the production of plastics for a long time. However, the number of studies dedicated to polyurethane research has shown an increase only recently. Usually, petrochemical components are used in polyurethane synthesis. Nowadays, there have been attemptsmade to replace polyols in polyurethanes with the modified oils and other natural raw materials. It is a promising and important scenario because the...
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Proton Conducting Ceramic Powder Synthesis by a Low Temperature Method
PublikacjaMolten salt synthesis (MSS) is a simple method for the preparation of ceramic powders with specific morphology. The main role of the molten salts is to increase the reaction rate and lower the reaction temperature. It occurs because of much higher mobility of reactants in the liquid medium than in the solid state. In this work the molten salt synthesis was applied to produce ceramic powders of La0995Ca0005NbO4 and BaCe09−xZrxY01O3....
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Unexpected thioketene derivative formation during thioacyl dithiophosphate synthesis.
PublikacjaZbadano zakres i ograniczenia tioacylowania opartego na ditiofosforanach tioacylu. Ditiofosforany tioacylo otrzymano w wyniku reakcji ditiofosforanów acylu z kwasem ditiofosforowym. Obecność dwóch podstawników w pozycji alfa we fragmencie acylowym faworyzowała tworzenie pochodnych tioketenu tym samym obniżając wydajność oczekiwanych ditiofosforanów tioacylu.
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Synthesis of ester derivatives of propylene glycol in the presence of zinc carboxylates.
PublikacjaZbadano wpływ temperatury i stężenia karboksylanów cynku na przebieg estryfikacji glikolu propylenowego kwasami tłuszczowymi. Otrzymano emulgatory, w których maksymalne stężenie monoestru wynosiło 55-57%.
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Cell-penetrating peptides – mechanism of transduction and synthesis – short review
PublikacjaPotential antimicrobial agents may be effective if they are delivered efficiently to their site of action. In many cases, lack of permeability through the cell membrane is the main problem. One of the possible solutions could be a novel intracellular delivery system involving cell-penetrating peptides (CPPs), which may improve the efficiency of many new biophar-maceuticals. Among other things, CPPs are capable of trans-porting...
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Influence of synthesis conditions on zinc oxide nanorode layer morphology
PublikacjaIn recent years one dimensional (1D) nanostructures (nanotubes, nanowires, nanoribbons and nanorods) have been widely studied. Among studied nano-materials, the greatest interest can be seen for zinc oxide (ZnO). However, there is still a need for simple, inexpensive and reproducible fabrication method. In the literature different fabrication methods can be found, most of them requires expensive equipment and involve complex...
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Eigenvalue approach to synthesis of prototype filters with source/load coupling
PublikacjaArtykuł przedstawia nową, szybko zbieżną, technikę syntezy macierzy sprzężeń filtrów o charaktrystyce Czebyszewa. Synteza opiera się na zastosowaniu metody najmniejszych kwadratów w odniesieniu do wartości własnych macierzy sprzężeń oraz jej podmacierzy.
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Synthesis of polyglycerol esters of fatty acid with defined hydrophilic properties
PublikacjaOtrzymane w odrębnej reakcji mieszaniny poligliceroli poddano estryfikacji kwasami tłuszczowymi oktadekanowym i izooktadekanowym, w obecności odpowiednich mydeł sodu powstających in situ. Zaobserwowano wpływ stężenia karboksylanów sodu oraz budowy kwasu tłuszczowego na przebieg estryfikacji mieszaniny polioli. Stwierdzono, że zastosowany sposób prowadzenia reakcji pozwala zsyntetyzować efektywne emulgatory emulsji O/W, o wartościach...
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Multivariate models of inter-resonator couplings for microwave filter synthesis
PublikacjaArtykuł przedstawia technikę budowy modeli częstotliwości rezonansowej, współczynnika sprzężenia między rezonatorami oraz sprzężenia ze źródłem/obciążeniem. Przedstawiony jest model siedmiu zmiennych uwzglęgniający topologię rezonatorów. Na podstawie modelu wykonana została synteza filtrów mikrofalowych.
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The template synthesis and complexation properties of the methoxypyrogal-lo[4]arene
PublikacjaZaprezentowano metodę syntezy templatowej MPA. Obserwowano kompleksowanie silnych akceptorów elektronów przez MPA. Analiza widm ESI-MS wykazała właściwości kompleksujące w stosunku do kationów metali alkalicznych. Właściwości jonoforowe związku badano w membranowych elektrodach jonoselektywnych.
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Synthesis, Antimicrobial and Mutagenic Activity of a New Class of d-Xylopyranosides
PublikacjaEight N-[2-(2′,3′,4′-tri-O-acetyl-α/β-d-xylopyranosyloxy)ethyl]ammonium bromides, a new class of d-xylopyranosides containing a quaternary ammonium aglycone, were obtained. Their complete structure was confirmed using NMR spectroscopy (1H, 13C, COSY and HSQC) and high-resolution mass spectrometry (HRMS). An antimicrobial activity against fungi (Candida albicans, Candida glabrata) and bacteria (Staphylococcus aureus, Escherichia...
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Oxolane Ammonium Salts (Muscarine-Like)—Synthesis and Microbiological Activity
PublikacjaCommercially available 2-deoxy-D-ribose was used to synthesize the appropriate oxolane derivative—(2R,3S)-2-(hydroxymethyl)oxolan-3-ol—by reduction and dehydration/cyclization in an acidic aqueous solution. Its monotosyl derivative, as a result of the quaternization reaction, allowed us to obtain eight new muscarine-type derivatives containing a quaternary nitrogen atom and a hydroxyl group linked to the oxolane ring. Their structure...
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Synthesis of a state feedback controller for an averaging tank with variable filling
PublikacjaIn paper, a nonlinear averaging tank with variable filling is considered. The main purpose of this research work was the modelling and control system synthesis of an averaging tank. The control objectives included ensuring stability and zero steady-state error of the system and achieving settling time as short as possible, while maintaining a minimal overshoot. In order to achieve the intended purpose, firstly a mathematical model...
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Design, synthesis, and biological evaluation of tetrahydroquinolinones and tetrahydroquinolines with anticancer activity
PublikacjaColorectal cancer (CRC) is the most commonly diagnosed cancer in Europe and the United States and the second leading cause of cancer related mortality. A therapeutic strategy used for the treatment of CRC involves targeting the intracellular levels of reactive oxygen species (ROS). In this study, we synthesized a series of novel tetrahydroquinolinones and assessed their ability to inhibit CRC growth and proliferation by evoking...
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Synthesis, physical and chemical properties of polyetherurethanes modified by natural antioxidant
PublikacjaOtrzymano nowe polieterouretany modyfikowane witaminą E. Ten naturalny przeciwutleniacz związany został z makrocząsteczkami w postaci bocznych odgałęzień poprzez wiązanie eterowe lub uretanowe, zależnie od użytego w syntezie jednego z dwóch rodzajów otrzymanych uprzednio monomerów. Polimery scharakteryzowano mierząc wytrzymałość na rozciąganie i twardość oraz absorpcję wody i oleju słonecznikowego. Odporność chemiczną badano oznaczając...
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Synthesis and biological activity of mycophenolic acid-amino acid derivatives
PublikacjaIn search of new immunosuppressants, mycophenolic acid (MPA) was coupled with amino acid methyl esters followed by hydrolysis to analogs bearing free carboxylic groups. The obtained compunds were tested in vitro as growth inhibitors of lymphoid cell line (Jurkat) and human peripheral blood mononuclear cells (PBMC) from healthy donors. According to obtained results recovering of free carboxylic group increased their activity. Additionally,...
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Synthesis and Physicochemical Characteristics of Chitosan-Based Polyurethane Flexible Foams
PublikacjaThe use of shrimp waste to obtain chitosan (Ch) is an essential issue, considering a circular economy, waste management, and its application to environmentally friendly materials. In this study, northern prawn shells were utilized to obtain Ch, which could then be used for synthesizing chitosan-based polyurethane (PUR+Ch) foams with different Ch concentration. The chemical structure, morphology, hardness, thermal properties, viscoelastic...
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Synthesis and Characterization of Poly(zwitterionic) Structures for Energy Conversion and Storage
PublikacjaZwitterions are unique class of molecules that possess two functional groups bearing electric charges, one positive and second negative. This setup results in peculiar properties such as high water retention and anti-fouling capability. Therefore, zwitterionic coatings and gels are commonly applied in e.g. biosensing and bioelectronic devices. Despite those applications, there are other perspectives for zwitterionic materials....
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Au–Si plasmonic platforms: synthesis, structure and FDTD simulations
PublikacjaPlasmonic platforms based on Au nanostructures have been successfully synthesized by directional solidification of a eutectic from Au and the substrate. In order to determine homogeneous shape and space distribution, the influence of annealing conditions and the initial thickness of the Au film on the nanostructures was analyzed. For the surface morphology studies, SEM and AFM measurements were performed. The structure of platforms...
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Synthesis and characterization of novel aliphatic polyurethanes for tissue engineering applications
PublikacjaSummarizing, in this thesis was described the synthesis of novel PUR system, which was obtained by using aliphatic diisocyanate (HDI), amorphous macrodiol (PEBA) and chain extender (BDO). This PUR system was established as suitable for TE purpose and successfully modified with AA, which as expected improved its biocompatibility. According to this, AA-modified HDI-based PURs is the PUR system ready for further studies including...
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Convenient and efficient synthesis of functionalized unsymmetrical Z-alkenyl disulfanes
PublikacjaWe developed a simple and efficient method for the synthesis of functionalized unsymmetrical Z-alkenyl disulfanes under mild conditions in moderate to good yields. The designed method is based on the reaction of Z-alkenyl thiotosylates with thiols in the presence of base. The developed method allows the preparation of unsymmetrical Z-alkenyl disulfanes bearing additional hydroxy, carboxy, or amino functionalities.
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Objective, observer-independent evaluation of myocardial perfusion and function: the role of SPECT
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Surface roughness analysis of hardened steel after high‐speed milling
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Energy conversion in small water plants with variable speed PM generator
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Small Hydropower Plant With Integrated Turbine-Generators Working at Variable Speed
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Speed sensorless nonlinear control of induction motor in the field weakening region
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ANALYSIS OF THE POSSIBILITIES OF HIGH SPEED SHAFT BEARING SYSTEM DURABILITY INCREASE
PublikacjaDuring the operation of wind turbines with a gearbox of traditional configuration, a high failure rate of high-speed shaft bearings is observed. Such a high failures frequency is not reflected in standard bearing durability calculation methods, which can be attributed to atypical failure mechanism. To avoid observed problems in the 1.5 MW wind turbine, the modification of the existing bearing system is proposed. Multiple options,...
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Effect of FSW Traverse Speed on Mechanical Properties of Copper Plate Joints
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Speed management on local government managed roads – research, recommendations and guidelines
PublikacjaCommissioned by the National Road Safety Council Secretariat, the project “Guidelines for speed management on local government managed roads” studied car driver be haviour when subjected to selected speed management measures such a local speed restrictions, surveillance, traffic calming and restricted speed areas. In addition, analyses were conducted on the impact of selected me asures...
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Measurements of High-Speed Data Transmission Radio Link for Special Applications
PublikacjaIn the article measurements of high-speed data transmission radio link for special applications were presented. Build measurement stand, measurement scenario and obtained results were briefly described. All conducted research work took place in real maritime environment.
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Speed sensorless induction motor drive with motor choke and predictive control
PublikacjaArtykuł przedstawia układ napędowy z silnikiem indukcyjnym, zasilanym z falownika napięcia przy zastosowaniu filtru silnikowego. System pracuje bez czujnika prędkości obrotowej. Głównym aspektem pracy jest zwrócenie uwagi na to, że zastosowanie dławika silnikowego wymaga odpowiednich zmian w strukturach sterowania i estymacji zmiennych. Zaproponowano odpowiednie rozwiązanie dla układu napędowego z regulatorem predykcyjnym prądu....
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Mechatronic design for the high speed milling surveillance of the complex and flexible details
PublikacjaW pracy przedstawiono mechatroniczny system tworzenia mapy optymalnych prędkości obrotowych wrzeciona. W trakcie frezowania szybkościowego przedmiotów podatnych mogą wystąpić drgania samowzbudne typu chatter. Używana zazwyczaj procedura ustawiania wymaganej prędkości obrotowej wrzeciona metodą prób i błędów, w wielu przypadkach nie jest zalecana. Przedstawiona procedura nadzorowania może doprowadzić do uniknięcia ryzyka wystąpienia...
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Speed sensorless asynchronous motor drive with inverter output lc filter
PublikacjaIn this paper a speed sensorless ac drive with inverter and output LC filter is proposed. A nonlinear, decoupled field oriented control algorithm with a flux and speed close-loop observer is used. In spite of using LC filter on the inverter output, the sensorless system works precisely. That result are obtained as a result of the appropriate estimation and control system use. The theory, simulation, and experimental results are...
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Applying artificial neural networks for modelling ship speed and fuel consumption
PublikacjaThis paper deals with modelling ship speed and fuel consumption using artificial neural network (ANN) techniques. These tools allowed us to develop ANN models that can be used for predicting both the fuel consumption and the travel time to the destination for commanded outputs (the ship driveline shaft speed and the propeller pitch) selected by the ship operator. In these cases, due to variable environmental conditions, making...
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The Method of Finding the Optimal Spindle Speed When Milling Flexible Details
PublikacjaThe paper presents a new method of vibration reduction during milling of flexible details. The method consists in selecting the optimal spindle speed, based on the natural frequency of the workpiece. For this purpose, an original method was created, which is based on minimizing the work of cutting forces in the direction of the depth of cutting. The effectiveness of the method has been proved by comparing the RMS values of vibration...
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Synchronized six-step voltage generation in high-speed PMSM drive
PublikacjaSynchronized voltage generation has already been considered in the context of pulse width modulation (PWM). References prove that synchronized PWM substantially decreases subharmonics in inverter output voltage when operating with low switching-to-fundamental frequency ratio. This paper identifies problems of unsynchronized voltage generation in electric drives under six-step inverter operation. Guidelines for the synchronization...
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The contactless method of chip-to-chip high-speed data transmission monitoring
PublikacjaThis paper presents a technique of decoupling differential signals transmitted in a pair of microstrip lines on a printed circuit board (PCB), using dedicated coupler for high speed data transmission monitoring in chip-to-chip interconnections. The coupler used for signal probing is overlayed on the pair of microstrip lines under test, and provides a signal to the next blocks of the measurement system without disturbing transmission...
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High speed milling vibration surveillance using modal model of the tool
PublikacjaPraca poświęcona jest nadzorowaniu drgań wirujących narzędzi w nowoczesnych frezarkach. Przedmiotem rozważań jest proces frezowania szybkościowego smukłym frezem kulistym na 5-osiowym centrum obróbkowym Deckel Maho DMU 50eVolution. Frezowanie smukłymi narzędziami jest często stosowane w przypadku nowoczesnych centrów obróbkowych. Uzasadnienie technologiczne wynika z konieczności dokładnego wykonywania złożonych kształtów geometrycznych...
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Innovative optimization algorithm of variable speed pumps in district heating systems.
PublikacjaW referacie przedstawiono innowacyjny algorytm matematyczny optymalizacji pracy pomp zmienno prędkościowych w systemach ciepłowniczych. Algorytm wykorzystuje procedurę iterecyjnego wyznaczania parametrów pracy pomp, których charakterystyki są linearyzowane odcinkami w układzie dwóch współrzędnych. Do rozwiązania modelu całkowitoliczbowego zaproponowano wykorzystanie systemu GAMS. W pracy przedstawiono podstawy metodologiczne i...
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A New Coupler Concept for Contactless High-Speed Data Transmission Monitoring
PublikacjaThis paper presents a new concept of a couplerthat can be applied to high-speed data transmission contactlessmeasurements. The proposed approach is dedicated for differentialsignal transmission monitoring in microstrip coupled lineson printed circuit boards (PCBs). The coupler, produced on aseparate PCB, is overlayed on the transmission line with thedifferential signal and delivers decoupled differential signal tothe main measurement...
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Induction motor control application in high-speed train electric drive
PublikacjaThe chapter presents an application of induction motor mechanical speed and load torque observers in high-speed train drives. The observers are applied for a 1.2-MW electric drive with an induction motor. The goal of using such observers is to utilize computed variables for diagnostic purposes of speed sensors and torque transmission system. The concept of diagnostic system is presented in this paper, and proper criteria are proposed....
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The Effect of Steaming Beech, Birch and Maple Woods on Qualitative Indicators of the Surface
PublikacjaThis work presents the effect of steaming beech, birch and maple woods on the resulting quality of the milled wood surface. The steaming process of the studied woods results in a targeted change in the color of the wood, which changes from the original light white-gray color to fine reddishbrown to dark brown color shades that are more or less saturated depending on the temperature of the saturated water steam. The color changes...
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The effect of thermal modification on the quality of the milled surface of beech and pine wood
PublikacjaThe article deals with the effect of thermal modification on the quality of the created surface during milling on CNC milling cutters. The quality of the created surface is evaluated based on surface roughness, specifically its roughness parameter Ra. The observed surface is created by a shank cutter with a diameter of 20 mm and three cutting edges in a spiral at a standard speed of 18,000. min-1. The article compares thermally...
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Analysis of Vibration and Acoustic Signals for Noncontact Measurement of Engine Rotation Speed
PublikacjaThe non-contact measurement of engine speed can be realized by analyzing engine vibration frequency. However, the vibration signal is distorted by harmonics and noise in the measurement. This paper presents a novel method for the measurement of engine rotation speed by using the cross-correlation of vibration and acoustic signals. This method can enhance the same frequency components in engine vibration and acoustic signal. After...
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Sensorless low speed PMSM motor control with cogging torque compensation
PublikacjaThe paper presents sensorless control of a low speed permanent magnet synchronous machine with use of modified state observer. An overview of the PMSM motor used in the research setup was presented. The problem of drive torque ripple, resulting mainly from the occurrence of a significant cogging torque, was discussed. A solution compensating the torque ripple of the PMSM motor was proposed. A start-up procedure of the speed control...
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A mobile loop order–disorder transition modulates the speed of chaperonin cycling
PublikacjaMolecular machines order and disorder polypeptides as they form and dissolve large intermolecular interfaces, but the biological significance of coupled ordering and binding has been established in few, if any, macromolecular systems. The ordering and binding of GroES co-chaperonin mobile loops accompany an ATP-dependent conformational change in the GroEL chaperonin that promotes client protein folding. Following ATP hydrolysis,...
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Non-Adaptive Speed and Position Observer of Doubly-Fed Induction Generator
PublikacjaThe non-adaptive speed and position estimation of a doubly-fed induction generator (DFIG) is presented in this paper. The speed observer is based on the mathematical model of DFIG and to stabilize the structure the Lyapunov method is used. The classic stator field-oriented control to active and reactive power control is used in the sensorless control system. The performance of the proposed algorithm of a speed observer is validated...
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Analysis of Failures of High Speed Shaft Bearing System in a Wind Turbine
PublikacjaDuring the operation of wind turbines with gearbox of traditional configuration, consisting of one planetary stage and two helical stages high failure rate of high speed shaft bearings is observed. Such a high failures frequency is not reflected in the results of standard calculations of bearing durability. Most probably it can be attributed to atypical failure mechanism. The authors studied problems in 1.5 MW wind turbines of...
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High-Speed Serial Embedded Deterministic Test for System-on-Chip Designs
PublikacjaThe paper presents a high-speed serial interface between external tester and Embedded Deterministic Test (EDT) compression logic hosted by SoC designs. With only a single bidirectional link, the system is capable of feeding distributed heterogeneous cores with hundreds of test channels. Moreover, it synergistically supports EDT bandwidth management to improve the overall test performance. A detailed study indicates a high potential...
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WYKORZYSTANIE SIECI NEURONOWYCH DO SYNTEZY MOWY WYRAŻAJĄCEJ EMOCJE
PublikacjaW niniejszym artykule przedstawiono analizę rozwiązań do rozpoznawania emocji opartych na mowie i możliwości ich wykorzystania w syntezie mowy z emocjami, wykorzystując do tego celu sieci neuronowe. Przedstawiono aktualne rozwiązania dotyczące rozpoznawania emocji w mowie i metod syntezy mowy za pomocą sieci neuronowych. Obecnie obserwuje się znaczny wzrost zainteresowania i wykorzystania uczenia głębokiego w aplikacjach związanych...