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Search results for: P-TYPE METAL OXIDE SENSOR,LIGHT-ASSISTED GAS SENSING,IN-SITU FTIR SPECTROSCOPY,NANOPOROUS NIO,GAS SENSING
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Evaluation of pitting corrosion by means of dynamic electrochemical impedance spectroscopy
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Promotion of borophene/NiO-based electrocatalyst for oxygen evolution reaction
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Promotion of borophene/NiO-based electrocatalyst for oxygen evolution reaction
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Microwave-assisted synthesis of a TiO2-CuO heterojunction with enhanced photocatalytic activity against tetracycline
PublicationA microwave method was used for the synthesis of TiO2-CuO oxide systems. A detailed investigation was made of the effect of the molar ratio of components (TiO2:CuO=9:1, 7:3, 5:5, 3:7, 1:9) on the crystalline structure and morphology. Transmission electron microscopy (TEM) confirmed the presence of octahedral and rod-shaped titania particles and sheet copper(II) oxide particles; moreover, HRTEM analysis indicated the presence of...
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LaNi1-xCoxO3-δ(x=0.4 to 0.7) cathodes for solid oxide fuel cells by infiltration
PublicationPerformance of LaNi 1-x Co x O 3−δ (LNC) (x=0.4 to 0.7) as a cathode in solid oxide fuel cell (SOFC) is evaluated. Symmetrical cathode/electrolyte/cathode cells for electrochemical testing are prepared by infiltration of yttria stabilized zirconia (YSZ) backbone with LNC solutions. It is showed that the cathode infiltrated with LaNi 0.5 Co 0.5 O 3−δ (LNC155) has the lowest polarization resistance and activation energy, 197 mΩ cm...
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Nowoczesne metody termochemicznej konwersji biomasy w paliwa gazowe, ciekłe i stałe = Modern methods of thermochemical biomass conversion into gas, liquid and solid fuels
PublicationBiomass utilization through direct- or co-combustion with coal, based on coal, hydrogen and oxygen compounds chemical energy conversion into heat in boilers, is simultaneously the cheapest and - according to experts - economically least effective solution. In case of heat and electricity production in cogeneration process in biomass fueled heat and power stations (wood, straw, energetic plants, RDF etc), investment costs are little...
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Position of LiF:Mg,Cu,P TL peak as an alternative method for ultra-high-dose dosimetry
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Suppression of distortions in signals received from Doppler sensor for vehicle speed measurement
PublicationDoppler sensors are commonly used for movement detection and speed measurement. However, electromagnetic interference and imperfections in sensor construction result in degradation of the signal to noise ratio. As a result, detection of signals reflected from moving objects becomes problematic. The paper proposes an algorithm for reduction of distortions and noise in the signal received from a simple, dual-channel type of a Doppler...
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On the possible increasing of efficiency of ship power plant with the system combined of marine diesel engine, gas turbine and steam turbine in case of main engine cooperation with the gas turbine fed in parallel and the steam turbine
PublicationW pracy przedstawiono koncepcję układu kombinowanego okrętowego dużej mocy złożonego z wiodącego silnika głównego spalinowego silnika tłokowego i skojarzonych z nim turbiny gazowej mocy i układu turbiny parowej, wykorzystujących energię zawartą w spalinach wylotowych głównego silnika spalinowego. Rozpatrzono wariant układu kombinowanego, w którym główny jest silnik tłokowy skojarzony z turbiną gazową mocy i układem turbiny parowej,...
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On the possible increasing of efficiency of ship power plant with the system combined of marine diesel engine, gas turbine and steam turbine in case of main engine cooperation with the gas turbine fed in series and the steam turbine
PublicationW pracy przedstawiono koncepcję układu kombinowanego okrętowego dużej mocy złożonego z wiodącego silnika głównego silnika spalinowego tłokowego oraz skojarzonych z nim turbiny gazowej mocy i układu turbiny parowej, wykorzystujących energię zawartą w spalinach wylotowych silnika spalinowego. Rozpatrywano wariant układu kombinowanego, którym turbina mocy jest zasilana szeregowo spalinami wylotowymi. Podano algorytm i obliczenia...
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Dielectric Spectroscopy Studies and Modelling of Piezoelectric Properties of Multiferroic Ceramics
PublicationCompounds and solid solutions of bismuth ferrite (BiFeO3)—barium titanate (BaTiO3) system are of great scientific and engineering interest as multiferroic and potential high-temperature lead-free piezoelectric materials. In the present paper, the results of research on the synthesis and characterisation of 0.67Bi1.02FeO3–0.33BaTiO3 (67BFBT) ceramics in terms of crystal structure and dielectric and piezoelectric properties are reported....
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Influence of Two-Stage Anodization on Properties of the Oxide Coatings on the Ti–13Nb–13Zr Alloy
PublicationThe increasing demand for titanium and its alloys used for implants results in need of such innovative surface treatment that may jointly increase corrosion resistance and biocompatibility, and demonstrate antibacterial protection at no cytotoxicity. The purpose of this research was to characterize the effect of two-stage anodization, performed for 30 min in phosphoric acid, at the presence of hydrofluoric acid in the second stage....
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Characterization of Bioactivity of Selective Molecules in Fruit Wines by FTIR and NMR Spectroscopies, Fluorescence and Docking Calculations
PublicationFourier transform infrared (FTIR) and proton nuclear magnetic resonance (1H NMR) spectroscopies were applied to characterize and compare the chemical shifts in the polyphenols’ regions of some fruit wines. The obtained results showed that FTIR spectra (1800–900 cm−1) and 1H NMR (δ 6.5–9.3 ppm) of different fruit wines can be used as main indices of the year of vintage and quality of fruit wines. In addition to the classical determination...
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Endometrial nitric oxide production and nitric oxide synthases in the equine endometrium: Relationship with microvascular density during the estrus cycle
PublicationNitric oxide (NO) plays an important role in angiogenesis and in the regulation of the blood flow. This study was carried out to investigate (i) the effects of endogenous estrogens and progestins and exogenous progesterone (P(4)) (5 ng/ml or 1 microg/ml) or estradiol 17beta (E(2)beta) (50 pg/ml or 1 microg/ml) on in vitro endometrial NO synthesis; (ii) the presence of different isoforms of NO synthase;...
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ZnO ALD-Coated Microsphere-Based Sensors for Temperature Measurements
PublicationIn this paper, the application of a microsphere-based fiber-optic sensor with a 200 nm zinc oxide (ZnO) coating, deposited by the Atomic Layer Deposition (ALD) method, for temperature measurements between 100 and 300°C, is presented. The main advantage of integrating a fiber-optic microsphere with a sensing device is the possibility of monitoring the integrity of the sensor head in real-time, which allows for higher accuracy during...
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An Impact Analysis of Artificial Light at Night (ALAN) on Bats. A Case Study of the Historic Monument and Natura 2000 Wisłoujście Fortress in Gdansk, Poland
PublicationThe artificial light at night (ALAN) present in many cities and towns has a negative impact on numerous organisms that live alongside humans, including bats. Therefore, we investigated if the artificial illumination of the historic Wisłoujście Fortress in Gdańsk, Poland (part of the Natura 2000 network), during nighttime events, which included an outdoor electronic dance music (EDM) festival, might be responsible for increased...
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Enhanced trap-assisted recombination in organic semiconductors
PublicationAn analytical model to describe the interaction of excitons and charge transfer states with deep traps is formulated for the case of molecular materials. Here, we have considered the influence of a trap-assisted recombination on this phenomenon. The final expression for the effective recombination rate has been derived from the Shockley–Read–Hall theory and kinetic equations which characterize different photophysical processes....
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Real-time isothermal DNA amplification monitoring in picoliter volumes using an optical fiber sensor
PublicationRolling circle amplification (RCA) of DNA can be considered as a great alternative to the gold standard polymerase chain reaction (PCR), especially during this pandemic period, where rapid, sensitive, and reliable test results for hundreds of thousands of samples are required daily. This work presents the first research to date on direct, real-time and label-free isothermal DNA amplification monitoring using a microcavity in-line...
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ChemInform Abstract: Modern Methods of Thermochemical Biomass Conversion into Gas, Liquid and Solid Fuels
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Multidimensional Gas Chromatography in Essential Oil Analysis. Part 2: Application to Characterisation and Identification
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Comprehensive two-dimensional gas chromatography-mass spectrometry: Recent evolution and current trends
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Essential-Oil Analysis of Irradiated Spices by Using Comprehensive Two-Dimensional Gas Chromatography
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Analysis of essential oils through comprehensive two-dimensional gas chromatography: General utility
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Headspace Liquid-Phase Microextraction of Chlorobenzenes in Soil with Gas Chromatography-Electron Capture Detection
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Trust in the source of received information as a factor related to public perception of shale gas drilling
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Review of Small Gas Turbine Engines and Their Adaptation for Automotive Waste Heat Recovery Systems
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Piecewise continuous distribution function method: Fluid equations and wave disturbances at stratified gas
PublicationUkład równań typu hydrodynamicznego dla warstwowych gazów w polu grawitacyjnym pochodzi od równania BGK metodą częściowej ciągłej funkcji dystrybucji. Otrzymany system równań uogólnia układ Naviera-Stokesa w dowolnych liczbach Knudsena. Rozwiązania WBK dla ultradźwięku wprowadza się w przypadku stratyfikacji exponecjalnej.
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A simple gas chromatograph for educational purposes = Prosty chromatograf gazowy do celów dydaktycznych
PublicationOpisano prosty chromatograf gazowy zaprojektowany specjalny do celów dydaktycznych, oraz serię doświadczeń laboratoryjnych z wykorzystaniem tego instrumentu w celu nauczania podstaw chromatografii studentów chemii analitycznej.
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Inert gas condensation made bimetallic FeCu nanoparticles - plasmonic response and magnetic ordering
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Determination of volatile organic compounds using solventless sample preparation techniques and gas chromatography
PublicationIn this paper the latest advances in the determination of volatile organic compounds using solvent-free extraction techniques in the sample preparation step are presented. A paper is focus mainly on one of the most popular sample preparation technique: solid-phase microextraction technique (SPME) combined with different detection systems and its applications to sampling of VOCs from the samples with different matrices. This paper...
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Radioisotope measurement of selected parameters of liquid-gas flow using single detector system
PublicationTo determine the parameters of two-phase flows using radioisotopes, usually two detectors are used. Knowing the distance between them, the velocity of the dispersed phase is calculated based on time delay estimation. Such a measurement system requires the use of two gamma-ray sealed sources. But in some situations it is also possible to determine velocity of dispersed phase using only one scintillation probe and one gamma-ray source....
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Application of static headspace gas chromatography for routine analysis of VFAs in cattle farm wastewater
PublicationOznaczanie lotnych kwasów tłuszczowych w próbkach środowiskowych jest tematem coraz powszechniej analizowanym z uwagi na ich uciążliwość w środowisku. Celem pracy było wykorzystanie techniki statycznej analizy headspace (HS) w połączeniu z analizą chromatograficzną do oznaczania lotnych kwasów monokarboksylowych w wodnych próbkach środowiskowych pochodzących z hodowli bydła.
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Furan Fragmentation in the Gas Phase: New Insights from Statistical and Molecular Dynamics Calculations
PublicationWe present a complete exploration of the different fragmentation mechanisms of furan (C4H4O) operating at low and high energies. Three different theoretical approaches are combined to determine the structure of all possible reaction intermediates, many of them not described in previous studies, and a large number of pathways involving three types of fundamental elementary mechanisms: isomerization, fragmentation, and H/H2 loss...
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Influence of ethylene glycol on CaCO3 particles formation via carbonation in the gas-slurry system
PublicationStrącanie węgalnu wapnia przebiegało w układzie gaz-zawiesina w reakcji wodorotlenku wapnia z dwutlenkiem węgla. Proces precypitacji był prowadzony w obecności glikolu etylenowego. Użyty dodatek organiczny zmieniał lepkość mieszaniny reakcyjnej oraz rozpuszczalność dwutlenku węgla i węgalnu wapnia, co miało wpływ na warunki precypitacji CaCO3. Wzrost stężnia glikolu etylenowego w mieszaninie reakcyjnej powodował większe zużycie...
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Determination of solvents residues in vegetable oils and pharmaceuticals by headspace analysis and capillary gas chromatography.
PublicationPrzedstawiono wyniki zastosowania techniki analizy fazy nadpowierzchniowej w połączeniu z kapilarną chromatografią gazową do oznaczania wybranych rozpuszczalników organicznych w próbkach olejów jadalnych i produktów farmaceutycznych. Oznaczane rozpuszczalniki to: benzen, toluen, heksan oraz chlorowcopochodne węglowodorów alifatycznych. Opracowaną procedurę poddano walidacji. Wyznaczono granicę wytrzymalności, oznaczalności, liniowość...
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Development and evaluation of headspace gas chromatography method for the analysis of carbonyl compounds in spirits and vodkas
PublicationPrzedstawiono wyniki oznaczania związków karbonylowych (po przeprowadzeniu w pochodne przy użyciu odczynnika derywatyzującego - o-PFBHA) przy wykorzystaniu techniki analizy fazy nadpowierzchniowej w połączeniu z chromatografią gazową i detektorem wychwytu elektronów(ECD). Przedstawiono optymalizację metodyki oraz wyniki uzyskane podczas próbek rzeczywistych wybranych wyrobów spirytusowych.
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Problem of proper decomposition and initialization of acoustic and entropy modes in a gas affected by the mass force
PublicationThe relations connecting perturbations specific for acoustic and entropy modes in an accelerated fluid or in a fluid affected by constant mass force, are derived. They allow to decompose the total vector of perturbations and the overall energy into acoustic and non-acoustic parts uniquely at any instant. In order to do this, three quantities are required, for example total perturbations in entropy, pressure and velocity. The evaluations...
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Evaluation of the usefulness and optimization of the separation conditions in Empty Column Gas Chromatography (EC-GC)
PublicationDotychczasowe badania wykazały, że możliwe jest rozdzielanie wysokowrzących mieszanin techniką chromatografii gazowej z zastosowaniem pustej rurki kapilarnej z topionej krzemionki, zamiast kolumn zawierających fazę stacjonarną. Operacja rozdzielania chromatograficznego ma miejsce jedynie na zasadzie różnicy temperatur wrzenia rozdzielanych substancji. Wysoki stopień podobieństwa warunków rozdzielania, osiąganych w ten sposób, z...
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Reliability of flue gas desulphurisation installations - the essential condition of efficient air pollution control
PublicationW celu minimalizacji niekorzystnego wpływu SO2 i SO3 na środowisko naturalne w wielu instalacjach skrubery odsiarczające gaz spalinowy (FGD) stosowane są do usuwania tlenków siarki z gazów wylotowych. Ostre warunki pracy skruberów i dodatkowego osprzętu powodują problemy korozyjne w powszechnie stosowanych materiałach konstrukcyjnych a awarie wywierają długookresowy wpływ na środowisko. Opisano najnowsze doświadczenia związane...
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Signals features extraction in radioisotope liquid-gas flow measurements using wavelet analysis
PublicationKnowledge of the structure of a flow is significant for the proper conduct of a number of industrial processes. In this case, a description of a two-phase flow regimes is possible by use of the time-series analysis in time, frequency and state-space domain. In this article the Discrete Wavelet Transform (DWT) is applied for analysis of signals obtained for water-air flow using gamma ray absorption. The presented method was illustrated...
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Magnetoacoustic Heating of Plasma Caused by Periodic MagnetosoundPerturbations with Discontinuities in a Quasi-Isentropic Magnetic Gas
PublicationThe magnetoacoustic heating of plasma by harmonic or periodic saw-tooth perturbations at a trans-ducer is theoretically studied. The planar fast and slow magnetosound waves are considered. The wavevector may form an arbitrary angleθwith the equilibrium straight magnetic field. In view of variableθand plasma-β, the description of magnetosound perturbations and appropriate magnetosound heatingis fairly difficult. The scenario of...
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High temperature air/steam gasification of biomass in view of hydrogen rich gas production.
PublicationArtykuł przedstawia opis nowej i zaawansowanej metody konwersji termochemicznej biomasy i miejskich odpadów stałych w paliwo gazowe, bogate w wodór. W porównaniu z tradycyjnym procesem gazyfikacji, w metodzie tej wykorzystuje się powietrze/parę wodną przegrzane do wysokiej temperatury (powyżej 1300 st. C). Przegrzanie powietrza lub pary wodnej odbywa się z zastosowaniem ceramicznego przegrzewacza wysokotemperaturowego. W celu...
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Hydrogen rich gas production from high temperature air/steam gasification of biomass
PublicationW pracy przedstawiono nowoczesną technikę konwersji biomasy oraz stałych odpadów komunalnych w celu produkcji paliwa gazowego bogatego w wodór. Opisany proces gazyfikacji przebiega w wysokiej temperaturze przy obniżonej koncentracji tlenu i udziale pary wodnej. Dzięki temu możliwa jest produkcja gazów palnych, w szczególności H2, który można wykorzystać do produkcji energii elektrycznej i cieplnej.
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Miniaturized passive emission test chamber for in-situ measurement of emissions of organic compounds
PublicationThe results of many different studies have demonstrated unequivocally that the quality of indoor air is often much worse than that of atmospheric air (outdoor). One of the main groups of chemical compounds present in indoor air, with proven harmfulness to health,are volatile organic compounds (VOCs). VOCs present indoor comprise a wide variety of hydrocarbons and hydrocarbons derivatives including aliphatic, aromatics, alkylbenzens,...
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THE ROLE OF THIN FUNCTIONAL LAYERS IN SOLID OXIDE FUEL CELLS
PublicationWidespread commercialization of solid oxide fuel cells requires lowering its cost. It is generally accepted that to lower the cost of solid oxide fuel cells it is necessary to use metal alloys as interconnectors and, consequently, lower its operating temperature to slow down interconnectors degradation. As a result the area specific resistance of the cathodes should be lowered to sustain the performance of the cells. In order to...
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Direct-Ultrasonic Assisted Microextraction Coupled with RTL-GC-FID/GC-MS as a Future Standard Procedure for Monitoring 26 potentially Allergenic Fragrances in Water Samples
PublicationThis research topic grew up as a result of awareness of constant anthropogenic and natural input to the environment constituents of personal care products (PCPs) residues. This group of emerging pollutants encompasses a wide range of chemicals, including potentially allergenic fragrance compounds. The aim of the present study was to investigate presence of 26 fragrance allergens in water samples. Simple and rapid methodology based...
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Visible light-induced photocatalytic reaction of gold-modified titanium(IV) oxide particles: action spectrum analysis
PublicationAnalizy spektrum działania wykazały, ze wzbudzenie powierzchniowego plazmonu złota inicjuje utlenianie 2-propanolu w świetle widzialnym w napowietrzonej zawiesinie tlenku(IV) tytanu zmodyfikowanego zlotem. Badania przeprowadzone z użyciem światła polichromatycznego wykazały, ze szybkość reakcji foto-utleniania zależy od właściwości tlenku(IV) tytanu, takich jak rozmiar ziaren, pola powierzchni właściwej, formy krystalicznej (anataz...
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Determination of parent and methylated polycyclic aromatic hydrocarbons in water samples by dispersive liquid–liquid microextraction–two dimensional gas chromatography–time-of-flight mass spectrometry
PublicationPolycyclic aromatic hydrocarbons (PAHs) are contaminants frequently found in environmental waters. Owing to their toxic effects, it is important to develop analytical methodologies that allow their fast and reliable determination. Dispersive liquid–liquid microextraction (DLLME) allows a quick extraction of analytes with little organic solvent consumption. The best results regarding sample preparation are obtained when 40 mL of...
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Analysis of Properties of an Active Linear Gesture Sensor
PublicationBasic gesture sensors can play a significant role as input units in mobile smart devices. However, they have to handle a wide variety of gestures while preserving the advantages of basic sensors. In this paper a user-determined approach to the design of a sparse optical gesture sensor is proposed. The statistical research on a study group of individuals includes the measurement of user-related parameters like the speed of a performed...
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Application of NIR and Raman Spectroscopy in Biotechnology
PublicationStudium Press LLC, U.S.A.