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Search results for: COPPER(II) COMPLEXES
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Experimental Investigations on the Influence of Coil Arrangement on Melting/Solidification Processes
PublicationThe latent heat thermal energy storage units are very popular because of their high energy density and almost close to constant temperature during the charging/discharging. In the present study has been proposed new shell-and-coil geometry with a shifted coil position to enhance the performance of phase change thermal magazine. The experimental investigations have been performed both for the melting and solidification process of...
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Effect of Ion and Binding Site on the Conformation of Chosen Glycosaminoglycans at the Albumin Surface
PublicationAlbumin is one of the major components of synovial fluid. Due to its negative surface charge, it plays an essential role in many physiological processes, including the ability to form molecular complexes. In addition, glycosaminoglycans such as hyaluronic acid and chondroitin sulfate are crucial components of synovial fluid involved in the boundary lubrication regime. This study presents the influence of Na+, Mg2+ and Ca2+ ions...
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Ab initio chemical kinetics of Isopropyl acetate oxidation with OH radicals
PublicationGlobal reactivity descriptors of isopropyl acetate (IPA) and thermo-kinetic aspects of its oxidation via OH radicals have been studied. Transition state theory (TST) was utilized to estimate the bimolecular rate constants. Ten oxidation pathways have been investigated, and all of them are exothermic. The potential energy diagram has been sketched using different pre- and post-reactive complexes for all reaction pathways. Rate coefficient...
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Smart Weighing Scale with Feet-Sampled ECG
PublicationIn a smart home, health and well-being monitoring systems could be embedded in everyday devices providing a pervasive care. A home bathroom scale is an example of such a device, typically used to measure body weight and very often its composition (e.g. body water/fat percentage). In this paper, we analyzed a potential use of the bathroom scale to measure electrocardiogram (ECG) from electrodes located on the scale's tile. In particular...
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Możliwości sterowania kinetyką wydzielania z roztworu pojedynczych jonów w procesie jednoczesnej flotacji kilku jonów metali
PublicationZbadano wpływ pH surówki flotacyjnej, stężenia kolektora i prędkości przepływu powietrza na przebieg flotacji jonowej i precypitacyjnej mieszaniny Al(III), Cu(II) i Zn(II). Najwyższe wartości stałych szybkości flotacji badanych metali uzyskano dla procesów prowadzonych dla pH około 8, tj. w warunkach flotacji precypitacyjnej. Wykazano, że stałe szybkości flotacji badanych metali są proporcjonalne do prędkości przepływu powietrza flotującego...
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Anonymity Architecture for Mobile Agent Systems
PublicationThe paper presents a new security architecture for MAS, which supports anonymity of agent owners. The architecture is composed of two main elements: Module I: Untraceability Protocol Infrastructure and Module II: Additional Untraceability Support. Module I is based on the recently proposed untraceability protocol for MAS and it forms the core of the anonymity architecture, which can be supported by the ele- ments of the second...
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Near Field Coupled Wireless Microwave Sensor
PublicationThis paper presents a wireless planar microwave sensor operating at industrial scientific and medical (ISM) frequency for the detection of dielectric materials. The microwave sensor consists of a reader (ground defected microstrip coupled line) and a passive tag where a complementary split-ring resonator (CSRR) is made on the commercially available copper-foil. The CSRR is a peel-off type tag that is excited using the near field...
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Czynniki kształtujące strukturę modalną wypadków w transporcie
PublicationArtykuł jest podrozdziałem rozdziału 8 (problemy bezpieczeństwa wielomodalnego transportu osób i towarów) tomu II monografii ZSBT
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Zielony pomnik
PublicationArtykuł przedstawia założenia, projekt i realizację symbolicznego zielonego pomnika Jana Pawła II w Gdańsku na Zaspie.
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Chińczycy w Gdańsku
PublicationPrzedstawiono sylwetki trzech Chińczyków, którzy przed II wojną światową uzyskali dyplomy inżyniera niemieckiej politechniki w Gdańsku.
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Induction of chirality in 4,4'-azopyridine by halogen-bonding interaction with optically active ditopic donors
PublicationOptically active ditopic halogen bond donors bearing two 4-iodotetrafluorophenyl groups were obtained by reaction of chiral diols with iodopentafluorobenzene. Co-crystallization of these donors with anti-4,4′-azopyridine afforded binary complexes containing infinite chains of the alternating component molecules connected by halogen bonds. The solid state CD measurements confirmed that complexation induces optical activity of the...
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Synteza i właściwości nowych pochodnych 1,4,7,10-tetraazacyklododekanu
PublicationCelem pracy była synteza i zbadanie właściwości pochodych 1,4,7,10-tetraazacyklododekanu (cyklenu). Otrzymano trzy grupy związków: alkilowe pochodne cyklenu, acylowe pochodne cyklenu i pochodne posiadające w swojej budowie ugrupowanie azowe. Acylowe pochodne zostały zsyntezowane w reakcji z wykorzystaniem p-nitrofenylowych estrów aktywnych, co nie było do tej pory stosowane w chemii cyklenu. Jest to jednoetapowa reakcja w wyniku...
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Deep Eutectic Solvents as Agents for Improving the Solubility of Edaravone: Experimental and Theoretical Considerations
PublicationIn this study, both practical and theoretical aspects of the solubility of edaravone (EDA) in Deep Eutectic Solvents (DESs) were considered. The solubility of edaravone in some media, including water, can be limited, which creates the need for new efficient and environmentally safe solvents. The solubility of EDA was measured spectrophotometrically and the complex intermolecular interactions within the systems were studied with...
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Deep Eutectic Solvents as Agents for Improving the Solubility of Edaravone: Experimental and Theoretical Considerations
PublicationIn this study, both practical and theoretical aspects of the solubility of edaravone (EDA) in Deep Eutectic Solvents (DESs) were considered. The solubility of edaravone in some media, including water, can be limited, which creates the need for new efficient and environmentally safe solvents. The solubility of EDA was measured spectrophotometrically and the complex intermolecular interactions within the systems were studied with...
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The Interaction of Heptakis (2,6-di-O-Methyl)-β-Cyclodextrin with Mianserin Hydrochloride and Its Influence on the Drug Toxicity
PublicationOne tetracyclic antidepressant, mianserin hydrochloride (MIA), has quite significant side effects on a patients’ health. Cyclodextrins, which are most commonly used to reduce the undesirable features of contained drugs within their hydrophobic interior, also have the potential to alter the toxic behavior of the drug. The present paper contains investigations and the characteristics of interaction mechanisms for MIA and the heptakis...
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An inclination in Thermal Energy Using Nanoparticles with Casson Liquid Past an Expanding Porous Surface
PublicationPhysical aspects of inclined MHD nanofluid towards a stretching sheet embedded in a porous medium are visualized. Two types of nanoparticles are used named as copper and alumna dioxide with water as base fluid. Similarity transformations are used to convert the partial differential equations into the set of ordinary differential equation. Closed solutions are found to examine the velocity and the temperature profiles. It is examined...
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Początki fortyfikacji nadbrzeżnych Gdańska
Publicationartykuł dotyczy początków fortyfikacji w rejonie ujścia Wisły, od twierdzy Wisłoujście do baterii artyleryjskich z II połowy XIX w.
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Renesans historycznych przestrzeni publicznych na przykładzie Słupska
PublicationUwarunkowania historyczne i ekonomiczno - społeczne rozwoju miasta Słupska od zakończenia II wojny światowej; opis śródmiejskich przestrzeni publicznych w Słupsku.
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Chromogenic derivatives of new bis(phenylhydrazono-1H-tetrazol-5-yl-acetonitriles) - synthesis and properties
PublicationDerivatives of bis(phenylhydrazono-1H-tetrazol-5-yl-acetonitriles) with oxygen and sulphur atoms in the structure of aliphatic chains were successfully synthesised. The correlation between the ligand structure and its complexation properties was investigated by absorption spectroscopy. The formation of complexes of presented compounds with metal cations (Cu2+, Ni2+, Zn2+, Co2+, Fe2+ and Pb2+) was studied. Ligands 5-8 were additionally...
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Efektywność flotacji jonowej i precypitacyjnej mieszaniny jonów cynku i glinu
PublicationPrzedmiotem badań była ocena wpływu pH surówki oraz stężenia kolektora na efektywność półperiodycznych flotacji jonowej i precypitacyjnej, zachodzących w roztworach zawierających mieszaniny jonów Zn(II) i Al(III). Stwierdzono, iż w warunkach flotacji jonowej, zachodzących w roztworach kwaśnych, występuje konkurencja pomiędzy flotowanymi kationami w tworzeniu związków z kolektorem. Dla roztworów o pH>11 możliwa jest selektywna flotacja...
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Near-Field Wireless Sensing of Plastics and Papers Using Frugal Peel-Off Passive Tag
PublicationThis article presents a novel frugal approach of testing plastics and papers using a near-field microwave sensing technique with a peel-off tag. The proposed sensing technique involves two electrical entities: the sensor, which may be regarded as a reader, and a disposable tag. The reader is a modified design of a gap-coupled microstrip line (GCML) sensor, while the passive tag is a standard double-ring complementary split-ring...
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Geochemical fractionation of organic matter in the Jurassic-Cretaceous Vaca Muerta shale, Argentina
PublicationSeveral studies have indicated the presence of more than one generation of bitumen that could be isolated from rocks through sequential extraction or after demineralization or both. Nabbefeld et al. (2010a) and Holman et al. (2012, 2014) termed bitumen obtained after solvent extraction from the undigested rock as “Bitumen I" and that obtained by extraction after demineralization of rock as “Bitumen II.” The occurrence of different...
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Studies on the solid-liquid equilibria and intermolecular interactions Urea binary mixtures with Sulfanilamide and Sulfacetamide
PublicationThe binary phase diagrams of Sulfanilamide-Urea (SN-U) and Sulfacetamide-Urea (SC-U) were measured using differential scanning calorimetry technique (DSC). Both examined mixtures were found to form simple binary eutectics. The limited miscibility in the solid state observed by DSC, proving inability of co-crystallization in new multi-molecular form, was also confirmed using PXRD and FTIR-ATR measurements of solid dispersions...
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Mechanism of reaction of RNA-dependent RNA polymerase from SARS-CoV-2
PublicationWe combine molecular dynamics, statistical mechanics, and hybrid quantum mechanics/molecular mechanics simulations to describe mechanistically the severe acute respiratory syndrome coronavirus 2 (SARS-CoV-2) RNA-dependent RNA polymerase (RdRp). Our study analyzes the binding mode of both natural triphosphate substrates as well as remdesivir triphosphate (the active form of drug), which is bound preferentially over ATP by RdRp while...
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Monitoring of Odour Nuisance from Landfill Using Electronic Nose
PublicationThe paper presents the results of investigation on classification of atmospheric air samples collected in a vicinity of municipal landfill with respect to their odour nuisance. The research was conducted using a prototype of electronic nose instrument and a commercial electronic nose of Fast/Flash GC type –HERACLES II. The prototype was equipped with a set of six semiconductor sensors by FIGARO Co.. Classification of the air samples...
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Spectroscopic studies on physicochemical properties of selected unsymmetrical bisacridine derivatives and NMR analysis of their interactions with the model sequence Pu22 aided by molecular dynamics
PublicationIn recent years, new promising acridine derivatives have appeared, belonging to the unsymmetrical bisacridines (UAs) family with high anticancer activity. Both their physicochemical properties and their mechanism of action at the molecular level have not been thoroughly analyzed so far. Four derivatives were selected for the study, termed as: C-2028, C-2041, C-2045 and C-2053. The first aim of this work was to determine the protonation...
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Selected organophosphorus compounds with biological activity. Applications in medicine
PublicationThe purpose of this article is to provide an overview of the latest applications of organophosphorus compounds (OPs) that exhibit biological activity. A large family of OPs have become popular in recent years. The practical application of OPs in modern medicine has been attributed to their unique properties. In this article, the methods used to select these compounds will be emphasized. This paper will first outline the findings...
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The influence of fresh cabbage and sauerkraut juices on the activity of protective enzymes in human cell lines
PublicationMechanizmami przeciwrakotwórczego działania związków zawartych w kapuście jest m.in. metaboliczna aktywacja enzymów II fazy detoksykacji, indukcja enzymów naprawczych DNA oraz aktywnośc przeciwutleniająca. Do enzymów II fazy odtruwania należą m.in. S-transferazy glutationowe (GST) oraz oksydoreduktaza chinonowa NQO1 zwana też DT-diaforazą. GST katalizują reakcję sprzęgania glutationu z wieloma różnymi typami ksenobiotyków, ułatwiając...
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A New Canon of the Modernist Villa of the 1930s - a Villa with a Semicircular Veranda. The Post-War Continuation of the Idea
PublicationThe articcle presents a new type of villa, which started to be popular in Gdynia in the 1930s. It was a villa with a semicircular veranda. Villas of that type were continously built also after the II World War
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Rozwój gospodarczy i rozwój społeczny : próba pomiaru
PublicationArtykuł stanowi analizę zróżnicowania poziomu gospodarczego pomiędzy poszczególnymi krajami. Do analizy zostały wykorzystane wskaźnkiki: PKB per capita, HDI, HPI-I oraz HPI-II.
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Bis(ć-di-tert-butylphosphido)bis[(triethylphospine)palladium(I)](Pd-Pd). A-cta Crist. Sec. E [online]**2003 vol. 59 [dostęp 31 May 2003] s. 376-377, 1 rys. 1 tab. bibliogr. 13 poz. Dost. w Intern. http://journals.iucr.org/e.Bis(ć-di-tert-butylphosphido)bis[(triethylphospine)palladium(I)](Pd-Pd).
PublicationBis.... powstaje w reakcji di-tert-butylfosfino-fosfanylideno-ĺ4-fosforanu zchlorkiem di-trietylofosfinopalladu(II) w obecności naftalidku sodu. Krystalizuje w grupie przestrzennej P1.
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Changes of microbiological quality of water in distribution system. Zmiany mikrobiologicznej jakości wody w sieci dystrybucyjnej.
PublicationW artykule przedstawiono mikrobiologiczną jakość wody podziemnej uzdatnianej w dwóch stacjach oczyszczania wody (WTP I i WTP II), w sieci dystrybucyjnej. Obie stacje uzdatniania stosują dezynfekcję za pomocą dwutlenku chloru. Badania wykazały wzrost ogólnej liczby bakterii w miarę zwiększania się odległości od stacji uzdatniania.In the paper microbiological quality of water in distribution system produced in two ground water treatment...
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Comparison of different types of electronic nose instruments for evaluation of odour nuisance from landfill
PublicationThe paper presents and compares the results of investigation on classification of atmospheric air samples collected in a vicinity of municipal landfill with respect to their odour nuisance. The research was conducted using a prototype of electronic nose instrument and a commercial electronic nose of Fast/Flash GC type – HERACLES II. The prototype was equipped with six semiconductor sensors of TGS type. Classification of the air...
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Synthesis and characterisation of starch cuprate
PublicationThe cupration of granular potato starch with ammonium tetrachlorocuprate(II) was performed by a 20 min lasting microwave-assisted process and by 40 min convectional heating. In both cases the degree of esterification (DE) did not exceed 0.0064. A higher dose of cuprate had a positive effect on DE, regardless of whether the microwave irradiation or the convectional heating was applied, and on the thermal stability of the starch...
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Catalysts for advanced oxidation processes: Deep eutectic solvents-assisted synthesis – A review
PublicationNew catalyst synthesis techniques, including green materials, are extensively studied for heterogeneous photocatalytic advanced oxidation processes (AOPs) on spotlight of sustainable development. Deep eutectic solvents (DESs) started to be used in this field as environmentally friendly alternative to ionic liquids (ILs). During the catalyst synthesis, DESs can act as stabilizers, capping agents, structure directing agents, templates,...
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Ultrasonic-assisted Electrodeposition of Cu-Sn-TiO2 Nanocomposite Coatings with Enhanced Antibacterial Activity
PublicationCopper-based coatings are known for their high antibacterial activity. In this study, nanocomposite Cu–Sn–TiO2 coatings were obtained by electrodeposition from an oxalic acid bath additionally containing 4 g/dm3 TiO2 with mechanical and ultrasonic agitation. Ultrasound treatment was performed at 26 kHz frequency and 32 W/dm3 power. The influence of agitation mode and the current load on the inclusion and distribution of the TiO2...
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EMI mitigation of GaN power inverter leg by local shielding techniques
PublicationThis paper presents local shielding techniques applied to a half-bridge inverter leg with the aim to reduce the common mode (CM) current noise at converter’s DC input. The research study is conducted for 650V Enhancement mode Gallium Nitride (GaN) power transistor switches. Main contributors of parasitic capacitances referred to the inverter-leg middle point node are identified. Then, shielding solutions are proposed to reduce...
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Structural optimization of microjet array cooling system
PublicationThe single phase heat transfer from an upward facing, horizontal copper surface to arrays of impinging water jets was experimentally investigated. Experimental configuration allows for a free-surface unconfined jets flow. Square nozzles 50 × 100 μm arranged in four different geometries were used. Additionally, for the set of two jets array geometry was varied by adjusting the nozzle to nozzle distance. The area averaged heat transfer...
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Biological and mechanical research of titanium implants covered with bactericidal coating
PublicationThe paper concerns the biological and mechanical properties of titanium implants with an antibacterial coating. The Ti13Zr13Nb alloy samples were coated with hydroxyapatite (HAp) coatings using the electrophoretic deposition technique (EPD). Subsequently, the surface of the samples was modified with silver, copper, and nickel nanoparticles by the immersion method. Different titanium sample types (i.e. HAp-only and nanometals-enriched...
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New heterometallic Co/Zn, Ag/Co, and Ag/Zn imidazolates: structural characterization and catalytic activity in the oxidation of organic compounds
PublicationNanocrystalline powders of monometallic and bimetallic imidazolates of Co, Zn, and Ag were produced by a reaction carried out in water. The powders were characterized by powder X-ray diffraction and the crystal structures of new compounds Ag2ZnIm4 and Ag2CoIm4 (Im = imidazolate) were solved. Heterometallic Co/Zn imidazolates showed the standard ZIF-8 crystal structure while Ag/Zn and Ag/Co systems were isostructural with the copper...
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The Influence of Abrasive Machine on Temperature During One Side Lapping
PublicationPrzedstawiono wyniki badań temperatury układu wykonawczego docierarki jednotarczowej. Analizowano temperaturę trzech pierścieni prowadzących separatory przy wykorzystaniu kamery termograficznej V-20 II firmy VIGO System S.A.
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Comparison of Evaluation of Air Odour Quality in Vicinity of Petroleum Plant Using a Prototype of Electronic Nose Instrument and Fast GC Technique
PublicationThe paper presents the results of investigation on classification of the ambient air samples collected in a vicinity of the LOTOS Group S.A. petroleum plant with respect to odour. The investigations were carried out with an electronic nose prototype and a commercial electronic nose of Fast GC-type – HERACLES II. The prototype was equipped with a set of six semiconductor sensors by FIGARO Co. and a photoionization sensor of PID-type....
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Mono- and bimetallic (Pt/Cu) titanium(IV) oxide core–shell photocatalysts with UV/Vis light activity and magnetic separability
PublicationTitanium(IV) oxide is one of the most widely investigated photocatalysts. However, separation of nano-sized particulate titania might result in profitless technologies for commercial applications. Additionally, bare titania is almost inactive under the Vis range of solar spectrum due to its wide bandgap. Therefore, the present study aims to prepare novel coreinterlayer- shell TiO2 magnetic photocatalysts modified with metal nanoparticles...
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Detoxification of the tricyclic antidepressant opipramol and its analog – IS-noh by UGT enzymes before and after activation by phase I enzymes in rat liver microsomes
PublicationThe present studies were carried out to evaluate the simultaneous one-pot metabolism of opipramol (IS-opi) and analog (IS-noh) by phase I and phase II enzymes present in rat liver microsomes (RLM) as an alternative to separate testing with recombinant enzymes. This approach allows for more time-saving and cost-effective screening of the metabolism of newly discovered drugs. We also considered that the lack of results for phase...
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DECT: nadzieja na integrację komunikacji
PublicationW artykule przedstawiono strukturę systemu DECT ze szczególnym uwzględnieniem sposobu realizacji transmisji danych. Przedstawiono koncepcję integracji systemu DECT z systemami telefonii komórkowej II i III generacji.
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Historic centre of Gdańsk as a unique example of postwar socialist city creation = Historyczne śródmieście Gdańska jako unikalny przykład powojennej kreacji miasta socjalistycznego
PublicationThe historic centre of Gdańsk, totally destroyed towards the end of the Second World War, became an area of postwar creation of a socialist town. During over a dozen first years, three projects were prepared for implementation within its borders, first in the convention of reconstruction and rest simply as development, for three consecutive historic city complexes: The Main Town (1948), The Old Town (1955) and The Old Suburbs (1958),...
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Ćwierćwiecze polskich nadań architektonicznych, prac budowlanych i konserwatorskich w dawnych założeniach cysterskich
PublicationArtykuł stanowi podsumowanie dotychczasowych wyników badań w kościołach i klasztorach pocysterskich. Przedstawiono także podjęte i wykonane po II wojnie światowej prace konserwatorsko budowlane, ich zakres i znaczenie.
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Błędy występujące w projektowaniu i wykonawstwie pali.
PublicationPrzedstawiono i omówiono podstawowe błędy w projektowaniu i wykonawstwie pali. Opracowanie podzielono na dwie części: część I ogólną oraz część II, w której opisano przykłady popełnionych błędów.
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Functionalization of graphene oxide coatings with phosphorus atoms and their corrosion resistance in sodium chloride environment
PublicationIn this work, we compared corrosion resistance of graphene oxide, and phosphorus functionalized reduced graphene oxide coatings obtained as a result of electrophoretic deposition on the copper substrate. Doping graphene oxide with phosphorus atoms was performed by a hydrothermal method in the presence of different amounts of phosphoric acid. Structural studies confirmed the insertion of phosphorus atoms into the graphene oxide...
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Fabrication and photoactivity of organic-inorganic systems based on titania nanotubes and PEDOT containing redox centres formed by different Prussian Blue analogues
PublicationHerein, the heterojunction composed of an inorganic substrate: ordered hydrogenated titania nanotubes (H-TiO2NTs) and a deposited organic film: poly(3,4-ethylenedioxythiophene) (PEDOT) is reported. The conducting polymer is modified with different transition metal haxacyanoferrates (Mehcf), wherein as metal: copper, iron, cobalt and nickel are introduced. The presence of various metal centres provides characteristic redox activity...